data_mhw03_sq
# start Validation Reply Form
_vrf_PLAT342_mhw03_sq
;
PROBLEM: Low Bond Precision on C-C Bonds ............... 0.02238 Ang.
RESPONSE: The flexibility of the modelled structure is reflected in the low
precision of C-C bonds.
;
_audit_author_name                ?
_audit_author_email               ?
_audit_author_address             ?
_audit_creation_method
;FinalCif V156 by Daniel Kratzert, Freiburg 2026, 
https://dkratzert.de/finalcif.html
;
_publ_section_references
;Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8.
Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_shelx_SHELXL_version_number      '2019/3'
_chemical_name_systematic         ?
_chemical_name_common             ?
_chemical_formula_sum             'C552 H324 B5 F20 N60 O64 P16 Pd12'
_chemical_formula_moiety          ?
_chemical_formula_weight          11027.06
_chemical_melting_point           ?
_chemical_absolute_configuration  ?
_space_group_crystal_system       tetragonal
_space_group_IT_number            78
_space_group_name_H-M_alt         'P 43'
_space_group_name_Hall            'P 4cw'
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x, z+3/4'
'-x, -y, z+1/2'
'y, -x, z+1/4'

_cell_length_a                    34.9006(7)
_cell_length_b                    34.9006(7)
_cell_length_c                    56.377(2)
_cell_angle_alpha                 90
_cell_angle_beta                  90
_cell_angle_gamma                 90
_cell_volume                      68670(4)
_cell_formula_units_Z             4
_cell_measurement_temperature     193(2)
_cell_measurement_reflns_used     9471
_cell_measurement_theta_min       2.6505
_cell_measurement_theta_max       66.578
_exptl_crystal_description        block
_exptl_crystal_colour             yellow
_exptl_crystal_recrystallization_method ?
_exptl_crystal_density_meas       ?
_exptl_crystal_density_method     ?
_exptl_crystal_density_diffrn     1.067
_exptl_crystal_F_000              22260
_exptl_crystal_size_max           0.2
_exptl_crystal_size_mid           0.2
_exptl_crystal_size_min           0.2
_exptl_absorpt_coefficient_mu     0.406
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_correction_T_min   0.5442
_exptl_absorpt_correction_T_max   0.7531
_exptl_absorpt_process_details
;SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: 
Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 
(2015) 3-10
;
_exptl_absorpt_special_details    ?
_shelx_estimated_absorpt_T_min    ?
_shelx_estimated_absorpt_T_max    ?
_exptl_transmission_factor_min    ?
_exptl_transmission_factor_max    ?
_exptl_special_details            ?
_diffrn_ambient_temperature       193(2)
_diffrn_ambient_environment       N~2~
_diffrn_radiation_type            MoK\a
_diffrn_radiation_wavelength      0.71073
_diffrn_radiation_monochromator   'mirror optics'
_diffrn_measurement_ambient_temperature_device_make 'Oxford Cryostream 800'
_diffrn_radiation_probe           x-ray
_diffrn_source                    'microfocus sealed X-ray tube'
_diffrn_source_type               'Incoatec I\ms'
_diffrn_source_voltage            ?
_diffrn_source_current            ?
_diffrn_detector                  CPAD
_diffrn_detector_type             'Bruker PHOTON III'
_diffrn_detector_area_resol_mean  7.41
_diffrn_measurement_device        'three-circle diffractometer'
_diffrn_measurement_device_type   'Bruker D8 VENTURE dual wavelength Mo/Cu'
_diffrn_measurement_method        'ω and φ scans'
_diffrn_measurement_specimen_support 'MiTeGen micromount'
_diffrn_reflns_number             1245995
_diffrn_reflns_av_unetI/netI      0.0751
_diffrn_reflns_av_R_equivalents   0.1505
_diffrn_reflns_theta_min          0.825
_diffrn_reflns_theta_max          25.515
_diffrn_reflns_theta_full         25.242
_diffrn_reflns_limit_h_min        -42
_diffrn_reflns_limit_h_max        41
_diffrn_reflns_limit_k_min        -42
_diffrn_reflns_limit_k_max        42
_diffrn_reflns_limit_l_min        -66
_diffrn_reflns_limit_l_max        68
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.987
_diffrn_reflns_point_group_measured_fraction_full 0.994
_reflns_number_total              126434
_reflns_number_gt                 99350
_reflns_threshold_expression      'I > 2σ(I)'
_reflns_Friedel_coverage          0.960
_reflns_Friedel_fraction_max      0.978
_reflns_Friedel_fraction_full     0.988
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_computing_data_collection        ?
_computing_cell_refinement        'SAINT V8.41'
_computing_data_reduction         'SAINT V8.41'
_computing_structure_solution     'SHELXD (G. Sheldrick)'
_computing_structure_refinement   'SHELXL-2019/2 (Sheldrick, 2019)'
_computing_molecular_graphics     ?
_computing_publication_material   ?
_refine_special_details           ?
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details      'w=1/[σ²(Fo²)+(0.2500P)²] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary      'dual space'
_atom_sites_solution_secondary    ?
_atom_sites_solution_hydrogens    geom
_refine_ls_hydrogen_treatment     constr
_refine_ls_number_reflns          126434
_refine_ls_number_parameters      6562
_refine_ls_number_restraints      13489
_refine_ls_R_factor_all           0.1491
_refine_ls_R_factor_gt            0.1331
_refine_ls_wR_factor_ref          0.3486
_refine_ls_wR_factor_gt           0.3320
_refine_ls_goodness_of_fit_ref    1.176
_refine_ls_restrained_S_all       1.134
_refine_ls_shift/su_max           0.012
_refine_ls_shift/su_mean          0.000
_refine_diff_density_max          1.344
_refine_diff_density_min          -2.191
_refine_diff_density_rms          0.186
_refine_ls_extinction_method      none
_refine_ls_extinction_coef        .
_refine_ls_abs_structure_Flack    -0.197(10)
_refine_ls_abs_structure_details
;
 Flack x determined using 35147 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
'C'  'C'  0.0033  0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'H'  'H'  0.0000  0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'N'  'N'  0.0061  0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'O'  'O'  0.0106  0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'P'  'P'  0.1023  0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'Pd' 'Pd' -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'B'  'B'  0.0013  0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
'F'  'F'  0.0171  0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pd1_1  Pd 0.15073(3)  -0.00497(3) 0.54596(3)  0.0577(3)  Uani 1 1 d    . . . . .
Pd2_1  Pd 0.52254(3)  0.09816(3)  0.54084(3)  0.0558(3)  Uani 1 1 d    . . . . .
Pd3_1  Pd 0.30168(4)  0.20544(4)  0.72267(3)  0.0607(3)  Uani 1 1 d    . . . . .
Pd4_1  Pd 0.05353(3)  0.36622(4)  0.57242(3)  0.0601(3)  Uani 1 1 d    . . . . .
Pd5_1  Pd 0.27349(4)  0.25737(5)  0.39015(3)  0.0663(3)  Uani 1 1 d    . . . . .
Pd6_1  Pd 0.42167(3)  0.46615(3)  0.56716(3)  0.0571(3)  Uani 1 1 d    . . . . .
N1_2   N  0.1283(4)   0.0045(3)   0.5783(2)   0.064(3)   Uani 1 1 d    D U . . .
C2_2   C  0.1043(6)   -0.0194(6)  0.5893(3)   0.083(5)   Uani 1 1 d    D U . . .
H2_2   H  0.092149    -0.038872   0.580251    0.099      Uiso 1 1 calc R U . . .
C3_2   C  0.0961(10)  -0.0173(7)  0.6133(4)   0.115(9)   Uani 1 1 d    D U . . .
H3_2   H  0.083430    -0.037603   0.621337    0.138      Uiso 1 1 calc R U . . .
C4_2   C  0.1073(7)   0.0157(6)   0.6252(3)   0.094(7)   Uani 1 1 d    D U . . .
H4_2   H  0.098150    0.020803    0.640760    0.113      Uiso 1 1 calc R U . . .
C5_2   C  0.1321(5)   0.0413(4)   0.6139(2)   0.085(6)   Uani 1 1 d    D U . . .
C6_2   C  0.1422(4)   0.0340(4)   0.5907(2)   0.066(4)   Uani 1 1 d    D U . . .
H6_2   H  0.159885    0.050701    0.583213    0.079      Uiso 1 1 calc R U . . .
C7_2   C  0.1468(5)   0.0751(4)   0.6271(3)   0.083(5)   Uani 1 1 d    D U . . .
C8_2   C  0.1592(5)   0.0724(5)   0.6499(3)   0.065(4)   Uani 1 1 d    D U . . .
H8_2   H  0.157651    0.048355    0.657711    0.079      Uiso 1 1 calc R U . . .
C9_2   C  0.1744(4)   0.1045(4)   0.6627(3)   0.064(4)   Uani 1 1 d    D U . . .
H9_2   H  0.181530    0.102071    0.678857    0.077      Uiso 1 1 calc R U . . .
C10_2  C  0.1785(5)   0.1385(4)   0.6512(3)   0.068(4)   Uani 1 1 d    D U . . .
C11_2  C  0.1668(5)   0.1443(5)   0.6277(3)   0.081(5)   Uani 1 1 d    D U . . .
C12_2  C  0.1489(6)   0.1116(5)   0.6165(3)   0.082(4)   Uani 1 1 d    D U . . .
O13_2  O  0.1291(5)   0.1182(4)   0.5949(3)   0.084(4)   Uani 1 1 d    D U . . .
C14_2  C  0.1066(5)   0.1511(5)   0.5938(3)   0.077(4)   Uani 1 1 d    D U . . .
C15_2  C  0.0706(5)   0.1497(5)   0.5849(4)   0.081(5)   Uani 1 1 d    D U . . .
H15_2  H  0.060974    0.126752    0.578062    0.098      Uiso 1 1 calc R U . . .
C16_2  C  0.0474(6)   0.1832(5)   0.5861(4)   0.092(6)   Uani 1 1 d    D U . . .
H16_2  H  0.021938    0.182018    0.580111    0.110      Uiso 1 1 calc R U . . .
C17_2  C  0.0601(5)   0.2171(4)   0.5954(4)   0.090(6)   Uani 1 1 d    D U . . .
C18_2  C  0.0979(6)   0.2175(6)   0.6043(4)   0.099(6)   Uani 1 1 d    D U . . .
C19_2  C  0.1209(5)   0.1853(5)   0.6028(3)   0.077(4)   Uani 1 1 d    D U . . .
P20_2  P  0.16809(15) 0.18799(16) 0.61393(11) 0.0733(12) Uani 1 1 d    D U . . .
C21_2  C  0.1559(5)   0.2156(5)   0.6391(3)   0.072(4)   Uani 1 1 d    D U . . .
C22_2  C  0.1296(5)   0.2447(5)   0.6374(3)   0.079(4)   Uani 1 1 d    D U . . .
C23_2  C  0.1198(7)   0.2655(6)   0.6567(3)   0.084(5)   Uani 1 1 d    D U . . .
H23_2  H  0.102008    0.285940    0.655325    0.101      Uiso 1 1 calc R U . . .
C24_2  C  0.1364(6)   0.2567(5)   0.6794(3)   0.083(5)   Uani 1 1 d    D U . . .
H24_2  H  0.128834    0.270598    0.693107    0.100      Uiso 1 1 calc R U . . .
C25_2  C  0.1636(4)   0.2277(4)   0.6810(2)   0.070(4)   Uani 1 1 d    D U . . .
C26_2  C  0.1709(5)   0.2041(5)   0.6613(3)   0.068(4)   Uani 1 1 d    D U . . .
O27_2  O  0.1909(5)   0.1706(3)   0.6638(3)   0.086(4)   Uani 1 1 d    D U . . .
O28_2  O  0.1108(4)   0.2504(5)   0.6159(3)   0.086(4)   Uani 1 1 d    D U . . .
O29_2  O  0.2006(5)   0.1982(6)   0.5985(4)   0.105(5)   Uani 1 1 d    D U . . .
C30_2  C  0.1843(4)   0.2202(5)   0.7035(2)   0.074(4)   Uani 1 1 d    D U . . .
C31_2  C  0.1642(5)   0.2166(7)   0.7248(3)   0.094(6)   Uani 1 1 d    D U . . .
H31_2  H  0.137012    0.217442    0.724988    0.113      Uiso 1 1 calc R U . . .
C32_2  C  0.1849(5)   0.2119(7)   0.7457(3)   0.100(7)   Uani 1 1 d    D U . . .
H32_2  H  0.171978    0.210495    0.760502    0.120      Uiso 1 1 calc R U . . .
C33_2  C  0.2242(5)   0.2092(7)   0.7447(3)   0.094(6)   Uani 1 1 d    D U . . .
H33_2  H  0.237922    0.205472    0.759018    0.113      Uiso 1 1 calc R U . . .
N34_2  N  0.2438(3)   0.2115(5)   0.7246(2)   0.071(4)   Uani 1 1 d    D U . . .
C35_2  C  0.2241(4)   0.2159(4)   0.7044(3)   0.068(4)   Uani 1 1 d    D U . . .
H35_2  H  0.237863    0.216175    0.689855    0.081      Uiso 1 1 calc R U . . .
C36_2  C  0.0361(4)   0.2523(4)   0.5958(3)   0.074(4)   Uani 1 1 d    D U . . .
C37_2  C  -0.0011(5)  0.2518(5)   0.6049(4)   0.089(6)   Uani 1 1 d    D U . . .
H37_2  H  -0.011512   0.229034    0.611474    0.107      Uiso 1 1 calc R U . . .
C38_2  C  -0.0224(5)  0.2850(5)   0.6040(5)   0.106(8)   Uani 1 1 d    D U . . .
H38_2  H  -0.047830   0.285771    0.610027    0.127      Uiso 1 1 calc R U . . .
C39_2  C  -0.0059(5)  0.3172(5)   0.5941(5)   0.092(6)   Uani 1 1 d    D U . . .
H39_2  H  -0.020623   0.340115    0.593755    0.110      Uiso 1 1 calc R U . . .
N40_2  N  0.0297(4)   0.3184(4)   0.5848(3)   0.070(3)   Uani 1 1 d    D U . . .
C41_2  C  0.0501(4)   0.2865(4)   0.5869(4)   0.073(4)   Uani 1 1 d    D U . . .
H41_2  H  0.076108    0.287165    0.582015    0.087      Uiso 1 1 calc R U . . .
N1_3   N  0.1063(3)   0.0250(3)   0.5325(3)   0.064(3)   Uani 1 1 d    D U . . .
C2_3   C  0.0761(5)   0.0066(4)   0.5234(5)   0.087(6)   Uani 1 1 d    D U . . .
H2_3   H  0.075452    -0.020626   0.523642    0.104      Uiso 1 1 calc R U . . .
C3_3   C  0.0459(5)   0.0267(5)   0.5137(5)   0.091(6)   Uani 1 1 d    D U . . .
H3_3   H  0.025431    0.013517    0.506187    0.109      Uiso 1 1 calc R U . . .
C4_3   C  0.0455(5)   0.0659(4)   0.5151(4)   0.084(5)   Uani 1 1 d    D U . . .
H4_3   H  0.023092    0.079575    0.510701    0.101      Uiso 1 1 calc R U . . .
C5_3   C  0.0774(4)   0.0855(3)   0.5228(3)   0.076(5)   Uani 1 1 d    D U . . .
C6_3   C  0.1075(4)   0.0629(3)   0.5317(3)   0.064(4)   Uani 1 1 d    D U . . .
H6_3   H  0.129752    0.075409    0.537454    0.076      Uiso 1 1 calc R U . . .
C7_3   C  0.0807(4)   0.1280(3)   0.5223(3)   0.071(4)   Uani 1 1 d    D U . . .
C8_3   C  0.0524(6)   0.1523(5)   0.5311(4)   0.084(5)   Uani 1 1 d    D U . . .
H8_3   H  0.030358    0.140954    0.538040    0.100      Uiso 1 1 calc R U . . .
C9_3   C  0.0543(5)   0.1930(5)   0.5303(4)   0.082(5)   Uani 1 1 d    D U . . .
H9_3   H  0.032940    0.208409    0.534487    0.098      Uiso 1 1 calc R U . . .
C10_3  C  0.0881(5)   0.2088(4)   0.5232(3)   0.079(5)   Uani 1 1 d    D U . . .
C11_3  C  0.1186(5)   0.1857(5)   0.5148(3)   0.070(4)   Uani 1 1 d    D U . . .
C12_3  C  0.1139(5)   0.1453(5)   0.5132(3)   0.067(4)   Uani 1 1 d    D U . . .
O13_3  O  0.1401(4)   0.1237(4)   0.5012(2)   0.076(3)   Uani 1 1 d    D U . . .
C14_3  C  0.1489(5)   0.1375(4)   0.4788(3)   0.067(4)   Uani 1 1 d    D U . . .
C15_3  C  0.1484(6)   0.1154(5)   0.4596(3)   0.076(4)   Uani 1 1 d    D U . . .
H15_3  H  0.141122    0.089284    0.460765    0.092      Uiso 1 1 calc R U . . .
C16_3  C  0.1591(7)   0.1315(5)   0.4372(3)   0.085(5)   Uani 1 1 d    D U . . .
H16_3  H  0.158872    0.115658    0.423554    0.102      Uiso 1 1 calc R U . . .
C17_3  C  0.1698(5)   0.1695(4)   0.4349(3)   0.078(4)   Uani 1 1 d    D U . . .
C18_3  C  0.1690(5)   0.1916(5)   0.4553(3)   0.075(4)   Uani 1 1 d    D U . . .
C19_3  C  0.1599(4)   0.1757(4)   0.4782(3)   0.067(4)   Uani 1 1 d    D U . . .
P20_3  P  0.16014(15) 0.20578(14) 0.50275(11) 0.0714(12) Uani 1 1 d    D U . . .
C21_3  C  0.1368(5)   0.2442(4)   0.4890(3)   0.072(4)   Uani 1 1 d    D U . . .
C22_3  C  0.1460(4)   0.2530(4)   0.4657(3)   0.068(4)   Uani 1 1 d    D U . . .
C23_3  C  0.1273(5)   0.2825(5)   0.4547(3)   0.075(4)   Uani 1 1 d    D U . . .
H23_3  H  0.133171    0.289080    0.438755    0.090      Uiso 1 1 calc R U . . .
C24_3  C  0.0994(5)   0.3028(5)   0.4674(3)   0.071(4)   Uani 1 1 d    D U . . .
H24_3  H  0.087267    0.323887    0.459804    0.086      Uiso 1 1 calc R U . . .
C25_3  C  0.0884(4)   0.2941(4)   0.4903(3)   0.069(4)   Uani 1 1 d    D U . . .
C26_3  C  0.1063(5)   0.2624(5)   0.5004(3)   0.078(5)   Uani 1 1 d    D U . . .
O27_3  O  0.0918(5)   0.2478(4)   0.5217(2)   0.078(4)   Uani 1 1 d    D U . . .
O28_3  O  0.1733(4)   0.2319(3)   0.4534(3)   0.074(3)   Uani 1 1 d    D U . . .
O29_3  O  0.1944(5)   0.2120(4)   0.5166(3)   0.084(4)   Uani 1 1 d    D U . . .
C30_3  C  0.0592(4)   0.3171(4)   0.5032(2)   0.068(4)   Uani 1 1 d    D U . . .
C31_3  C  0.0248(5)   0.3275(8)   0.4926(4)   0.115(9)   Uani 1 1 d    D U . . .
H31_3  H  0.019275    0.319903    0.476743    0.138      Uiso 1 1 calc R U . . .
C32_3  C  -0.0013(5)  0.3491(7)   0.5054(4)   0.107(8)   Uani 1 1 d    D U . . .
H32_3  H  -0.024574   0.357453    0.498392    0.128      Uiso 1 1 calc R U . . .
C33_3  C  0.0073(5)   0.3584(7)   0.5288(4)   0.090(6)   Uani 1 1 d    D U . . .
H33_3  H  -0.010684   0.373230    0.537533    0.108      Uiso 1 1 calc R U . . .
N34_3  N  0.0393(3)   0.3475(5)   0.5395(3)   0.077(4)   Uani 1 1 d    D U . . .
C35_3  C  0.0644(4)   0.3270(5)   0.5269(3)   0.076(5)   Uani 1 1 d    D U . . .
H35_3  H  0.087176    0.318672    0.534553    0.092      Uiso 1 1 calc R U . . .
C36_3  C  0.1816(4)   0.1865(4)   0.4118(2)   0.079(4)   Uani 1 1 d    D U . . .
C37_3  C  0.1606(5)   0.1813(5)   0.3912(3)   0.077(4)   Uani 1 1 d    D U . . .
H37_3  H  0.137291    0.167249    0.391674    0.093      Uiso 1 1 calc R U . . .
C38_3  C  0.1734(5)   0.1963(6)   0.3701(3)   0.092(6)   Uani 1 1 d    D U . . .
H38_3  H  0.159409    0.192176    0.355853    0.110      Uiso 1 1 calc R U . . .
C39_3  C  0.2066(5)   0.2174(6)   0.3698(2)   0.081(5)   Uani 1 1 d    D U . . .
H39_3  H  0.216787    0.226062    0.355107    0.097      Uiso 1 1 calc R U . . .
N40_3  N  0.2246(4)   0.2256(5)   0.3898(2)   0.075(4)   Uani 1 1 d    D U . . .
C41_3  C  0.2144(5)   0.2094(5)   0.4103(2)   0.071(4)   Uani 1 1 d    D U . . .
H41_3  H  0.229577    0.213508    0.424007    0.085      Uiso 1 1 calc R U . . .
N1_4   N  0.1736(5)   -0.0126(4)  0.5139(3)   0.086(5)   Uani 1 1 d    D U . . .
C2_4   C  0.1776(9)   -0.0465(5)  0.5033(4)   0.109(9)   Uani 1 1 d    D U . . .
H2_4   H  0.164168    -0.067699   0.509908    0.131      Uiso 1 1 calc R U . . .
C3_4   C  0.1997(9)   -0.0531(5)  0.4836(5)   0.109(9)   Uani 1 1 d    D U . . .
H3_4   H  0.202665    -0.078204   0.477382    0.131      Uiso 1 1 calc R U . . .
C4_4   C  0.2175(8)   -0.0219(5)  0.4729(4)   0.108(8)   Uani 1 1 d    D U . . .
H4_4   H  0.233027    -0.025278   0.459176    0.129      Uiso 1 1 calc R U . . .
C5_4   C  0.2121(6)   0.0143(4)   0.4826(3)   0.099(7)   Uani 1 1 d    D U . . .
C6_4   C  0.1906(5)   0.0176(4)   0.5033(3)   0.083(5)   Uani 1 1 d    D U . . .
H6_4   H  0.187779    0.042215    0.510193    0.099      Uiso 1 1 calc R U . . .
C7_4   C  0.2304(4)   0.0490(4)   0.4724(2)   0.063(3)   Uani 1 1 d    D U . . .
C8_4   C  0.2224(5)   0.0645(5)   0.4508(3)   0.074(4)   Uani 1 1 d    D U . . .
H8_4   H  0.200530    0.055463    0.442441    0.089      Uiso 1 1 calc R U . . .
C9_4   C  0.2452(5)   0.0936(6)   0.4402(3)   0.077(5)   Uani 1 1 d    D U . . .
H9_4   H  0.241824    0.100399    0.423993    0.092      Uiso 1 1 calc R U . . .
C10_4  C  0.2721(5)   0.1117(5)   0.4539(4)   0.087(5)   Uani 1 1 d    D U . . .
C11_4  C  0.2809(5)   0.0983(5)   0.4774(3)   0.071(4)   Uani 1 1 d    D U . . .
C12_4  C  0.2611(5)   0.0661(5)   0.4855(3)   0.071(4)   Uani 1 1 d    D U . . .
O13_4  O  0.2731(3)   0.0486(5)   0.5058(3)   0.082(4)   Uani 1 1 d    D U . . .
C14_4  C  0.3117(4)   0.0433(5)   0.5080(4)   0.080(5)   Uani 1 1 d    D U . . .
C15_4  C  0.3259(5)   0.0086(4)   0.5152(4)   0.081(5)   Uani 1 1 d    D U . . .
H15_4  H  0.309610    -0.012328   0.518886    0.097      Uiso 1 1 calc R U . . .
C16_4  C  0.3665(5)   0.0058(6)   0.5169(5)   0.092(6)   Uani 1 1 d    D U . . .
H16_4  H  0.376989    -0.017405   0.522942    0.111      Uiso 1 1 calc R U . . .
C17_4  C  0.3916(3)   0.0344(5)   0.5105(4)   0.081(5)   Uani 1 1 d    D U . . .
C18_4  C  0.3759(5)   0.0680(5)   0.5022(3)   0.075(4)   Uani 1 1 d    D U . . .
C19_4  C  0.3363(5)   0.0743(5)   0.5024(3)   0.079(5)   Uani 1 1 d    D U . . .
P20_4  P  0.31626(14) 0.11885(16) 0.49411(11) 0.0717(12) Uani 1 1 d    D U . . .
C21_4  C  0.3468(5)   0.1241(5)   0.4704(3)   0.080(5)   Uani 1 1 d    D U . . .
C22_4  C  0.3866(4)   0.1121(5)   0.4715(3)   0.075(4)   Uani 1 1 d    D U . . .
C23_4  C  0.4101(5)   0.1162(6)   0.4528(3)   0.081(5)   Uani 1 1 d    D U . . .
H23_4  H  0.435924    0.107622    0.453294    0.097      Uiso 1 1 calc R U . . .
C24_4  C  0.3949(4)   0.1339(6)   0.4322(4)   0.086(5)   Uani 1 1 d    D U . . .
H24_4  H  0.412007    0.139374    0.419523    0.103      Uiso 1 1 calc R U . . .
C25_4  C  0.3572(4)   0.1436(5)   0.4294(3)   0.080(4)   Uani 1 1 d    D U . . .
C26_4  C  0.3322(5)   0.1372(5)   0.4489(3)   0.080(5)   Uani 1 1 d    D U . . .
O27_4  O  0.2932(4)   0.1427(4)   0.4459(3)   0.076(3)   Uani 1 1 d    D U . . .
O28_4  O  0.3989(4)   0.0961(4)   0.4925(3)   0.081(4)   Uani 1 1 d    D U . . .
O29_4  O  0.3075(6)   0.1488(5)   0.5127(4)   0.104(5)   Uani 1 1 d    D U . . .
C30_4  C  0.3429(4)   0.1603(5)   0.4068(3)   0.086(5)   Uani 1 1 d    D U . . .
C31_4  C  0.3507(6)   0.1448(6)   0.3848(3)   0.095(6)   Uani 1 1 d    D U . . .
H31_4  H  0.366028    0.122341    0.383743    0.114      Uiso 1 1 calc R U . . .
C32_4  C  0.3366(7)   0.1614(6)   0.3644(3)   0.113(8)   Uani 1 1 d    D U . . .
H32_4  H  0.342073    0.150710    0.349321    0.135      Uiso 1 1 calc R U . . .
C33_4  C  0.3144(7)   0.1937(6)   0.3665(3)   0.091(6)   Uani 1 1 d    D U . . .
H33_4  H  0.304787    0.205609    0.352526    0.109      Uiso 1 1 calc R U . . .
N34_4  N  0.3060(4)   0.2088(4)   0.3874(2)   0.068(3)   Uani 1 1 d    D U . . .
C35_4  C  0.3213(5)   0.1939(5)   0.4071(3)   0.075(4)   Uani 1 1 d    D U . . .
H35_4  H  0.317238    0.206596    0.421796    0.090      Uiso 1 1 calc R U . . .
C36_4  C  0.4339(3)   0.0293(4)   0.5122(3)   0.072(4)   Uani 1 1 d    D U . . .
C37_4  C  0.4528(4)   -0.0039(5)  0.5045(4)   0.086(6)   Uani 1 1 d    D U . . .
H37_4  H  0.438684    -0.024481   0.497819    0.103      Uiso 1 1 calc R U . . .
C38_4  C  0.4925(5)   -0.0063(5)  0.5069(4)   0.090(6)   Uani 1 1 d    D U . . .
H38_4  H  0.505826    -0.028204   0.501113    0.108      Uiso 1 1 calc R U . . .
C39_4  C  0.5124(5)   0.0232(5)   0.5176(5)   0.092(7)   Uani 1 1 d    D U . . .
H39_4  H  0.539329    0.020991    0.519765    0.111      Uiso 1 1 calc R U . . .
N40_4  N  0.4944(3)   0.0550(4)   0.5250(4)   0.081(5)   Uani 1 1 d    D U . . .
C41_4  C  0.4562(4)   0.0572(5)   0.5223(4)   0.074(5)   Uani 1 1 d    D U . . .
H41_4  H  0.443770    0.079663    0.527846    0.088      Uiso 1 1 calc R U . . .
N1_5   N  0.1969(4)   -0.0325(4)  0.5598(3)   0.067(3)   Uani 1 1 d    D U . . .
C2_5   C  0.1982(5)   -0.0703(4)  0.5628(5)   0.087(6)   Uani 1 1 d    D U . . .
H2_5   H  0.176126    -0.084878   0.558862    0.104      Uiso 1 1 calc R U . . .
C3_5   C  0.2301(5)   -0.0896(4)  0.5713(5)   0.088(6)   Uani 1 1 d    D U . . .
H3_5   H  0.230066    -0.116725   0.572975    0.106      Uiso 1 1 calc R U . . .
C4_5   C  0.2620(5)   -0.0680(4)  0.5772(5)   0.095(7)   Uani 1 1 d    D U . . .
H4_5   H  0.283620    -0.079947   0.584337    0.114      Uiso 1 1 calc R U . . .
C5_5   C  0.2623(3)   -0.0293(4)  0.5728(3)   0.073(4)   Uani 1 1 d    D U . . .
C6_5   C  0.2286(3)   -0.0126(4)  0.5645(3)   0.069(4)   Uani 1 1 d    D U . . .
H6_5   H  0.228192    0.014359    0.562071    0.083      Uiso 1 1 calc R U . . .
C7_5   C  0.2971(4)   -0.0055(5)  0.5757(3)   0.080(5)   Uani 1 1 d    D U . . .
C8_5   C  0.3327(4)   -0.0175(6)  0.5679(5)   0.090(6)   Uani 1 1 d    D U . . .
H8_5   H  0.335490    -0.041228   0.559876    0.108      Uiso 1 1 calc R U . . .
C9_5   C  0.3652(5)   0.0064(5)   0.5723(5)   0.080(5)   Uani 1 1 d    D U . . .
H9_5   H  0.389878    -0.003181   0.568357    0.096      Uiso 1 1 calc R U . . .
C10_5  C  0.3625(4)   0.0418(4)   0.5817(3)   0.067(4)   Uani 1 1 d    D U . . .
C11_5  C  0.3266(5)   0.0542(5)   0.5885(3)   0.083(5)   Uani 1 1 d    D U . . .
C12_5  C  0.2949(4)   0.0312(5)   0.5869(3)   0.071(4)   Uani 1 1 d    D U . . .
O13_5  O  0.2607(3)   0.0408(3)   0.5988(2)   0.065(3)   Uani 1 1 d    D U . . .
C14_5  C  0.2662(4)   0.0577(5)   0.6205(3)   0.072(4)   Uani 1 1 d    D U . . .
C15_5  C  0.2417(5)   0.0456(7)   0.6380(3)   0.088(5)   Uani 1 1 d    D U . . .
H15_5  H  0.220063    0.030207    0.634194    0.105      Uiso 1 1 calc R U . . .
C16_5  C  0.2492(5)   0.0563(6)   0.6617(3)   0.080(5)   Uani 1 1 d    D U . . .
H16_5  H  0.234120    0.045242    0.673905    0.096      Uiso 1 1 calc R U . . .
C17_5  C  0.2774(4)   0.0822(5)   0.6679(2)   0.075(4)   Uani 1 1 d    D U . . .
C18_5  C  0.3023(4)   0.0941(4)   0.6489(3)   0.059(3)   Uani 1 1 d    D U . . .
C19_5  C  0.2942(4)   0.0833(5)   0.6256(3)   0.072(4)   Uani 1 1 d    D U . . .
P20_5  P  0.32367(13) 0.09938(14) 0.60223(11) 0.0675(11) Uani 1 1 d    D U . . .
C21_5  C  0.3664(5)   0.0952(5)   0.6181(3)   0.074(4)   Uani 1 1 d    D U . . .
C22_5  C  0.3687(4)   0.1042(5)   0.6427(3)   0.069(4)   Uani 1 1 d    D U . . .
C23_5  C  0.4019(4)   0.1009(6)   0.6550(3)   0.078(5)   Uani 1 1 d    D U . . .
H23_5  H  0.403049    0.107267    0.671374    0.093      Uiso 1 1 calc R U . . .
C24_5  C  0.4350(4)   0.0879(5)   0.6429(3)   0.067(4)   Uani 1 1 d    D U . . .
H24_5  H  0.458394    0.085619    0.651339    0.080      Uiso 1 1 calc R U . . .
C25_5  C  0.4342(4)   0.0783(4)   0.6191(3)   0.067(3)   Uani 1 1 d    D U . . .
C26_5  C  0.4003(5)   0.0791(5)   0.6078(3)   0.074(4)   Uani 1 1 d    D U . . .
O27_5  O  0.3949(3)   0.0634(5)   0.5857(2)   0.078(4)   Uani 1 1 d    D U . . .
O28_5  O  0.3352(4)   0.1150(4)   0.6542(3)   0.078(3)   Uani 1 1 d    D U . . .
O29_5  O  0.3112(5)   0.1350(5)   0.5906(3)   0.093(4)   Uani 1 1 d    D U . . .
C30_5  C  0.4699(3)   0.0674(4)   0.6064(2)   0.068(4)   Uani 1 1 d    D U . . .
C31_5  C  0.4965(4)   0.0426(5)   0.6168(3)   0.070(4)   Uani 1 1 d    D U . . .
H31_5  H  0.490739    0.030631    0.631465    0.084      Uiso 1 1 calc R U . . .
C32_5  C  0.5312(5)   0.0353(5)   0.6056(3)   0.081(5)   Uani 1 1 d    D U . . .
H32_5  H  0.549993    0.019138    0.612610    0.098      Uiso 1 1 calc R U . . .
C33_5  C  0.5370(4)   0.0527(5)   0.5839(3)   0.066(4)   Uani 1 1 d    D U . . .
H33_5  H  0.561129    0.049117    0.576437    0.080      Uiso 1 1 calc R U . . .
N34_5  N  0.5113(3)   0.0739(4)   0.5728(2)   0.065(3)   Uani 1 1 d    D U . . .
C35_5  C  0.4780(4)   0.0809(4)   0.5838(2)   0.059(3)   Uani 1 1 d    D U . . .
H35_5  H  0.459208    0.095673    0.575800    0.071      Uiso 1 1 calc R U . . .
C36_5  C  0.2835(4)   0.0954(4)   0.6926(2)   0.070(4)   Uani 1 1 d    D U . . .
C37_5  C  0.2815(6)   0.0713(5)   0.7120(3)   0.080(5)   Uani 1 1 d    D U . . .
H37_5  H  0.276728    0.044752    0.710005    0.096      Uiso 1 1 calc R U . . .
C38_5  C  0.2867(7)   0.0866(4)   0.7345(3)   0.097(7)   Uani 1 1 d    D U . . .
H38_5  H  0.285127    0.070541    0.748112    0.117      Uiso 1 1 calc R U . . .
C39_5  C  0.2941(7)   0.1251(4)   0.7370(3)   0.080(5)   Uani 1 1 d    D U . . .
H39_5  H  0.297051    0.135329    0.752526    0.096      Uiso 1 1 calc R U . . .
N40_5  N  0.2971(4)   0.1485(3)   0.7186(2)   0.064(3)   Uani 1 1 d    D U . . .
C41_5  C  0.2908(4)   0.1339(4)   0.6972(2)   0.063(3)   Uani 1 1 d    D U . . .
H41_5  H  0.291255    0.150933    0.684125    0.076      Uiso 1 1 calc R U . . .
N1_6   N  0.4428(4)   0.4483(3)   0.5976(2)   0.063(3)   Uani 1 1 d    D U . . .
C2_6   C  0.4616(6)   0.4714(5)   0.6125(3)   0.077(5)   Uani 1 1 d    D U . . .
H2_6   H  0.464231    0.497656    0.608352    0.092      Uiso 1 1 calc R U . . .
C3_6   C  0.4772(6)   0.4593(4)   0.6336(3)   0.076(5)   Uani 1 1 d    D U . . .
H3_6   H  0.494094    0.475305    0.642298    0.091      Uiso 1 1 calc R U . . .
C4_6   C  0.4676(5)   0.4228(4)   0.6420(3)   0.067(4)   Uani 1 1 d    D U . . .
H4_6   H  0.476350    0.414427    0.657116    0.081      Uiso 1 1 calc R U . . .
C5_6   C  0.4451(4)   0.3989(3)   0.6280(2)   0.062(3)   Uani 1 1 d    D U . . .
C6_6   C  0.4345(4)   0.4131(4)   0.6059(2)   0.065(4)   Uani 1 1 d    D U . . .
H6_6   H  0.420075    0.396604    0.595924    0.078      Uiso 1 1 calc R U . . .
C7_6   C  0.4316(5)   0.3609(4)   0.6365(3)   0.071(4)   Uani 1 1 d    D U . . .
C8_6   C  0.4225(7)   0.3535(4)   0.6598(3)   0.075(5)   Uani 1 1 d    D U . . .
H8_6   H  0.425983    0.373412    0.671107    0.090      Uiso 1 1 calc R U . . .
C9_6   C  0.4083(6)   0.3181(4)   0.6677(4)   0.079(5)   Uani 1 1 d    D U . . .
H9_6   H  0.401498    0.314222    0.683797    0.095      Uiso 1 1 calc R U . . .
C10_6  C  0.4048(5)   0.2897(4)   0.6515(3)   0.079(5)   Uani 1 1 d    D U . . .
C11_6  C  0.4160(4)   0.2946(4)   0.6274(3)   0.064(3)   Uani 1 1 d    D U . . .
C12_6  C  0.4306(5)   0.3294(4)   0.6205(3)   0.063(4)   Uani 1 1 d    D U . . .
O13_6  O  0.4490(4)   0.3326(3)   0.5990(2)   0.071(3)   Uani 1 1 d    D U . . .
C14_6  C  0.4712(5)   0.3011(4)   0.5922(3)   0.073(5)   Uani 1 1 d    D U . . .
C15_6  C  0.5069(6)   0.3071(4)   0.5827(5)   0.093(7)   Uani 1 1 d    D U . . .
H15_6  H  0.517184    0.332218    0.581680    0.111      Uiso 1 1 calc R U . . .
C16_6  C  0.5279(5)   0.2757(3)   0.5744(3)   0.062(4)   Uani 1 1 d    D U . . .
H16_6  H  0.549660    0.280283    0.564637    0.075      Uiso 1 1 calc R U . . .
C17_6  C  0.5184(4)   0.2382(3)   0.5798(3)   0.069(4)   Uani 1 1 d    D U . . .
C18_6  C  0.4840(5)   0.2316(4)   0.5922(3)   0.070(4)   Uani 1 1 d    D U . . .
C19_6  C  0.4582(5)   0.2625(4)   0.5966(3)   0.065(4)   Uani 1 1 d    D U . . .
P20_6  P  0.41377(14) 0.25460(13) 0.60859(9)  0.0633(10) Uani 1 1 d    D U . . .
C21_6  C  0.4303(4)   0.2219(4)   0.6291(3)   0.058(3)   Uani 1 1 d    D U . . .
C22_6  C  0.4596(4)   0.1952(4)   0.6233(3)   0.060(3)   Uani 1 1 d    D U . . .
C23_6  C  0.4712(5)   0.1680(5)   0.6390(3)   0.065(4)   Uani 1 1 d    D U . . .
H23_6  H  0.487754    0.147885    0.634098    0.078      Uiso 1 1 calc R U . . .
C24_6  C  0.4583(5)   0.1700(4)   0.6628(3)   0.063(3)   Uani 1 1 d    D U . . .
H24_6  H  0.469262    0.153486    0.674295    0.075      Uiso 1 1 calc R U . . .
C25_6  C  0.4300(4)   0.1956(4)   0.6695(2)   0.057(3)   Uani 1 1 d    D U . . .
C26_6  C  0.4185(4)   0.2232(4)   0.6523(3)   0.061(3)   Uani 1 1 d    D U . . .
O27_6  O  0.3950(4)   0.2535(3)   0.6602(3)   0.070(3)   Uani 1 1 d    D U . . .
O28_6  O  0.4749(3)   0.1961(3)   0.6010(2)   0.063(3)   Uani 1 1 d    D U . . .
O29_6  O  0.3804(4)   0.2486(4)   0.5933(3)   0.081(4)   Uani 1 1 d    D U . . .
C30_6  C  0.4136(3)   0.1962(4)   0.6938(2)   0.062(3)   Uani 1 1 d    D U . . .
C31_6  C  0.4378(5)   0.1944(9)   0.7136(3)   0.104(8)   Uani 1 1 d    D U . . .
H31_6  H  0.464749    0.192369    0.711680    0.125      Uiso 1 1 calc R U . . .
C32_6  C  0.4219(6)   0.1958(9)   0.7359(3)   0.127(10)  Uani 1 1 d    D U . . .
H32_6  H  0.437889    0.194239    0.749500    0.152      Uiso 1 1 calc R U . . .
C33_6  C  0.3827(5)   0.1994(8)   0.7385(3)   0.097(7)   Uani 1 1 d    D U . . .
H33_6  H  0.372014    0.199552    0.753973    0.116      Uiso 1 1 calc R U . . .
N34_6  N  0.3593(4)   0.2028(6)   0.7196(2)   0.080(4)   Uani 1 1 d    D U . . .
C35_6  C  0.3748(4)   0.1994(6)   0.6981(2)   0.072(4)   Uani 1 1 d    D U . . .
H35_6  H  0.358006    0.199099    0.684893    0.086      Uiso 1 1 calc R U . . .
C36_6  C  0.5439(3)   0.2062(3)   0.5726(3)   0.062(3)   Uani 1 1 d    D U . . .
C37_6  C  0.5837(4)   0.2100(4)   0.5725(3)   0.069(4)   Uani 1 1 d    D U . . .
H37_6  H  0.595508    0.232627    0.578306    0.083      Uiso 1 1 calc R U . . .
C38_6  C  0.6058(4)   0.1799(4)   0.5636(3)   0.071(4)   Uani 1 1 d    D U . . .
H38_6  H  0.632894    0.181771    0.562970    0.086      Uiso 1 1 calc R U . . .
C39_6  C  0.5869(4)   0.1471(5)   0.5559(4)   0.091(6)   Uani 1 1 d    D U . . .
H39_6  H  0.601727    0.126284    0.550112    0.110      Uiso 1 1 calc R U . . .
N40_6  N  0.5489(4)   0.1438(4)   0.5561(4)   0.080(4)   Uani 1 1 d    D U . . .
C41_6  C  0.5280(4)   0.1730(3)   0.5639(3)   0.065(4)   Uani 1 1 d    D U . . .
H41_6  H  0.500869    0.170866    0.563350    0.078      Uiso 1 1 calc R U . . .
N1_7   N  0.4002(4)   0.4829(4)   0.5362(3)   0.068(3)   Uani 1 1 d    D U . . .
C2_7   C  0.4082(6)   0.5169(5)   0.5261(4)   0.091(6)   Uani 1 1 d    D U . . .
H2_7   H  0.425373    0.533399    0.534224    0.109      Uiso 1 1 calc R U . . .
C3_7   C  0.3934(8)   0.5296(6)   0.5048(5)   0.115(8)   Uani 1 1 d    D U . . .
H3_7   H  0.400168    0.553900    0.498520    0.138      Uiso 1 1 calc R U . . .
C4_7   C  0.3685(8)   0.5056(6)   0.4931(5)   0.114(8)   Uani 1 1 d    D U . . .
H4_7   H  0.356897    0.513521    0.478673    0.137      Uiso 1 1 calc R U . . .
C5_7   C  0.3604(4)   0.4696(4)   0.5025(3)   0.081(4)   Uani 1 1 d    D U . . .
C6_7   C  0.3769(4)   0.4598(4)   0.5240(3)   0.068(4)   Uani 1 1 d    D U . . .
H6_7   H  0.371420    0.435238    0.530427    0.081      Uiso 1 1 calc R U . . .
C7_7   C  0.3343(4)   0.4422(5)   0.4904(3)   0.079(4)   Uani 1 1 d    D U . . .
C8_7   C  0.3370(5)   0.4352(6)   0.4667(3)   0.078(4)   Uani 1 1 d    D U . . .
H8_7   H  0.355485    0.449189    0.457898    0.094      Uiso 1 1 calc R U . . .
C9_7   C  0.3131(5)   0.4075(5)   0.4541(3)   0.074(4)   Uani 1 1 d    D U . . .
H9_7   H  0.315235    0.404613    0.437364    0.089      Uiso 1 1 calc R U . . .
C10_7  C  0.2883(4)   0.3864(4)   0.4665(3)   0.064(3)   Uani 1 1 d    D U . . .
C11_7  C  0.2834(5)   0.3926(6)   0.4916(3)   0.084(5)   Uani 1 1 d    D U . . .
C12_7  C  0.3054(4)   0.4221(6)   0.5025(3)   0.078(4)   Uani 1 1 d    D U . . .
O13_7  O  0.2962(4)   0.4334(5)   0.5260(3)   0.088(4)   Uani 1 1 d    D U . . .
C14_7  C  0.2569(5)   0.4359(6)   0.5299(4)   0.090(6)   Uani 1 1 d    D U . . .
C15_7  C  0.2428(5)   0.4681(6)   0.5402(5)   0.092(6)   Uani 1 1 d    D U . . .
H15_7  H  0.258570    0.489794    0.542940    0.111      Uiso 1 1 calc R U . . .
C16_7  C  0.2030(5)   0.4681(7)   0.5468(5)   0.096(7)   Uani 1 1 d    D U . . .
H16_7  H  0.194370    0.487660    0.557250    0.116      Uiso 1 1 calc R U . . .
C17_7  C  0.1767(4)   0.4415(5)   0.5390(4)   0.089(5)   Uani 1 1 d    D U . . .
C18_7  C  0.1914(6)   0.4102(6)   0.5259(4)   0.091(5)   Uani 1 1 d    D U . . .
C19_7  C  0.2317(5)   0.4061(5)   0.5231(3)   0.082(5)   Uani 1 1 d    D U . . .
P20_7  P  0.25041(15) 0.36651(16) 0.50863(12) 0.0764(13) Uani 1 1 d    D U . . .
C21_7  C  0.2163(5)   0.3672(5)   0.4861(3)   0.075(4)   Uani 1 1 d    D U . . .
C22_7  C  0.1774(5)   0.3755(6)   0.4913(3)   0.087(5)   Uani 1 1 d    D U . . .
C23_7  C  0.1498(5)   0.3737(6)   0.4746(3)   0.086(5)   Uani 1 1 d    D U . . .
H23_7  H  0.123653    0.377243    0.478622    0.103      Uiso 1 1 calc R U . . .
C24_7  C  0.1610(5)   0.3665(6)   0.4508(4)   0.085(5)   Uani 1 1 d    D U . . .
H24_7  H  0.141950    0.366847    0.438720    0.103      Uiso 1 1 calc R U . . .
C25_7  C  0.1976(4)   0.3592(4)   0.4446(2)   0.070(4)   Uani 1 1 d    D U . . .
C26_7  C  0.2262(5)   0.3608(6)   0.4624(3)   0.080(5)   Uani 1 1 d    D U . . .
O27_7  O  0.2646(4)   0.3588(4)   0.4562(3)   0.079(3)   Uani 1 1 d    D U . . .
O28_7  O  0.1683(4)   0.3845(5)   0.5146(3)   0.093(4)   Uani 1 1 d    D U . . .
O29_7  O  0.2638(6)   0.3302(6)   0.5205(4)   0.115(6)   Uani 1 1 d    D U . . .
C30_7  C  0.2089(4)   0.3484(4)   0.4201(2)   0.070(4)   Uani 1 1 d    D U . . .
C31_7  C  0.1956(5)   0.3691(6)   0.4007(3)   0.101(7)   Uani 1 1 d    D U . . .
H31_7  H  0.180234    0.391251    0.402868    0.121      Uiso 1 1 calc R U . . .
C32_7  C  0.2050(5)   0.3568(6)   0.3782(3)   0.094(6)   Uani 1 1 d    D U . . .
H32_7  H  0.195542    0.369943    0.364661    0.113      Uiso 1 1 calc R U . . .
C33_7  C  0.2283(6)   0.3252(6)   0.3757(3)   0.092(6)   Uani 1 1 d    D U . . .
H33_7  H  0.236798    0.318688    0.360219    0.110      Uiso 1 1 calc R U . . .
N34_7  N  0.2396(4)   0.3033(4)   0.3938(2)   0.069(3)   Uani 1 1 d    D U . . .
C35_7  C  0.2318(5)   0.3164(5)   0.4156(3)   0.074(4)   Uani 1 1 d    D U . . .
H35_7  H  0.242394    0.303077    0.428769    0.089      Uiso 1 1 calc R U . . .
C36_7  C  0.1352(3)   0.4444(4)   0.5446(3)   0.077(5)   Uani 1 1 d    D U . . .
C37_7  C  0.1153(5)   0.4787(5)   0.5442(5)   0.101(7)   Uani 1 1 d    D U . . .
H37_7  H  0.128272    0.501740    0.540173    0.122      Uiso 1 1 calc R U . . .
C38_7  C  0.0764(5)   0.4796(5)   0.5497(5)   0.108(8)   Uani 1 1 d    D U . . .
H38_7  H  0.061918    0.502617    0.548792    0.130      Uiso 1 1 calc R U . . .
C39_7  C  0.0599(5)   0.4451(4)   0.5564(4)   0.086(6)   Uani 1 1 d    D U . . .
H39_7  H  0.033112    0.444928    0.559498    0.103      Uiso 1 1 calc R U . . .
N40_7  N  0.0787(3)   0.4122(4)   0.5590(4)   0.081(5)   Uani 1 1 d    D U . . .
C41_7  C  0.1157(4)   0.4119(5)   0.5525(4)   0.082(5)   Uani 1 1 d    D U . . .
H41_7  H  0.129363    0.388360    0.553405    0.098      Uiso 1 1 calc R U . . .
N1_8   N  0.4665(4)   0.4415(3)   0.5510(3)   0.080(4)   Uani 1 1 d    D U . . .
C2_8   C  0.4991(4)   0.4602(4)   0.5465(4)   0.066(4)   Uani 1 1 d    D U . . .
H2_8   H  0.500557    0.486197    0.551365    0.079      Uiso 1 1 calc R U . . .
C3_8   C  0.5306(5)   0.4449(4)   0.5356(4)   0.072(5)   Uani 1 1 d    D U . . .
H3_8   H  0.553947    0.458815    0.534508    0.086      Uiso 1 1 calc R U . . .
C4_8   C  0.5270(4)   0.4083(3)   0.5261(3)   0.066(4)   Uani 1 1 d    D U . . .
H4_8   H  0.546651    0.397973    0.516359    0.079      Uiso 1 1 calc R U . . .
C5_8   C  0.4947(3)   0.3874(3)   0.5311(3)   0.057(3)   Uani 1 1 d    D U . . .
C6_8   C  0.4645(4)   0.4052(4)   0.5432(3)   0.080(5)   Uani 1 1 d    D U . . .
H6_8   H  0.441636    0.391005    0.545925    0.096      Uiso 1 1 calc R U . . .
C7_8   C  0.4917(4)   0.3464(3)   0.5240(3)   0.068(4)   Uani 1 1 d    D U . . .
C8_8   C  0.5214(5)   0.3209(5)   0.5274(4)   0.078(5)   Uani 1 1 d    D U . . .
H8_8   H  0.544464    0.329859    0.534415    0.094      Uiso 1 1 calc R U . . .
C9_8   C  0.5186(5)   0.2814(5)   0.5207(4)   0.076(4)   Uani 1 1 d    D U . . .
H9_8   H  0.540209    0.264947    0.521803    0.091      Uiso 1 1 calc R U . . .
C10_8  C  0.4844(5)   0.2679(4)   0.5129(3)   0.076(4)   Uani 1 1 d    D U . . .
C11_8  C  0.4525(5)   0.2928(5)   0.5100(3)   0.082(5)   Uani 1 1 d    D U . . .
C12_8  C  0.4578(4)   0.3312(5)   0.5143(3)   0.068(4)   Uani 1 1 d    D U . . .
O13_8  O  0.4262(4)   0.3551(4)   0.5073(3)   0.077(3)   Uani 1 1 d    D U . . .
C14_8  C  0.4123(4)   0.3467(5)   0.4850(3)   0.070(4)   Uani 1 1 d    D U . . .
C15_8  C  0.4081(7)   0.3760(5)   0.4693(3)   0.081(5)   Uani 1 1 d    D U . . .
H15_8  H  0.414245    0.401619    0.473611    0.097      Uiso 1 1 calc R U . . .
C16_8  C  0.3942(6)   0.3672(5)   0.4460(4)   0.082(5)   Uani 1 1 d    D U . . .
H16_8  H  0.392519    0.387451    0.434781    0.098      Uiso 1 1 calc R U . . .
C17_8  C  0.3832(5)   0.3316(4)   0.4390(3)   0.076(4)   Uani 1 1 d    D U . . .
C18_8  C  0.3898(5)   0.3017(5)   0.4556(4)   0.078(5)   Uani 1 1 d    D U . . .
C19_8  C  0.4019(5)   0.3095(5)   0.4782(3)   0.080(4)   Uani 1 1 d    D U . . .
P20_8  P  0.40914(15) 0.27384(14) 0.49965(11) 0.0721(12) Uani 1 1 d    D U . . .
C21_8  C  0.4301(5)   0.2412(5)   0.4789(3)   0.084(5)   Uani 1 1 d    D U . . .
C22_8  C  0.4164(5)   0.2391(4)   0.4553(3)   0.076(4)   Uani 1 1 d    D U . . .
C23_8  C  0.4324(6)   0.2130(6)   0.4399(4)   0.085(5)   Uani 1 1 d    D U . . .
H23_8  H  0.421699    0.208840    0.424630    0.102      Uiso 1 1 calc R U . . .
C24_8  C  0.4655(7)   0.1923(7)   0.4474(3)   0.090(6)   Uani 1 1 d    D U . . .
H24_8  H  0.478372    0.176872    0.436014    0.108      Uiso 1 1 calc R U . . .
C25_8  C  0.4798(4)   0.1933(4)   0.4698(3)   0.075(4)   Uani 1 1 d    D U . . .
C26_8  C  0.4629(5)   0.2202(4)   0.4864(3)   0.064(3)   Uani 1 1 d    D U . . .
O27_8  O  0.4812(5)   0.2288(4)   0.5080(3)   0.084(4)   Uani 1 1 d    D U . . .
O28_8  O  0.3876(4)   0.2634(4)   0.4480(3)   0.084(4)   Uani 1 1 d    D U . . .
O29_8  O  0.3783(5)   0.2588(4)   0.5142(4)   0.094(5)   Uani 1 1 d    D U . . .
C30_8  C  0.5101(4)   0.1671(4)   0.4788(2)   0.070(4)   Uani 1 1 d    D U . . .
C31_8  C  0.5432(5)   0.1597(7)   0.4660(4)   0.098(7)   Uani 1 1 d    D U . . .
H31_8  H  0.547902    0.172782    0.451472    0.118      Uiso 1 1 calc R U . . .
C32_8  C  0.5694(6)   0.1329(7)   0.4745(4)   0.114(9)   Uani 1 1 d    D U . . .
H32_8  H  0.591897    0.127044    0.465704    0.137      Uiso 1 1 calc R U . . .
C33_8  C  0.5624(5)   0.1151(6)   0.4957(3)   0.085(5)   Uani 1 1 d    D U . . .
H33_8  H  0.580074    0.096433    0.501261    0.102      Uiso 1 1 calc R U . . .
N34_8  N  0.5315(4)   0.1229(4)   0.5089(3)   0.075(4)   Uani 1 1 d    D U . . .
C35_8  C  0.5058(4)   0.1485(5)   0.5005(3)   0.067(4)   Uani 1 1 d    D U . . .
H35_8  H  0.483889    0.154105    0.509905    0.080      Uiso 1 1 calc R U . . .
C36_8  C  0.3673(4)   0.3232(4)   0.4152(3)   0.075(4)   Uani 1 1 d    D U . . .
C37_8  C  0.3818(6)   0.3410(7)   0.3951(3)   0.102(7)   Uani 1 1 d    D U . . .
H37_8  H  0.403856    0.356842    0.396250    0.123      Uiso 1 1 calc R U . . .
C38_8  C  0.3642(6)   0.3359(7)   0.3734(3)   0.110(8)   Uani 1 1 d    D U . . .
H38_8  H  0.372813    0.349266    0.359751    0.132      Uiso 1 1 calc R U . . .
C39_8  C  0.3337(5)   0.3110(6)   0.3722(3)   0.091(6)   Uani 1 1 d    D U . . .
H39_8  H  0.321871    0.306584    0.357291    0.109      Uiso 1 1 calc R U . . .
N40_8  N  0.3203(4)   0.2928(4)   0.3911(2)   0.069(3)   Uani 1 1 d    D U . . .
C41_8  C  0.3372(4)   0.2982(5)   0.4120(3)   0.079(5)   Uani 1 1 d    D U . . .
H41_8  H  0.328050    0.284178    0.425346    0.095      Uiso 1 1 calc R U . . .
N1_9   N  0.3759(4)   0.4877(5)   0.5839(4)   0.089(5)   Uani 1 1 d    D U . . .
C2_9   C  0.3772(7)   0.5221(7)   0.5937(7)   0.131(11)  Uani 1 1 d    D U . . .
H2_9   H  0.399835    0.536944    0.592071    0.157      Uiso 1 1 calc R U . . .
C3_9   C  0.3465(8)   0.5373(7)   0.6062(8)   0.143(12)  Uani 1 1 d    D U . . .
H3_9   H  0.346658    0.563061    0.611609    0.171      Uiso 1 1 calc R U . . .
C4_9   C  0.3157(7)   0.5134(6)   0.6105(7)   0.138(11)  Uani 1 1 d    D U . . .
H4_9   H  0.295991    0.521289    0.621037    0.166      Uiso 1 1 calc R U . . .
C5_9   C  0.3135(4)   0.4780(4)   0.5995(4)   0.084(6)   Uani 1 1 d    D U . . .
C6_9   C  0.3452(4)   0.4656(4)   0.5867(4)   0.080(6)   Uani 1 1 d    D U . . .
H6_9   H  0.344998    0.440742    0.579900    0.096      Uiso 1 1 calc R U . . .
C7_9   C  0.2792(4)   0.4533(4)   0.6019(3)   0.072(4)   Uani 1 1 d    D U . . .
C8_9   C  0.2428(4)   0.4659(6)   0.5960(4)   0.080(5)   Uani 1 1 d    D U . . .
H8_9   H  0.239852    0.490698    0.589323    0.096      Uiso 1 1 calc R U . . .
C9_9   C  0.2093(5)   0.4427(5)   0.5998(5)   0.086(5)   Uani 1 1 d    D U . . .
H9_9   H  0.184265    0.452804    0.597431    0.104      Uiso 1 1 calc R U . . .
C10_9  C  0.2145(4)   0.4061(5)   0.6068(3)   0.080(5)   Uani 1 1 d    D U . . .
C11_9  C  0.2517(4)   0.3928(5)   0.6120(3)   0.068(4)   Uani 1 1 d    D U . . .
C12_9  C  0.2834(4)   0.4164(4)   0.6105(3)   0.066(4)   Uani 1 1 d    D U . . .
O13_9  O  0.3191(3)   0.4059(4)   0.6185(3)   0.079(4)   Uani 1 1 d    D U . . .
C14_9  C  0.3173(4)   0.3858(5)   0.6396(3)   0.071(4)   Uani 1 1 d    D U . . .
C15_9  C  0.3421(4)   0.3954(6)   0.6576(3)   0.079(5)   Uani 1 1 d    D U . . .
H15_9  H  0.360600    0.415014    0.655295    0.095      Uiso 1 1 calc R U . . .
C16_9  C  0.3397(5)   0.3757(6)   0.6798(4)   0.085(6)   Uani 1 1 d    D U . . .
H16_9  H  0.357144    0.382675    0.691922    0.102      Uiso 1 1 calc R U . . .
C17_9  C  0.3136(4)   0.3474(4)   0.6845(2)   0.069(4)   Uani 1 1 d    D U . . .
C18_9  C  0.2862(4)   0.3394(5)   0.6667(3)   0.073(5)   Uani 1 1 d    D U . . .
C19_9  C  0.2911(4)   0.3576(4)   0.6441(3)   0.065(4)   Uani 1 1 d    D U . . .
P20_9  P  0.25846(14) 0.34493(16) 0.62183(10) 0.0707(12) Uani 1 1 d    D U . . .
C21_9  C  0.2169(4)   0.3445(5)   0.6393(3)   0.068(4)   Uani 1 1 d    D U . . .
C22_9  C  0.2200(4)   0.3299(5)   0.6627(3)   0.077(4)   Uani 1 1 d    D U . . .
C23_9  C  0.1902(4)   0.3331(6)   0.6776(3)   0.076(5)   Uani 1 1 d    D U . . .
H23_9  H  0.192912    0.326370    0.693882    0.091      Uiso 1 1 calc R U . . .
C24_9  C  0.1548(5)   0.3466(7)   0.6691(3)   0.081(5)   Uani 1 1 d    D U . . .
H24_9  H  0.132861    0.344696    0.678962    0.097      Uiso 1 1 calc R U . . .
C25_9  C  0.1508(3)   0.3626(4)   0.6467(3)   0.070(4)   Uani 1 1 d    D U . . .
C26_9  C  0.1832(4)   0.3621(5)   0.6316(3)   0.062(3)   Uani 1 1 d    D U . . .
O27_9  O  0.1837(3)   0.3817(4)   0.6106(3)   0.076(3)   Uani 1 1 d    D U . . .
O28_9  O  0.2545(3)   0.3165(3)   0.6708(3)   0.072(3)   Uani 1 1 d    D U . . .
O29_9  O  0.2636(5)   0.3131(4)   0.6048(3)   0.086(4)   Uani 1 1 d    D U . . .
C30_9  C  0.1136(3)   0.3774(5)   0.6377(2)   0.068(4)   Uani 1 1 d    D U . . .
C31_9  C  0.0909(4)   0.4028(6)   0.6510(3)   0.084(5)   Uani 1 1 d    D U . . .
H31_9  H  0.098308    0.409960    0.666590    0.101      Uiso 1 1 calc R U . . .
C32_9  C  0.0575(5)   0.4174(6)   0.6411(4)   0.113(9)   Uani 1 1 d    D U . . .
H32_9  H  0.041854    0.434846    0.649679    0.136      Uiso 1 1 calc R U . . .
C33_9  C  0.0478(5)   0.4058(7)   0.6188(4)   0.095(7)   Uani 1 1 d    D U . . .
H33_9  H  0.025385    0.416498    0.611959    0.113      Uiso 1 1 calc R U . . .
N34_9  N  0.0674(4)   0.3806(5)   0.6059(2)   0.069(3)   Uani 1 1 d    D U . . .
C35_9  C  0.1007(4)   0.3681(6)   0.6152(3)   0.075(4)   Uani 1 1 d    D U . . .
H35_9  H  0.116256    0.351933    0.605676    0.089      Uiso 1 1 calc R U . . .
C36_9  C  0.3137(4)   0.3250(4)   0.7069(2)   0.070(4)   Uani 1 1 d    D U . . .
C37_9  C  0.3211(5)   0.3416(4)   0.7288(3)   0.073(4)   Uani 1 1 d    D U . . .
H37_9  H  0.325298    0.368385    0.730031    0.088      Uiso 1 1 calc R U . . .
C38_9  C  0.3223(6)   0.3185(4)   0.7490(3)   0.086(5)   Uani 1 1 d    D U . . .
H38_9  H  0.327749    0.329327    0.764087    0.103      Uiso 1 1 calc R U . . .
C39_9  C  0.3154(6)   0.2793(5)   0.7468(3)   0.077(5)   Uani 1 1 d    D U . . .
H39_9  H  0.316585    0.263604    0.760483    0.092      Uiso 1 1 calc R U . . .
N40_9  N  0.3071(5)   0.2634(3)   0.7260(2)   0.070(4)   Uani 1 1 d    D U . . .
C41_9  C  0.3072(6)   0.2857(4)   0.7065(2)   0.068(4)   Uani 1 1 d    D U . . .
H41_9  H  0.302491    0.273903    0.691649    0.081      Uiso 1 1 calc R U . . .
Pd1_10 Pd 0.54720(4)  0.60204(3)  0.57302(3)  0.0595(3)  Uani 1 1 d    . . . . .
Pd2_10 Pd 0.77343(4)  0.70024(4)  0.39361(2)  0.0583(3)  Uani 1 1 d    . . . . .
Pd3_10 Pd 1.01976(3)  0.86942(4)  0.54371(2)  0.0561(3)  Uani 1 1 d    . . . . .
Pd4_10 Pd 0.64891(4)  0.96567(3)  0.54185(3)  0.0600(3)  Uani 1 1 d    . . . . .
Pd5_10 Pd 0.92060(4)  0.49857(4)  0.57518(3)  0.0605(3)  Uani 1 1 d    . . . . .
Pd6_10 Pd 0.79522(4)  0.76856(5)  0.72453(3)  0.0668(3)  Uani 1 1 d    . . . . .
N1_11  N  0.5365(4)   0.6289(4)   0.6038(3)   0.071(4)   Uani 1 1 d    D U . . .
C2_11  C  0.5048(5)   0.6255(6)   0.6171(4)   0.092(6)   Uani 1 1 d    D U . . .
H2_11  H  0.483962    0.611049    0.610889    0.111      Uiso 1 1 calc R U . . .
C3_11  C  0.5009(5)   0.6417(6)   0.6390(4)   0.088(6)   Uani 1 1 d    D U . . .
H3_11  H  0.479648    0.635387    0.648857    0.106      Uiso 1 1 calc R U . . .
C4_11  C  0.5284(5)   0.6675(6)   0.6467(3)   0.083(5)   Uani 1 1 d    D U . . .
H4_11  H  0.524801    0.681696    0.660930    0.099      Uiso 1 1 calc R U . . .
C5_11  C  0.5613(4)   0.6722(4)   0.6331(3)   0.076(4)   Uani 1 1 d    D U . . .
C6_11  C  0.5636(4)   0.6525(4)   0.6117(3)   0.070(4)   Uani 1 1 d    D U . . .
H6_11  H  0.585780    0.656082    0.602140    0.085      Uiso 1 1 calc R U . . .
C7_11  C  0.5931(4)   0.6979(4)   0.6410(3)   0.074(4)   Uani 1 1 d    D U . . .
C8_11  C  0.6052(6)   0.6973(5)   0.6643(3)   0.077(5)   Uani 1 1 d    D U . . .
H8_11  H  0.592546    0.681401    0.675544    0.092      Uiso 1 1 calc R U . . .
C9_11  C  0.6370(6)   0.7206(6)   0.6717(4)   0.085(5)   Uani 1 1 d    D U . . .
H9_11  H  0.645821    0.719098    0.687570    0.102      Uiso 1 1 calc R U . . .
C10_11 C  0.6545(5)   0.7447(4)   0.6564(3)   0.074(4)   Uani 1 1 d    D U . . .
C11_11 C  0.6432(5)   0.7467(4)   0.6318(3)   0.068(4)   Uani 1 1 d    D U . . .
C12_11 C  0.6119(5)   0.7232(4)   0.6252(3)   0.072(4)   Uani 1 1 d    D U . . .
O13_11 O  0.5957(5)   0.7303(3)   0.6027(3)   0.079(3)   Uani 1 1 d    D U . . .
C14_11 C  0.5911(5)   0.7675(4)   0.5954(3)   0.077(5)   Uani 1 1 d    D U . . .
C15_11 C  0.5576(6)   0.7796(6)   0.5852(5)   0.097(7)   Uani 1 1 d    D U . . .
H15_11 H  0.537932    0.761723    0.581547    0.116      Uiso 1 1 calc R U . . .
C16_11 C  0.5528(6)   0.8184(5)   0.5802(4)   0.087(5)   Uani 1 1 d    D U . . .
H16_11 H  0.528891    0.826668    0.573934    0.104      Uiso 1 1 calc R U . . .
C17_11 C  0.5813(5)   0.8458(4)   0.5839(3)   0.074(4)   Uani 1 1 d    D U . . .
C18_11 C  0.6159(4)   0.8334(5)   0.5947(3)   0.067(4)   Uani 1 1 d    D U . . .
C19_11 C  0.6213(5)   0.7947(5)   0.5990(3)   0.069(4)   Uani 1 1 d    D U . . .
P20_11 P  0.66464(15) 0.77733(14) 0.61226(10) 0.0697(12) Uani 1 1 d    D U . . .
C21_11 C  0.6683(5)   0.8145(5)   0.6321(3)   0.079(4)   Uani 1 1 d    D U . . .
C22_11 C  0.6565(4)   0.8522(5)   0.6259(3)   0.073(4)   Uani 1 1 d    D U . . .
C23_11 C  0.6587(6)   0.8812(6)   0.6418(3)   0.090(5)   Uani 1 1 d    D U . . .
H23_11 H  0.651860    0.906550    0.637302    0.108      Uiso 1 1 calc R U . . .
C24_11 C  0.6718(5)   0.8732(5)   0.6659(3)   0.074(4)   Uani 1 1 d    D U . . .
H24_11 H  0.671774    0.893261    0.677251    0.089      Uiso 1 1 calc R U . . .
C25_11 C  0.6841(5)   0.8372(5)   0.6726(3)   0.084(5)   Uani 1 1 d    D U . . .
C26_11 C  0.6797(5)   0.8076(5)   0.6560(3)   0.077(4)   Uani 1 1 d    D U . . .
O27_11 O  0.6825(5)   0.7699(4)   0.6637(3)   0.085(4)   Uani 1 1 d    D U . . .
O28_11 O  0.6437(4)   0.8587(4)   0.6030(3)   0.087(4)   Uani 1 1 d    D U . . .
O29_11 O  0.6977(4)   0.7652(4)   0.5973(2)   0.072(3)   Uani 1 1 d    D U . . .
C30_11 C  0.6998(5)   0.8303(4)   0.6966(2)   0.079(4)   Uani 1 1 d    D U . . .
C31_11 C  0.6849(6)   0.8488(6)   0.7164(3)   0.090(5)   Uani 1 1 d    D U . . .
H31_11 H  0.664228    0.866291    0.714940    0.108      Uiso 1 1 calc R U . . .
C32_11 C  0.7012(5)   0.8410(5)   0.7381(3)   0.077(4)   Uani 1 1 d    D U . . .
H32_11 H  0.690572    0.852397    0.751943    0.092      Uiso 1 1 calc R U . . .
C33_11 C  0.7324(5)   0.8170(5)   0.7404(3)   0.079(4)   Uani 1 1 d    D U . . .
H33_11 H  0.742331    0.811002    0.755623    0.095      Uiso 1 1 calc R U . . .
N34_11 N  0.7484(4)   0.8022(5)   0.7208(3)   0.084(4)   Uani 1 1 d    D U . . .
C35_11 C  0.7310(5)   0.8070(6)   0.7001(3)   0.081(5)   Uani 1 1 d    D U . . .
H35_11 H  0.740735    0.793438    0.686762    0.097      Uiso 1 1 calc R U . . .
C36_11 C  0.5763(4)   0.8864(4)   0.5763(3)   0.081(5)   Uani 1 1 d    D U . . .
C37_11 C  0.5420(5)   0.9058(5)   0.5807(5)   0.106(8)   Uani 1 1 d    D U . . .
H37_11 H  0.521356    0.893789    0.588728    0.127      Uiso 1 1 calc R U . . .
C38_11 C  0.5394(5)   0.9438(5)   0.5729(4)   0.087(6)   Uani 1 1 d    D U . . .
H38_11 H  0.516611    0.958148    0.575107    0.105      Uiso 1 1 calc R U . . .
C39_11 C  0.5706(5)   0.9597(5)   0.5618(4)   0.091(6)   Uani 1 1 d    D U . . .
H39_11 H  0.568373    0.985529    0.556625    0.109      Uiso 1 1 calc R U . . .
N40_11 N  0.6039(4)   0.9421(4)   0.5578(3)   0.071(4)   Uani 1 1 d    D U . . .
C41_11 C  0.6059(5)   0.9057(4)   0.5650(4)   0.078(5)   Uani 1 1 d    D U . . .
H41_11 H  0.628991    0.892133    0.562086    0.094      Uiso 1 1 calc R U . . .
N1_12  N  0.8287(4)   0.8143(4)   0.7182(2)   0.073(4)   Uani 1 1 d    D U . . .
C2_12  C  0.8420(6)   0.8359(6)   0.7358(3)   0.086(5)   Uani 1 1 d    D U . . .
H2_12  H  0.834288    0.829819    0.751491    0.104      Uiso 1 1 calc R U . . .
C3_12  C  0.8665(6)   0.8668(6)   0.7326(3)   0.089(5)   Uani 1 1 d    D U . . .
H3_12  H  0.874725    0.881956    0.745623    0.107      Uiso 1 1 calc R U . . .
C4_12  C  0.8786(6)   0.8746(6)   0.7098(3)   0.087(5)   Uani 1 1 d    D U . . .
H4_12  H  0.897769    0.893390    0.707004    0.105      Uiso 1 1 calc R U . . .
C5_12  C  0.8623(4)   0.8544(4)   0.6908(2)   0.071(4)   Uani 1 1 d    D U . . .
C6_12  C  0.8380(4)   0.8242(4)   0.6962(3)   0.073(4)   Uani 1 1 d    D U . . .
H6_12  H  0.827493    0.809812    0.683513    0.088      Uiso 1 1 calc R U . . .
C7_12  C  0.8728(5)   0.8635(6)   0.6659(2)   0.087(5)   Uani 1 1 d    D U . . .
C8_12  C  0.9102(4)   0.8727(6)   0.6597(3)   0.080(5)   Uani 1 1 d    D U . . .
H8_12  H  0.928863    0.874700    0.671857    0.096      Uiso 1 1 calc R U . . .
C9_12  C  0.9217(5)   0.8793(8)   0.6359(3)   0.088(5)   Uani 1 1 d    D U . . .
H9_12  H  0.947585    0.884871    0.632111    0.105      Uiso 1 1 calc R U . . .
C10_12 C  0.8947(5)   0.8773(6)   0.6187(3)   0.086(5)   Uani 1 1 d    D U . . .
C11_12 C  0.8562(5)   0.8668(6)   0.6237(4)   0.085(5)   Uani 1 1 d    D U . . .
C12_12 C  0.8457(6)   0.8616(7)   0.6477(4)   0.101(6)   Uani 1 1 d    D U . . .
O13_12 O  0.8064(4)   0.8569(4)   0.6532(3)   0.083(4)   Uani 1 1 d    D U . . .
C14_12 C  0.7831(4)   0.8829(4)   0.6410(3)   0.067(3)   Uani 1 1 d    D U . . .
C15_12 C  0.7548(6)   0.9007(6)   0.6538(4)   0.086(5)   Uani 1 1 d    D U . . .
H15_12 H  0.749486    0.893544    0.669681    0.103      Uiso 1 1 calc R U . . .
C16_12 C  0.7340(5)   0.9300(7)   0.6424(3)   0.087(6)   Uani 1 1 d    D U . . .
H16_12 H  0.716968    0.944782    0.651827    0.104      Uiso 1 1 calc R U . . .
C17_12 C  0.7364(4)   0.9387(5)   0.6189(3)   0.075(4)   Uani 1 1 d    D U . . .
C18_12 C  0.7656(4)   0.9214(6)   0.6055(3)   0.077(4)   Uani 1 1 d    D U . . .
C19_12 C  0.7867(4)   0.8915(5)   0.6166(3)   0.069(4)   Uani 1 1 d    D U . . .
P20_12 P  0.82228(15) 0.86598(16) 0.60105(10) 0.0726(12) Uani 1 1 d    D U . . .
C21_12 C  0.8395(5)   0.9063(5)   0.5860(3)   0.082(5)   Uani 1 1 d    D U . . .
C22_12 C  0.8137(4)   0.9360(5)   0.5786(3)   0.078(4)   Uani 1 1 d    D U . . .
C23_12 C  0.8274(4)   0.9698(5)   0.5700(4)   0.073(4)   Uani 1 1 d    D U . . .
H23_12 H  0.811332    0.991470    0.567724    0.088      Uiso 1 1 calc R U . . .
C24_12 C  0.8675(4)   0.9705(5)   0.5645(3)   0.070(4)   Uani 1 1 d    D U . . .
H24_12 H  0.876593    0.990578    0.554635    0.084      Uiso 1 1 calc R U . . .
C25_12 C  0.8936(3)   0.9446(5)   0.5725(3)   0.077(4)   Uani 1 1 d    D U . . .
C26_12 C  0.8780(5)   0.9117(5)   0.5847(3)   0.074(4)   Uani 1 1 d    D U . . .
O27_12 O  0.9040(4)   0.8883(5)   0.5959(3)   0.092(4)   Uani 1 1 d    D U . . .
O28_12 O  0.7756(3)   0.9329(5)   0.5825(2)   0.081(4)   Uani 1 1 d    D U . . .
O29_12 O  0.8130(6)   0.8309(5)   0.5881(3)   0.098(5)   Uani 1 1 d    D U . . .
C30_12 C  0.9354(3)   0.9478(4)   0.5686(3)   0.082(5)   Uani 1 1 d    D U . . .
C31_12 C  0.9551(4)   0.9823(5)   0.5713(4)   0.092(6)   Uani 1 1 d    D U . . .
H31_12 H  0.941797    1.004605    0.576299    0.110      Uiso 1 1 calc R U . . .
C32_12 C  0.9941(4)   0.9838(5)   0.5667(4)   0.087(5)   Uani 1 1 d    D U . . .
H32_12 H  1.008163    1.006925    0.568714    0.104      Uiso 1 1 calc R U . . .
C33_12 C  1.0120(5)   0.9504(5)   0.5591(4)   0.087(6)   Uani 1 1 d    D U . . .
H33_12 H  1.038923    0.950914    0.556520    0.105      Uiso 1 1 calc R U . . .
N34_12 N  0.9931(3)   0.9176(4)   0.5552(3)   0.071(4)   Uani 1 1 d    D U . . .
C35_12 C  0.9555(3)   0.9165(4)   0.5603(4)   0.068(4)   Uani 1 1 d    D U . . .
H35_12 H  0.942141    0.893000    0.558212    0.082      Uiso 1 1 calc R U . . .
C36_12 C  0.7096(4)   0.9656(4)   0.6069(2)   0.070(4)   Uani 1 1 d    D U . . .
C37_12 C  0.6989(6)   0.9991(4)   0.6186(3)   0.085(5)   Uani 1 1 d    D U . . .
H37_12 H  0.708943    1.005060    0.633793    0.102      Uiso 1 1 calc R U . . .
C38_12 C  0.6731(6)   1.0237(4)   0.6075(3)   0.094(6)   Uani 1 1 d    D U . . .
H38_12 H  0.665240    1.046912    0.614816    0.113      Uiso 1 1 calc R U . . .
C39_12 C  0.6594(5)   1.0127(4)   0.5854(3)   0.075(4)   Uani 1 1 d    D U . . .
H39_12 H  0.640560    1.028521    0.578173    0.090      Uiso 1 1 calc R U . . .
N40_12 N  0.6708(4)   0.9817(4)   0.5734(3)   0.068(3)   Uani 1 1 d    D U . . .
C41_12 C  0.6964(4)   0.9588(4)   0.5842(2)   0.063(3)   Uani 1 1 d    D U . . .
H41_12 H  0.705835    0.937165    0.575836    0.075      Uiso 1 1 calc R U . . .
N1_13  N  0.8442(4)   0.7380(4)   0.7265(2)   0.077(4)   Uani 1 1 d    D U . . .
C2_13  C  0.8613(6)   0.7286(8)   0.7467(3)   0.097(6)   Uani 1 1 d    D U . . .
H2_13  H  0.850003    0.737833    0.760976    0.117      Uiso 1 1 calc R U . . .
C3_13  C  0.8940(7)   0.7067(9)   0.7488(3)   0.107(7)   Uani 1 1 d    D U . . .
H3_13  H  0.906550    0.703311    0.763639    0.129      Uiso 1 1 calc R U . . .
C4_13  C  0.9075(6)   0.6899(6)   0.7283(3)   0.090(5)   Uani 1 1 d    D U . . .
H4_13  H  0.929377    0.673741    0.728709    0.108      Uiso 1 1 calc R U . . .
C5_13  C  0.8885(4)   0.6968(5)   0.7069(2)   0.081(4)   Uani 1 1 d    D U . . .
C6_13  C  0.8571(4)   0.7212(4)   0.7069(3)   0.072(4)   Uani 1 1 d    D U . . .
H6_13  H  0.844432    0.726132    0.692267    0.087      Uiso 1 1 calc R U . . .
C7_13  C  0.9023(5)   0.6789(4)   0.6846(3)   0.080(4)   Uani 1 1 d    D U . . .
C8_13  C  0.9131(6)   0.6408(4)   0.6833(3)   0.077(4)   Uani 1 1 d    D U . . .
H8_13  H  0.914481    0.626441    0.697558    0.093      Uiso 1 1 calc R U . . .
C9_13  C  0.9221(7)   0.6222(6)   0.6614(3)   0.097(6)   Uani 1 1 d    D U . . .
H9_13  H  0.926967    0.595400    0.660982    0.116      Uiso 1 1 calc R U . . .
C10_13 C  0.9237(4)   0.6436(5)   0.6413(3)   0.073(4)   Uani 1 1 d    D U . . .
C11_13 C  0.9139(4)   0.6832(5)   0.6418(3)   0.072(4)   Uani 1 1 d    D U . . .
C12_13 C  0.9057(4)   0.7013(5)   0.6636(3)   0.065(3)   Uani 1 1 d    D U . . .
O13_13 O  0.9036(4)   0.7409(4)   0.6652(3)   0.080(3)   Uani 1 1 d    D U . . .
C14_13 C  0.9320(5)   0.7602(5)   0.6520(3)   0.083(5)   Uani 1 1 d    D U . . .
C15_13 C  0.9488(5)   0.7905(5)   0.6625(3)   0.073(4)   Uani 1 1 d    D U . . .
H15_13 H  0.941598    0.798314    0.678007    0.087      Uiso 1 1 calc R U . . .
C16_13 C  0.9784(5)   0.8109(5)   0.6495(3)   0.067(4)   Uani 1 1 d    D U . . .
H16_13 H  0.990301    0.832479    0.656619    0.081      Uiso 1 1 calc R U . . .
C17_13 C  0.9896(4)   0.8001(5)   0.6272(3)   0.070(4)   Uani 1 1 d    D U . . .
C18_13 C  0.9747(5)   0.7655(4)   0.6171(3)   0.069(4)   Uani 1 1 d    D U . . .
C19_13 C  0.9430(5)   0.7480(4)   0.6294(3)   0.071(4)   Uani 1 1 d    D U . . .
P20_13 P  0.91937(15) 0.71010(15) 0.61615(11) 0.0744(13) Uani 1 1 d    D U . . .
C21_13 C  0.9613(5)   0.6884(5)   0.6059(3)   0.074(4)   Uani 1 1 d    D U . . .
C22_13 C  0.9923(5)   0.7090(4)   0.5979(3)   0.077(4)   Uani 1 1 d    D U . . .
C23_13 C  1.0257(5)   0.6920(5)   0.5908(5)   0.087(6)   Uani 1 1 d    D U . . .
H23_13 H  1.047600    0.706729    0.586617    0.104      Uiso 1 1 calc R U . . .
C24_13 C  1.0261(6)   0.6508(5)   0.5898(4)   0.086(6)   Uani 1 1 d    D U . . .
H24_13 H  1.047641    0.638423    0.583013    0.103      Uiso 1 1 calc R U . . .
C25_13 C  0.9959(4)   0.6282(3)   0.5985(3)   0.068(4)   Uani 1 1 d    D U . . .
C26_13 C  0.9631(4)   0.6469(4)   0.6079(3)   0.068(4)   Uani 1 1 d    D U . . .
O27_13 O  0.9342(4)   0.6274(4)   0.6201(3)   0.079(4)   Uani 1 1 d    D U . . .
O28_13 O  0.9896(5)   0.7490(4)   0.5974(3)   0.089(4)   Uani 1 1 d    D U . . .
O29_13 O  0.8861(5)   0.7169(5)   0.6001(3)   0.093(4)   Uani 1 1 d    D U . . .
C30_13 C  0.9980(4)   0.5857(3)   0.5982(3)   0.079(5)   Uani 1 1 d    D U . . .
C31_13 C  1.0292(5)   0.5659(4)   0.6073(4)   0.080(5)   Uani 1 1 d    D U . . .
H31_13 H  1.050397    0.579264    0.613839    0.096      Uiso 1 1 calc R U . . .
C32_13 C  1.0287(5)   0.5263(5)   0.6065(4)   0.104(8)   Uani 1 1 d    D U . . .
H32_13 H  1.049804    0.511927    0.612361    0.125      Uiso 1 1 calc R U . . .
C33_13 C  0.9971(4)   0.5078(4)   0.5972(4)   0.086(6)   Uani 1 1 d    D U . . .
H33_13 H  0.996911    0.480613    0.597009    0.103      Uiso 1 1 calc R U . . .
N34_13 N  0.9672(3)   0.5261(3)   0.5885(4)   0.076(4)   Uani 1 1 d    D U . . .
C35_13 C  0.9667(4)   0.5642(3)   0.5905(4)   0.069(4)   Uani 1 1 d    D U . . .
H35_13 H  0.943779    0.577388    0.586502    0.083      Uiso 1 1 calc R U . . .
C36_13 C  1.0179(4)   0.8228(4)   0.6136(2)   0.070(4)   Uani 1 1 d    D U . . .
C37_13 C  1.0512(4)   0.8366(6)   0.6241(3)   0.079(5)   Uani 1 1 d    D U . . .
H37_13 H  1.057753    0.829313    0.639788    0.095      Uiso 1 1 calc R U . . .
C38_13 C  1.0747(5)   0.8613(6)   0.6113(3)   0.084(5)   Uani 1 1 d    D U . . .
H38_13 H  1.096976    0.872075    0.618321    0.101      Uiso 1 1 calc R U . . .
C39_13 C  1.0650(5)   0.8697(5)   0.5881(3)   0.079(5)   Uani 1 1 d    D U . . .
H39_13 H  1.081121    0.886496    0.579383    0.095      Uiso 1 1 calc R U . . .
N40_13 N  1.0340(3)   0.8552(4)   0.5775(3)   0.069(3)   Uani 1 1 d    D U . . .
C41_13 C  1.0109(4)   0.8322(4)   0.5900(2)   0.062(3)   Uani 1 1 d    D U . . .
H41_13 H  0.988869    0.821861    0.582484    0.074      Uiso 1 1 calc R U . . .
N1_14  N  0.7623(4)   0.7212(4)   0.7286(3)   0.066(3)   Uani 1 1 d    D U . . .
C2_14  C  0.7548(6)   0.7074(6)   0.7500(3)   0.088(5)   Uani 1 1 d    D U . . .
H2_14  H  0.768544    0.717487    0.763102    0.105      Uiso 1 1 calc R U . . .
C3_14  C  0.7279(8)   0.6791(7)   0.7541(3)   0.099(7)   Uani 1 1 d    D U . . .
H3_14  H  0.718268    0.674641    0.769645    0.119      Uiso 1 1 calc R U . . .
C4_14  C  0.7152(6)   0.6572(7)   0.7348(3)   0.095(6)   Uani 1 1 d    D U . . .
H4_14  H  0.699848    0.635050    0.737007    0.114      Uiso 1 1 calc R U . . .
C5_14  C  0.7261(4)   0.6691(4)   0.7121(2)   0.075(4)   Uani 1 1 d    D U . . .
C6_14  C  0.7494(5)   0.7010(5)   0.7102(3)   0.084(5)   Uani 1 1 d    D U . . .
H6_14  H  0.756593    0.709121    0.694713    0.101      Uiso 1 1 calc R U . . .
C7_14  C  0.7110(4)   0.6508(5)   0.6901(3)   0.086(5)   Uani 1 1 d    D U . . .
C8_14  C  0.6735(5)   0.6392(8)   0.6877(4)   0.096(7)   Uani 1 1 d    D U . . .
H8_14  H  0.656945    0.639375    0.701090    0.115      Uiso 1 1 calc R U . . .
C9_14  C  0.6594(6)   0.6267(7)   0.6652(3)   0.091(5)   Uani 1 1 d    D U . . .
H9_14  H  0.632885    0.621431    0.663196    0.109      Uiso 1 1 calc R U . . .
C10_14 C  0.6835(5)   0.6226(5)   0.6469(3)   0.080(5)   Uani 1 1 d    D U . . .
C11_14 C  0.7227(5)   0.6312(5)   0.6490(4)   0.087(5)   Uani 1 1 d    D U . . .
C12_14 C  0.7365(4)   0.6429(5)   0.6703(4)   0.083(5)   Uani 1 1 d    D U . . .
O13_14 O  0.7751(4)   0.6461(5)   0.6734(4)   0.109(6)   Uani 1 1 d    D U . . .
C14_14 C  0.7976(4)   0.6163(6)   0.6658(4)   0.093(6)   Uani 1 1 d    D U . . .
C15_14 C  0.8273(7)   0.6022(9)   0.6789(5)   0.118(8)   Uani 1 1 d    D U . . .
H15_14 H  0.831517    0.610532    0.694750    0.142      Uiso 1 1 calc R U . . .
C16_14 C  0.8516(7)   0.5749(9)   0.6682(5)   0.114(9)   Uani 1 1 d    D U . . .
H16_14 H  0.875672    0.569936    0.675463    0.137      Uiso 1 1 calc R U . . .
C17_14 C  0.8423(6)   0.5550(5)   0.6479(4)   0.111(8)   Uani 1 1 d    D U . . .
C18_14 C  0.8093(5)   0.5676(6)   0.6352(4)   0.085(5)   Uani 1 1 d    D U . . .
C19_14 C  0.7905(5)   0.6006(5)   0.6435(3)   0.084(5)   Uani 1 1 d    D U . . .
P20_14 P  0.75361(17) 0.62213(16) 0.62535(12) 0.0798(14) Uani 1 1 d    D U . . .
C21_14 C  0.7324(5)   0.5776(5)   0.6176(3)   0.081(5)   Uani 1 1 d    D U . . .
C22_14 C  0.7558(4)   0.5460(5)   0.6133(4)   0.082(5)   Uani 1 1 d    D U . . .
C23_14 C  0.7387(5)   0.5127(5)   0.6079(4)   0.078(5)   Uani 1 1 d    D U . . .
H23_14 H  0.754164    0.490853    0.604787    0.093      Uiso 1 1 calc R U . . .
C24_14 C  0.6982(5)   0.5092(5)   0.6066(4)   0.079(4)   Uani 1 1 d    D U . . .
H24_14 H  0.687073    0.485254    0.602460    0.094      Uiso 1 1 calc R U . . .
C25_14 C  0.6754(3)   0.5397(5)   0.6111(3)   0.075(4)   Uani 1 1 d    D U . . .
C26_14 C  0.6933(5)   0.5751(5)   0.6180(4)   0.086(5)   Uani 1 1 d    D U . . .
O27_14 O  0.6695(4)   0.6048(5)   0.6259(3)   0.083(4)   Uani 1 1 d    D U . . .
O28_14 O  0.7948(3)   0.5479(6)   0.6159(3)   0.101(5)   Uani 1 1 d    D U . . .
O29_14 O  0.7637(4)   0.6481(5)   0.6059(3)   0.087(4)   Uani 1 1 d    D U . . .
C30_14 C  0.6327(3)   0.5379(5)   0.6097(3)   0.082(5)   Uani 1 1 d    D U . . .
C31_14 C  0.6117(5)   0.5102(7)   0.6222(4)   0.104(8)   Uani 1 1 d    D U . . .
H31_14 H  0.624177    0.492686    0.632533    0.125      Uiso 1 1 calc R U . . .
C32_14 C  0.5721(5)   0.5088(7)   0.6191(4)   0.125(11)  Uani 1 1 d    D U . . .
H32_14 H  0.557297    0.489862    0.627026    0.150      Uiso 1 1 calc R U . . .
C33_14 C  0.5545(5)   0.5352(6)   0.6043(4)   0.085(6)   Uani 1 1 d    D U . . .
H33_14 H  0.527515    0.533859    0.602201    0.103      Uiso 1 1 calc R U . . .
N34_14 N  0.5737(4)   0.5623(4)   0.5929(3)   0.071(3)   Uani 1 1 d    D U . . .
C35_14 C  0.6119(4)   0.5614(5)   0.5946(3)   0.068(4)   Uani 1 1 d    D U . . .
H35_14 H  0.625994    0.578263    0.584683    0.082      Uiso 1 1 calc R U . . .
C36_14 C  0.8642(5)   0.5214(5)   0.6392(3)   0.090(5)   Uani 1 1 d    D U . . .
C37_14 C  0.8692(8)   0.4881(6)   0.6525(4)   0.105(7)   Uani 1 1 d    D U . . .
H37_14 H  0.857855    0.485857    0.667795    0.127      Uiso 1 1 calc R U . . .
C38_14 C  0.8909(7)   0.4585(6)   0.6433(4)   0.115(8)   Uani 1 1 d    D U . . .
H38_14 H  0.895187    0.436125    0.652513    0.138      Uiso 1 1 calc R U . . .
C39_14 C  0.9063(6)   0.4611(4)   0.6211(3)   0.086(5)   Uani 1 1 d    D U . . .
H39_14 H  0.921197    0.440549    0.615089    0.103      Uiso 1 1 calc R U . . .
N40_14 N  0.9008(5)   0.4922(4)   0.6078(3)   0.082(4)   Uani 1 1 d    D U . . .
C41_14 C  0.8815(7)   0.5215(6)   0.6170(3)   0.095(6)   Uani 1 1 d    D U . . .
H41_14 H  0.879444    0.544085    0.607713    0.114      Uiso 1 1 calc R U . . .
N1_15  N  0.8739(3)   0.4708(3)   0.5637(3)   0.068(4)   Uani 1 1 d    D U . . .
C2_15  C  0.8713(4)   0.4328(4)   0.5608(5)   0.078(5)   Uani 1 1 d    D U . . .
H2_15  H  0.893774    0.417897    0.563142    0.094      Uiso 1 1 calc R U . . .
C3_15  C  0.8381(5)   0.4141(5)   0.5548(5)   0.092(7)   Uani 1 1 d    D U . . .
H3_15  H  0.837046    0.386874    0.554530    0.111      Uiso 1 1 calc R U . . .
C4_15  C  0.8061(4)   0.4358(4)   0.5490(4)   0.071(4)   Uani 1 1 d    D U . . .
H4_15  H  0.783241    0.423715    0.543698    0.086      Uiso 1 1 calc R U . . .
C5_15  C  0.8081(3)   0.4758(4)   0.5510(3)   0.070(4)   Uani 1 1 d    D U . . .
C6_15  C  0.8427(3)   0.4915(4)   0.5583(3)   0.061(4)   Uani 1 1 d    D U . . .
H6_15  H  0.844373    0.518578    0.559594    0.074      Uiso 1 1 calc R U . . .
C7_15  C  0.7738(4)   0.4996(5)   0.5461(4)   0.084(5)   Uani 1 1 d    D U . . .
C8_15  C  0.7370(4)   0.4883(5)   0.5529(4)   0.073(4)   Uani 1 1 d    D U . . .
H8_15  H  0.733217    0.463417    0.559368    0.087      Uiso 1 1 calc R U . . .
C9_15  C  0.7050(5)   0.5135(5)   0.5502(3)   0.070(4)   Uani 1 1 d    D U . . .
H9_15  H  0.680822    0.506890    0.556716    0.084      Uiso 1 1 calc R U . . .
C10_15 C  0.7096(4)   0.5470(4)   0.5382(3)   0.070(4)   Uani 1 1 d    D U . . .
C11_15 C  0.7466(4)   0.5591(5)   0.5306(3)   0.071(4)   Uani 1 1 d    D U . . .
C12_15 C  0.7778(4)   0.5341(5)   0.5337(3)   0.065(4)   Uani 1 1 d    D U . . .
O13_15 O  0.8121(3)   0.5430(5)   0.5220(2)   0.076(3)   Uani 1 1 d    D U . . .
C14_15 C  0.8079(4)   0.5568(4)   0.4990(3)   0.065(4)   Uani 1 1 d    D U . . .
C15_15 C  0.8287(4)   0.5392(5)   0.4818(3)   0.066(4)   Uani 1 1 d    D U . . .
H15_15 H  0.845711    0.518727    0.485350    0.080      Uiso 1 1 calc R U . . .
C16_15 C  0.8237(5)   0.5526(5)   0.4584(3)   0.071(4)   Uani 1 1 d    D U . . .
H16_15 H  0.839714    0.541865    0.446424    0.085      Uiso 1 1 calc R U . . .
C17_15 C  0.7981(4)   0.5793(4)   0.4516(2)   0.063(3)   Uani 1 1 d    D U . . .
C18_15 C  0.7752(5)   0.5944(4)   0.4701(3)   0.067(4)   Uani 1 1 d    D U . . .
C19_15 C  0.7813(5)   0.5840(5)   0.4940(3)   0.073(4)   Uani 1 1 d    D U . . .
P20_15 P  0.75181(13) 0.60218(14) 0.51572(10) 0.0653(11) Uani 1 1 d    D U . . .
C21_15 C  0.7090(4)   0.5990(5)   0.5002(3)   0.069(4)   Uani 1 1 d    D U . . .
C22_15 C  0.7094(4)   0.6087(4)   0.4762(3)   0.066(3)   Uani 1 1 d    D U . . .
C23_15 C  0.6761(5)   0.6088(8)   0.4648(4)   0.095(6)   Uani 1 1 d    D U . . .
H23_15 H  0.674339    0.621695    0.450039    0.114      Uiso 1 1 calc R U . . .
C24_15 C  0.6430(5)   0.5904(5)   0.4740(3)   0.070(4)   Uani 1 1 d    D U . . .
H24_15 H  0.622325    0.584011    0.463828    0.084      Uiso 1 1 calc R U . . .
C25_15 C  0.6412(4)   0.5818(4)   0.4980(3)   0.065(3)   Uani 1 1 d    D U . . .
C26_15 C  0.6758(4)   0.5837(4)   0.5105(3)   0.057(3)   Uani 1 1 d    D U . . .
O27_15 O  0.6786(3)   0.5715(4)   0.5336(2)   0.071(3)   Uani 1 1 d    D U . . .
O28_15 O  0.7434(4)   0.6164(4)   0.4652(3)   0.074(3)   Uani 1 1 d    D U . . .
O29_15 O  0.7614(5)   0.6377(6)   0.5286(4)   0.101(5)   Uani 1 1 d    D U . . .
C30_15 C  0.6047(4)   0.5706(4)   0.5093(2)   0.071(4)   Uani 1 1 d    D U . . .
C31_15 C  0.5798(5)   0.5453(6)   0.4979(3)   0.090(6)   Uani 1 1 d    D U . . .
H31_15 H  0.586420    0.534799    0.482850    0.108      Uiso 1 1 calc R U . . .
C32_15 C  0.5454(5)   0.5356(6)   0.5086(4)   0.102(7)   Uani 1 1 d    D U . . .
H32_15 H  0.528044    0.518381    0.501244    0.122      Uiso 1 1 calc R U . . .
C33_15 C  0.5373(6)   0.5519(7)   0.5305(4)   0.097(7)   Uani 1 1 d    D U . . .
H33_15 H  0.513436    0.546057    0.537793    0.116      Uiso 1 1 calc R U . . .
N34_15 N  0.5613(4)   0.5755(3)   0.5419(2)   0.065(3)   Uani 1 1 d    D U . . .
C35_15 C  0.5941(4)   0.5847(4)   0.5314(2)   0.062(3)   Uani 1 1 d    D U . . .
H35_15 H  0.611099    0.601638    0.539335    0.075      Uiso 1 1 calc R U . . .
C36_15 C  0.7925(4)   0.5922(4)   0.4268(2)   0.059(3)   Uani 1 1 d    D U . . .
C37_15 C  0.7925(6)   0.5664(4)   0.4080(3)   0.084(5)   Uani 1 1 d    D U . . .
H37_15 H  0.795439    0.539733    0.410775    0.100      Uiso 1 1 calc R U . . .
C38_15 C  0.7881(5)   0.5805(4)   0.3850(3)   0.076(5)   Uani 1 1 d    D U . . .
H38_15 H  0.788614    0.563628    0.371765    0.091      Uiso 1 1 calc R U . . .
C39_15 C  0.7832(6)   0.6188(4)   0.3817(3)   0.069(4)   Uani 1 1 d    D U . . .
H39_15 H  0.780601    0.628120    0.365981    0.083      Uiso 1 1 calc R U . . .
N40_15 N  0.7818(4)   0.6439(3)   0.3994(2)   0.061(3)   Uani 1 1 d    D U . . .
C41_15 C  0.7854(6)   0.6305(4)   0.4214(2)   0.073(4)   Uani 1 1 d    D U . . .
H41_15 H  0.783004    0.648070    0.434136    0.087      Uiso 1 1 calc R U . . .
N1_16  N  0.9387(4)   0.5062(3)   0.5417(2)   0.067(3)   Uani 1 1 d    D U . . .
C2_16  C  0.9600(7)   0.4790(5)   0.5310(3)   0.092(6)   Uani 1 1 d    D U . . .
H2_16  H  0.965511    0.455984    0.539317    0.110      Uiso 1 1 calc R U . . .
C3_16  C  0.9739(7)   0.4834(6)   0.5083(4)   0.094(6)   Uani 1 1 d    D U . . .
H3_16  H  0.989799    0.464455    0.501263    0.113      Uiso 1 1 calc R U . . .
C4_16  C  0.9641(6)   0.5166(5)   0.4960(3)   0.088(5)   Uani 1 1 d    D U . . .
H4_16  H  0.974628    0.520943    0.480663    0.105      Uiso 1 1 calc R U . . .
C5_16  C  0.9391(4)   0.5437(4)   0.5056(3)   0.075(4)   Uani 1 1 d    D U . . .
C6_16  C  0.9278(4)   0.5368(3)   0.5291(2)   0.059(3)   Uani 1 1 d    D U . . .
H6_16  H  0.911291    0.554850    0.536424    0.071      Uiso 1 1 calc R U . . .
C7_16  C  0.9254(4)   0.5781(4)   0.4925(3)   0.068(4)   Uani 1 1 d    D U . . .
C8_16  C  0.9124(5)   0.5760(4)   0.4693(3)   0.065(4)   Uani 1 1 d    D U . . .
H8_16  H  0.916281    0.552681    0.460894    0.078      Uiso 1 1 calc R U . . .
C9_16  C  0.8936(6)   0.6068(4)   0.4571(4)   0.079(5)   Uani 1 1 d    D U . . .
H9_16  H  0.883255    0.603483    0.441612    0.095      Uiso 1 1 calc R U . . .
C10_16 C  0.8911(6)   0.6411(4)   0.4686(4)   0.086(5)   Uani 1 1 d    D U . . .
C11_16 C  0.9038(5)   0.6445(4)   0.4911(3)   0.070(4)   Uani 1 1 d    D U . . .
C12_16 C  0.9224(5)   0.6138(4)   0.5036(3)   0.065(4)   Uani 1 1 d    D U . . .
O13_16 O  0.9389(4)   0.6210(4)   0.5255(2)   0.070(3)   Uani 1 1 d    D U . . .
C14_16 C  0.9602(4)   0.6538(4)   0.5268(3)   0.070(4)   Uani 1 1 d    D U . . .
C15_16 C  0.9959(5)   0.6505(5)   0.5360(4)   0.077(5)   Uani 1 1 d    D U . . .
H15_16 H  1.004036    0.627574    0.543587    0.093      Uiso 1 1 calc R U . . .
C16_16 C  1.0204(6)   0.6824(4)   0.5340(4)   0.076(5)   Uani 1 1 d    D U . . .
H16_16 H  1.046293    0.679803    0.538951    0.091      Uiso 1 1 calc R U . . .
C17_16 C  1.0085(4)   0.7172(4)   0.5253(3)   0.077(5)   Uani 1 1 d    D U . . .
C18_16 C  0.9714(5)   0.7182(5)   0.5151(3)   0.077(4)   Uani 1 1 d    D U . . .
C19_16 C  0.9471(5)   0.6880(5)   0.5166(3)   0.076(4)   Uani 1 1 d    D U . . .
P20_16 P  0.90148(15) 0.68956(15) 0.50513(11) 0.0737(13) Uani 1 1 d    D U . . .
C21_16 C  0.9145(5)   0.7162(5)   0.4801(4)   0.082(5)   Uani 1 1 d    D U . . .
C22_16 C  0.9429(5)   0.7442(4)   0.4819(3)   0.077(4)   Uani 1 1 d    D U . . .
C23_16 C  0.9521(6)   0.7653(6)   0.4626(3)   0.095(6)   Uani 1 1 d    D U . . .
H23_16 H  0.970670    0.785106    0.463772    0.114      Uiso 1 1 calc R U . . .
C24_16 C  0.9338(5)   0.7576(5)   0.4407(4)   0.080(5)   Uani 1 1 d    D U . . .
H24_16 H  0.940219    0.772714    0.427220    0.096      Uiso 1 1 calc R U . . .
C25_16 C  0.9068(4)   0.7288(4)   0.4382(2)   0.067(3)   Uani 1 1 d    D U . . .
C26_16 C  0.8984(4)   0.7053(5)   0.4579(3)   0.069(4)   Uani 1 1 d    D U . . .
O27_16 O  0.8770(4)   0.6727(3)   0.4561(3)   0.077(3)   Uani 1 1 d    D U . . .
O28_16 O  0.9612(5)   0.7505(4)   0.5033(3)   0.095(5)   Uani 1 1 d    D U . . .
O29_16 O  0.8669(4)   0.7022(5)   0.5190(4)   0.092(5)   Uani 1 1 d    D U . . .
C30_16 C  0.8884(3)   0.7228(4)   0.4150(2)   0.068(3)   Uani 1 1 d    D U . . .
C31_16 C  0.9063(5)   0.7297(7)   0.3935(3)   0.092(5)   Uani 1 1 d    D U . . .
H31_16 H  0.931848    0.739233    0.393305    0.110      Uiso 1 1 calc R U . . .
C32_16 C  0.8875(5)   0.7229(6)   0.3720(3)   0.097(6)   Uani 1 1 d    D U . . .
H32_16 H  0.900107    0.726540    0.357246    0.116      Uiso 1 1 calc R U . . .
C33_16 C  0.8500(5)   0.7108(7)   0.3729(3)   0.090(6)   Uani 1 1 d    D U . . .
H33_16 H  0.837139    0.704605    0.358543    0.108      Uiso 1 1 calc R U . . .
N34_16 N  0.8312(4)   0.7075(6)   0.3934(2)   0.081(5)   Uani 1 1 d    D U . . .
C35_16 C  0.8497(3)   0.7131(4)   0.4137(2)   0.060(3)   Uani 1 1 d    D U . . .
H35_16 H  0.835817    0.710402    0.428128    0.072      Uiso 1 1 calc R U . . .
C36_16 C  1.0336(4)   0.7514(3)   0.5269(3)   0.072(4)   Uani 1 1 d    D U . . .
C37_16 C  1.0726(4)   0.7481(4)   0.5235(4)   0.076(5)   Uani 1 1 d    D U . . .
H37_16 H  1.083382    0.723773    0.519784    0.091      Uiso 1 1 calc R U . . .
C38_16 C  1.0962(4)   0.7800(4)   0.5253(4)   0.079(5)   Uani 1 1 d    D U . . .
H38_16 H  1.123085    0.777824    0.523128    0.095      Uiso 1 1 calc R U . . .
C39_16 C  1.0796(4)   0.8148(5)   0.5303(4)   0.080(5)   Uani 1 1 d    D U . . .
H39_16 H  1.095512    0.836825    0.531322    0.095      Uiso 1 1 calc R U . . .
N40_16 N  1.0419(3)   0.8189(4)   0.5339(3)   0.069(4)   Uani 1 1 d    D U . . .
C41_16 C  1.0196(4)   0.7880(3)   0.5313(3)   0.065(4)   Uani 1 1 d    D U . . .
H41_16 H  0.992686    0.791233    0.532610    0.078      Uiso 1 1 calc R U . . .
N1_17  N  0.7649(3)   0.7565(3)   0.3892(2)   0.050(2)   Uani 1 1 d    D U . . .
C2_17  C  0.7557(7)   0.7708(5)   0.3681(3)   0.081(5)   Uani 1 1 d    D U . . .
H2_17  H  0.757801    0.755223    0.354351    0.097      Uiso 1 1 calc R U . . .
C3_17  C  0.7430(9)   0.8086(5)   0.3660(3)   0.102(7)   Uani 1 1 d    D U . . .
H3_17  H  0.730304    0.817007    0.352043    0.122      Uiso 1 1 calc R U . . .
C4_17  C  0.7493(9)   0.8335(5)   0.3845(3)   0.105(8)   Uani 1 1 d    D U . . .
H4_17  H  0.746669    0.860283    0.382143    0.126      Uiso 1 1 calc R U . . .
C5_17  C  0.7596(5)   0.8193(4)   0.4067(2)   0.080(5)   Uani 1 1 d    D U . . .
C6_17  C  0.7673(5)   0.7803(3)   0.4076(3)   0.069(4)   Uani 1 1 d    D U . . .
H6_17  H  0.774876    0.769858    0.422408    0.083      Uiso 1 1 calc R U . . .
C7_17  C  0.7596(5)   0.8426(4)   0.4287(3)   0.075(4)   Uani 1 1 d    D U . . .
C8_17  C  0.7325(5)   0.8697(4)   0.4337(3)   0.074(4)   Uani 1 1 d    D U . . .
H8_17  H  0.714530    0.875405    0.421505    0.088      Uiso 1 1 calc R U . . .
C9_17  C  0.7286(6)   0.8902(5)   0.4554(3)   0.082(5)   Uani 1 1 d    D U . . .
H9_17  H  0.708841    0.908542    0.457554    0.098      Uiso 1 1 calc R U . . .
C10_17 C  0.7546(4)   0.8825(4)   0.4730(3)   0.071(4)   Uani 1 1 d    D U . . .
C11_17 C  0.7835(4)   0.8538(4)   0.4688(3)   0.070(4)   Uani 1 1 d    D U . . .
C12_17 C  0.7875(4)   0.8358(4)   0.4461(3)   0.065(4)   Uani 1 1 d    D U . . .
O13_17 O  0.8214(4)   0.8146(4)   0.4414(3)   0.077(4)   Uani 1 1 d    D U . . .
C14_17 C  0.8550(4)   0.8310(5)   0.4508(3)   0.069(4)   Uani 1 1 d    D U . . .
C15_17 C  0.8857(4)   0.8337(6)   0.4360(3)   0.071(4)   Uani 1 1 d    D U . . .
H15_17 H  0.883591    0.825645    0.419942    0.086      Uiso 1 1 calc R U . . .
C16_17 C  0.9213(4)   0.8489(5)   0.4448(3)   0.071(4)   Uani 1 1 d    D U . . .
H16_17 H  0.943350    0.848500    0.434926    0.085      Uiso 1 1 calc R U . . .
C17_17 C  0.9243(3)   0.8642(4)   0.4675(3)   0.063(3)   Uani 1 1 d    D U . . .
C18_17 C  0.8916(4)   0.8639(4)   0.4817(3)   0.067(4)   Uani 1 1 d    D U . . .
C19_17 C  0.8575(4)   0.8442(4)   0.4734(3)   0.063(3)   Uani 1 1 d    D U . . .
P20_17 P  0.81690(13) 0.84378(14) 0.49144(10) 0.0680(11) Uani 1 1 d    D U . . .
C21_17 C  0.8220(4)   0.8910(5)   0.5013(3)   0.073(5)   Uani 1 1 d    D U . . .
C22_17 C  0.8592(4)   0.9058(4)   0.5071(3)   0.068(4)   Uani 1 1 d    D U . . .
C23_17 C  0.8628(5)   0.9428(5)   0.5137(4)   0.076(5)   Uani 1 1 d    D U . . .
H23_17 H  0.886987    0.952530    0.518621    0.091      Uiso 1 1 calc R U . . .
C24_17 C  0.8303(4)   0.9669(5)   0.5134(4)   0.074(5)   Uani 1 1 d    D U . . .
H24_17 H  0.833965    0.993511    0.516002    0.089      Uiso 1 1 calc R U . . .
C25_17 C  0.7940(4)   0.9541(4)   0.5096(3)   0.073(4)   Uani 1 1 d    D U . . .
C26_17 C  0.7900(5)   0.9158(5)   0.5017(3)   0.069(4)   Uani 1 1 d    D U . . .
O27_17 O  0.7539(4)   0.9034(4)   0.4935(3)   0.079(4)   Uani 1 1 d    D U . . .
O28_17 O  0.8900(3)   0.8816(4)   0.5037(2)   0.069(3)   Uani 1 1 d    D U . . .
O29_17 O  0.8117(5)   0.8118(5)   0.5079(3)   0.088(4)   Uani 1 1 d    D U . . .
C30_17 C  0.7605(4)   0.9800(4)   0.5124(3)   0.081(5)   Uani 1 1 d    D U . . .
C31_17 C  0.7617(5)   1.0184(5)   0.5052(5)   0.111(9)   Uani 1 1 d    D U . . .
H31_17 H  0.784353    1.029024    0.498623    0.133      Uiso 1 1 calc R U . . .
C32_17 C  0.7287(5)   1.0405(5)   0.5078(4)   0.098(7)   Uani 1 1 d    D U . . .
H32_17 H  0.728388    1.066702    0.503128    0.118      Uiso 1 1 calc R U . . .
C33_17 C  0.6966(5)   1.0236(4)   0.5173(4)   0.080(5)   Uani 1 1 d    D U . . .
H33_17 H  0.673842    1.038538    0.518257    0.096      Uiso 1 1 calc R U . . .
N34_17 N  0.6953(4)   0.9877(3)   0.5251(3)   0.064(3)   Uani 1 1 d    D U . . .
C35_17 C  0.7266(4)   0.9663(4)   0.5219(3)   0.068(4)   Uani 1 1 d    D U . . .
H35_17 H  0.725453    0.940035    0.526312    0.082      Uiso 1 1 calc R U . . .
C36_17 C  0.9608(3)   0.8803(4)   0.4770(2)   0.061(3)   Uani 1 1 d    D U . . .
C37_17 C  0.9844(5)   0.9044(6)   0.4640(3)   0.085(6)   Uani 1 1 d    D U . . .
H37_17 H  0.977414    0.911751    0.448409    0.102      Uiso 1 1 calc R U . . .
C38_17 C  1.0179(5)   0.9176(5)   0.4739(3)   0.083(5)   Uani 1 1 d    D U . . .
H38_17 H  1.034379    0.933952    0.465120    0.099      Uiso 1 1 calc R U . . .
C39_17 C  1.0274(4)   0.9069(5)   0.4968(3)   0.069(4)   Uani 1 1 d    D U . . .
H39_17 H  1.050054    0.916900    0.503836    0.082      Uiso 1 1 calc R U . . .
N40_17 N  1.0056(3)   0.8829(4)   0.5092(2)   0.067(3)   Uani 1 1 d    D U . . .
C41_17 C  0.9725(4)   0.8711(5)   0.4999(3)   0.069(4)   Uani 1 1 d    D U . . .
H41_17 H  0.956119    0.855747    0.509398    0.083      Uiso 1 1 calc R U . . .
N1_18  N  0.7158(4)   0.6938(4)   0.3940(2)   0.067(3)   Uani 1 1 d    D U . . .
C2_18  C  0.6973(5)   0.6784(8)   0.3756(3)   0.091(6)   Uani 1 1 d    D U . . .
H2_18  H  0.710830    0.675060    0.361110    0.110      Uiso 1 1 calc R U . . .
C3_18  C  0.6595(4)   0.6672(8)   0.3766(3)   0.090(6)   Uani 1 1 d    D U . . .
H3_18  H  0.647664    0.654310    0.363683    0.108      Uiso 1 1 calc R U . . .
C4_18  C  0.6393(5)   0.6756(8)   0.3971(3)   0.096(7)   Uani 1 1 d    D U . . .
H4_18  H  0.612214    0.672922    0.397478    0.115      Uiso 1 1 calc R U . . .
C5_18  C  0.6589(4)   0.6879(4)   0.4172(2)   0.069(4)   Uani 1 1 d    D U . . .
C6_18  C  0.6974(4)   0.6973(5)   0.4144(3)   0.075(4)   Uani 1 1 d    D U . . .
H6_18  H  0.711109    0.706597    0.427806    0.090      Uiso 1 1 calc R U . . .
C7_18  C  0.6401(4)   0.6919(4)   0.4407(2)   0.069(4)   Uani 1 1 d    D U . . .
C8_18  C  0.6117(6)   0.6668(5)   0.4483(3)   0.081(5)   Uani 1 1 d    D U . . .
H8_18  H  0.603050    0.647301    0.437819    0.097      Uiso 1 1 calc R U . . .
C9_18  C  0.5954(4)   0.6696(4)   0.4708(3)   0.067(4)   Uani 1 1 d    D U . . .
H9_18  H  0.574624    0.653273    0.474804    0.080      Uiso 1 1 calc R U . . .
C10_18 C  0.6084(5)   0.6947(5)   0.4872(3)   0.083(5)   Uani 1 1 d    D U . . .
C11_18 C  0.6364(5)   0.7203(5)   0.4805(3)   0.077(4)   Uani 1 1 d    D U . . .
C12_18 C  0.6501(4)   0.7214(5)   0.4571(3)   0.071(4)   Uani 1 1 d    D U . . .
O13_18 O  0.6707(4)   0.7518(3)   0.4492(3)   0.082(4)   Uani 1 1 d    D U . . .
C14_18 C  0.6616(5)   0.7881(4)   0.4578(3)   0.076(4)   Uani 1 1 d    D U . . .
C15_18 C  0.6620(8)   0.8180(5)   0.4429(4)   0.098(6)   Uani 1 1 d    D U . . .
H15_18 H  0.673745    0.815252    0.427832    0.117      Uiso 1 1 calc R U . . .
C16_18 C  0.6452(6)   0.8541(5)   0.4493(3)   0.081(5)   Uani 1 1 d    D U . . .
H16_18 H  0.641938    0.873590    0.437689    0.097      Uiso 1 1 calc R U . . .
C17_18 C  0.6335(5)   0.8605(4)   0.4728(3)   0.072(4)   Uani 1 1 d    D U . . .
C18_18 C  0.6354(6)   0.8294(5)   0.4881(3)   0.077(5)   Uani 1 1 d    D U . . .
C19_18 C  0.6508(5)   0.7945(5)   0.4808(3)   0.080(5)   Uani 1 1 d    D U . . .
P20_18 P  0.65173(16) 0.75439(16) 0.50078(11) 0.0758(13) Uani 1 1 d    D U . . .
C21_18 C  0.6068(5)   0.7625(4)   0.5131(3)   0.069(4)   Uani 1 1 d    D U . . .
C22_18 C  0.5939(5)   0.8013(4)   0.5169(4)   0.080(5)   Uani 1 1 d    D U . . .
C23_18 C  0.5581(6)   0.8081(6)   0.5249(5)   0.092(6)   Uani 1 1 d    D U . . .
H23_18 H  0.549479    0.833532    0.527621    0.111      Uiso 1 1 calc R U . . .
C24_18 C  0.5331(6)   0.7754(5)   0.5294(5)   0.091(6)   Uani 1 1 d    D U . . .
H24_18 H  0.506980    0.779810    0.533353    0.109      Uiso 1 1 calc R U . . .
C25_18 C  0.5463(5)   0.7387(4)   0.5282(4)   0.088(6)   Uani 1 1 d    D U . . .
C26_18 C  0.5828(5)   0.7327(4)   0.5176(4)   0.082(6)   Uani 1 1 d    D U . . .
O27_18 O  0.5927(4)   0.6961(4)   0.5092(3)   0.084(4)   Uani 1 1 d    D U . . .
O28_18 O  0.6179(4)   0.8310(3)   0.5108(3)   0.077(3)   Uani 1 1 d    D U . . .
O29_18 O  0.6854(4)   0.7480(4)   0.5159(3)   0.083(4)   Uani 1 1 d    D U . . .
C30_18 C  0.5230(4)   0.7058(4)   0.5366(3)   0.080(5)   Uani 1 1 d    D U . . .
C31_18 C  0.4836(4)   0.7051(5)   0.5342(4)   0.090(7)   Uani 1 1 d    D U . . .
H31_18 H  0.470750    0.725978    0.526883    0.108      Uiso 1 1 calc R U . . .
C32_18 C  0.4626(4)   0.6740(5)   0.5423(4)   0.096(7)   Uani 1 1 d    D U . . .
H32_18 H  0.435516    0.673680    0.540903    0.115      Uiso 1 1 calc R U . . .
C33_18 C  0.4818(4)   0.6438(5)   0.5524(4)   0.081(5)   Uani 1 1 d    D U . . .
H33_18 H  0.467678    0.621999    0.557441    0.097      Uiso 1 1 calc R U . . .
N34_18 N  0.5197(4)   0.6444(4)   0.5553(4)   0.089(5)   Uani 1 1 d    D U . . .
C35_18 C  0.5396(4)   0.6749(4)   0.5484(4)   0.080(5)   Uani 1 1 d    D U . . .
H35_18 H  0.566285    0.675585    0.551551    0.096      Uiso 1 1 calc R U . . .
C36_18 C  0.6212(5)   0.8986(4)   0.4814(3)   0.080(5)   Uani 1 1 d    D U . . .
C37_18 C  0.5957(7)   0.9218(5)   0.4684(3)   0.098(7)   Uani 1 1 d    D U . . .
H37_18 H  0.585542    0.913047    0.453769    0.117      Uiso 1 1 calc R U . . .
C38_18 C  0.5856(6)   0.9571(5)   0.4771(3)   0.089(6)   Uani 1 1 d    D U . . .
H38_18 H  0.567483    0.972635    0.469048    0.107      Uiso 1 1 calc R U . . .
C39_18 C  0.6024(6)   0.9694(5)   0.4977(3)   0.082(5)   Uani 1 1 d    D U . . .
H39_18 H  0.595525    0.993951    0.503600    0.098      Uiso 1 1 calc R U . . .
N40_18 N  0.6278(5)   0.9490(4)   0.5099(3)   0.072(4)   Uani 1 1 d    D U . . .
C41_18 C  0.6359(6)   0.9138(4)   0.5022(3)   0.077(5)   Uani 1 1 d    D U . . .
H41_18 H  0.652481    0.898323    0.511506    0.093      Uiso 1 1 calc R U . . .
B1_19  B  0.5966(7)   0.4183(7)   0.4726(5)   0.132(8)   Uani 1 1 d    D U . . .
F2_19  F  0.5919(7)   0.4506(5)   0.4868(4)   0.143(8)   Uani 1 1 d    D U . . .
F3_19  F  0.5863(7)   0.3865(6)   0.4854(6)   0.170(10)  Uani 1 1 d    D U . . .
F4_19  F  0.5787(6)   0.4199(7)   0.4508(4)   0.149(7)   Uani 1 1 d    D U . . .
F5_19  F  0.6365(5)   0.4174(6)   0.4691(4)   0.127(6)   Uani 1 1 d    D U . . .
B1_20  B  0.1326(8)   0.6697(8)   0.5495(5)   0.123(7)   Uani 1 1 d    D U . . .
F2_20  F  0.1033(6)   0.6776(9)   0.5647(4)   0.155(8)   Uani 1 1 d    D U . . .
F3_20  F  0.1606(7)   0.6457(8)   0.5581(4)   0.152(8)   Uani 1 1 d    D U . . .
F4_20  F  0.1460(6)   0.7065(6)   0.5443(6)   0.169(10)  Uani 1 1 d    D U . . .
F5_20  F  0.1153(8)   0.6539(8)   0.5288(3)   0.153(8)   Uani 1 1 d    D U . . .
B1_21  B  0.6247(7)   0.3175(7)   0.5615(4)   0.099(6)   Uani 1 1 d    D U . . .
F2_21  F  0.5961(7)   0.3447(7)   0.5603(6)   0.171(10)  Uani 1 1 d    D U . . .
F3_21  F  0.6164(6)   0.2903(6)   0.5452(3)   0.135(6)   Uani 1 1 d    D U . . .
F4_21  F  0.6220(5)   0.2985(6)   0.5835(3)   0.113(5)   Uani 1 1 d    D U . . .
F5_21  F  0.6599(5)   0.3348(8)   0.5598(4)   0.145(8)   Uani 1 1 d    D U . . .
N1_22  N  0.4337(6)   0.1476(7)   0.5444(5)   0.099(6)   Uani 1 1 d    D U . . .
C2_22  C  0.4050(5)   0.1650(6)   0.5482(4)   0.075(5)   Uani 1 1 d    D U . . .
C3_22  C  0.3684(6)   0.1854(6)   0.5502(4)   0.078(5)   Uani 1 1 d    D U . . .
H3A_22 H  0.360658    0.194832    0.534601    0.118      Uiso 1 1 calc R U . . .
H3B_22 H  0.371363    0.207041    0.561148    0.118      Uiso 1 1 calc R U . . .
H3C_22 H  0.348841    0.167855    0.556358    0.118      Uiso 1 1 calc R U . . .
N1_23  N  0.2032(9)   0.0804(7)   0.5487(4)   0.107(7)   Uani 1 1 d    D U . . .
C2_23  C  0.2180(8)   0.1099(6)   0.5503(5)   0.095(7)   Uani 1 1 d    D U . . .
C3_23  C  0.2379(10)  0.1465(6)   0.5521(4)   0.098(8)   Uani 1 1 d    D U . . .
H3A_23 H  0.264497    0.142074    0.556906    0.117      Uiso 1 1 calc R U . . .
H3B_23 H  0.225080    0.162554    0.563951    0.117      Uiso 1 1 calc R U . . .
H3C_23 H  0.237393    0.159398    0.536677    0.117      Uiso 1 1 calc R U . . .
N1_24  N  0.2766(6)   0.2504(9)   0.4534(4)   0.106(7)   Uani 1 1 d    D U . . .
C2_24  C  0.2784(6)   0.2445(7)   0.4743(4)   0.086(5)   Uani 1 1 d    D U . . .
C3_24  C  0.2852(7)   0.2417(8)   0.4995(4)   0.092(6)   Uani 1 1 d    D U . . .
H3A_24 H  0.280859    0.215223    0.504651    0.137      Uiso 1 1 calc R U . . .
H3B_24 H  0.267673    0.258824    0.507908    0.137      Uiso 1 1 calc R U . . .
H3C_24 H  0.311730    0.249011    0.502907    0.137      Uiso 1 1 calc R U . . .
N1_25  N  0.7727(6)   0.7185(6)   0.4547(4)   0.088(5)   Uani 1 1 d    D U . . .
C2_25  C  0.7746(5)   0.7192(5)   0.4749(4)   0.069(4)   Uani 1 1 d    D U . . .
C3_25  C  0.7790(7)   0.7203(5)   0.5005(4)   0.079(5)   Uani 1 1 d    D U . . .
H3A_25 H  0.788128    0.695327    0.506167    0.095      Uiso 1 1 calc R U . . .
H3B_25 H  0.754167    0.726010    0.507897    0.095      Uiso 1 1 calc R U . . .
H3C_25 H  0.797503    0.740161    0.504841    0.095      Uiso 1 1 calc R U . . .
N1_26  N  0.8688(6)   0.5860(5)   0.5664(9)   0.167(16)  Uani 1 1 d    D U . . .
C2_26  C  0.8545(5)   0.6145(6)   0.5688(5)   0.079(6)   Uani 1 1 d    D U . . .
C3_26  C  0.8304(11)  0.6498(9)   0.5685(7)   0.120(11)  Uani 1 1 d    D U . . .
H3A_26 H  0.846911    0.672458    0.568470    0.180      Uiso 1 1 calc R U . . .
H3B_26 H  0.813952    0.650162    0.582575    0.180      Uiso 1 1 calc R U . . .
H3C_26 H  0.814358    0.649855    0.554191    0.180      Uiso 1 1 calc R U . . .
N1_27  N  0.6970(8)   0.8749(6)   0.5458(5)   0.108(7)   Uani 1 1 d    D U . . .
C2_27  C  0.7150(7)   0.8485(5)   0.5492(4)   0.087(6)   Uani 1 1 d    D U . . .
C3_27  C  0.7345(8)   0.8116(6)   0.5517(6)   0.098(7)   Uani 1 1 d    D U . . .
H3A_27 H  0.719444    0.791569    0.543795    0.117      Uiso 1 1 calc R U . . .
H3B_27 H  0.737301    0.805323    0.568515    0.117      Uiso 1 1 calc R U . . .
H3C_27 H  0.759948    0.813048    0.544301    0.117      Uiso 1 1 calc R U . . .
N1_28  N  0.9317(5)   0.8184(5)   0.5534(6)   0.103(8)   Uani 1 1 d    D U . . .
C2_28  C  0.9022(7)   0.8042(8)   0.5504(8)   0.129(13)  Uani 1 1 d    D U . . .
C3_28  C  0.8697(6)   0.7765(7)   0.5552(7)   0.108(10)  Uani 1 1 d    D U . . .
H3A_28 H  0.845647    0.790779    0.556630    0.162      Uiso 1 1 calc R U . . .
H3B_28 H  0.874732    0.762726    0.570046    0.162      Uiso 1 1 calc R U . . .
H3C_28 H  0.867806    0.758180    0.542127    0.162      Uiso 1 1 calc R U . . .
N1_29  N  0.7961(10)  0.7528(10)  0.6618(5)   0.132(10)  Uani 1 1 d    D U . . .
C2_29  C  0.7985(12)  0.7506(10)  0.6415(5)   0.122(11)  Uani 1 1 d    D U . . .
C3_29  C  0.7975(15)  0.7398(11)  0.6163(4)   0.153(18)  Uani 1 1 d    D U . . .
H3A_29 H  0.772589    0.746865    0.609551    0.230      Uiso 1 1 calc R U . . .
H3B_29 H  0.801193    0.712056    0.614830    0.230      Uiso 1 1 calc R U . . .
H3C_29 H  0.817913    0.753218    0.607807    0.230      Uiso 1 1 calc R U . . .
N1_31  N  0.2941(6)   0.2150(6)   0.6606(3)   0.081(4)   Uani 1 1 d    D U . . .
C2_31  C  0.2953(7)   0.2186(6)   0.6407(3)   0.076(5)   Uani 1 1 d    D U . . .
C3_31  C  0.2943(8)   0.2254(8)   0.6147(4)   0.091(6)   Uani 1 1 d    D U . . .
H3A_31 H  0.299497    0.201354    0.606361    0.136      Uiso 1 1 calc R U . . .
H3B_31 H  0.313867    0.244391    0.610462    0.136      Uiso 1 1 calc R U . . .
H3C_31 H  0.268983    0.235020    0.610179    0.136      Uiso 1 1 calc R U . . .
N1_32  N  0.1419(5)   0.3157(7)   0.5677(4)   0.096(6)   Uani 1 1 d    D U . . .
C2_32  C  0.1715(6)   0.3009(6)   0.5634(5)   0.084(6)   Uani 1 1 d    D U . . .
C3_32  C  0.2051(6)   0.2765(7)   0.5616(5)   0.086(6)   Uani 1 1 d    D U . . .
H3A_32 H  0.197090    0.249589    0.560901    0.130      Uiso 1 1 calc R U . . .
H3B_32 H  0.221606    0.280428    0.575426    0.130      Uiso 1 1 calc R U . . .
H3C_32 H  0.219342    0.282930    0.547116    0.130      Uiso 1 1 calc R U . . .
N1_33  N  0.3713(9)   0.3780(6)   0.5632(5)   0.110(7)   Uani 1 1 d    D U . . .
C2_33  C  0.3553(6)   0.3484(5)   0.5613(5)   0.080(5)   Uani 1 1 d    D U . . .
C3_33  C  0.3339(8)   0.3122(7)   0.5583(7)   0.105(8)   Uani 1 1 d    D U . . .
H3A_33 H  0.306432    0.317667    0.557513    0.157      Uiso 1 1 calc R U . . .
H3B_33 H  0.339060    0.295347    0.571896    0.157      Uiso 1 1 calc R U . . .
H3C_33 H  0.342110    0.299476    0.543688    0.157      Uiso 1 1 calc R U . . .
B1_34  B  0.4414(8)   0.5657(7)   0.6534(5)   0.120(7)   Uani 1 1 d    D U . . .
F2_34  F  0.4511(10)  0.5883(10)  0.6728(4)   0.214(15)  Uani 1 1 d    D U . . .
F3_34  F  0.4164(7)   0.5356(7)   0.6595(6)   0.186(11)  Uani 1 1 d    D U . . .
F4_34  F  0.4732(5)   0.5487(5)   0.6432(3)   0.117(5)   Uani 1 1 d    D U . . .
F5_34  F  0.4238(9)   0.5848(8)   0.6346(4)   0.190(12)  Uani 1 1 d    D U . . .
N1_35  N  0.7731(6)   0.6896(6)   0.3371(3)   0.085(5)   Uani 1 1 d    D U . . .
C2_35  C  0.7663(8)   0.6926(8)   0.3170(3)   0.087(6)   Uani 1 1 d    D U . . .
C3_35  C  0.7632(15)  0.7030(13)  0.2922(4)   0.152(16)  Uani 1 1 d    D U . . .
H3A_35 H  0.775800    0.683390    0.282475    0.227      Uiso 1 1 calc R U . . .
H3B_35 H  0.775630    0.727791    0.289565    0.227      Uiso 1 1 calc R U . . .
H3C_35 H  0.736117    0.704703    0.287786    0.227      Uiso 1 1 calc R U . . .
B1_36  B  0.8098(8)   0.2949(9)   0.5482(4)   0.132(8)   Uani 1 1 d    D U . . .
F2_36  F  0.7995(10)  0.3145(11)  0.5277(4)   0.210(13)  Uani 1 1 d    D U . . .
F3_36  F  0.8376(7)   0.2699(7)   0.5397(5)   0.163(8)   Uani 1 1 d    D U . . .
F4_36  F  0.7762(7)   0.2780(7)   0.5557(5)   0.163(9)   Uani 1 1 d    D U . . .
F5_36  F  0.8241(7)   0.3190(8)   0.5647(4)   0.154(8)   Uani 1 1 d    D U . . .


loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pd1_1  N1_4   1.992(14) . ?
Pd1_1  N1_2   2.013(12) . ?
Pd1_1  N1_3   2.019(12) . ?
Pd1_1  N1_5   2.031(13) . ?
Pd2_1  N40_4  2.007(13) . ?
Pd2_1  N34_8  2.023(14) . ?
Pd2_1  N34_5  2.028(12) . ?
Pd2_1  N40_6  2.032(14) . ?
Pd3_1  N40_5  2.007(12) . ?
Pd3_1  N34_6  2.020(14) . ?
Pd3_1  N34_2  2.033(11) . ?
Pd3_1  N40_9  2.038(11) . ?
Pd4_1  N40_7  1.981(14) . ?
Pd4_1  N40_2  1.990(14) . ?
Pd4_1  N34_9  2.012(13) . ?
Pd4_1  N34_3  2.026(14) . ?
Pd5_1  N34_7  2.002(13) . ?
Pd5_1  N40_3  2.036(13) . ?
Pd5_1  N34_4  2.044(13) . ?
Pd5_1  N40_8  2.051(12) . ?
Pd6_1  N1_6   1.969(13) . ?
Pd6_1  N1_7   1.987(14) . ?
Pd6_1  N1_9   2.002(13) . ?
Pd6_1  N1_8   2.004(13) . ?
N1_2   C6_2   1.335(12) . ?
N1_2   C2_2   1.337(14) . ?
C2_2   C3_2   1.383(17) . ?
C3_2   C4_2   1.387(15) . ?
C4_2   C5_2   1.398(14) . ?
C5_2   C6_2   1.377(12) . ?
C5_2   C7_2   1.485(10) . ?
C7_2   C8_2   1.360(19) . ?
C7_2   C12_2  1.41(2)   . ?
C8_2   C9_2   1.433(18) . ?
C9_2   C10_2  1.358(17) . ?
C10_2  O27_2  1.396(16) . ?
C10_2  C11_2  1.40(2)   . ?
C11_2  C12_2  1.45(2)   . ?
C11_2  P20_2  1.71(2)   . ?
C12_2  O13_2  1.42(2)   . ?
O13_2  C14_2  1.393(18) . ?
C14_2  C15_2  1.353(17) . ?
C14_2  C19_2  1.39(2)   . ?
C15_2  C16_2  1.43(2)   . ?
C16_2  C17_2  1.369(19) . ?
C17_2  C18_2  1.41(2)   . ?
C17_2  C36_2  1.486(10) . ?
C18_2  C19_2  1.38(3)   . ?
C18_2  O28_2  1.40(2)   . ?
C19_2  P20_2  1.765(19) . ?
P20_2  O29_2  1.473(17) . ?
P20_2  C21_2  1.769(19) . ?
C21_2  C22_2  1.37(2)   . ?
C21_2  C26_2  1.41(2)   . ?
C22_2  C23_2  1.354(18) . ?
C22_2  O28_2  1.389(18) . ?
C23_2  C24_2  1.43(2)   . ?
C24_2  C25_2  1.395(18) . ?
C25_2  C26_2  1.40(2)   . ?
C25_2  C30_2  1.483(10) . ?
C26_2  O27_2  1.37(2)   . ?
C30_2  C31_2  1.393(14) . ?
C30_2  C35_2  1.397(12) . ?
C31_2  C32_2  1.391(15) . ?
C32_2  C33_2  1.377(17) . ?
C33_2  N34_2  1.326(15) . ?
N34_2  C35_2  1.338(12) . ?
C36_2  C41_2  1.386(12) . ?
C36_2  C37_2  1.392(14) . ?
C37_2  C38_2  1.380(15) . ?
C38_2  C39_2  1.381(17) . ?
C39_2  N40_2  1.349(14) . ?
N40_2  C41_2  1.327(12) . ?
N1_3   C6_3   1.321(12) . ?
N1_3   C2_3   1.337(14) . ?
C2_3   C3_3   1.381(17) . ?
C3_3   C4_3   1.368(15) . ?
C4_3   C5_3   1.376(14) . ?
C5_3   C6_3   1.408(12) . ?
C5_3   C7_3   1.487(10) . ?
C7_3   C8_3   1.391(18) . ?
C7_3   C12_3  1.41(2)   . ?
C8_3   C9_3   1.42(2)   . ?
C9_3   C10_3  1.362(18) . ?
C10_3  O27_3  1.368(17) . ?
C10_3  C11_3  1.42(2)   . ?
C11_3  C12_3  1.42(2)   . ?
C11_3  P20_3  1.748(17) . ?
C12_3  O13_3  1.363(19) . ?
O13_3  C14_3  1.389(17) . ?
C14_3  C15_3  1.325(17) . ?
C14_3  C19_3  1.39(2)   . ?
C15_3  C16_3  1.43(2)   . ?
C16_3  C17_3  1.384(18) . ?
C17_3  C18_3  1.38(2)   . ?
C17_3  C36_3  1.490(10) . ?
C18_3  O28_3  1.421(19) . ?
C18_3  C19_3  1.44(2)   . ?
C19_3  P20_3  1.736(18) . ?
P20_3  O29_3  1.445(17) . ?
P20_3  C21_3  1.749(18) . ?
C21_3  C22_3  1.39(2)   . ?
C21_3  C26_3  1.39(2)   . ?
C22_3  C23_3  1.366(17) . ?
C22_3  O28_3  1.392(16) . ?
C23_3  C24_3  1.403(19) . ?
C24_3  C25_3  1.382(18) . ?
C25_3  C26_3  1.39(2)   . ?
C25_3  C30_3  1.488(10) . ?
C26_3  O27_3  1.40(2)   . ?
C30_3  C31_3  1.390(14) . ?
C30_3  C35_3  1.390(12) . ?
C31_3  C32_3  1.388(15) . ?
C32_3  C33_3  1.390(17) . ?
C33_3  N34_3  1.328(14) . ?
N34_3  C35_3  1.336(12) . ?
C36_3  C37_3  1.386(14) . ?
C36_3  C41_3  1.396(12) . ?
C37_3  C38_3  1.377(15) . ?
C38_3  C39_3  1.372(17) . ?
C39_3  N40_3  1.323(14) . ?
N40_3  C41_3  1.332(12) . ?
N1_4   C2_4   1.334(14) . ?
N1_4   C6_4   1.351(12) . ?
C2_4   C3_4   1.374(17) . ?
C3_4   C4_4   1.391(15) . ?
C4_4   C5_4   1.391(15) . ?
C5_4   C6_4   1.389(13) . ?
C5_4   C7_4   1.485(10) . ?
C7_4   C8_4   1.360(18) . ?
C7_4   C12_4  1.43(2)   . ?
C8_4   C9_4   1.424(19) . ?
C9_4   C10_4  1.371(18) . ?
C10_4  O27_4  1.384(17) . ?
C10_4  C11_4  1.44(2)   . ?
C11_4  C12_4  1.40(2)   . ?
C11_4  P20_4  1.710(18) . ?
C12_4  O13_4  1.37(2)   . ?
O13_4  C14_4  1.363(16) . ?
C14_4  C15_4  1.371(17) . ?
C14_4  C19_4  1.42(2)   . ?
C15_4  C16_4  1.42(2)   . ?
C16_4  C17_4  1.377(19) . ?
C17_4  C18_4  1.38(2)   . ?
C17_4  C36_4  1.490(10) . ?
C18_4  O28_4  1.38(2)   . ?
C18_4  C19_4  1.40(2)   . ?
C19_4  P20_4  1.767(18) . ?
P20_4  O29_4  1.511(18) . ?
P20_4  C21_4  1.718(19) . ?
C21_4  C26_4  1.39(2)   . ?
C21_4  C22_4  1.45(2)   . ?
C22_4  C23_4  1.347(17) . ?
C22_4  O28_4  1.373(18) . ?
C23_4  C24_4  1.42(2)   . ?
C24_4  C25_4  1.367(18) . ?
C25_4  C26_4  1.42(2)   . ?
C25_4  C30_4  1.488(10) . ?
C26_4  O27_4  1.39(2)   . ?
C30_4  C31_4  1.382(15) . ?
C30_4  C35_4  1.393(12) . ?
C31_4  C32_4  1.379(15) . ?
C32_4  C33_4  1.375(17) . ?
C33_4  N34_4  1.326(14) . ?
N34_4  C35_4  1.336(12) . ?
C36_4  C41_4  1.371(12) . ?
C36_4  C37_4  1.400(14) . ?
C37_4  C38_4  1.396(14) . ?
C38_4  C39_4  1.383(17) . ?
C39_4  N40_4  1.344(14) . ?
N40_4  C41_4  1.341(12) . ?
N1_5   C2_5   1.332(14) . ?
N1_5   C6_5   1.333(12) . ?
C2_5   C3_5   1.386(17) . ?
C3_5   C4_5   1.386(15) . ?
C4_5   C5_5   1.374(14) . ?
C5_5   C6_5   1.394(12) . ?
C5_5   C7_5   1.483(10) . ?
C7_5   C8_5   1.380(19) . ?
C7_5   C12_5  1.43(2)   . ?
C8_5   C9_5   1.429(19) . ?
C9_5   C10_5  1.348(17) . ?
C10_5  O27_5  1.379(16) . ?
C10_5  C11_5  1.38(2)   . ?
C11_5  C12_5  1.37(2)   . ?
C11_5  P20_5  1.761(19) . ?
C12_5  O13_5  1.410(18) . ?
O13_5  C14_5  1.371(17) . ?
C14_5  C19_5  1.36(2)   . ?
C14_5  C15_5  1.371(17) . ?
C15_5  C16_5  1.41(2)   . ?
C16_5  C17_5  1.381(18) . ?
C17_5  C18_5  1.44(2)   . ?
C17_5  C36_5  1.485(10) . ?
C18_5  O28_5  1.394(19) . ?
C18_5  C19_5  1.40(2)   . ?
C19_5  P20_5  1.763(18) . ?
P20_5  O29_5  1.474(17) . ?
P20_5  C21_5  1.746(18) . ?
C21_5  C22_5  1.42(2)   . ?
C21_5  C26_5  1.43(2)   . ?
C22_5  C23_5  1.357(17) . ?
C22_5  O28_5  1.387(16) . ?
C23_5  C24_5  1.416(19) . ?
C24_5  C25_5  1.380(18) . ?
C25_5  C26_5  1.35(2)   . ?
C25_5  C30_5  1.485(10) . ?
C26_5  O27_5  1.37(2)   . ?
C30_5  C35_5  1.388(12) . ?
C30_5  C31_5  1.396(14) . ?
C31_5  C32_5  1.388(14) . ?
C32_5  C33_5  1.383(17) . ?
C33_5  N34_5  1.320(14) . ?
N34_5  C35_5  1.339(12) . ?
C36_5  C37_5  1.382(14) . ?
C36_5  C41_5  1.390(12) . ?
C37_5  C38_5  1.387(15) . ?
C38_5  C39_5  1.376(16) . ?
C39_5  N40_5  1.328(14) . ?
N40_5  C41_5  1.324(12) . ?
N1_6   C2_6   1.339(14) . ?
N1_6   C6_6   1.346(12) . ?
C2_6   C3_6   1.374(17) . ?
C3_6   C4_6   1.398(14) . ?
C4_6   C5_6   1.392(14) . ?
C5_6   C6_6   1.387(12) . ?
C5_6   C7_6   1.489(10) . ?
C7_6   C8_6   1.378(18) . ?
C7_6   C12_6  1.422(19) . ?
C8_6   C9_6   1.404(19) . ?
C9_6   C10_6  1.351(18) . ?
C10_6  O27_6  1.399(15) . ?
C10_6  C11_6  1.43(2)   . ?
C11_6  C12_6  1.37(2)   . ?
C11_6  P20_6  1.755(17) . ?
C12_6  O13_6  1.375(19) . ?
O13_6  C14_6  1.397(15) . ?
C14_6  C15_6  1.374(17) . ?
C14_6  C19_6  1.443(19) . ?
C15_6  C16_6  1.399(18) . ?
C16_6  C17_6  1.386(16) . ?
C17_6  C18_6  1.41(2)   . ?
C17_6  C36_6  1.486(10) . ?
C18_6  O28_6  1.372(18) . ?
C18_6  C19_6  1.42(2)   . ?
C19_6  P20_6  1.715(17) . ?
P20_6  O29_6  1.464(15) . ?
P20_6  C21_6  1.724(15) . ?
C21_6  C26_6  1.37(2)   . ?
C21_6  C22_6  1.424(19) . ?
C22_6  C23_6  1.360(16) . ?
C22_6  O28_6  1.367(16) . ?
C23_6  C24_6  1.414(19) . ?
C24_6  C25_6  1.386(16) . ?
C25_6  C26_6  1.423(19) . ?
C25_6  C30_6  1.482(10) . ?
C26_6  O27_6  1.411(18) . ?
C30_6  C35_6  1.381(12) . ?
C30_6  C31_6  1.402(14) . ?
C31_6  C32_6  1.373(15) . ?
C32_6  C33_6  1.382(18) . ?
C33_6  N34_6  1.347(14) . ?
N34_6  C35_6  1.331(12) . ?
C36_6  C41_6  1.375(12) . ?
C36_6  C37_6  1.395(14) . ?
C37_6  C38_6  1.393(14) . ?
C38_6  C39_6  1.392(17) . ?
C39_6  N40_6  1.330(14) . ?
N40_6  C41_6  1.328(12) . ?
N1_7   C6_7   1.335(12) . ?
N1_7   C2_7   1.345(14) . ?
C2_7   C3_7   1.378(18) . ?
C3_7   C4_7   1.377(15) . ?
C4_7   C5_7   1.392(15) . ?
C5_7   C6_7   1.385(12) . ?
C5_7   C7_7   1.489(10) . ?
C7_7   C8_7   1.358(19) . ?
C7_7   C12_7  1.41(2)   . ?
C8_7   C9_7   1.46(2)   . ?
C9_7   C10_7  1.338(17) . ?
C10_7  O27_7  1.395(17) . ?
C10_7  C11_7  1.44(2)   . ?
C11_7  C12_7  1.42(2)   . ?
C11_7  P20_7  1.75(2)   . ?
C12_7  O13_7  1.42(2)   . ?
O13_7  C14_7  1.391(17) . ?
C14_7  C15_7  1.358(18) . ?
C14_7  C19_7  1.41(2)   . ?
C15_7  C16_7  1.44(2)   . ?
C16_7  C17_7  1.378(19) . ?
C17_7  C18_7  1.41(2)   . ?
C17_7  C36_7  1.485(10) . ?
C18_7  O28_7  1.36(2)   . ?
C18_7  C19_7  1.42(2)   . ?
C19_7  P20_7  1.73(2)   . ?
P20_7  O29_7  1.506(18) . ?
P20_7  C21_7  1.741(18) . ?
C21_7  C26_7  1.40(2)   . ?
C21_7  C22_7  1.42(2)   . ?
C22_7  C23_7  1.347(18) . ?
C22_7  O28_7  1.389(18) . ?
C23_7  C24_7  1.42(2)   . ?
C24_7  C25_7  1.350(18) . ?
C25_7  C26_7  1.41(2)   . ?
C25_7  C30_7  1.485(10) . ?
C26_7  O27_7  1.39(2)   . ?
C30_7  C31_7  1.391(14) . ?
C30_7  C35_7  1.398(12) . ?
C31_7  C32_7  1.376(15) . ?
C32_7  C33_7  1.377(18) . ?
C33_7  N34_7  1.335(14) . ?
N34_7  C35_7  1.340(12) . ?
C36_7  C37_7  1.384(14) . ?
C36_7  C41_7  1.396(12) . ?
C37_7  C38_7  1.393(15) . ?
C38_7  C39_7  1.390(17) . ?
C39_7  N40_7  1.328(14) . ?
N40_7  C41_7  1.344(12) . ?
N1_8   C2_8   1.336(14) . ?
N1_8   C6_8   1.344(12) . ?
C2_8   C3_8   1.368(16) . ?
C3_8   C4_8   1.390(13) . ?
C4_8   C5_8   1.373(14) . ?
C5_8   C6_8   1.401(12) . ?
C5_8   C7_8   1.488(10) . ?
C7_8   C8_8   1.380(17) . ?
C7_8   C12_8  1.41(2)   . ?
C8_8   C9_8   1.434(19) . ?
C9_8   C10_8  1.358(18) . ?
C10_8  O27_8  1.397(16) . ?
C10_8  C11_8  1.42(2)   . ?
C11_8  C12_8  1.37(2)   . ?
C11_8  P20_8  1.751(18) . ?
C12_8  O13_8  1.436(18) . ?
O13_8  C14_8  1.376(17) . ?
C14_8  C15_8  1.363(17) . ?
C14_8  C19_8  1.40(2)   . ?
C15_8  C16_8  1.43(2)   . ?
C16_8  C17_8  1.359(18) . ?
C17_8  C18_8  1.42(2)   . ?
C17_8  C36_8  1.479(10) . ?
C18_8  C19_8  1.37(2)   . ?
C18_8  O28_8  1.41(2)   . ?
C19_8  P20_8  1.751(18) . ?
P20_8  O29_8  1.449(17) . ?
P20_8  C21_8  1.791(19) . ?
C21_8  C22_8  1.41(2)   . ?
C21_8  C26_8  1.42(2)   . ?
C22_8  O28_8  1.379(17) . ?
C22_8  C23_8  1.380(18) . ?
C23_8  C24_8  1.43(2)   . ?
C24_8  C25_8  1.359(19) . ?
C25_8  C26_8  1.45(2)   . ?
C25_8  C30_8  1.488(10) . ?
C26_8  O27_8  1.41(2)   . ?
C30_8  C31_8  1.388(14) . ?
C30_8  C35_8  1.394(12) . ?
C31_8  C32_8  1.395(15) . ?
C32_8  C33_8  1.370(17) . ?
C33_8  N34_8  1.337(14) . ?
N34_8  C35_8  1.349(12) . ?
C36_8  C41_8  1.378(12) . ?
C36_8  C37_8  1.389(15) . ?
C37_8  C38_8  1.378(15) . ?
C38_8  C39_8  1.377(17) . ?
C39_8  N40_8  1.322(14) . ?
N40_8  C41_8  1.334(12) . ?
N1_9   C2_9   1.323(15) . ?
N1_9   C6_9   1.328(12) . ?
C2_9   C3_9   1.387(18) . ?
C3_9   C4_9   1.381(15) . ?
C4_9   C5_9   1.385(15) . ?
C5_9   C6_9   1.390(12) . ?
C5_9   C7_9   1.479(10) . ?
C7_9   C12_9  1.38(2)   . ?
C7_9   C8_9   1.385(18) . ?
C8_9   C9_9   1.439(19) . ?
C9_9   C10_9  1.350(18) . ?
C10_9  O27_9  1.389(16) . ?
C10_9  C11_9  1.41(2)   . ?
C11_9  C12_9  1.385(19) . ?
C11_9  P20_9  1.776(18) . ?
C12_9  O13_9  1.377(18) . ?
O13_9  C14_9  1.384(17) . ?
C14_9  C19_9  1.37(2)   . ?
C14_9  C15_9  1.372(17) . ?
C15_9  C16_9  1.43(2)   . ?
C16_9  C17_9  1.369(17) . ?
C17_9  C18_9  1.414(19) . ?
C17_9  C36_9  1.485(10) . ?
C18_9  O28_9  1.385(17) . ?
C18_9  C19_9  1.43(2)   . ?
C19_9  P20_9  1.752(16) . ?
P20_9  O29_9  1.480(15) . ?
P20_9  C21_9  1.754(16) . ?
C21_9  C26_9  1.39(2)   . ?
C21_9  C22_9  1.42(2)   . ?
C22_9  C23_9  1.344(18) . ?
C22_9  O28_9  1.369(16) . ?
C23_9  C24_9  1.407(19) . ?
C24_9  C25_9  1.385(18) . ?
C25_9  C26_9  1.42(2)   . ?
C25_9  C30_9  1.485(10) . ?
C26_9  O27_9  1.37(2)   . ?
C30_9  C35_9  1.389(12) . ?
C30_9  C31_9  1.405(14) . ?
C31_9  C32_9  1.387(14) . ?
C32_9  C33_9  1.365(17) . ?
C33_9  N34_9  1.331(14) . ?
N34_9  C35_9  1.344(12) . ?
C36_9  C37_9  1.389(14) . ?
C36_9  C41_9  1.390(12) . ?
C37_9  C38_9  1.396(15) . ?
C38_9  C39_9  1.393(16) . ?
C39_9  N40_9  1.330(14) . ?
N40_9  C41_9  1.344(12) . ?
Pd1_10 N1_11  2.006(14) . ?
Pd1_10 N34_14 2.007(13) . ?
Pd1_10 N34_18 2.025(14) . ?
Pd1_10 N34_15 2.045(13) . ?
Pd2_10 N1_17  2.003(10) . ?
Pd2_10 N40_15 2.013(12) . ?
Pd2_10 N1_18  2.026(13) . ?
Pd2_10 N34_16 2.031(13) . ?
Pd3_10 N40_16 2.004(12) . ?
Pd3_10 N34_12 2.027(14) . ?
Pd3_10 N40_13 2.028(14) . ?
Pd3_10 N40_17 2.061(13) . ?
Pd4_10 N40_11 1.990(14) . ?
Pd4_10 N40_12 2.016(14) . ?
Pd4_10 N34_17 2.027(13) . ?
Pd4_10 N40_18 2.033(14) . ?
Pd5_10 N40_14 1.980(15) . ?
Pd5_10 N1_15  2.006(12) . ?
Pd5_10 N1_16  2.009(13) . ?
Pd5_10 N34_13 2.033(13) . ?
Pd6_10 N1_12  2.010(14) . ?
Pd6_10 N1_13  2.016(15) . ?
Pd6_10 N34_11 2.022(15) . ?
Pd6_10 N1_14  2.025(13) . ?
N1_11  C6_11  1.332(12) . ?
N1_11  C2_11  1.341(14) . ?
C2_11  C3_11  1.370(17) . ?
C3_11  C4_11  1.385(14) . ?
C4_11  C5_11  1.391(15) . ?
C5_11  C6_11  1.394(12) . ?
C5_11  C7_11  1.495(10) . ?
C7_11  C8_11  1.384(19) . ?
C7_11  C12_11 1.41(2)   . ?
C8_11  C9_11  1.436(19) . ?
C9_11  C10_11 1.349(18) . ?
C10_11 O27_11 1.379(17) . ?
C10_11 C11_11 1.44(2)   . ?
C11_11 C12_11 1.42(2)   . ?
C11_11 P20_11 1.709(17) . ?
C12_11 O13_11 1.41(2)   . ?
O13_11 C14_11 1.375(16) . ?
C14_11 C15_11 1.367(17) . ?
C14_11 C19_11 1.43(2)   . ?
C15_11 C16_11 1.40(2)   . ?
C16_11 C17_11 1.397(19) . ?
C17_11 C18_11 1.42(2)   . ?
C17_11 C36_11 1.489(10) . ?
C18_11 C19_11 1.39(2)   . ?
C18_11 O28_11 1.39(2)   . ?
C19_11 P20_11 1.791(17) . ?
P20_11 O29_11 1.492(14) . ?
P20_11 C21_11 1.72(2)   . ?
C21_11 C22_11 1.42(2)   . ?
C21_11 C26_11 1.43(2)   . ?
C22_11 C23_11 1.356(18) . ?
C22_11 O28_11 1.382(18) . ?
C23_11 C24_11 1.46(2)   . ?
C24_11 C25_11 1.378(18) . ?
C25_11 C26_11 1.40(2)   . ?
C25_11 C30_11 1.483(10) . ?
C26_11 O27_11 1.39(2)   . ?
C30_11 C35_11 1.370(12) . ?
C30_11 C31_11 1.389(14) . ?
C31_11 C32_11 1.378(15) . ?
C32_11 C33_11 1.379(17) . ?
C33_11 N34_11 1.340(15) . ?
N34_11 C35_11 1.331(12) . ?
C36_11 C41_11 1.387(12) . ?
C36_11 C37_11 1.399(14) . ?
C37_11 C38_11 1.399(15) . ?
C38_11 C39_11 1.372(17) . ?
C39_11 N40_11 1.332(14) . ?
N40_11 C41_11 1.334(12) . ?
N1_12  C6_12  1.327(12) . ?
N1_12  C2_12  1.329(15) . ?
C2_12  C3_12  1.388(17) . ?
C3_12  C4_12  1.380(15) . ?
C4_12  C5_12  1.403(14) . ?
C5_12  C6_12  1.387(12) . ?
C5_12  C7_12  1.485(10) . ?
C7_12  C8_12  1.389(18) . ?
C7_12  C12_12 1.40(2)   . ?
C8_12  C9_12  1.42(2)   . ?
C9_12  C10_12 1.353(18) . ?
C10_12 O27_12 1.379(18) . ?
C10_12 C11_12 1.42(2)   . ?
C11_12 C12_12 1.41(3)   . ?
C11_12 P20_12 1.743(19) . ?
C12_12 O13_12 1.42(2)   . ?
O13_12 C14_12 1.399(17) . ?
C14_12 C15_12 1.372(18) . ?
C14_12 C19_12 1.41(2)   . ?
C15_12 C16_12 1.41(2)   . ?
C16_12 C17_12 1.363(18) . ?
C17_12 C18_12 1.40(2)   . ?
C17_12 C36_12 1.488(10) . ?
C18_12 O28_12 1.40(2)   . ?
C18_12 C19_12 1.42(2)   . ?
C19_12 P20_12 1.762(16) . ?
P20_12 O29_12 1.462(17) . ?
P20_12 C21_12 1.75(2)   . ?
C21_12 C26_12 1.36(2)   . ?
C21_12 C22_12 1.43(2)   . ?
C22_12 O28_12 1.351(16) . ?
C22_12 C23_12 1.363(18) . ?
C23_12 C24_12 1.436(18) . ?
C24_12 C25_12 1.359(18) . ?
C25_12 C26_12 1.45(2)   . ?
C25_12 C30_12 1.483(10) . ?
C26_12 O27_12 1.37(2)   . ?
C30_12 C35_12 1.380(12) . ?
C30_12 C31_12 1.391(15) . ?
C31_12 C32_12 1.389(14) . ?
C32_12 C33_12 1.390(17) . ?
C33_12 N34_12 1.342(15) . ?
N34_12 C35_12 1.344(12) . ?
C36_12 C41_12 1.381(12) . ?
C36_12 C37_12 1.395(14) . ?
C37_12 C38_12 1.388(14) . ?
C38_12 C39_12 1.393(17) . ?
C39_12 N40_12 1.334(14) . ?
N40_12 C41_12 1.344(12) . ?
N1_13  C2_13  1.329(15) . ?
N1_13  C6_13  1.332(12) . ?
C2_13  C3_13  1.380(18) . ?
C3_13  C4_13  1.381(15) . ?
C4_13  C5_13  1.397(14) . ?
C5_13  C6_13  1.386(12) . ?
C5_13  C7_13  1.487(10) . ?
C7_13  C8_13  1.381(17) . ?
C7_13  C12_13 1.42(2)   . ?
C8_13  C9_13  1.43(2)   . ?
C9_13  C10_13 1.360(18) . ?
C10_13 O27_13 1.374(17) . ?
C10_13 C11_13 1.43(2)   . ?
C11_13 C12_13 1.41(2)   . ?
C11_13 P20_13 1.736(19) . ?
C12_13 O13_13 1.39(2)   . ?
O13_13 C14_13 1.409(18) . ?
C14_13 C15_13 1.346(18) . ?
C14_13 C19_13 1.40(2)   . ?
C15_13 C16_13 1.453(19) . ?
C16_13 C17_13 1.369(18) . ?
C17_13 C18_13 1.43(2)   . ?
C17_13 C36_13 1.481(10) . ?
C18_13 O28_13 1.35(2)   . ?
C18_13 C19_13 1.44(2)   . ?
C19_13 P20_13 1.726(18) . ?
P20_13 O29_13 1.490(18) . ?
P20_13 C21_13 1.746(18) . ?
C21_13 C22_13 1.38(2)   . ?
C21_13 C26_13 1.45(2)   . ?
C22_13 C23_13 1.368(18) . ?
C22_13 O28_13 1.400(17) . ?
C23_13 C24_13 1.44(2)   . ?
C24_13 C25_13 1.405(18) . ?
C25_13 C26_13 1.42(2)   . ?
C25_13 C30_13 1.485(10) . ?
C26_13 O27_13 1.395(19) . ?
C30_13 C31_13 1.387(14) . ?
C30_13 C35_13 1.394(12) . ?
C31_13 C32_13 1.385(15) . ?
C32_13 C33_13 1.381(17) . ?
C33_13 N34_13 1.318(14) . ?
N34_13 C35_13 1.334(12) . ?
C36_13 C41_13 1.389(12) . ?
C36_13 C37_13 1.390(14) . ?
C37_13 C38_13 1.392(15) . ?
C38_13 C39_13 1.379(17) . ?
C39_13 N40_13 1.339(14) . ?
N40_13 C41_13 1.338(12) . ?
N1_14  C2_14  1.324(15) . ?
N1_14  C6_14  1.335(12) . ?
C2_14  C3_14  1.382(17) . ?
C3_14  C4_14  1.405(15) . ?
C4_14  C5_14  1.397(14) . ?
C5_14  C6_14  1.383(12) . ?
C5_14  C7_14  1.488(10) . ?
C7_14  C8_14  1.377(18) . ?
C7_14  C12_14 1.46(2)   . ?
C8_14  C9_14  1.43(2)   . ?
C9_14  C10_14 1.338(18) . ?
C10_14 C11_14 1.41(2)   . ?
C10_14 O27_14 1.425(18) . ?
C11_14 C12_14 1.35(3)   . ?
C11_14 P20_14 1.75(2)   . ?
C12_14 O13_14 1.37(2)   . ?
O13_14 C14_14 1.370(18) . ?
C14_14 C15_14 1.365(19) . ?
C14_14 C19_14 1.40(2)   . ?
C15_14 C16_14 1.41(2)   . ?
C16_14 C17_14 1.38(2)   . ?
C17_14 C18_14 1.43(2)   . ?
C17_14 C36_14 1.485(11) . ?
C18_14 O28_14 1.38(2)   . ?
C18_14 C19_14 1.41(3)   . ?
C19_14 P20_14 1.81(2)   . ?
P20_14 O29_14 1.463(17) . ?
P20_14 C21_14 1.776(18) . ?
C21_14 C26_14 1.37(2)   . ?
C21_14 C22_14 1.39(2)   . ?
C22_14 C23_14 1.342(17) . ?
C22_14 O28_14 1.370(17) . ?
C23_14 C24_14 1.42(2)   . ?
C24_14 C25_14 1.352(18) . ?
C25_14 C26_14 1.44(2)   . ?
C25_14 C30_14 1.497(10) . ?
C26_14 O27_14 1.40(2)   . ?
C30_14 C35_14 1.387(12) . ?
C30_14 C31_14 1.402(14) . ?
C31_14 C32_14 1.393(15) . ?
C32_14 C33_14 1.390(17) . ?
C33_14 N34_14 1.323(14) . ?
N34_14 C35_14 1.338(12) . ?
C36_14 C41_14 1.388(13) . ?
C36_14 C37_14 1.395(15) . ?
C37_14 C38_14 1.384(15) . ?
C38_14 C39_14 1.364(18) . ?
C39_14 N40_14 1.332(15) . ?
N40_14 C41_14 1.327(13) . ?
N1_15  C2_15  1.339(14) . ?
N1_15  C6_15  1.340(12) . ?
C2_15  C3_15  1.374(16) . ?
C3_15  C4_15  1.388(14) . ?
C4_15  C5_15  1.402(14) . ?
C5_15  C6_15  1.390(12) . ?
C5_15  C7_15  1.482(10) . ?
C7_15  C8_15  1.397(18) . ?
C7_15  C12_15 1.40(2)   . ?
C8_15  C9_15  1.431(19) . ?
C9_15  C10_15 1.359(17) . ?
C10_15 O27_15 1.404(16) . ?
C10_15 C11_15 1.42(2)   . ?
C11_15 C12_15 1.41(2)   . ?
C11_15 P20_15 1.732(19) . ?
C12_15 O13_15 1.401(19) . ?
O13_15 C14_15 1.393(17) . ?
C14_15 C15_15 1.357(17) . ?
C14_15 C19_15 1.36(2)   . ?
C15_15 C16_15 1.411(19) . ?
C16_15 C17_15 1.348(17) . ?
C17_15 C18_15 1.42(2)   . ?
C17_15 C36_15 1.482(10) . ?
C18_15 O28_15 1.38(2)   . ?
C18_15 C19_15 1.41(2)   . ?
C19_15 P20_15 1.720(17) . ?
P20_15 O29_15 1.475(16) . ?
P20_15 C21_15 1.733(16) . ?
C21_15 C22_15 1.40(2)   . ?
C21_15 C26_15 1.40(2)   . ?
C22_15 C23_15 1.327(18) . ?
C22_15 O28_15 1.362(17) . ?
C23_15 C24_15 1.42(2)   . ?
C24_15 C25_15 1.386(18) . ?
C25_15 C26_15 1.40(2)   . ?
C25_15 C30_15 1.477(10) . ?
C26_15 O27_15 1.377(19) . ?
C30_15 C35_15 1.390(12) . ?
C30_15 C31_15 1.395(14) . ?
C31_15 C32_15 1.387(15) . ?
C32_15 C33_15 1.390(18) . ?
C33_15 N34_15 1.339(14) . ?
N34_15 C35_15 1.328(12) . ?
C36_15 C37_15 1.390(14) . ?
C36_15 C41_15 1.392(12) . ?
C37_15 C38_15 1.397(15) . ?
C38_15 C39_15 1.360(16) . ?
C39_15 N40_15 1.327(13) . ?
N40_15 C41_15 1.330(12) . ?
N1_16  C6_16  1.337(12) . ?
N1_16  C2_16  1.350(14) . ?
C2_16  C3_16  1.376(18) . ?
C3_16  C4_16  1.394(14) . ?
C4_16  C5_16  1.394(14) . ?
C5_16  C6_16  1.401(12) . ?
C5_16  C7_16  1.490(10) . ?
C7_16  C8_16  1.386(18) . ?
C7_16  C12_16 1.40(2)   . ?
C8_16  C9_16  1.437(19) . ?
C9_16  C10_16 1.362(17) . ?
C10_16 C11_16 1.35(2)   . ?
C10_16 O27_16 1.398(17) . ?
C11_16 C12_16 1.44(2)   . ?
C11_16 P20_16 1.762(16) . ?
C12_16 O13_16 1.38(2)   . ?
O13_16 C14_16 1.368(17) . ?
C14_16 C15_16 1.356(17) . ?
C14_16 C19_16 1.40(2)   . ?
C15_16 C16_16 1.41(2)   . ?
C16_16 C17_16 1.372(18) . ?
C17_16 C18_16 1.42(2)   . ?
C17_16 C36_16 1.483(10) . ?
C18_16 C19_16 1.35(2)   . ?
C18_16 O28_16 1.35(2)   . ?
C19_16 P20_16 1.719(17) . ?
P20_16 O29_16 1.504(16) . ?
P20_16 C21_16 1.75(2)   . ?
C21_16 C22_16 1.40(2)   . ?
C21_16 C26_16 1.42(2)   . ?
C22_16 C23_16 1.351(18) . ?
C22_16 O28_16 1.385(17) . ?
C23_16 C24_16 1.42(2)   . ?
C24_16 C25_16 1.384(17) . ?
C25_16 C26_16 1.41(2)   . ?
C25_16 C30_16 1.476(10) . ?
C26_16 O27_16 1.36(2)   . ?
C30_16 C31_16 1.385(14) . ?
C30_16 C35_16 1.395(12) . ?
C31_16 C32_16 1.399(15) . ?
C32_16 C33_16 1.376(17) . ?
C33_16 N34_16 1.333(14) . ?
N34_16 C35_16 1.331(12) . ?
C36_16 C37_16 1.381(14) . ?
C36_16 C41_16 1.388(12) . ?
C37_16 C38_16 1.389(14) . ?
C38_16 C39_16 1.376(17) . ?
C39_16 N40_16 1.336(14) . ?
N40_16 C41_16 1.339(12) . ?
N1_17  C2_17  1.327(14) . ?
N1_17  C6_17  1.333(12) . ?
C2_17  C3_17  1.397(17) . ?
C3_17  C4_17  1.373(15) . ?
C4_17  C5_17  1.393(14) . ?
C5_17  C6_17  1.386(12) . ?
C5_17  C7_17  1.485(10) . ?
C7_17  C8_17  1.367(17) . ?
C7_17  C12_17 1.40(2)   . ?
C8_17  C9_17  1.42(2)   . ?
C9_17  C10_17 1.372(17) . ?
C10_17 O27_17 1.368(16) . ?
C10_17 C11_17 1.439(19) . ?
C11_17 C12_17 1.44(2)   . ?
C11_17 P20_17 1.765(17) . ?
C12_17 O13_17 1.420(19) . ?
O13_17 C14_17 1.407(17) . ?
C14_17 C19_17 1.36(2)   . ?
C14_17 C15_17 1.362(17) . ?
C15_17 C16_17 1.443(19) . ?
C16_17 C17_17 1.390(18) . ?
C17_17 C18_17 1.39(2)   . ?
C17_17 C36_17 1.492(10) . ?
C18_17 O28_17 1.39(2)   . ?
C18_17 C19_17 1.45(2)   . ?
C19_17 P20_17 1.743(17) . ?
P20_17 O29_17 1.462(17) . ?
P20_17 C21_17 1.750(17) . ?
C21_17 C26_17 1.41(2)   . ?
C21_17 C22_17 1.43(2)   . ?
C22_17 C23_17 1.351(17) . ?
C22_17 O28_17 1.380(16) . ?
C23_17 C24_17 1.412(19) . ?
C24_17 C25_17 1.361(18) . ?
C25_17 C26_17 1.41(2)   . ?
C25_17 C30_17 1.486(10) . ?
C26_17 O27_17 1.41(2)   . ?
C30_17 C35_17 1.385(12) . ?
C30_17 C31_17 1.399(15) . ?
C31_17 C32_17 1.396(15) . ?
C32_17 C33_17 1.374(17) . ?
C33_17 N34_17 1.329(14) . ?
N34_17 C35_17 1.336(12) . ?
C36_17 C37_17 1.386(14) . ?
C36_17 C41_17 1.390(12) . ?
C37_17 C38_17 1.376(15) . ?
C38_17 C39_17 1.384(17) . ?
C39_17 N40_17 1.331(14) . ?
N40_17 C41_17 1.332(12) . ?
N1_18  C6_18  1.323(12) . ?
N1_18  C2_18  1.335(14) . ?
C2_18  C3_18  1.377(17) . ?
C3_18  C4_18  1.386(15) . ?
C4_18  C5_18  1.390(14) . ?
C5_18  C6_18  1.392(12) . ?
C5_18  C7_18  1.487(10) . ?
C7_18  C8_18  1.389(17) . ?
C7_18  C12_18 1.43(2)   . ?
C8_18  C9_18  1.395(19) . ?
C9_18  C10_18 1.351(17) . ?
C10_18 O27_18 1.355(18) . ?
C10_18 C11_18 1.38(2)   . ?
C11_18 C12_18 1.40(2)   . ?
C11_18 P20_18 1.734(18) . ?
C12_18 O13_18 1.36(2)   . ?
O13_18 C14_18 1.392(16) . ?
C14_18 C15_18 1.338(18) . ?
C14_18 C19_18 1.37(2)   . ?
C15_18 C16_18 1.44(2)   . ?
C16_18 C17_18 1.404(18) . ?
C17_18 C18_18 1.39(2)   . ?
C17_18 C36_18 1.476(10) . ?
C18_18 C19_18 1.40(2)   . ?
C18_18 O28_18 1.42(2)   . ?
C19_18 P20_18 1.794(18) . ?
P20_18 O29_18 1.469(17) . ?
P20_18 C21_18 1.738(17) . ?
C21_18 C26_18 1.36(2)   . ?
C21_18 C22_18 1.44(2)   . ?
C22_18 C23_18 1.348(18) . ?
C22_18 O28_18 1.378(17) . ?
C23_18 C24_18 1.46(2)   . ?
C24_18 C25_18 1.364(19) . ?
C25_18 C26_18 1.42(2)   . ?
C25_18 C30_18 1.484(10) . ?
C26_18 O27_18 1.406(19) . ?
C30_18 C31_18 1.383(14) . ?
C30_18 C35_18 1.394(12) . ?
C31_18 C32_18 1.383(14) . ?
C32_18 C33_18 1.372(17) . ?
C33_18 N34_18 1.336(14) . ?
N34_18 C35_18 1.328(12) . ?
C36_18 C41_18 1.387(12) . ?
C36_18 C37_18 1.407(14) . ?
C37_18 C38_18 1.372(15) . ?
C38_18 C39_18 1.369(17) . ?
C39_18 N40_18 1.328(14) . ?
N40_18 C41_18 1.333(12) . ?
B1_19  F3_19  1.37(2)   . ?
B1_19  F4_19  1.38(3)   . ?
B1_19  F2_19  1.39(2)   . ?
B1_19  F5_19  1.41(2)   . ?
B1_20  F2_20  1.37(2)   . ?
B1_20  F3_20  1.38(2)   . ?
B1_20  F4_20  1.40(2)   . ?
B1_20  F5_20  1.42(2)   . ?
B1_21  F3_21  1.35(2)   . ?
B1_21  F5_21  1.37(2)   . ?
B1_21  F2_21  1.38(2)   . ?
B1_21  F4_21  1.41(2)   . ?
N1_22  C2_22  1.19(2)   . ?
C2_22  C3_22  1.47(2)   . ?
N1_23  C2_23  1.15(3)   . ?
C2_23  C3_23  1.46(3)   . ?
N1_24  C2_24  1.20(3)   . ?
C2_24  C3_24  1.44(3)   . ?
N1_25  C2_25  1.14(2)   . ?
C2_25  C3_25  1.46(3)   . ?
N1_26  C2_26  1.12(2)   . ?
C2_26  C3_26  1.49(2)   . ?
N1_27  C2_27  1.13(3)   . ?
C2_27  C3_27  1.46(3)   . ?
N1_28  C2_28  1.15(3)   . ?
C2_28  C3_28  1.51(3)   . ?
N1_29  C2_29  1.15(3)   . ?
C2_29  C3_29  1.47(3)   . ?
N1_31  C2_31  1.13(2)   . ?
C2_31  C3_31  1.49(3)   . ?
N1_32  C2_32  1.18(2)   . ?
C2_32  C3_32  1.45(2)   . ?
N1_33  C2_33  1.18(3)   . ?
C2_33  C3_33  1.48(3)   . ?
B1_34  F4_34  1.39(2)   . ?
B1_34  F2_34  1.39(2)   . ?
B1_34  F5_34  1.39(3)   . ?
B1_34  F3_34  1.41(2)   . ?
N1_35  C2_35  1.16(2)   . ?
C2_35  C3_35  1.45(3)   . ?
B1_36  F5_36  1.35(2)   . ?
B1_36  F4_36  1.38(2)   . ?
B1_36  F2_36  1.39(3)   . ?
B1_36  F3_36  1.39(3)   . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1_4   Pd1_1  N1_2   178.1(5)  . . ?
N1_4   Pd1_1  N1_3   92.1(7)   . . ?
N1_2   Pd1_1  N1_3   87.5(6)   . . ?
N1_4   Pd1_1  N1_5   88.1(8)   . . ?
N1_2   Pd1_1  N1_5   92.2(6)   . . ?
N1_3   Pd1_1  N1_5   177.0(5)  . . ?
N40_4  Pd2_1  N34_8  90.0(8)   . . ?
N40_4  Pd2_1  N34_5  89.2(8)   . . ?
N34_8  Pd2_1  N34_5  177.7(5)  . . ?
N40_4  Pd2_1  N40_6  176.9(6)  . . ?
N34_8  Pd2_1  N40_6  88.5(8)   . . ?
N34_5  Pd2_1  N40_6  92.3(7)   . . ?
N40_5  Pd3_1  N34_6  91.3(7)   . . ?
N40_5  Pd3_1  N34_2  91.8(6)   . . ?
N34_6  Pd3_1  N34_2  176.2(7)  . . ?
N40_5  Pd3_1  N40_9  178.4(6)  . . ?
N34_6  Pd3_1  N40_9  87.8(8)   . . ?
N34_2  Pd3_1  N40_9  89.1(7)   . . ?
N40_7  Pd4_1  N40_2  177.1(7)  . . ?
N40_7  Pd4_1  N34_9  92.9(8)   . . ?
N40_2  Pd4_1  N34_9  89.0(7)   . . ?
N40_7  Pd4_1  N34_3  91.1(8)   . . ?
N40_2  Pd4_1  N34_3  87.0(7)   . . ?
N34_9  Pd4_1  N34_3  175.6(7)  . . ?
N34_7  Pd5_1  N40_3  86.6(7)   . . ?
N34_7  Pd5_1  N34_4  176.9(6)  . . ?
N40_3  Pd5_1  N34_4  90.7(7)   . . ?
N34_7  Pd5_1  N40_8  89.2(7)   . . ?
N40_3  Pd5_1  N40_8  175.8(7)  . . ?
N34_4  Pd5_1  N40_8  93.4(6)   . . ?
N1_6   Pd6_1  N1_7   178.6(5)  . . ?
N1_6   Pd6_1  N1_9   90.5(8)   . . ?
N1_7   Pd6_1  N1_9   90.0(8)   . . ?
N1_6   Pd6_1  N1_8   88.2(7)   . . ?
N1_7   Pd6_1  N1_8   91.3(7)   . . ?
N1_9   Pd6_1  N1_8   176.6(6)  . . ?
C6_2   N1_2   C2_2   117.7(12) . . ?
C6_2   N1_2   Pd1_1  117.4(9)  . . ?
C2_2   N1_2   Pd1_1  124.2(10) . . ?
N1_2   C2_2   C3_2   123.3(14) . . ?
C2_2   C3_2   C4_2   117.3(14) . . ?
C3_2   C4_2   C5_2   119.0(13) . . ?
C6_2   C5_2   C4_2   118.1(10) . . ?
C6_2   C5_2   C7_2   122.3(12) . . ?
C4_2   C5_2   C7_2   119.5(12) . . ?
N1_2   C6_2   C5_2   123.2(11) . . ?
C8_2   C7_2   C12_2  116.5(13) . . ?
C8_2   C7_2   C5_2   122.0(14) . . ?
C12_2  C7_2   C5_2   121.6(15) . . ?
C7_2   C8_2   C9_2   122.6(15) . . ?
C10_2  C9_2   C8_2   118.8(15) . . ?
C9_2   C10_2  O27_2  119.3(15) . . ?
C9_2   C10_2  C11_2  123.2(14) . . ?
O27_2  C10_2  C11_2  117.1(15) . . ?
C10_2  C11_2  C12_2  114.9(16) . . ?
C10_2  C11_2  P20_2  123.4(14) . . ?
C12_2  C11_2  P20_2  121.3(14) . . ?
C7_2   C12_2  O13_2  119.0(16) . . ?
C7_2   C12_2  C11_2  123.6(16) . . ?
O13_2  C12_2  C11_2  117.1(16) . . ?
C14_2  O13_2  C12_2  116.6(14) . . ?
C15_2  C14_2  C19_2  120.0(15) . . ?
C15_2  C14_2  O13_2  120.7(15) . . ?
C19_2  C14_2  O13_2  119.2(15) . . ?
C14_2  C15_2  C16_2  118.8(16) . . ?
C17_2  C16_2  C15_2  122.8(17) . . ?
C16_2  C17_2  C18_2  116.6(14) . . ?
C16_2  C17_2  C36_2  122.4(15) . . ?
C18_2  C17_2  C36_2  121.0(15) . . ?
C19_2  C18_2  O28_2  120.8(17) . . ?
C19_2  C18_2  C17_2  120.8(17) . . ?
O28_2  C18_2  C17_2  118.3(17) . . ?
C18_2  C19_2  C14_2  120.8(17) . . ?
C18_2  C19_2  P20_2  118.3(14) . . ?
C14_2  C19_2  P20_2  120.8(14) . . ?
O29_2  P20_2  C11_2  120.1(11) . . ?
O29_2  P20_2  C19_2  121.5(11) . . ?
C11_2  P20_2  C19_2  95.1(9)   . . ?
O29_2  P20_2  C21_2  121.9(10) . . ?
C11_2  P20_2  C21_2  96.6(9)   . . ?
C19_2  P20_2  C21_2  95.2(8)   . . ?
C22_2  C21_2  C26_2  121.4(16) . . ?
C22_2  C21_2  P20_2  120.3(13) . . ?
C26_2  C21_2  P20_2  117.9(13) . . ?
C23_2  C22_2  C21_2  120.4(16) . . ?
C23_2  C22_2  O28_2  120.4(16) . . ?
C21_2  C22_2  O28_2  119.0(15) . . ?
C22_2  C23_2  C24_2  120.2(16) . . ?
C25_2  C24_2  C23_2  119.3(16) . . ?
C24_2  C25_2  C26_2  119.8(13) . . ?
C24_2  C25_2  C30_2  121.1(13) . . ?
C26_2  C25_2  C30_2  119.1(13) . . ?
O27_2  C26_2  C25_2  120.8(15) . . ?
O27_2  C26_2  C21_2  121.3(15) . . ?
C25_2  C26_2  C21_2  117.8(15) . . ?
C26_2  O27_2  C10_2  118.5(14) . . ?
C22_2  O28_2  C18_2  116.2(16) . . ?
C31_2  C30_2  C35_2  117.5(11) . . ?
C31_2  C30_2  C25_2  120.4(12) . . ?
C35_2  C30_2  C25_2  122.1(12) . . ?
C32_2  C31_2  C30_2  118.5(13) . . ?
C33_2  C32_2  C31_2  119.3(14) . . ?
N34_2  C33_2  C32_2  123.1(15) . . ?
C33_2  N34_2  C35_2  117.9(12) . . ?
C33_2  N34_2  Pd3_1  123.4(11) . . ?
C35_2  N34_2  Pd3_1  118.6(10) . . ?
N34_2  C35_2  C30_2  123.5(12) . . ?
C41_2  C36_2  C37_2  118.1(11) . . ?
C41_2  C36_2  C17_2  120.4(12) . . ?
C37_2  C36_2  C17_2  121.5(12) . . ?
C38_2  C37_2  C36_2  118.7(13) . . ?
C37_2  C38_2  C39_2  118.2(14) . . ?
N40_2  C39_2  C38_2  124.5(14) . . ?
C41_2  N40_2  C39_2  115.6(13) . . ?
C41_2  N40_2  Pd4_1  120.8(10) . . ?
C39_2  N40_2  Pd4_1  123.1(11) . . ?
N40_2  C41_2  C36_2  124.6(12) . . ?
C6_3   N1_3   C2_3   119.5(12) . . ?
C6_3   N1_3   Pd1_1  120.5(9)  . . ?
C2_3   N1_3   Pd1_1  120.0(10) . . ?
N1_3   C2_3   C3_3   120.6(13) . . ?
C4_3   C3_3   C2_3   119.5(14) . . ?
C3_3   C4_3   C5_3   120.6(13) . . ?
C4_3   C5_3   C6_3   115.8(11) . . ?
C4_3   C5_3   C7_3   123.7(11) . . ?
C6_3   C5_3   C7_3   120.6(11) . . ?
N1_3   C6_3   C5_3   123.4(12) . . ?
C8_3   C7_3   C12_3  117.0(13) . . ?
C8_3   C7_3   C5_3   123.1(14) . . ?
C12_3  C7_3   C5_3   119.9(13) . . ?
C7_3   C8_3   C9_3   124.3(16) . . ?
C10_3  C9_3   C8_3   117.1(16) . . ?
C9_3   C10_3  O27_3  120.3(16) . . ?
C9_3   C10_3  C11_3  121.1(15) . . ?
O27_3  C10_3  C11_3  118.3(14) . . ?
C10_3  C11_3  C12_3  119.9(15) . . ?
C10_3  C11_3  P20_3  121.7(12) . . ?
C12_3  C11_3  P20_3  117.8(12) . . ?
O13_3  C12_3  C7_3   119.8(14) . . ?
O13_3  C12_3  C11_3  120.2(15) . . ?
C7_3   C12_3  C11_3  119.8(14) . . ?
C12_3  O13_3  C14_3  114.2(12) . . ?
C15_3  C14_3  C19_3  122.9(15) . . ?
C15_3  C14_3  O13_3  122.6(15) . . ?
C19_3  C14_3  O13_3  114.5(14) . . ?
C14_3  C15_3  C16_3  119.1(16) . . ?
C17_3  C16_3  C15_3  121.9(16) . . ?
C18_3  C17_3  C16_3  116.8(14) . . ?
C18_3  C17_3  C36_3  120.7(13) . . ?
C16_3  C17_3  C36_3  122.5(14) . . ?
C17_3  C18_3  O28_3  119.2(15) . . ?
C17_3  C18_3  C19_3  122.4(14) . . ?
O28_3  C18_3  C19_3  118.0(15) . . ?
C14_3  C19_3  C18_3  116.7(15) . . ?
C14_3  C19_3  P20_3  124.3(13) . . ?
C18_3  C19_3  P20_3  118.9(12) . . ?
O29_3  P20_3  C19_3  121.7(9)  . . ?
O29_3  P20_3  C11_3  122.3(9)  . . ?
C19_3  P20_3  C11_3  93.7(8)   . . ?
O29_3  P20_3  C21_3  120.7(9)  . . ?
C19_3  P20_3  C21_3  96.3(7)   . . ?
C11_3  P20_3  C21_3  95.3(8)   . . ?
C22_3  C21_3  C26_3  120.5(16) . . ?
C22_3  C21_3  P20_3  118.8(11) . . ?
C26_3  C21_3  P20_3  120.2(14) . . ?
C23_3  C22_3  C21_3  119.2(14) . . ?
C23_3  C22_3  O28_3  119.9(15) . . ?
C21_3  C22_3  O28_3  120.9(14) . . ?
C22_3  C23_3  C24_3  118.7(16) . . ?
C25_3  C24_3  C23_3  124.0(15) . . ?
C24_3  C25_3  C26_3  115.5(12) . . ?
C24_3  C25_3  C30_3  121.9(13) . . ?
C26_3  C25_3  C30_3  122.6(14) . . ?
C25_3  C26_3  C21_3  121.3(15) . . ?
C25_3  C26_3  O27_3  118.5(15) . . ?
C21_3  C26_3  O27_3  120.2(16) . . ?
C10_3  O27_3  C26_3  116.8(13) . . ?
C22_3  O28_3  C18_3  114.5(12) . . ?
C31_3  C30_3  C35_3  117.6(11) . . ?
C31_3  C30_3  C25_3  121.4(12) . . ?
C35_3  C30_3  C25_3  120.9(11) . . ?
C32_3  C31_3  C30_3  118.8(14) . . ?
C31_3  C32_3  C33_3  118.8(14) . . ?
N34_3  C33_3  C32_3  123.2(14) . . ?
C33_3  N34_3  C35_3  117.5(13) . . ?
C33_3  N34_3  Pd4_1  122.1(11) . . ?
C35_3  N34_3  Pd4_1  120.0(9)  . . ?
N34_3  C35_3  C30_3  124.0(13) . . ?
C37_3  C36_3  C41_3  117.1(11) . . ?
C37_3  C36_3  C17_3  122.3(11) . . ?
C41_3  C36_3  C17_3  120.5(12) . . ?
C38_3  C37_3  C36_3  120.2(12) . . ?
C39_3  C38_3  C37_3  119.3(14) . . ?
N40_3  C39_3  C38_3  120.4(13) . . ?
C39_3  N40_3  C41_3  121.4(13) . . ?
C39_3  N40_3  Pd5_1  121.5(10) . . ?
C41_3  N40_3  Pd5_1  116.6(9)  . . ?
N40_3  C41_3  C36_3  121.0(12) . . ?
C2_4   N1_4   C6_4   116.5(13) . . ?
C2_4   N1_4   Pd1_1  124.5(11) . . ?
C6_4   N1_4   Pd1_1  118.4(10) . . ?
N1_4   C2_4   C3_4   124.7(15) . . ?
C2_4   C3_4   C4_4   118.2(14) . . ?
C5_4   C4_4   C3_4   118.6(13) . . ?
C6_4   C5_4   C4_4   118.6(11) . . ?
C6_4   C5_4   C7_4   119.4(12) . . ?
C4_4   C5_4   C7_4   121.9(12) . . ?
N1_4   C6_4   C5_4   123.2(13) . . ?
C8_4   C7_4   C12_4  116.8(12) . . ?
C8_4   C7_4   C5_4   125.6(14) . . ?
C12_4  C7_4   C5_4   117.4(14) . . ?
C7_4   C8_4   C9_4   123.0(15) . . ?
C10_4  C9_4   C8_4   118.4(16) . . ?
C9_4   C10_4  O27_4  122.6(17) . . ?
C9_4   C10_4  C11_4  121.1(15) . . ?
O27_4  C10_4  C11_4  116.2(15) . . ?
C12_4  C11_4  C10_4  117.2(15) . . ?
C12_4  C11_4  P20_4  120.9(13) . . ?
C10_4  C11_4  P20_4  121.8(13) . . ?
O13_4  C12_4  C11_4  118.8(14) . . ?
O13_4  C12_4  C7_4   118.6(14) . . ?
C11_4  C12_4  C7_4   122.4(14) . . ?
C14_4  O13_4  C12_4  116.1(13) . . ?
O13_4  C14_4  C15_4  120.2(14) . . ?
O13_4  C14_4  C19_4  118.4(14) . . ?
C15_4  C14_4  C19_4  121.3(14) . . ?
C14_4  C15_4  C16_4  116.3(14) . . ?
C17_4  C16_4  C15_4  124.4(17) . . ?
C16_4  C17_4  C18_4  116.9(13) . . ?
C16_4  C17_4  C36_4  121.8(15) . . ?
C18_4  C17_4  C36_4  121.3(14) . . ?
C17_4  C18_4  O28_4  120.5(14) . . ?
C17_4  C18_4  C19_4  121.8(15) . . ?
O28_4  C18_4  C19_4  117.7(15) . . ?
C18_4  C19_4  C14_4  118.6(15) . . ?
C18_4  C19_4  P20_4  122.0(13) . . ?
C14_4  C19_4  P20_4  119.3(12) . . ?
O29_4  P20_4  C11_4  121.8(10) . . ?
O29_4  P20_4  C21_4  126.2(10) . . ?
C11_4  P20_4  C21_4  93.5(9)   . . ?
O29_4  P20_4  C19_4  120.4(11) . . ?
C11_4  P20_4  C19_4  93.6(8)   . . ?
C21_4  P20_4  C19_4  93.0(9)   . . ?
C26_4  C21_4  C22_4  118.8(16) . . ?
C26_4  C21_4  P20_4  119.2(13) . . ?
C22_4  C21_4  P20_4  121.8(14) . . ?
C23_4  C22_4  O28_4  121.9(15) . . ?
C23_4  C22_4  C21_4  121.1(16) . . ?
O28_4  C22_4  C21_4  117.0(14) . . ?
C22_4  C23_4  C24_4  117.6(15) . . ?
C25_4  C24_4  C23_4  124.2(16) . . ?
C24_4  C25_4  C26_4  117.6(14) . . ?
C24_4  C25_4  C30_4  121.3(14) . . ?
C26_4  C25_4  C30_4  121.1(13) . . ?
O27_4  C26_4  C21_4  120.7(16) . . ?
O27_4  C26_4  C25_4  119.1(15) . . ?
C21_4  C26_4  C25_4  120.1(15) . . ?
C10_4  O27_4  C26_4  111.9(14) . . ?
C22_4  O28_4  C18_4  116.5(14) . . ?
C31_4  C30_4  C35_4  116.6(11) . . ?
C31_4  C30_4  C25_4  123.1(12) . . ?
C35_4  C30_4  C25_4  120.3(13) . . ?
C32_4  C31_4  C30_4  120.8(14) . . ?
C33_4  C32_4  C31_4  118.5(15) . . ?
N34_4  C33_4  C32_4  121.7(14) . . ?
C33_4  N34_4  C35_4  119.7(13) . . ?
C33_4  N34_4  Pd5_1  121.2(11) . . ?
C35_4  N34_4  Pd5_1  118.9(10) . . ?
N34_4  C35_4  C30_4  122.4(13) . . ?
C41_4  C36_4  C37_4  116.6(10) . . ?
C41_4  C36_4  C17_4  120.4(12) . . ?
C37_4  C36_4  C17_4  123.0(12) . . ?
C38_4  C37_4  C36_4  119.3(13) . . ?
C39_4  C38_4  C37_4  119.6(13) . . ?
N40_4  C39_4  C38_4  121.1(13) . . ?
C41_4  N40_4  C39_4  118.5(13) . . ?
C41_4  N40_4  Pd2_1  119.6(9)  . . ?
C39_4  N40_4  Pd2_1  121.9(10) . . ?
N40_4  C41_4  C36_4  124.8(12) . . ?
C2_5   N1_5   C6_5   117.5(12) . . ?
C2_5   N1_5   Pd1_1  123.0(10) . . ?
C6_5   N1_5   Pd1_1  119.2(9)  . . ?
N1_5   C2_5   C3_5   123.7(13) . . ?
C2_5   C3_5   C4_5   117.6(13) . . ?
C5_5   C4_5   C3_5   119.7(13) . . ?
C4_5   C5_5   C6_5   117.9(10) . . ?
C4_5   C5_5   C7_5   122.5(11) . . ?
C6_5   C5_5   C7_5   119.6(11) . . ?
N1_5   C6_5   C5_5   123.3(12) . . ?
C8_5   C7_5   C12_5  117.5(13) . . ?
C8_5   C7_5   C5_5   122.2(14) . . ?
C12_5  C7_5   C5_5   120.3(13) . . ?
C7_5   C8_5   C9_5   118.9(16) . . ?
C10_5  C9_5   C8_5   123.2(15) . . ?
C9_5   C10_5  O27_5  120.7(15) . . ?
C9_5   C10_5  C11_5  117.3(14) . . ?
O27_5  C10_5  C11_5  121.8(14) . . ?
C12_5  C11_5  C10_5  122.2(16) . . ?
C12_5  C11_5  P20_5  120.4(14) . . ?
C10_5  C11_5  P20_5  117.1(12) . . ?
C11_5  C12_5  O13_5  121.0(15) . . ?
C11_5  C12_5  C7_5   120.5(14) . . ?
O13_5  C12_5  C7_5   118.1(13) . . ?
C14_5  O13_5  C12_5  114.0(12) . . ?
C19_5  C14_5  O13_5  125.0(14) . . ?
C19_5  C14_5  C15_5  120.0(15) . . ?
O13_5  C14_5  C15_5  114.9(14) . . ?
C14_5  C15_5  C16_5  118.8(15) . . ?
C17_5  C16_5  C15_5  123.0(15) . . ?
C16_5  C17_5  C18_5  115.5(12) . . ?
C16_5  C17_5  C36_5  122.9(13) . . ?
C18_5  C17_5  C36_5  121.4(13) . . ?
O28_5  C18_5  C19_5  120.7(14) . . ?
O28_5  C18_5  C17_5  119.3(14) . . ?
C19_5  C18_5  C17_5  120.0(13) . . ?
C14_5  C19_5  C18_5  121.6(15) . . ?
C14_5  C19_5  P20_5  118.2(14) . . ?
C18_5  C19_5  P20_5  120.0(12) . . ?
O29_5  P20_5  C21_5  123.5(9)  . . ?
O29_5  P20_5  C11_5  125.2(10) . . ?
C21_5  P20_5  C11_5  95.9(8)   . . ?
O29_5  P20_5  C19_5  115.5(10) . . ?
C21_5  P20_5  C19_5  95.0(8)   . . ?
C11_5  P20_5  C19_5  94.4(8)   . . ?
C22_5  C21_5  C26_5  116.0(15) . . ?
C22_5  C21_5  P20_5  122.0(12) . . ?
C26_5  C21_5  P20_5  121.8(13) . . ?
C23_5  C22_5  O28_5  120.3(15) . . ?
C23_5  C22_5  C21_5  121.7(14) . . ?
O28_5  C22_5  C21_5  117.9(13) . . ?
C22_5  C23_5  C24_5  118.5(15) . . ?
C25_5  C24_5  C23_5  122.1(14) . . ?
C26_5  C25_5  C24_5  118.2(12) . . ?
C26_5  C25_5  C30_5  121.0(13) . . ?
C24_5  C25_5  C30_5  120.9(13) . . ?
C25_5  C26_5  O27_5  122.8(15) . . ?
C25_5  C26_5  C21_5  122.7(15) . . ?
O27_5  C26_5  C21_5  114.5(14) . . ?
C26_5  O27_5  C10_5  118.7(13) . . ?
C22_5  O28_5  C18_5  116.9(12) . . ?
C35_5  C30_5  C31_5  117.2(10) . . ?
C35_5  C30_5  C25_5  121.8(12) . . ?
C31_5  C30_5  C25_5  121.0(11) . . ?
C32_5  C31_5  C30_5  120.4(12) . . ?
C33_5  C32_5  C31_5  116.6(13) . . ?
N34_5  C33_5  C32_5  124.6(13) . . ?
C33_5  N34_5  C35_5  118.0(12) . . ?
C33_5  N34_5  Pd2_1  121.6(9)  . . ?
C35_5  N34_5  Pd2_1  120.2(9)  . . ?
N34_5  C35_5  C30_5  122.8(11) . . ?
C37_5  C36_5  C41_5  116.5(11) . . ?
C37_5  C36_5  C17_5  123.3(12) . . ?
C41_5  C36_5  C17_5  120.2(12) . . ?
C36_5  C37_5  C38_5  119.0(13) . . ?
C39_5  C38_5  C37_5  119.5(14) . . ?
N40_5  C39_5  C38_5  122.4(14) . . ?
C41_5  N40_5  C39_5  117.4(12) . . ?
C41_5  N40_5  Pd3_1  120.0(9)  . . ?
C39_5  N40_5  Pd3_1  121.7(10) . . ?
N40_5  C41_5  C36_5  125.0(12) . . ?
C2_6   N1_6   C6_6   115.8(12) . . ?
C2_6   N1_6   Pd6_1  122.7(9)  . . ?
C6_6   N1_6   Pd6_1  120.9(9)  . . ?
N1_6   C2_6   C3_6   123.5(13) . . ?
C2_6   C3_6   C4_6   118.7(13) . . ?
C5_6   C4_6   C3_6   119.0(12) . . ?
C6_6   C5_6   C4_6   116.6(10) . . ?
C6_6   C5_6   C7_6   121.4(11) . . ?
C4_6   C5_6   C7_6   121.9(11) . . ?
N1_6   C6_6   C5_6   125.4(12) . . ?
C8_6   C7_6   C12_6  117.1(12) . . ?
C8_6   C7_6   C5_6   123.1(12) . . ?
C12_6  C7_6   C5_6   119.6(12) . . ?
C7_6   C8_6   C9_6   123.2(14) . . ?
C10_6  C9_6   C8_6   117.8(16) . . ?
C9_6   C10_6  O27_6  116.8(15) . . ?
C9_6   C10_6  C11_6  121.9(14) . . ?
O27_6  C10_6  C11_6  120.6(13) . . ?
C12_6  C11_6  C10_6  118.7(15) . . ?
C12_6  C11_6  P20_6  123.2(13) . . ?
C10_6  C11_6  P20_6  118.0(11) . . ?
C11_6  C12_6  O13_6  119.8(13) . . ?
C11_6  C12_6  C7_6   120.8(14) . . ?
O13_6  C12_6  C7_6   119.0(13) . . ?
C12_6  O13_6  C14_6  115.7(12) . . ?
C15_6  C14_6  O13_6  119.4(13) . . ?
C15_6  C14_6  C19_6  119.5(13) . . ?
O13_6  C14_6  C19_6  121.0(13) . . ?
C14_6  C15_6  C16_6  119.3(14) . . ?
C17_6  C16_6  C15_6  122.7(14) . . ?
C16_6  C17_6  C18_6  117.9(11) . . ?
C16_6  C17_6  C36_6  120.4(12) . . ?
C18_6  C17_6  C36_6  121.8(11) . . ?
O28_6  C18_6  C17_6  121.4(13) . . ?
O28_6  C18_6  C19_6  118.3(13) . . ?
C17_6  C18_6  C19_6  120.2(13) . . ?
C18_6  C19_6  C14_6  118.6(14) . . ?
C18_6  C19_6  P20_6  121.2(11) . . ?
C14_6  C19_6  P20_6  120.0(11) . . ?
O29_6  P20_6  C19_6  120.6(9)  . . ?
O29_6  P20_6  C21_6  124.6(8)  . . ?
C19_6  P20_6  C21_6  94.0(7)   . . ?
O29_6  P20_6  C11_6  120.3(8)  . . ?
C19_6  P20_6  C11_6  94.1(7)   . . ?
C21_6  P20_6  C11_6  96.1(7)   . . ?
C26_6  C21_6  C22_6  117.2(13) . . ?
C26_6  C21_6  P20_6  121.3(11) . . ?
C22_6  C21_6  P20_6  121.3(12) . . ?
C23_6  C22_6  O28_6  120.1(13) . . ?
C23_6  C22_6  C21_6  121.4(13) . . ?
O28_6  C22_6  C21_6  118.5(12) . . ?
C22_6  C23_6  C24_6  119.2(14) . . ?
C25_6  C24_6  C23_6  121.3(13) . . ?
C24_6  C25_6  C26_6  116.7(12) . . ?
C24_6  C25_6  C30_6  122.5(12) . . ?
C26_6  C25_6  C30_6  120.7(12) . . ?
C21_6  C26_6  O27_6  119.9(13) . . ?
C21_6  C26_6  C25_6  122.9(13) . . ?
O27_6  C26_6  C25_6  117.1(14) . . ?
C10_6  O27_6  C26_6  115.1(12) . . ?
C22_6  O28_6  C18_6  116.4(12) . . ?
C35_6  C30_6  C31_6  116.8(11) . . ?
C35_6  C30_6  C25_6  122.9(11) . . ?
C31_6  C30_6  C25_6  120.2(11) . . ?
C32_6  C31_6  C30_6  119.0(14) . . ?
C31_6  C32_6  C33_6  120.0(15) . . ?
N34_6  C33_6  C32_6  121.7(14) . . ?
C35_6  N34_6  C33_6  117.6(13) . . ?
C35_6  N34_6  Pd3_1  119.1(10) . . ?
C33_6  N34_6  Pd3_1  122.7(11) . . ?
N34_6  C35_6  C30_6  124.7(12) . . ?
C41_6  C36_6  C37_6  118.8(10) . . ?
C41_6  C36_6  C17_6  119.3(11) . . ?
C37_6  C36_6  C17_6  121.7(11) . . ?
C38_6  C37_6  C36_6  118.7(12) . . ?
C39_6  C38_6  C37_6  118.1(12) . . ?
N40_6  C39_6  C38_6  122.7(13) . . ?
C41_6  N40_6  C39_6  119.0(13) . . ?
C41_6  N40_6  Pd2_1  119.4(10) . . ?
C39_6  N40_6  Pd2_1  121.0(10) . . ?
N40_6  C41_6  C36_6  122.8(12) . . ?
C6_7   N1_7   C2_7   116.1(13) . . ?
C6_7   N1_7   Pd6_1  120.3(10) . . ?
C2_7   N1_7   Pd6_1  123.6(11) . . ?
N1_7   C2_7   C3_7   125.1(15) . . ?
C4_7   C3_7   C2_7   117.3(15) . . ?
C3_7   C4_7   C5_7   119.6(14) . . ?
C6_7   C5_7   C4_7   118.2(11) . . ?
C6_7   C5_7   C7_7   119.9(12) . . ?
C4_7   C5_7   C7_7   121.9(12) . . ?
N1_7   C6_7   C5_7   123.7(12) . . ?
C8_7   C7_7   C12_7  115.9(13) . . ?
C8_7   C7_7   C5_7   121.6(14) . . ?
C12_7  C7_7   C5_7   122.6(15) . . ?
C7_7   C8_7   C9_7   123.9(16) . . ?
C10_7  C9_7   C8_7   118.5(17) . . ?
C9_7   C10_7  O27_7  123.1(15) . . ?
C9_7   C10_7  C11_7  120.6(15) . . ?
O27_7  C10_7  C11_7  116.3(14) . . ?
C12_7  C11_7  C10_7  118.0(16) . . ?
C12_7  C11_7  P20_7  119.6(14) . . ?
C10_7  C11_7  P20_7  122.4(13) . . ?
C7_7   C12_7  O13_7  118.4(15) . . ?
C7_7   C12_7  C11_7  122.7(16) . . ?
O13_7  C12_7  C11_7  118.8(15) . . ?
C14_7  O13_7  C12_7  112.8(14) . . ?
C15_7  C14_7  O13_7  118.6(17) . . ?
C15_7  C14_7  C19_7  119.8(15) . . ?
O13_7  C14_7  C19_7  121.6(17) . . ?
C14_7  C15_7  C16_7  117.6(16) . . ?
C17_7  C16_7  C15_7  124.1(17) . . ?
C16_7  C17_7  C18_7  116.5(14) . . ?
C16_7  C17_7  C36_7  122.5(15) . . ?
C18_7  C17_7  C36_7  121.0(14) . . ?
O28_7  C18_7  C17_7  122.6(17) . . ?
O28_7  C18_7  C19_7  117.7(17) . . ?
C17_7  C18_7  C19_7  119.6(17) . . ?
C14_7  C19_7  C18_7  120.7(17) . . ?
C14_7  C19_7  P20_7  118.6(14) . . ?
C18_7  C19_7  P20_7  120.4(14) . . ?
O29_7  P20_7  C19_7  125.2(12) . . ?
O29_7  P20_7  C21_7  123.2(12) . . ?
C19_7  P20_7  C21_7  94.3(9)   . . ?
O29_7  P20_7  C11_7  118.4(10) . . ?
C19_7  P20_7  C11_7  95.3(9)   . . ?
C21_7  P20_7  C11_7  92.5(9)   . . ?
C26_7  C21_7  C22_7  117.7(16) . . ?
C26_7  C21_7  P20_7  121.7(13) . . ?
C22_7  C21_7  P20_7  120.6(14) . . ?
C23_7  C22_7  O28_7  120.7(16) . . ?
C23_7  C22_7  C21_7  122.0(16) . . ?
O28_7  C22_7  C21_7  117.3(15) . . ?
C22_7  C23_7  C24_7  118.3(16) . . ?
C25_7  C24_7  C23_7  122.4(17) . . ?
C24_7  C25_7  C26_7  118.5(14) . . ?
C24_7  C25_7  C30_7  122.5(14) . . ?
C26_7  C25_7  C30_7  119.0(13) . . ?
O27_7  C26_7  C21_7  119.2(15) . . ?
O27_7  C26_7  C25_7  119.9(16) . . ?
C21_7  C26_7  C25_7  120.7(15) . . ?
C26_7  O27_7  C10_7  115.5(13) . . ?
C18_7  O28_7  C22_7  117.3(15) . . ?
C31_7  C30_7  C35_7  117.5(11) . . ?
C31_7  C30_7  C25_7  121.0(12) . . ?
C35_7  C30_7  C25_7  121.5(12) . . ?
C32_7  C31_7  C30_7  119.0(13) . . ?
C31_7  C32_7  C33_7  118.9(14) . . ?
N34_7  C33_7  C32_7  123.7(15) . . ?
C33_7  N34_7  C35_7  116.4(13) . . ?
C33_7  N34_7  Pd5_1  123.7(11) . . ?
C35_7  N34_7  Pd5_1  119.1(10) . . ?
N34_7  C35_7  C30_7  123.8(12) . . ?
C37_7  C36_7  C41_7  117.7(11) . . ?
C37_7  C36_7  C17_7  123.0(12) . . ?
C41_7  C36_7  C17_7  119.1(12) . . ?
C36_7  C37_7  C38_7  120.3(14) . . ?
C39_7  C38_7  C37_7  116.4(14) . . ?
N40_7  C39_7  C38_7  125.0(15) . . ?
C39_7  N40_7  C41_7  117.0(13) . . ?
C39_7  N40_7  Pd4_1  121.4(10) . . ?
C41_7  N40_7  Pd4_1  121.5(10) . . ?
N40_7  C41_7  C36_7  123.2(13) . . ?
C2_8   N1_8   C6_8   116.3(12) . . ?
C2_8   N1_8   Pd6_1  122.8(9)  . . ?
C6_8   N1_8   Pd6_1  120.9(10) . . ?
N1_8   C2_8   C3_8   125.5(12) . . ?
C2_8   C3_8   C4_8   117.3(12) . . ?
C5_8   C4_8   C3_8   119.0(12) . . ?
C4_8   C5_8   C6_8   118.8(10) . . ?
C4_8   C5_8   C7_8   121.0(10) . . ?
C6_8   C5_8   C7_8   120.2(11) . . ?
N1_8   C6_8   C5_8   122.5(12) . . ?
C8_8   C7_8   C12_8  116.2(12) . . ?
C8_8   C7_8   C5_8   121.9(13) . . ?
C12_8  C7_8   C5_8   121.8(12) . . ?
C7_8   C8_8   C9_8   122.3(15) . . ?
C10_8  C9_8   C8_8   118.6(15) . . ?
C9_8   C10_8  O27_8  118.1(15) . . ?
C9_8   C10_8  C11_8  120.9(14) . . ?
O27_8  C10_8  C11_8  121.0(15) . . ?
C12_8  C11_8  C10_8  118.1(15) . . ?
C12_8  C11_8  P20_8  122.9(13) . . ?
C10_8  C11_8  P20_8  118.9(12) . . ?
C11_8  C12_8  C7_8   123.3(14) . . ?
C11_8  C12_8  O13_8  114.5(14) . . ?
C7_8   C12_8  O13_8  122.2(14) . . ?
C14_8  O13_8  C12_8  113.4(12) . . ?
C15_8  C14_8  O13_8  118.2(15) . . ?
C15_8  C14_8  C19_8  119.4(15) . . ?
O13_8  C14_8  C19_8  122.4(15) . . ?
C14_8  C15_8  C16_8  118.1(16) . . ?
C17_8  C16_8  C15_8  124.0(16) . . ?
C16_8  C17_8  C18_8  115.6(13) . . ?
C16_8  C17_8  C36_8  123.5(14) . . ?
C18_8  C17_8  C36_8  120.8(13) . . ?
C19_8  C18_8  O28_8  119.3(15) . . ?
C19_8  C18_8  C17_8  121.3(15) . . ?
O28_8  C18_8  C17_8  119.1(16) . . ?
C18_8  C19_8  C14_8  121.1(15) . . ?
C18_8  C19_8  P20_8  123.0(13) . . ?
C14_8  C19_8  P20_8  115.6(14) . . ?
O29_8  P20_8  C11_8  126.2(11) . . ?
O29_8  P20_8  C19_8  122.7(10) . . ?
C11_8  P20_8  C19_8  94.8(9)   . . ?
O29_8  P20_8  C21_8  116.2(9)  . . ?
C11_8  P20_8  C21_8  96.0(9)   . . ?
C19_8  P20_8  C21_8  93.4(9)   . . ?
C22_8  C21_8  C26_8  121.7(16) . . ?
C22_8  C21_8  P20_8  120.6(13) . . ?
C26_8  C21_8  P20_8  117.5(14) . . ?
O28_8  C22_8  C23_8  120.8(17) . . ?
O28_8  C22_8  C21_8  119.9(15) . . ?
C23_8  C22_8  C21_8  119.3(15) . . ?
C22_8  C23_8  C24_8  118.5(16) . . ?
C25_8  C24_8  C23_8  124.0(16) . . ?
C24_8  C25_8  C26_8  117.8(13) . . ?
C24_8  C25_8  C30_8  124.3(14) . . ?
C26_8  C25_8  C30_8  117.9(13) . . ?
O27_8  C26_8  C21_8  120.9(15) . . ?
O27_8  C26_8  C25_8  120.6(14) . . ?
C21_8  C26_8  C25_8  118.0(14) . . ?
C10_8  O27_8  C26_8  114.2(13) . . ?
C22_8  O28_8  C18_8  116.9(14) . . ?
C31_8  C30_8  C35_8  117.5(11) . . ?
C31_8  C30_8  C25_8  121.8(12) . . ?
C35_8  C30_8  C25_8  120.6(12) . . ?
C30_8  C31_8  C32_8  119.3(13) . . ?
C33_8  C32_8  C31_8  119.2(14) . . ?
N34_8  C33_8  C32_8  122.4(15) . . ?
C33_8  N34_8  C35_8  118.6(13) . . ?
C33_8  N34_8  Pd2_1  122.1(11) . . ?
C35_8  N34_8  Pd2_1  119.3(10) . . ?
N34_8  C35_8  C30_8  122.8(12) . . ?
C41_8  C36_8  C37_8  117.1(11) . . ?
C41_8  C36_8  C17_8  121.9(12) . . ?
C37_8  C36_8  C17_8  120.9(12) . . ?
C38_8  C37_8  C36_8  120.2(14) . . ?
C39_8  C38_8  C37_8  118.0(15) . . ?
N40_8  C39_8  C38_8  122.4(15) . . ?
C39_8  N40_8  C41_8  119.3(13) . . ?
C39_8  N40_8  Pd5_1  123.4(10) . . ?
C41_8  N40_8  Pd5_1  117.3(10) . . ?
N40_8  C41_8  C36_8  122.6(13) . . ?
C2_9   N1_9   C6_9   120.2(13) . . ?
C2_9   N1_9   Pd6_1  120.7(11) . . ?
C6_9   N1_9   Pd6_1  118.9(11) . . ?
N1_9   C2_9   C3_9   122.2(15) . . ?
C4_9   C3_9   C2_9   117.3(15) . . ?
C3_9   C4_9   C5_9   120.3(14) . . ?
C4_9   C5_9   C6_9   117.7(11) . . ?
C4_9   C5_9   C7_9   121.5(12) . . ?
C6_9   C5_9   C7_9   120.8(11) . . ?
N1_9   C6_9   C5_9   121.7(12) . . ?
C12_9  C7_9   C8_9   118.4(12) . . ?
C12_9  C7_9   C5_9   119.1(13) . . ?
C8_9   C7_9   C5_9   122.5(14) . . ?
C7_9   C8_9   C9_9   122.2(16) . . ?
C10_9  C9_9   C8_9   117.7(16) . . ?
C9_9   C10_9  O27_9  121.3(15) . . ?
C9_9   C10_9  C11_9  119.9(14) . . ?
O27_9  C10_9  C11_9  118.7(14) . . ?
C12_9  C11_9  C10_9  121.9(15) . . ?
C12_9  C11_9  P20_9  118.3(12) . . ?
C10_9  C11_9  P20_9  119.8(11) . . ?
O13_9  C12_9  C7_9   117.5(12) . . ?
O13_9  C12_9  C11_9  123.0(14) . . ?
C7_9   C12_9  C11_9  119.5(13) . . ?
C12_9  O13_9  C14_9  112.2(12) . . ?
C19_9  C14_9  C15_9  117.5(15) . . ?
C19_9  C14_9  O13_9  123.7(14) . . ?
C15_9  C14_9  O13_9  118.8(14) . . ?
C14_9  C15_9  C16_9  119.3(15) . . ?
C17_9  C16_9  C15_9  123.9(15) . . ?
C16_9  C17_9  C18_9  117.0(13) . . ?
C16_9  C17_9  C36_9  123.0(13) . . ?
C18_9  C17_9  C36_9  120.1(12) . . ?
O28_9  C18_9  C17_9  122.4(15) . . ?
O28_9  C18_9  C19_9  120.0(14) . . ?
C17_9  C18_9  C19_9  117.5(13) . . ?
C14_9  C19_9  C18_9  124.2(14) . . ?
C14_9  C19_9  P20_9  118.9(13) . . ?
C18_9  C19_9  P20_9  116.7(11) . . ?
O29_9  P20_9  C19_9  125.1(9)  . . ?
O29_9  P20_9  C21_9  117.3(9)  . . ?
C19_9  P20_9  C21_9  97.9(8)   . . ?
O29_9  P20_9  C11_9  121.4(9)  . . ?
C19_9  P20_9  C11_9  94.2(8)   . . ?
C21_9  P20_9  C11_9  94.1(7)   . . ?
C26_9  C21_9  C22_9  120.9(14) . . ?
C26_9  C21_9  P20_9  121.3(13) . . ?
C22_9  C21_9  P20_9  117.4(11) . . ?
C23_9  C22_9  O28_9  120.1(16) . . ?
C23_9  C22_9  C21_9  119.4(14) . . ?
O28_9  C22_9  C21_9  120.1(14) . . ?
C22_9  C23_9  C24_9  119.6(16) . . ?
C25_9  C24_9  C23_9  122.5(16) . . ?
C24_9  C25_9  C26_9  117.5(12) . . ?
C24_9  C25_9  C30_9  122.6(13) . . ?
C26_9  C25_9  C30_9  119.7(13) . . ?
O27_9  C26_9  C21_9  118.6(14) . . ?
O27_9  C26_9  C25_9  121.7(13) . . ?
C21_9  C26_9  C25_9  119.3(14) . . ?
C26_9  O27_9  C10_9  116.8(13) . . ?
C22_9  O28_9  C18_9  116.6(13) . . ?
C35_9  C30_9  C31_9  116.7(10) . . ?
C35_9  C30_9  C25_9  121.1(11) . . ?
C31_9  C30_9  C25_9  122.1(12) . . ?
C32_9  C31_9  C30_9  119.5(13) . . ?
C33_9  C32_9  C31_9  118.0(13) . . ?
N34_9  C33_9  C32_9  125.0(14) . . ?
C33_9  N34_9  C35_9  116.4(12) . . ?
C33_9  N34_9  Pd4_1  123.6(10) . . ?
C35_9  N34_9  Pd4_1  119.5(10) . . ?
N34_9  C35_9  C30_9  124.2(12) . . ?
C37_9  C36_9  C41_9  116.9(10) . . ?
C37_9  C36_9  C17_9  122.5(11) . . ?
C41_9  C36_9  C17_9  120.5(12) . . ?
C36_9  C37_9  C38_9  119.4(12) . . ?
C39_9  C38_9  C37_9  119.1(13) . . ?
N40_9  C39_9  C38_9  121.9(13) . . ?
C39_9  N40_9  C41_9  118.3(11) . . ?
C39_9  N40_9  Pd3_1  121.1(10) . . ?
C41_9  N40_9  Pd3_1  120.1(9)  . . ?
N40_9  C41_9  C36_9  124.2(12) . . ?
N1_11  Pd1_10 N34_14 85.8(6)   . . ?
N1_11  Pd1_10 N34_18 89.8(8)   . . ?
N34_14 Pd1_10 N34_18 175.6(8)  . . ?
N1_11  Pd1_10 N34_15 176.8(5)  . . ?
N34_14 Pd1_10 N34_15 93.2(6)   . . ?
N34_18 Pd1_10 N34_15 91.2(8)   . . ?
N1_17  Pd2_10 N40_15 177.8(5)  . . ?
N1_17  Pd2_10 N1_18  87.9(5)   . . ?
N40_15 Pd2_10 N1_18  91.9(6)   . . ?
N1_17  Pd2_10 N34_16 91.5(7)   . . ?
N40_15 Pd2_10 N34_16 88.7(7)   . . ?
N1_18  Pd2_10 N34_16 179.2(7)  . . ?
N40_16 Pd3_10 N34_12 174.4(6)  . . ?
N40_16 Pd3_10 N40_13 87.1(6)   . . ?
N34_12 Pd3_10 N40_13 90.9(6)   . . ?
N40_16 Pd3_10 N40_17 91.9(7)   . . ?
N34_12 Pd3_10 N40_17 90.1(6)   . . ?
N40_13 Pd3_10 N40_17 179.0(6)  . . ?
N40_11 Pd4_10 N40_12 90.8(7)   . . ?
N40_11 Pd4_10 N34_17 177.9(6)  . . ?
N40_12 Pd4_10 N34_17 90.2(6)   . . ?
N40_11 Pd4_10 N40_18 89.8(7)   . . ?
N40_12 Pd4_10 N40_18 178.9(6)  . . ?
N34_17 Pd4_10 N40_18 89.1(7)   . . ?
N40_14 Pd5_10 N1_15  87.8(7)   . . ?
N40_14 Pd5_10 N1_16  177.6(6)  . . ?
N1_15  Pd5_10 N1_16  90.9(7)   . . ?
N40_14 Pd5_10 N34_13 89.4(8)   . . ?
N1_15  Pd5_10 N34_13 177.2(8)  . . ?
N1_16  Pd5_10 N34_13 91.9(7)   . . ?
N1_12  Pd6_10 N1_13  86.4(6)   . . ?
N1_12  Pd6_10 N34_11 89.4(7)   . . ?
N1_13  Pd6_10 N34_11 175.3(7)  . . ?
N1_12  Pd6_10 N1_14  176.0(6)  . . ?
N1_13  Pd6_10 N1_14  92.5(6)   . . ?
N34_11 Pd6_10 N1_14  91.6(7)   . . ?
C6_11  N1_11  C2_11  117.1(13) . . ?
C6_11  N1_11  Pd1_10 116.4(10) . . ?
C2_11  N1_11  Pd1_10 126.5(10) . . ?
N1_11  C2_11  C3_11  123.5(13) . . ?
C2_11  C3_11  C4_11  118.8(14) . . ?
C3_11  C4_11  C5_11  118.5(13) . . ?
C4_11  C5_11  C6_11  117.9(10) . . ?
C4_11  C5_11  C7_11  121.5(12) . . ?
C6_11  C5_11  C7_11  120.6(12) . . ?
N1_11  C6_11  C5_11  123.6(12) . . ?
C8_11  C7_11  C12_11 117.8(12) . . ?
C8_11  C7_11  C5_11  120.0(13) . . ?
C12_11 C7_11  C5_11  122.2(14) . . ?
C7_11  C8_11  C9_11  120.1(15) . . ?
C10_11 C9_11  C8_11  121.3(16) . . ?
C9_11  C10_11 O27_11 121.9(16) . . ?
C9_11  C10_11 C11_11 121.3(15) . . ?
O27_11 C10_11 C11_11 116.7(14) . . ?
C12_11 C11_11 C10_11 115.9(14) . . ?
C12_11 C11_11 P20_11 121.9(13) . . ?
C10_11 C11_11 P20_11 122.1(12) . . ?
O13_11 C12_11 C7_11  119.3(14) . . ?
O13_11 C12_11 C11_11 116.5(14) . . ?
C7_11  C12_11 C11_11 123.5(15) . . ?
C14_11 O13_11 C12_11 119.0(13) . . ?
C15_11 C14_11 O13_11 121.1(15) . . ?
C15_11 C14_11 C19_11 119.1(14) . . ?
O13_11 C14_11 C19_11 119.7(14) . . ?
C14_11 C15_11 C16_11 119.1(16) . . ?
C15_11 C16_11 C17_11 123.3(16) . . ?
C16_11 C17_11 C18_11 117.5(13) . . ?
C16_11 C17_11 C36_11 121.6(14) . . ?
C18_11 C17_11 C36_11 120.9(13) . . ?
C19_11 C18_11 O28_11 117.5(15) . . ?
C19_11 C18_11 C17_11 119.3(14) . . ?
O28_11 C18_11 C17_11 122.9(14) . . ?
C18_11 C19_11 C14_11 121.2(15) . . ?
C18_11 C19_11 P20_11 121.2(12) . . ?
C14_11 C19_11 P20_11 117.3(12) . . ?
O29_11 P20_11 C11_11 121.7(8)  . . ?
O29_11 P20_11 C21_11 121.7(9)  . . ?
C11_11 P20_11 C21_11 94.8(8)   . . ?
O29_11 P20_11 C19_11 120.9(8)  . . ?
C11_11 P20_11 C19_11 96.4(8)   . . ?
C21_11 P20_11 C19_11 94.5(8)   . . ?
C22_11 C21_11 C26_11 118.1(16) . . ?
C22_11 C21_11 P20_11 121.0(14) . . ?
C26_11 C21_11 P20_11 120.7(14) . . ?
C23_11 C22_11 O28_11 120.8(16) . . ?
C23_11 C22_11 C21_11 120.7(16) . . ?
O28_11 C22_11 C21_11 118.4(15) . . ?
C22_11 C23_11 C24_11 119.3(17) . . ?
C25_11 C24_11 C23_11 121.8(16) . . ?
C24_11 C25_11 C26_11 117.2(14) . . ?
C24_11 C25_11 C30_11 121.0(14) . . ?
C26_11 C25_11 C30_11 121.8(14) . . ?
O27_11 C26_11 C25_11 119.1(16) . . ?
O27_11 C26_11 C21_11 118.2(15) . . ?
C25_11 C26_11 C21_11 122.3(16) . . ?
C10_11 O27_11 C26_11 117.6(14) . . ?
C22_11 O28_11 C18_11 115.7(14) . . ?
C35_11 C30_11 C31_11 117.3(11) . . ?
C35_11 C30_11 C25_11 121.4(12) . . ?
C31_11 C30_11 C25_11 121.2(12) . . ?
C32_11 C31_11 C30_11 117.9(13) . . ?
C31_11 C32_11 C33_11 121.8(14) . . ?
N34_11 C33_11 C32_11 119.2(14) . . ?
C35_11 N34_11 C33_11 118.9(14) . . ?
C35_11 N34_11 Pd6_10 122.2(11) . . ?
C33_11 N34_11 Pd6_10 118.5(11) . . ?
N34_11 C35_11 C30_11 124.2(13) . . ?
C41_11 C36_11 C37_11 118.8(11) . . ?
C41_11 C36_11 C17_11 120.6(12) . . ?
C37_11 C36_11 C17_11 120.6(12) . . ?
C36_11 C37_11 C38_11 117.3(13) . . ?
C39_11 C38_11 C37_11 118.4(14) . . ?
N40_11 C39_11 C38_11 125.4(15) . . ?
C39_11 N40_11 C41_11 115.8(13) . . ?
C39_11 N40_11 Pd4_10 124.9(11) . . ?
C41_11 N40_11 Pd4_10 119.3(10) . . ?
N40_11 C41_11 C36_11 124.3(13) . . ?
C6_12  N1_12  C2_12  117.5(13) . . ?
C6_12  N1_12  Pd6_10 121.0(10) . . ?
C2_12  N1_12  Pd6_10 121.4(11) . . ?
N1_12  C2_12  C3_12  124.0(15) . . ?
C4_12  C3_12  C2_12  117.5(14) . . ?
C3_12  C4_12  C5_12  119.3(13) . . ?
C6_12  C5_12  C4_12  117.3(11) . . ?
C6_12  C5_12  C7_12  121.5(12) . . ?
C4_12  C5_12  C7_12  121.1(12) . . ?
N1_12  C6_12  C5_12  123.8(13) . . ?
C8_12  C7_12  C12_12 117.6(14) . . ?
C8_12  C7_12  C5_12  121.2(14) . . ?
C12_12 C7_12  C5_12  121.1(15) . . ?
C7_12  C8_12  C9_12  122.7(15) . . ?
C10_12 C9_12  C8_12  118.2(16) . . ?
C9_12  C10_12 O27_12 119.3(17) . . ?
C9_12  C10_12 C11_12 121.8(17) . . ?
O27_12 C10_12 C11_12 118.7(15) . . ?
C12_12 C11_12 C10_12 118.1(16) . . ?
C12_12 C11_12 P20_12 121.5(14) . . ?
C10_12 C11_12 P20_12 120.0(15) . . ?
C7_12  C12_12 C11_12 121.3(17) . . ?
C7_12  C12_12 O13_12 120.1(18) . . ?
C11_12 C12_12 O13_12 118.5(16) . . ?
C14_12 O13_12 C12_12 112.3(15) . . ?
C15_12 C14_12 O13_12 116.9(16) . . ?
C15_12 C14_12 C19_12 118.6(14) . . ?
O13_12 C14_12 C19_12 124.5(14) . . ?
C14_12 C15_12 C16_12 117.4(17) . . ?
C17_12 C16_12 C15_12 124.9(17) . . ?
C16_12 C17_12 C18_12 118.2(13) . . ?
C16_12 C17_12 C36_12 122.9(13) . . ?
C18_12 C17_12 C36_12 118.9(13) . . ?
O28_12 C18_12 C17_12 123.8(15) . . ?
O28_12 C18_12 C19_12 119.1(15) . . ?
C17_12 C18_12 C19_12 117.1(15) . . ?
C14_12 C19_12 C18_12 122.6(14) . . ?
C14_12 C19_12 P20_12 115.9(11) . . ?
C18_12 C19_12 P20_12 121.3(13) . . ?
O29_12 P20_12 C11_12 121.9(10) . . ?
O29_12 P20_12 C21_12 120.5(11) . . ?
C11_12 P20_12 C21_12 96.3(9)   . . ?
O29_12 P20_12 C19_12 121.1(10) . . ?
C11_12 P20_12 C19_12 96.2(8)   . . ?
C21_12 P20_12 C19_12 94.3(8)   . . ?
C26_12 C21_12 C22_12 120.5(17) . . ?
C26_12 C21_12 P20_12 118.3(14) . . ?
C22_12 C21_12 P20_12 120.4(13) . . ?
O28_12 C22_12 C23_12 118.1(15) . . ?
O28_12 C22_12 C21_12 120.9(16) . . ?
C23_12 C22_12 C21_12 120.6(14) . . ?
C22_12 C23_12 C24_12 115.7(14) . . ?
C25_12 C24_12 C23_12 124.7(16) . . ?
C24_12 C25_12 C26_12 115.9(13) . . ?
C24_12 C25_12 C30_12 123.9(14) . . ?
C26_12 C25_12 C30_12 120.2(13) . . ?
C21_12 C26_12 O27_12 123.3(17) . . ?
C21_12 C26_12 C25_12 120.4(15) . . ?
O27_12 C26_12 C25_12 116.2(15) . . ?
C26_12 O27_12 C10_12 115.9(15) . . ?
C22_12 O28_12 C18_12 114.8(13) . . ?
C35_12 C30_12 C31_12 118.2(11) . . ?
C35_12 C30_12 C25_12 119.3(12) . . ?
C31_12 C30_12 C25_12 122.4(12) . . ?
C32_12 C31_12 C30_12 119.8(13) . . ?
C31_12 C32_12 C33_12 117.7(14) . . ?
N34_12 C33_12 C32_12 123.1(13) . . ?
C33_12 N34_12 C35_12 118.0(13) . . ?
C33_12 N34_12 Pd3_10 122.4(10) . . ?
C35_12 N34_12 Pd3_10 119.5(10) . . ?
N34_12 C35_12 C30_12 123.0(12) . . ?
C41_12 C36_12 C37_12 119.4(10) . . ?
C41_12 C36_12 C17_12 121.6(11) . . ?
C37_12 C36_12 C17_12 119.0(11) . . ?
C38_12 C37_12 C36_12 118.7(13) . . ?
C37_12 C38_12 C39_12 117.1(13) . . ?
N40_12 C39_12 C38_12 125.0(13) . . ?
C39_12 N40_12 C41_12 116.8(13) . . ?
C39_12 N40_12 Pd4_10 123.9(10) . . ?
C41_12 N40_12 Pd4_10 119.1(10) . . ?
N40_12 C41_12 C36_12 122.7(12) . . ?
C2_13  N1_13  C6_13  116.9(14) . . ?
C2_13  N1_13  Pd6_10 123.9(12) . . ?
C6_13  N1_13  Pd6_10 118.4(11) . . ?
N1_13  C2_13  C3_13  125.6(15) . . ?
C2_13  C3_13  C4_13  116.5(15) . . ?
C3_13  C4_13  C5_13  119.3(14) . . ?
C6_13  C5_13  C4_13  118.8(11) . . ?
C6_13  C5_13  C7_13  120.9(12) . . ?
C4_13  C5_13  C7_13  120.3(12) . . ?
N1_13  C6_13  C5_13  122.5(13) . . ?
C8_13  C7_13  C12_13 117.5(13) . . ?
C8_13  C7_13  C5_13  122.5(14) . . ?
C12_13 C7_13  C5_13  119.9(13) . . ?
C7_13  C8_13  C9_13  122.9(16) . . ?
C10_13 C9_13  C8_13  118.6(17) . . ?
C9_13  C10_13 O27_13 120.9(16) . . ?
C9_13  C10_13 C11_13 120.4(15) . . ?
O27_13 C10_13 C11_13 118.7(15) . . ?
C12_13 C11_13 C10_13 120.1(15) . . ?
C12_13 C11_13 P20_13 120.5(12) . . ?
C10_13 C11_13 P20_13 118.7(13) . . ?
O13_13 C12_13 C11_13 120.9(15) . . ?
O13_13 C12_13 C7_13  119.3(15) . . ?
C11_13 C12_13 C7_13  119.6(14) . . ?
C12_13 O13_13 C14_13 113.9(13) . . ?
C15_13 C14_13 C19_13 121.4(15) . . ?
C15_13 C14_13 O13_13 116.8(16) . . ?
C19_13 C14_13 O13_13 121.8(15) . . ?
C14_13 C15_13 C16_13 118.2(16) . . ?
C17_13 C16_13 C15_13 122.1(15) . . ?
C16_13 C17_13 C18_13 119.6(13) . . ?
C16_13 C17_13 C36_13 121.2(13) . . ?
C18_13 C17_13 C36_13 119.2(13) . . ?
O28_13 C18_13 C17_13 122.9(14) . . ?
O28_13 C18_13 C19_13 120.6(14) . . ?
C17_13 C18_13 C19_13 116.4(14) . . ?
C14_13 C19_13 C18_13 121.3(15) . . ?
C14_13 C19_13 P20_13 119.7(12) . . ?
C18_13 C19_13 P20_13 118.9(13) . . ?
O29_13 P20_13 C19_13 120.7(9)  . . ?
O29_13 P20_13 C11_13 120.4(9)  . . ?
C19_13 P20_13 C11_13 96.1(8)   . . ?
O29_13 P20_13 C21_13 121.4(10) . . ?
C19_13 P20_13 C21_13 94.3(8)   . . ?
C11_13 P20_13 C21_13 97.7(8)   . . ?
C22_13 C21_13 C26_13 120.8(15) . . ?
C22_13 C21_13 P20_13 122.7(13) . . ?
C26_13 C21_13 P20_13 116.2(12) . . ?
C23_13 C22_13 C21_13 122.7(15) . . ?
C23_13 C22_13 O28_13 118.9(15) . . ?
C21_13 C22_13 O28_13 118.4(15) . . ?
C22_13 C23_13 C24_13 116.9(15) . . ?
C25_13 C24_13 C23_13 122.9(15) . . ?
C24_13 C25_13 C26_13 118.4(12) . . ?
C24_13 C25_13 C30_13 121.4(13) . . ?
C26_13 C25_13 C30_13 120.2(13) . . ?
O27_13 C26_13 C25_13 122.8(13) . . ?
O27_13 C26_13 C21_13 119.6(14) . . ?
C25_13 C26_13 C21_13 117.6(14) . . ?
C10_13 O27_13 C26_13 114.8(12) . . ?
C18_13 O28_13 C22_13 115.4(14) . . ?
C31_13 C30_13 C35_13 117.5(10) . . ?
C31_13 C30_13 C25_13 122.1(12) . . ?
C35_13 C30_13 C25_13 120.1(11) . . ?
C32_13 C31_13 C30_13 118.4(12) . . ?
C33_13 C32_13 C31_13 119.2(13) . . ?
N34_13 C33_13 C32_13 123.2(13) . . ?
C33_13 N34_13 C35_13 117.5(12) . . ?
C33_13 N34_13 Pd5_10 122.8(10) . . ?
C35_13 N34_13 Pd5_10 119.5(9)  . . ?
N34_13 C35_13 C30_13 123.5(11) . . ?
C41_13 C36_13 C37_13 118.2(10) . . ?
C41_13 C36_13 C17_13 120.3(11) . . ?
C37_13 C36_13 C17_13 121.5(11) . . ?
C36_13 C37_13 C38_13 119.1(13) . . ?
C39_13 C38_13 C37_13 118.5(13) . . ?
N40_13 C39_13 C38_13 122.9(13) . . ?
C41_13 N40_13 C39_13 118.4(13) . . ?
C41_13 N40_13 Pd3_10 119.7(9)  . . ?
C39_13 N40_13 Pd3_10 121.8(10) . . ?
N40_13 C41_13 C36_13 122.7(12) . . ?
C2_14  N1_14  C6_14  116.7(13) . . ?
C2_14  N1_14  Pd6_10 120.8(11) . . ?
C6_14  N1_14  Pd6_10 122.3(10) . . ?
N1_14  C2_14  C3_14  123.3(15) . . ?
C2_14  C3_14  C4_14  118.1(15) . . ?
C5_14  C4_14  C3_14  117.7(13) . . ?
C6_14  C5_14  C4_14  118.0(11) . . ?
C6_14  C5_14  C7_14  119.2(12) . . ?
C4_14  C5_14  C7_14  122.5(12) . . ?
N1_14  C6_14  C5_14  124.3(13) . . ?
C8_14  C7_14  C12_14 116.6(13) . . ?
C8_14  C7_14  C5_14  123.0(14) . . ?
C12_14 C7_14  C5_14  120.3(13) . . ?
C7_14  C8_14  C9_14  120.4(16) . . ?
C10_14 C9_14  C8_14  120.0(17) . . ?
C9_14  C10_14 C11_14 121.7(17) . . ?
C9_14  C10_14 O27_14 118.2(15) . . ?
C11_14 C10_14 O27_14 119.8(15) . . ?
C12_14 C11_14 C10_14 119.0(16) . . ?
C12_14 C11_14 P20_14 120.8(14) . . ?
C10_14 C11_14 P20_14 119.9(15) . . ?
C11_14 C12_14 O13_14 119.4(16) . . ?
C11_14 C12_14 C7_14  121.3(14) . . ?
O13_14 C12_14 C7_14  119.2(16) . . ?
C12_14 O13_14 C14_14 117.5(15) . . ?
C15_14 C14_14 O13_14 122.6(18) . . ?
C15_14 C14_14 C19_14 118.7(17) . . ?
O13_14 C14_14 C19_14 118.6(17) . . ?
C14_14 C15_14 C16_14 118.0(19) . . ?
C17_14 C16_14 C15_14 123.6(17) . . ?
C16_14 C17_14 C18_14 117.0(14) . . ?
C16_14 C17_14 C36_14 123.6(16) . . ?
C18_14 C17_14 C36_14 119.5(16) . . ?
O28_14 C18_14 C19_14 119.8(16) . . ?
O28_14 C18_14 C17_14 122.6(17) . . ?
C19_14 C18_14 C17_14 117.5(16) . . ?
C14_14 C19_14 C18_14 122.7(17) . . ?
C14_14 C19_14 P20_14 118.2(14) . . ?
C18_14 C19_14 P20_14 119.1(14) . . ?
O29_14 P20_14 C11_14 127.5(10) . . ?
O29_14 P20_14 C21_14 117.1(10) . . ?
C11_14 P20_14 C21_14 95.1(9)   . . ?
O29_14 P20_14 C19_14 120.6(9)  . . ?
C11_14 P20_14 C19_14 94.7(10)  . . ?
C21_14 P20_14 C19_14 94.2(8)   . . ?
C26_14 C21_14 C22_14 122.5(16) . . ?
C26_14 C21_14 P20_14 118.0(13) . . ?
C22_14 C21_14 P20_14 119.3(13) . . ?
C23_14 C22_14 O28_14 120.5(16) . . ?
C23_14 C22_14 C21_14 117.6(15) . . ?
O28_14 C22_14 C21_14 121.9(15) . . ?
C22_14 C23_14 C24_14 121.9(15) . . ?
C25_14 C24_14 C23_14 120.5(15) . . ?
C24_14 C25_14 C26_14 118.2(13) . . ?
C24_14 C25_14 C30_14 123.0(14) . . ?
C26_14 C25_14 C30_14 118.7(14) . . ?
C21_14 C26_14 O27_14 123.1(16) . . ?
C21_14 C26_14 C25_14 118.9(15) . . ?
O27_14 C26_14 C25_14 117.9(15) . . ?
C26_14 O27_14 C10_14 112.7(14) . . ?
C22_14 O28_14 C18_14 117.9(14) . . ?
C35_14 C30_14 C31_14 116.3(11) . . ?
C35_14 C30_14 C25_14 121.9(12) . . ?
C31_14 C30_14 C25_14 121.6(12) . . ?
C32_14 C31_14 C30_14 118.6(13) . . ?
C33_14 C32_14 C31_14 119.4(14) . . ?
N34_14 C33_14 C32_14 122.9(14) . . ?
C33_14 N34_14 C35_14 116.8(13) . . ?
C33_14 N34_14 Pd1_10 122.1(11) . . ?
C35_14 N34_14 Pd1_10 121.1(9)  . . ?
N34_14 C35_14 C30_14 125.4(12) . . ?
C41_14 C36_14 C37_14 115.7(11) . . ?
C41_14 C36_14 C17_14 121.4(14) . . ?
C37_14 C36_14 C17_14 122.8(13) . . ?
C38_14 C37_14 C36_14 119.1(14) . . ?
C39_14 C38_14 C37_14 120.7(15) . . ?
N40_14 C39_14 C38_14 120.9(15) . . ?
C41_14 N40_14 C39_14 118.8(14) . . ?
C41_14 N40_14 Pd5_10 116.9(11) . . ?
C39_14 N40_14 Pd5_10 124.3(11) . . ?
N40_14 C41_14 C36_14 124.7(14) . . ?
C2_15  N1_15  C6_15  116.9(11) . . ?
C2_15  N1_15  Pd5_10 124.9(9)  . . ?
C6_15  N1_15  Pd5_10 118.2(9)  . . ?
N1_15  C2_15  C3_15  123.9(13) . . ?
C2_15  C3_15  C4_15  118.5(13) . . ?
C3_15  C4_15  C5_15  119.0(12) . . ?
C6_15  C5_15  C4_15  117.4(10) . . ?
C6_15  C5_15  C7_15  122.3(11) . . ?
C4_15  C5_15  C7_15  120.3(11) . . ?
N1_15  C6_15  C5_15  124.0(11) . . ?
C8_15  C7_15  C12_15 118.1(12) . . ?
C8_15  C7_15  C5_15  122.1(14) . . ?
C12_15 C7_15  C5_15  119.8(13) . . ?
C7_15  C8_15  C9_15  121.0(15) . . ?
C10_15 C9_15  C8_15  119.4(14) . . ?
C9_15  C10_15 O27_15 121.7(14) . . ?
C9_15  C10_15 C11_15 120.7(14) . . ?
O27_15 C10_15 C11_15 117.5(13) . . ?
C12_15 C11_15 C10_15 118.8(15) . . ?
C12_15 C11_15 P20_15 121.1(12) . . ?
C10_15 C11_15 P20_15 119.9(12) . . ?
C7_15  C12_15 O13_15 120.6(14) . . ?
C7_15  C12_15 C11_15 121.2(14) . . ?
O13_15 C12_15 C11_15 117.9(15) . . ?
C14_15 O13_15 C12_15 115.2(11) . . ?
C15_15 C14_15 C19_15 122.4(15) . . ?
C15_15 C14_15 O13_15 116.9(14) . . ?
C19_15 C14_15 O13_15 120.3(14) . . ?
C14_15 C15_15 C16_15 116.9(14) . . ?
C17_15 C16_15 C15_15 125.1(15) . . ?
C16_15 C17_15 C18_15 115.0(13) . . ?
C16_15 C17_15 C36_15 124.4(13) . . ?
C18_15 C17_15 C36_15 120.6(12) . . ?
O28_15 C18_15 C19_15 117.2(14) . . ?
O28_15 C18_15 C17_15 120.9(15) . . ?
C19_15 C18_15 C17_15 121.5(14) . . ?
C14_15 C19_15 C18_15 118.6(15) . . ?
C14_15 C19_15 P20_15 121.5(13) . . ?
C18_15 C19_15 P20_15 119.6(12) . . ?
O29_15 P20_15 C19_15 121.6(9)  . . ?
O29_15 P20_15 C11_15 120.9(11) . . ?
C19_15 P20_15 C11_15 95.0(8)   . . ?
O29_15 P20_15 C21_15 119.8(10) . . ?
C19_15 P20_15 C21_15 97.7(9)   . . ?
C11_15 P20_15 C21_15 95.7(8)   . . ?
C22_15 C21_15 C26_15 120.0(14) . . ?
C22_15 C21_15 P20_15 117.7(12) . . ?
C26_15 C21_15 P20_15 122.0(13) . . ?
C23_15 C22_15 O28_15 123.0(16) . . ?
C23_15 C22_15 C21_15 117.3(15) . . ?
O28_15 C22_15 C21_15 119.7(14) . . ?
C22_15 C23_15 C24_15 122.4(17) . . ?
C25_15 C24_15 C23_15 119.4(15) . . ?
C24_15 C25_15 C26_15 116.1(12) . . ?
C24_15 C25_15 C30_15 121.1(13) . . ?
C26_15 C25_15 C30_15 122.8(13) . . ?
O27_15 C26_15 C25_15 121.5(13) . . ?
O27_15 C26_15 C21_15 116.7(14) . . ?
C25_15 C26_15 C21_15 121.8(14) . . ?
C26_15 O27_15 C10_15 114.8(13) . . ?
C22_15 O28_15 C18_15 119.9(13) . . ?
C35_15 C30_15 C31_15 118.2(11) . . ?
C35_15 C30_15 C25_15 121.4(11) . . ?
C31_15 C30_15 C25_15 120.4(12) . . ?
C32_15 C31_15 C30_15 119.4(13) . . ?
C31_15 C32_15 C33_15 117.8(14) . . ?
N34_15 C33_15 C32_15 123.3(15) . . ?
C35_15 N34_15 C33_15 118.4(13) . . ?
C35_15 N34_15 Pd1_10 118.8(9)  . . ?
C33_15 N34_15 Pd1_10 122.6(11) . . ?
N34_15 C35_15 C30_15 122.9(12) . . ?
C37_15 C36_15 C41_15 116.9(10) . . ?
C37_15 C36_15 C17_15 121.5(11) . . ?
C41_15 C36_15 C17_15 121.5(11) . . ?
C36_15 C37_15 C38_15 118.7(12) . . ?
C39_15 C38_15 C37_15 119.0(13) . . ?
N40_15 C39_15 C38_15 123.6(13) . . ?
C39_15 N40_15 C41_15 117.5(12) . . ?
C39_15 N40_15 Pd2_10 121.9(10) . . ?
C41_15 N40_15 Pd2_10 120.6(9)  . . ?
N40_15 C41_15 C36_15 124.1(12) . . ?
C6_16  N1_16  C2_16  118.7(13) . . ?
C6_16  N1_16  Pd5_10 121.1(10) . . ?
C2_16  N1_16  Pd5_10 120.0(10) . . ?
N1_16  C2_16  C3_16  122.0(14) . . ?
C2_16  C3_16  C4_16  118.0(13) . . ?
C5_16  C4_16  C3_16  121.5(13) . . ?
C4_16  C5_16  C6_16  115.4(10) . . ?
C4_16  C5_16  C7_16  123.6(12) . . ?
C6_16  C5_16  C7_16  121.0(12) . . ?
N1_16  C6_16  C5_16  124.0(11) . . ?
C8_16  C7_16  C12_16 116.4(12) . . ?
C8_16  C7_16  C5_16  122.1(13) . . ?
C12_16 C7_16  C5_16  121.3(13) . . ?
C7_16  C8_16  C9_16  124.2(14) . . ?
C10_16 C9_16  C8_16  117.3(15) . . ?
C11_16 C10_16 C9_16  120.3(15) . . ?
C11_16 C10_16 O27_16 121.3(14) . . ?
C9_16  C10_16 O27_16 118.4(16) . . ?
C10_16 C11_16 C12_16 122.8(14) . . ?
C10_16 C11_16 P20_16 119.1(12) . . ?
C12_16 C11_16 P20_16 117.8(13) . . ?
O13_16 C12_16 C7_16  122.0(13) . . ?
O13_16 C12_16 C11_16 119.2(14) . . ?
C7_16  C12_16 C11_16 118.7(14) . . ?
C14_16 O13_16 C12_16 115.1(13) . . ?
C15_16 C14_16 O13_16 116.6(14) . . ?
C15_16 C14_16 C19_16 122.0(14) . . ?
O13_16 C14_16 C19_16 121.0(14) . . ?
C14_16 C15_16 C16_16 117.3(15) . . ?
C17_16 C16_16 C15_16 123.0(15) . . ?
C16_16 C17_16 C18_16 116.3(12) . . ?
C16_16 C17_16 C36_16 120.8(13) . . ?
C18_16 C17_16 C36_16 122.9(13) . . ?
C19_16 C18_16 O28_16 121.0(16) . . ?
C19_16 C18_16 C17_16 121.7(15) . . ?
O28_16 C18_16 C17_16 117.3(15) . . ?
C18_16 C19_16 C14_16 119.0(15) . . ?
C18_16 C19_16 P20_16 122.1(13) . . ?
C14_16 C19_16 P20_16 118.8(13) . . ?
O29_16 P20_16 C19_16 123.8(10) . . ?
O29_16 P20_16 C21_16 118.2(10) . . ?
C19_16 P20_16 C21_16 94.5(9)   . . ?
O29_16 P20_16 C11_16 122.1(9)  . . ?
C19_16 P20_16 C11_16 95.6(8)   . . ?
C21_16 P20_16 C11_16 95.7(9)   . . ?
C22_16 C21_16 C26_16 122.1(17) . . ?
C22_16 C21_16 P20_16 119.8(14) . . ?
C26_16 C21_16 P20_16 117.8(13) . . ?
C23_16 C22_16 O28_16 120.4(15) . . ?
C23_16 C22_16 C21_16 119.4(15) . . ?
O28_16 C22_16 C21_16 120.2(15) . . ?
C22_16 C23_16 C24_16 119.5(14) . . ?
C25_16 C24_16 C23_16 122.0(15) . . ?
C24_16 C25_16 C26_16 119.2(13) . . ?
C24_16 C25_16 C30_16 119.2(13) . . ?
C26_16 C25_16 C30_16 121.6(12) . . ?
O27_16 C26_16 C25_16 122.8(15) . . ?
O27_16 C26_16 C21_16 120.2(15) . . ?
C25_16 C26_16 C21_16 116.9(14) . . ?
C26_16 O27_16 C10_16 115.3(13) . . ?
C18_16 O28_16 C22_16 114.4(13) . . ?
C31_16 C30_16 C35_16 115.9(11) . . ?
C31_16 C30_16 C25_16 123.8(11) . . ?
C35_16 C30_16 C25_16 120.0(11) . . ?
C30_16 C31_16 C32_16 121.0(13) . . ?
C33_16 C32_16 C31_16 117.9(14) . . ?
N34_16 C33_16 C32_16 121.8(14) . . ?
C35_16 N34_16 C33_16 119.6(13) . . ?
C35_16 N34_16 Pd2_10 119.6(10) . . ?
C33_16 N34_16 Pd2_10 120.3(10) . . ?
N34_16 C35_16 C30_16 123.3(12) . . ?
C37_16 C36_16 C41_16 116.7(10) . . ?
C37_16 C36_16 C17_16 120.3(11) . . ?
C41_16 C36_16 C17_16 123.0(12) . . ?
C36_16 C37_16 C38_16 120.4(12) . . ?
C39_16 C38_16 C37_16 118.3(13) . . ?
N40_16 C39_16 C38_16 122.6(14) . . ?
C39_16 N40_16 C41_16 118.0(12) . . ?
C39_16 N40_16 Pd3_10 121.0(10) . . ?
C41_16 N40_16 Pd3_10 121.0(9)  . . ?
N40_16 C41_16 C36_16 123.8(11) . . ?
C2_17  N1_17  C6_17  118.6(11) . . ?
C2_17  N1_17  Pd2_10 121.1(9)  . . ?
C6_17  N1_17  Pd2_10 120.3(9)  . . ?
N1_17  C2_17  C3_17  120.5(14) . . ?
C4_17  C3_17  C2_17  118.8(14) . . ?
C3_17  C4_17  C5_17  119.9(13) . . ?
C6_17  C5_17  C4_17  115.5(10) . . ?
C6_17  C5_17  C7_17  120.5(12) . . ?
C4_17  C5_17  C7_17  123.8(12) . . ?
N1_17  C6_17  C5_17  124.8(12) . . ?
C8_17  C7_17  C12_17 117.1(13) . . ?
C8_17  C7_17  C5_17  123.4(14) . . ?
C12_17 C7_17  C5_17  119.4(13) . . ?
C7_17  C8_17  C9_17  126.0(15) . . ?
C10_17 C9_17  C8_17  117.5(14) . . ?
O27_17 C10_17 C9_17  119.8(14) . . ?
O27_17 C10_17 C11_17 121.4(13) . . ?
C9_17  C10_17 C11_17 118.6(14) . . ?
C12_17 C11_17 C10_17 121.3(14) . . ?
C12_17 C11_17 P20_17 119.6(11) . . ?
C10_17 C11_17 P20_17 118.8(12) . . ?
C7_17  C12_17 O13_17 122.6(14) . . ?
C7_17  C12_17 C11_17 118.8(13) . . ?
O13_17 C12_17 C11_17 118.3(13) . . ?
C14_17 O13_17 C12_17 114.4(11) . . ?
C19_17 C14_17 C15_17 120.1(14) . . ?
C19_17 C14_17 O13_17 123.0(14) . . ?
C15_17 C14_17 O13_17 116.9(15) . . ?
C14_17 C15_17 C16_17 119.5(15) . . ?
C17_17 C16_17 C15_17 121.6(14) . . ?
C16_17 C17_17 C18_17 117.6(12) . . ?
C16_17 C17_17 C36_17 122.5(13) . . ?
C18_17 C17_17 C36_17 119.8(13) . . ?
O28_17 C18_17 C17_17 122.8(13) . . ?
O28_17 C18_17 C19_17 117.8(13) . . ?
C17_17 C18_17 C19_17 119.4(14) . . ?
C14_17 C19_17 C18_17 121.1(14) . . ?
C14_17 C19_17 P20_17 119.5(11) . . ?
C18_17 C19_17 P20_17 118.8(12) . . ?
O29_17 P20_17 C19_17 118.4(8)  . . ?
O29_17 P20_17 C21_17 122.0(10) . . ?
C19_17 P20_17 C21_17 95.5(7)   . . ?
O29_17 P20_17 C11_17 121.9(10) . . ?
C19_17 P20_17 C11_17 96.5(8)   . . ?
C21_17 P20_17 C11_17 96.3(8)   . . ?
C26_17 C21_17 C22_17 119.5(15) . . ?
C26_17 C21_17 P20_17 120.1(12) . . ?
C22_17 C21_17 P20_17 120.2(12) . . ?
C23_17 C22_17 O28_17 123.3(14) . . ?
C23_17 C22_17 C21_17 119.5(14) . . ?
O28_17 C22_17 C21_17 117.0(13) . . ?
C22_17 C23_17 C24_17 119.3(14) . . ?
C25_17 C24_17 C23_17 123.8(14) . . ?
C24_17 C25_17 C26_17 116.8(12) . . ?
C24_17 C25_17 C30_17 121.0(13) . . ?
C26_17 C25_17 C30_17 122.1(13) . . ?
O27_17 C26_17 C25_17 118.8(14) . . ?
O27_17 C26_17 C21_17 120.9(14) . . ?
C25_17 C26_17 C21_17 120.3(14) . . ?
C10_17 O27_17 C26_17 115.3(12) . . ?
C22_17 O28_17 C18_17 115.2(13) . . ?
C35_17 C30_17 C31_17 117.9(10) . . ?
C35_17 C30_17 C25_17 120.1(12) . . ?
C31_17 C30_17 C25_17 122.0(12) . . ?
C32_17 C31_17 C30_17 118.4(13) . . ?
C33_17 C32_17 C31_17 118.4(13) . . ?
N34_17 C33_17 C32_17 124.1(13) . . ?
C33_17 N34_17 C35_17 117.1(12) . . ?
C33_17 N34_17 Pd4_10 122.7(10) . . ?
C35_17 N34_17 Pd4_10 120.2(9)  . . ?
N34_17 C35_17 C30_17 123.8(12) . . ?
C37_17 C36_17 C41_17 117.1(10) . . ?
C37_17 C36_17 C17_17 123.0(11) . . ?
C41_17 C36_17 C17_17 119.9(11) . . ?
C38_17 C37_17 C36_17 119.6(13) . . ?
C37_17 C38_17 C39_17 119.4(13) . . ?
N40_17 C39_17 C38_17 121.5(13) . . ?
C39_17 N40_17 C41_17 118.9(13) . . ?
C39_17 N40_17 Pd3_10 120.1(9)  . . ?
C41_17 N40_17 Pd3_10 120.6(10) . . ?
N40_17 C41_17 C36_17 123.3(12) . . ?
C6_18  N1_18  C2_18  118.8(13) . . ?
C6_18  N1_18  Pd2_10 118.7(10) . . ?
C2_18  N1_18  Pd2_10 121.1(10) . . ?
N1_18  C2_18  C3_18  123.0(14) . . ?
C2_18  C3_18  C4_18  117.5(14) . . ?
C3_18  C4_18  C5_18  119.7(13) . . ?
C4_18  C5_18  C6_18  117.2(11) . . ?
C4_18  C5_18  C7_18  122.6(11) . . ?
C6_18  C5_18  C7_18  120.2(11) . . ?
N1_18  C6_18  C5_18  122.8(13) . . ?
C8_18  C7_18  C12_18 115.5(13) . . ?
C8_18  C7_18  C5_18  122.0(13) . . ?
C12_18 C7_18  C5_18  122.5(12) . . ?
C7_18  C8_18  C9_18  121.7(15) . . ?
C10_18 C9_18  C8_18  122.2(14) . . ?
C9_18  C10_18 O27_18 120.9(15) . . ?
C9_18  C10_18 C11_18 118.0(15) . . ?
O27_18 C10_18 C11_18 121.1(15) . . ?
C10_18 C11_18 C12_18 121.2(16) . . ?
C10_18 C11_18 P20_18 118.8(14) . . ?
C12_18 C11_18 P20_18 119.7(13) . . ?
O13_18 C12_18 C11_18 120.8(15) . . ?
O13_18 C12_18 C7_18  118.6(15) . . ?
C11_18 C12_18 C7_18  120.3(14) . . ?
C12_18 O13_18 C14_18 118.3(13) . . ?
C15_18 C14_18 C19_18 118.0(15) . . ?
C15_18 C14_18 O13_18 119.1(17) . . ?
C19_18 C14_18 O13_18 122.8(15) . . ?
C14_18 C15_18 C16_18 121.6(17) . . ?
C17_18 C16_18 C15_18 119.6(17) . . ?
C18_18 C17_18 C16_18 116.6(13) . . ?
C18_18 C17_18 C36_18 121.0(13) . . ?
C16_18 C17_18 C36_18 122.3(14) . . ?
C17_18 C18_18 C19_18 121.4(15) . . ?
C17_18 C18_18 O28_18 120.6(14) . . ?
C19_18 C18_18 O28_18 117.7(15) . . ?
C14_18 C19_18 C18_18 121.7(16) . . ?
C14_18 C19_18 P20_18 117.6(13) . . ?
C18_18 C19_18 P20_18 120.3(14) . . ?
O29_18 P20_18 C11_18 121.7(9)  . . ?
O29_18 P20_18 C21_18 120.8(9)  . . ?
C11_18 P20_18 C21_18 95.6(8)   . . ?
O29_18 P20_18 C19_18 119.7(9)  . . ?
C11_18 P20_18 C19_18 96.7(9)   . . ?
C21_18 P20_18 C19_18 96.2(8)   . . ?
C26_18 C21_18 C22_18 119.8(15) . . ?
C26_18 C21_18 P20_18 120.5(13) . . ?
C22_18 C21_18 P20_18 119.5(11) . . ?
C23_18 C22_18 O28_18 121.1(15) . . ?
C23_18 C22_18 C21_18 120.3(14) . . ?
O28_18 C22_18 C21_18 118.5(14) . . ?
C22_18 C23_18 C24_18 118.4(16) . . ?
C25_18 C24_18 C23_18 121.5(16) . . ?
C24_18 C25_18 C26_18 117.5(12) . . ?
C24_18 C25_18 C30_18 121.6(14) . . ?
C26_18 C25_18 C30_18 120.9(13) . . ?
C21_18 C26_18 O27_18 118.8(15) . . ?
C21_18 C26_18 C25_18 121.3(14) . . ?
O27_18 C26_18 C25_18 119.6(14) . . ?
C10_18 O27_18 C26_18 116.0(14) . . ?
C22_18 O28_18 C18_18 117.3(13) . . ?
C31_18 C30_18 C35_18 116.4(10) . . ?
C31_18 C30_18 C25_18 121.9(12) . . ?
C35_18 C30_18 C25_18 121.5(12) . . ?
C30_18 C31_18 C32_18 120.5(12) . . ?
C33_18 C32_18 C31_18 118.8(13) . . ?
N34_18 C33_18 C32_18 121.5(13) . . ?
C35_18 N34_18 C33_18 119.5(13) . . ?
C35_18 N34_18 Pd1_10 118.9(10) . . ?
C33_18 N34_18 Pd1_10 121.3(10) . . ?
N34_18 C35_18 C30_18 123.0(12) . . ?
C41_18 C36_18 C37_18 116.8(11) . . ?
C41_18 C36_18 C17_18 121.0(12) . . ?
C37_18 C36_18 C17_18 122.1(12) . . ?
C38_18 C37_18 C36_18 119.6(13) . . ?
C39_18 C38_18 C37_18 118.3(14) . . ?
N40_18 C39_18 C38_18 123.7(14) . . ?
C39_18 N40_18 C41_18 117.9(13) . . ?
C39_18 N40_18 Pd4_10 123.1(10) . . ?
C41_18 N40_18 Pd4_10 118.3(10) . . ?
N40_18 C41_18 C36_18 123.4(13) . . ?
F3_19  B1_19  F4_19  113(2)    . . ?
F3_19  B1_19  F2_19  109(2)    . . ?
F4_19  B1_19  F2_19  115(2)    . . ?
F3_19  B1_19  F5_19  108(2)    . . ?
F4_19  B1_19  F5_19  109(2)    . . ?
F2_19  B1_19  F5_19  102(2)    . . ?
F2_20  B1_20  F3_20  116(2)    . . ?
F2_20  B1_20  F4_20  101(2)    . . ?
F3_20  B1_20  F4_20  113(2)    . . ?
F2_20  B1_20  F5_20  106(2)    . . ?
F3_20  B1_20  F5_20  111(2)    . . ?
F4_20  B1_20  F5_20  109(2)    . . ?
F3_21  B1_21  F5_21  117(2)    . . ?
F3_21  B1_21  F2_21  107(2)    . . ?
F5_21  B1_21  F2_21  110(2)    . . ?
F3_21  B1_21  F4_21  104.6(19) . . ?
F5_21  B1_21  F4_21  109.3(19) . . ?
F2_21  B1_21  F4_21  109(2)    . . ?
N1_22  C2_22  C3_22  174(3)    . . ?
N1_23  C2_23  C3_23  178(3)    . . ?
N1_24  C2_24  C3_24  171(3)    . . ?
N1_25  C2_25  C3_25  177(2)    . . ?
N1_26  C2_26  C3_26  169(4)    . . ?
N1_27  C2_27  C3_27  172(3)    . . ?
N1_28  C2_28  C3_28  156(3)    . . ?
N1_29  C2_29  C3_29  168(3)    . . ?
N1_31  C2_31  C3_31  176(3)    . . ?
N1_32  C2_32  C3_32  168(3)    . . ?
N1_33  C2_33  C3_33  178(3)    . . ?
F4_34  B1_34  F2_34  112(2)    . . ?
F4_34  B1_34  F5_34  104(2)    . . ?
F2_34  B1_34  F5_34  116(3)    . . ?
F4_34  B1_34  F3_34  106(2)    . . ?
F2_34  B1_34  F3_34  113(2)    . . ?
F5_34  B1_34  F3_34  106(3)    . . ?
N1_35  C2_35  C3_35  168(3)    . . ?
F5_36  B1_36  F4_36  112(2)    . . ?
F5_36  B1_36  F2_36  111(3)    . . ?
F4_36  B1_36  F2_36  104(2)    . . ?
F5_36  B1_36  F3_36  112(2)    . . ?
F4_36  B1_36  F3_36  116(2)    . . ?
F2_36  B1_36  F3_36  102(2)    . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C6_2   N1_2   C2_2   C3_2   -7(4)      . . . . ?
Pd1_1  N1_2   C2_2   C3_2   164(2)     . . . . ?
N1_2   C2_2   C3_2   C4_2   14(5)      . . . . ?
C2_2   C3_2   C4_2   C5_2   -12(5)     . . . . ?
C3_2   C4_2   C5_2   C6_2   5(3)       . . . . ?
C3_2   C4_2   C5_2   C7_2   -175(3)    . . . . ?
C2_2   N1_2   C6_2   C5_2   -2(2)      . . . . ?
Pd1_1  N1_2   C6_2   C5_2   -173.4(12) . . . . ?
C4_2   C5_2   C6_2   N1_2   3(2)       . . . . ?
C7_2   C5_2   C6_2   N1_2   -177.7(17) . . . . ?
C6_2   C5_2   C7_2   C8_2   -136.5(18) . . . . ?
C4_2   C5_2   C7_2   C8_2   43(2)      . . . . ?
C6_2   C5_2   C7_2   C12_2  43(2)      . . . . ?
C4_2   C5_2   C7_2   C12_2  -137(2)    . . . . ?
C12_2  C7_2   C8_2   C9_2   -1(2)      . . . . ?
C5_2   C7_2   C8_2   C9_2   178.2(16)  . . . . ?
C7_2   C8_2   C9_2   C10_2  -3(2)      . . . . ?
C8_2   C9_2   C10_2  O27_2  175.8(15)  . . . . ?
C8_2   C9_2   C10_2  C11_2  3(2)       . . . . ?
C9_2   C10_2  C11_2  C12_2  2(2)       . . . . ?
O27_2  C10_2  C11_2  C12_2  -171.2(15) . . . . ?
C9_2   C10_2  C11_2  P20_2  174.3(14)  . . . . ?
O27_2  C10_2  C11_2  P20_2  2(2)       . . . . ?
C8_2   C7_2   C12_2  O13_2  -166.5(17) . . . . ?
C5_2   C7_2   C12_2  O13_2  14(2)      . . . . ?
C8_2   C7_2   C12_2  C11_2  6(2)       . . . . ?
C5_2   C7_2   C12_2  C11_2  -173.0(16) . . . . ?
C10_2  C11_2  C12_2  C7_2   -7(2)      . . . . ?
P20_2  C11_2  C12_2  C7_2   -179.5(15) . . . . ?
C10_2  C11_2  C12_2  O13_2  166.5(16)  . . . . ?
P20_2  C11_2  C12_2  O13_2  -6(2)      . . . . ?
C7_2   C12_2  O13_2  C14_2  131.5(17)  . . . . ?
C11_2  C12_2  O13_2  C14_2  -42(2)     . . . . ?
C12_2  O13_2  C14_2  C15_2  -134(2)    . . . . ?
C12_2  O13_2  C14_2  C19_2  43(2)      . . . . ?
C19_2  C14_2  C15_2  C16_2  -3(3)      . . . . ?
O13_2  C14_2  C15_2  C16_2  174(2)     . . . . ?
C14_2  C15_2  C16_2  C17_2  1(4)       . . . . ?
C15_2  C16_2  C17_2  C18_2  -1(3)      . . . . ?
C15_2  C16_2  C17_2  C36_2  178(2)     . . . . ?
C16_2  C17_2  C18_2  C19_2  2(3)       . . . . ?
C36_2  C17_2  C18_2  C19_2  -176.6(17) . . . . ?
C16_2  C17_2  C18_2  O28_2  -174(2)    . . . . ?
C36_2  C17_2  C18_2  O28_2  7(2)       . . . . ?
O28_2  C18_2  C19_2  C14_2  172.2(19)  . . . . ?
C17_2  C18_2  C19_2  C14_2  -4(2)      . . . . ?
O28_2  C18_2  C19_2  P20_2  -5(2)      . . . . ?
C17_2  C18_2  C19_2  P20_2  179.2(16)  . . . . ?
C15_2  C14_2  C19_2  C18_2  4(2)       . . . . ?
O13_2  C14_2  C19_2  C18_2  -172.9(17) . . . . ?
C15_2  C14_2  C19_2  P20_2  -178.8(16) . . . . ?
O13_2  C14_2  C19_2  P20_2  4(2)       . . . . ?
C10_2  C11_2  P20_2  O29_2  97.3(17)   . . . . ?
C12_2  C11_2  P20_2  O29_2  -90.5(17)  . . . . ?
C10_2  C11_2  P20_2  C19_2  -131.6(15) . . . . ?
C12_2  C11_2  P20_2  C19_2  40.7(15)   . . . . ?
C10_2  C11_2  P20_2  C21_2  -35.7(15)  . . . . ?
C12_2  C11_2  P20_2  C21_2  136.5(14)  . . . . ?
C18_2  C19_2  P20_2  O29_2  -93.1(18)  . . . . ?
C14_2  C19_2  P20_2  O29_2  90.2(17)   . . . . ?
C18_2  C19_2  P20_2  C11_2  136.7(14)  . . . . ?
C14_2  C19_2  P20_2  C11_2  -40.1(15)  . . . . ?
C18_2  C19_2  P20_2  C21_2  39.6(15)   . . . . ?
C14_2  C19_2  P20_2  C21_2  -137.2(14) . . . . ?
O29_2  P20_2  C21_2  C22_2  92.1(17)   . . . . ?
C11_2  P20_2  C21_2  C22_2  -136.1(14) . . . . ?
C19_2  P20_2  C21_2  C22_2  -40.3(14)  . . . . ?
O29_2  P20_2  C21_2  C26_2  -94.3(16)  . . . . ?
C11_2  P20_2  C21_2  C26_2  37.5(13)   . . . . ?
C19_2  P20_2  C21_2  C26_2  133.2(12)  . . . . ?
C26_2  C21_2  C22_2  C23_2  6(2)       . . . . ?
P20_2  C21_2  C22_2  C23_2  179.1(16)  . . . . ?
C26_2  C21_2  C22_2  O28_2  -168.8(16) . . . . ?
P20_2  C21_2  C22_2  O28_2  5(2)       . . . . ?
C21_2  C22_2  C23_2  C24_2  -1(3)      . . . . ?
O28_2  C22_2  C23_2  C24_2  173(2)     . . . . ?
C22_2  C23_2  C24_2  C25_2  3(3)       . . . . ?
C23_2  C24_2  C25_2  C26_2  -8(3)      . . . . ?
C23_2  C24_2  C25_2  C30_2  173.8(19)  . . . . ?
C24_2  C25_2  C26_2  O27_2  -165.6(17) . . . . ?
C30_2  C25_2  C26_2  O27_2  12(2)      . . . . ?
C24_2  C25_2  C26_2  C21_2  12(2)      . . . . ?
C30_2  C25_2  C26_2  C21_2  -169.6(14) . . . . ?
C22_2  C21_2  C26_2  O27_2  166.7(16)  . . . . ?
P20_2  C21_2  C26_2  O27_2  -6.8(19)   . . . . ?
C22_2  C21_2  C26_2  C25_2  -11(2)     . . . . ?
P20_2  C21_2  C26_2  C25_2  175.1(12)  . . . . ?
C25_2  C26_2  O27_2  C10_2  139.4(17)  . . . . ?
C21_2  C26_2  O27_2  C10_2  -39(2)     . . . . ?
C9_2   C10_2  O27_2  C26_2  -131.5(18) . . . . ?
C11_2  C10_2  O27_2  C26_2  42(2)      . . . . ?
C23_2  C22_2  O28_2  C18_2  -132(2)    . . . . ?
C21_2  C22_2  O28_2  C18_2  43(2)      . . . . ?
C19_2  C18_2  O28_2  C22_2  -43(2)     . . . . ?
C17_2  C18_2  O28_2  C22_2  133.1(18)  . . . . ?
C24_2  C25_2  C30_2  C31_2  49(2)      . . . . ?
C26_2  C25_2  C30_2  C31_2  -128.7(18) . . . . ?
C24_2  C25_2  C30_2  C35_2  -131.9(18) . . . . ?
C26_2  C25_2  C30_2  C35_2  50(2)      . . . . ?
C35_2  C30_2  C31_2  C32_2  5(2)       . . . . ?
C25_2  C30_2  C31_2  C32_2  -176.4(16) . . . . ?
C30_2  C31_2  C32_2  C33_2  -3(2)      . . . . ?
C31_2  C32_2  C33_2  N34_2  1(2)       . . . . ?
C32_2  C33_2  N34_2  C35_2  -1(3)      . . . . ?
C32_2  C33_2  N34_2  Pd3_1  -177.5(14) . . . . ?
C33_2  N34_2  C35_2  C30_2  4(3)       . . . . ?
Pd3_1  N34_2  C35_2  C30_2  179.8(12)  . . . . ?
C31_2  C30_2  C35_2  N34_2  -5(2)      . . . . ?
C25_2  C30_2  C35_2  N34_2  175.9(15)  . . . . ?
C16_2  C17_2  C36_2  C41_2  -128(2)    . . . . ?
C18_2  C17_2  C36_2  C41_2  51(2)      . . . . ?
C16_2  C17_2  C36_2  C37_2  51(3)      . . . . ?
C18_2  C17_2  C36_2  C37_2  -130(2)    . . . . ?
C41_2  C36_2  C37_2  C38_2  2(3)       . . . . ?
C17_2  C36_2  C37_2  C38_2  -177.8(18) . . . . ?
C36_2  C37_2  C38_2  C39_2  0(2)       . . . . ?
C37_2  C38_2  C39_2  N40_2  1(2)       . . . . ?
C38_2  C39_2  N40_2  C41_2  -4(3)      . . . . ?
C38_2  C39_2  N40_2  Pd4_1  -176.2(16) . . . . ?
C39_2  N40_2  C41_2  C36_2  6(3)       . . . . ?
Pd4_1  N40_2  C41_2  C36_2  178.5(14)  . . . . ?
C37_2  C36_2  C41_2  N40_2  -5(3)      . . . . ?
C17_2  C36_2  C41_2  N40_2  174.2(18)  . . . . ?
C6_3   N1_3   C2_3   C3_3   -1(3)      . . . . ?
Pd1_1  N1_3   C2_3   C3_3   -179(2)    . . . . ?
N1_3   C2_3   C3_3   C4_3   -5(4)      . . . . ?
C2_3   C3_3   C4_3   C5_3   10(4)      . . . . ?
C3_3   C4_3   C5_3   C6_3   -8(3)      . . . . ?
C3_3   C4_3   C5_3   C7_3   173(2)     . . . . ?
C2_3   N1_3   C6_3   C5_3   3(2)       . . . . ?
Pd1_1  N1_3   C6_3   C5_3   -179.4(12) . . . . ?
C4_3   C5_3   C6_3   N1_3   1(2)       . . . . ?
C7_3   C5_3   C6_3   N1_3   -179.8(16) . . . . ?
C4_3   C5_3   C7_3   C8_3   49(2)      . . . . ?
C6_3   C5_3   C7_3   C8_3   -130.3(19) . . . . ?
C4_3   C5_3   C7_3   C12_3  -132.8(19) . . . . ?
C6_3   C5_3   C7_3   C12_3  48(2)      . . . . ?
C12_3  C7_3   C8_3   C9_3   3(3)       . . . . ?
C5_3   C7_3   C8_3   C9_3   -178(2)    . . . . ?
C7_3   C8_3   C9_3   C10_3  -9(4)      . . . . ?
C8_3   C9_3   C10_3  O27_3  179(2)     . . . . ?
C8_3   C9_3   C10_3  C11_3  6(3)       . . . . ?
C9_3   C10_3  C11_3  C12_3  1(2)       . . . . ?
O27_3  C10_3  C11_3  C12_3  -171.8(16) . . . . ?
C9_3   C10_3  C11_3  P20_3  173.0(17)  . . . . ?
O27_3  C10_3  C11_3  P20_3  0(2)       . . . . ?
C8_3   C7_3   C12_3  O13_3  -170.2(18) . . . . ?
C5_3   C7_3   C12_3  O13_3  11(2)      . . . . ?
C8_3   C7_3   C12_3  C11_3  4(2)       . . . . ?
C5_3   C7_3   C12_3  C11_3  -174.2(14) . . . . ?
C10_3  C11_3  C12_3  O13_3  167.9(16)  . . . . ?
P20_3  C11_3  C12_3  O13_3  -4.3(19)   . . . . ?
C10_3  C11_3  C12_3  C7_3   -7(2)      . . . . ?
P20_3  C11_3  C12_3  C7_3   -178.9(13) . . . . ?
C7_3   C12_3  O13_3  C14_3  125.6(16)  . . . . ?
C11_3  C12_3  O13_3  C14_3  -49(2)     . . . . ?
C12_3  O13_3  C14_3  C15_3  -130.3(18) . . . . ?
C12_3  O13_3  C14_3  C19_3  52.7(19)   . . . . ?
C19_3  C14_3  C15_3  C16_3  -1(3)      . . . . ?
O13_3  C14_3  C15_3  C16_3  -177.9(18) . . . . ?
C14_3  C15_3  C16_3  C17_3  0(3)       . . . . ?
C15_3  C16_3  C17_3  C18_3  -1(3)      . . . . ?
C15_3  C16_3  C17_3  C36_3  179.0(19)  . . . . ?
C16_3  C17_3  C18_3  O28_3  -169.5(18) . . . . ?
C36_3  C17_3  C18_3  O28_3  10(2)      . . . . ?
C16_3  C17_3  C18_3  C19_3  4(2)       . . . . ?
C36_3  C17_3  C18_3  C19_3  -176.2(15) . . . . ?
C15_3  C14_3  C19_3  C18_3  4(2)       . . . . ?
O13_3  C14_3  C19_3  C18_3  -179.3(13) . . . . ?
C15_3  C14_3  C19_3  P20_3  178.9(15)  . . . . ?
O13_3  C14_3  C19_3  P20_3  -4.1(18)   . . . . ?
C17_3  C18_3  C19_3  C14_3  -5(2)      . . . . ?
O28_3  C18_3  C19_3  C14_3  168.3(15)  . . . . ?
C17_3  C18_3  C19_3  P20_3  179.3(13)  . . . . ?
O28_3  C18_3  C19_3  P20_3  -7.1(19)   . . . . ?
C14_3  C19_3  P20_3  O29_3  95.3(15)   . . . . ?
C18_3  C19_3  P20_3  O29_3  -89.6(14)  . . . . ?
C14_3  C19_3  P20_3  C11_3  -36.8(14)  . . . . ?
C18_3  C19_3  P20_3  C11_3  138.3(13)  . . . . ?
C14_3  C19_3  P20_3  C21_3  -132.5(13) . . . . ?
C18_3  C19_3  P20_3  C21_3  42.5(13)   . . . . ?
C10_3  C11_3  P20_3  O29_3  95.9(15)   . . . . ?
C12_3  C11_3  P20_3  O29_3  -92.1(14)  . . . . ?
C10_3  C11_3  P20_3  C19_3  -132.5(14) . . . . ?
C12_3  C11_3  P20_3  C19_3  39.6(13)   . . . . ?
C10_3  C11_3  P20_3  C21_3  -35.8(14)  . . . . ?
C12_3  C11_3  P20_3  C21_3  136.2(13)  . . . . ?
O29_3  P20_3  C21_3  C22_3  93.3(15)   . . . . ?
C19_3  P20_3  C21_3  C22_3  -39.5(13)  . . . . ?
C11_3  P20_3  C21_3  C22_3  -133.8(13) . . . . ?
O29_3  P20_3  C21_3  C26_3  -94.5(16)  . . . . ?
C19_3  P20_3  C21_3  C26_3  132.7(13)  . . . . ?
C11_3  P20_3  C21_3  C26_3  38.3(14)   . . . . ?
C26_3  C21_3  C22_3  C23_3  7(2)       . . . . ?
P20_3  C21_3  C22_3  C23_3  178.6(14)  . . . . ?
C26_3  C21_3  C22_3  O28_3  -172.3(15) . . . . ?
P20_3  C21_3  C22_3  O28_3  -0.2(19)   . . . . ?
C21_3  C22_3  C23_3  C24_3  0(2)       . . . . ?
O28_3  C22_3  C23_3  C24_3  178.8(17)  . . . . ?
C22_3  C23_3  C24_3  C25_3  -2(3)      . . . . ?
C23_3  C24_3  C25_3  C26_3  -2(2)      . . . . ?
C23_3  C24_3  C25_3  C30_3  178.7(17)  . . . . ?
C24_3  C25_3  C26_3  C21_3  8(2)       . . . . ?
C30_3  C25_3  C26_3  C21_3  -172.2(14) . . . . ?
C24_3  C25_3  C26_3  O27_3  -168.6(16) . . . . ?
C30_3  C25_3  C26_3  O27_3  11(2)      . . . . ?
C22_3  C21_3  C26_3  C25_3  -11(2)     . . . . ?
P20_3  C21_3  C26_3  C25_3  177.0(13)  . . . . ?
C22_3  C21_3  C26_3  O27_3  165.8(16)  . . . . ?
P20_3  C21_3  C26_3  O27_3  -6(2)      . . . . ?
C9_3   C10_3  O27_3  C26_3  -129(2)    . . . . ?
C11_3  C10_3  O27_3  C26_3  44(2)      . . . . ?
C25_3  C26_3  O27_3  C10_3  135.4(18)  . . . . ?
C21_3  C26_3  O27_3  C10_3  -41(2)     . . . . ?
C23_3  C22_3  O28_3  C18_3  -131.5(17) . . . . ?
C21_3  C22_3  O28_3  C18_3  47(2)      . . . . ?
C17_3  C18_3  O28_3  C22_3  131.1(17)  . . . . ?
C19_3  C18_3  O28_3  C22_3  -43(2)     . . . . ?
C24_3  C25_3  C30_3  C31_3  47(2)      . . . . ?
C26_3  C25_3  C30_3  C31_3  -133(2)    . . . . ?
C24_3  C25_3  C30_3  C35_3  -137.3(18) . . . . ?
C26_3  C25_3  C30_3  C35_3  43(2)      . . . . ?
C35_3  C30_3  C31_3  C32_3  4(3)       . . . . ?
C25_3  C30_3  C31_3  C32_3  -179.6(18) . . . . ?
C30_3  C31_3  C32_3  C33_3  -2(2)      . . . . ?
C31_3  C32_3  C33_3  N34_3  0(2)       . . . . ?
C32_3  C33_3  N34_3  C35_3  1(3)       . . . . ?
C32_3  C33_3  N34_3  Pd4_1  173.3(17)  . . . . ?
C33_3  N34_3  C35_3  C30_3  1(3)       . . . . ?
Pd4_1  N34_3  C35_3  C30_3  -171.6(14) . . . . ?
C31_3  C30_3  C35_3  N34_3  -4(3)      . . . . ?
C25_3  C30_3  C35_3  N34_3  -180.0(18) . . . . ?
C18_3  C17_3  C36_3  C37_3  -131.8(18) . . . . ?
C16_3  C17_3  C36_3  C37_3  48(2)      . . . . ?
C18_3  C17_3  C36_3  C41_3  47(2)      . . . . ?
C16_3  C17_3  C36_3  C41_3  -134(2)    . . . . ?
C41_3  C36_3  C37_3  C38_3  4(2)       . . . . ?
C17_3  C36_3  C37_3  C38_3  -177.5(17) . . . . ?
C36_3  C37_3  C38_3  C39_3  -2(2)      . . . . ?
C37_3  C38_3  C39_3  N40_3  -5(2)      . . . . ?
C38_3  C39_3  N40_3  C41_3  10(3)      . . . . ?
C38_3  C39_3  N40_3  Pd5_1  -179.1(14) . . . . ?
C39_3  N40_3  C41_3  C36_3  -7(3)      . . . . ?
Pd5_1  N40_3  C41_3  C36_3  -178.9(14) . . . . ?
C37_3  C36_3  C41_3  N40_3  0(3)       . . . . ?
C17_3  C36_3  C41_3  N40_3  -178.1(18) . . . . ?
C6_4   N1_4   C2_4   C3_4   5(4)       . . . . ?
Pd1_1  N1_4   C2_4   C3_4   -167(3)    . . . . ?
N1_4   C2_4   C3_4   C4_4   -4(5)      . . . . ?
C2_4   C3_4   C4_4   C5_4   0(5)       . . . . ?
C3_4   C4_4   C5_4   C6_4   3(4)       . . . . ?
C3_4   C4_4   C5_4   C7_4   179(3)     . . . . ?
C2_4   N1_4   C6_4   C5_4   -1(2)      . . . . ?
Pd1_1  N1_4   C6_4   C5_4   170.6(15)  . . . . ?
C4_4   C5_4   C6_4   N1_4   -2(2)      . . . . ?
C7_4   C5_4   C6_4   N1_4   -178.8(19) . . . . ?
C6_4   C5_4   C7_4   C8_4   -116.8(19) . . . . ?
C4_4   C5_4   C7_4   C8_4   67(3)      . . . . ?
C6_4   C5_4   C7_4   C12_4  67.9(19)   . . . . ?
C4_4   C5_4   C7_4   C12_4  -108(2)    . . . . ?
C12_4  C7_4   C8_4   C9_4   6(3)       . . . . ?
C5_4   C7_4   C8_4   C9_4   -168.9(19) . . . . ?
C7_4   C8_4   C9_4   C10_4  -12(3)     . . . . ?
C8_4   C9_4   C10_4  O27_4  -174(2)    . . . . ?
C8_4   C9_4   C10_4  C11_4  8(3)       . . . . ?
C9_4   C10_4  C11_4  C12_4  0(2)       . . . . ?
O27_4  C10_4  C11_4  C12_4  -177.5(16) . . . . ?
C9_4   C10_4  C11_4  P20_4  176.3(17)  . . . . ?
O27_4  C10_4  C11_4  P20_4  -2(2)      . . . . ?
C10_4  C11_4  C12_4  O13_4  168.8(16)  . . . . ?
P20_4  C11_4  C12_4  O13_4  -7(2)      . . . . ?
C10_4  C11_4  C12_4  C7_4   -6(2)      . . . . ?
P20_4  C11_4  C12_4  C7_4   177.7(13)  . . . . ?
C8_4   C7_4   C12_4  O13_4  -172.1(17) . . . . ?
C5_4   C7_4   C12_4  O13_4  4(2)       . . . . ?
C8_4   C7_4   C12_4  C11_4  3(2)       . . . . ?
C5_4   C7_4   C12_4  C11_4  178.7(15)  . . . . ?
C11_4  C12_4  O13_4  C14_4  -44(2)     . . . . ?
C7_4   C12_4  O13_4  C14_4  131.0(17)  . . . . ?
C12_4  O13_4  C14_4  C15_4  -134(2)    . . . . ?
C12_4  O13_4  C14_4  C19_4  46(2)      . . . . ?
O13_4  C14_4  C15_4  C16_4  180(2)     . . . . ?
C19_4  C14_4  C15_4  C16_4  1(3)       . . . . ?
C14_4  C15_4  C16_4  C17_4  -4(4)      . . . . ?
C15_4  C16_4  C17_4  C18_4  1(3)       . . . . ?
C15_4  C16_4  C17_4  C36_4  -179(2)    . . . . ?
C16_4  C17_4  C18_4  O28_4  -171.6(19) . . . . ?
C36_4  C17_4  C18_4  O28_4  8(2)       . . . . ?
C16_4  C17_4  C18_4  C19_4  6(2)       . . . . ?
C36_4  C17_4  C18_4  C19_4  -174.4(16) . . . . ?
C17_4  C18_4  C19_4  C14_4  -9(2)      . . . . ?
O28_4  C18_4  C19_4  C14_4  168.3(17)  . . . . ?
C17_4  C18_4  C19_4  P20_4  174.5(15)  . . . . ?
O28_4  C18_4  C19_4  P20_4  -8(2)      . . . . ?
O13_4  C14_4  C19_4  C18_4  -173.5(18) . . . . ?
C15_4  C14_4  C19_4  C18_4  6(2)       . . . . ?
O13_4  C14_4  C19_4  P20_4  3(2)       . . . . ?
C15_4  C14_4  C19_4  P20_4  -177.9(18) . . . . ?
C12_4  C11_4  P20_4  O29_4  -86.8(16)  . . . . ?
C10_4  C11_4  P20_4  O29_4  97.4(16)   . . . . ?
C12_4  C11_4  P20_4  C21_4  135.9(14)  . . . . ?
C10_4  C11_4  P20_4  C21_4  -39.9(15)  . . . . ?
C12_4  C11_4  P20_4  C19_4  42.7(14)   . . . . ?
C10_4  C11_4  P20_4  C19_4  -133.1(14) . . . . ?
C18_4  C19_4  P20_4  O29_4  -93.7(17)  . . . . ?
C14_4  C19_4  P20_4  O29_4  90.2(17)   . . . . ?
C18_4  C19_4  P20_4  C11_4  135.9(15)  . . . . ?
C14_4  C19_4  P20_4  C11_4  -40.3(15)  . . . . ?
C18_4  C19_4  P20_4  C21_4  42.1(16)   . . . . ?
C14_4  C19_4  P20_4  C21_4  -134.0(15) . . . . ?
O29_4  P20_4  C21_4  C26_4  -91.2(18)  . . . . ?
C11_4  P20_4  C21_4  C26_4  43.2(15)   . . . . ?
C19_4  P20_4  C21_4  C26_4  137.0(14)  . . . . ?
O29_4  P20_4  C21_4  C22_4  94.1(17)   . . . . ?
C11_4  P20_4  C21_4  C22_4  -131.5(14) . . . . ?
C19_4  P20_4  C21_4  C22_4  -37.7(15)  . . . . ?
C26_4  C21_4  C22_4  C23_4  5(2)       . . . . ?
P20_4  C21_4  C22_4  C23_4  179.8(16)  . . . . ?
C26_4  C21_4  C22_4  O28_4  -174.3(16) . . . . ?
P20_4  C21_4  C22_4  O28_4  0(2)       . . . . ?
O28_4  C22_4  C23_4  C24_4  -178.5(19) . . . . ?
C21_4  C22_4  C23_4  C24_4  2(3)       . . . . ?
C22_4  C23_4  C24_4  C25_4  -7(3)      . . . . ?
C23_4  C24_4  C25_4  C26_4  3(3)       . . . . ?
C23_4  C24_4  C25_4  C30_4  -177(2)    . . . . ?
C22_4  C21_4  C26_4  O27_4  169.0(16)  . . . . ?
P20_4  C21_4  C26_4  O27_4  -6(2)      . . . . ?
C22_4  C21_4  C26_4  C25_4  -8(2)      . . . . ?
P20_4  C21_4  C26_4  C25_4  176.8(14)  . . . . ?
C24_4  C25_4  C26_4  O27_4  -173.0(18) . . . . ?
C30_4  C25_4  C26_4  O27_4  7(2)       . . . . ?
C24_4  C25_4  C26_4  C21_4  4(2)       . . . . ?
C30_4  C25_4  C26_4  C21_4  -175.4(15) . . . . ?
C9_4   C10_4  O27_4  C26_4  -128(2)    . . . . ?
C11_4  C10_4  O27_4  C26_4  50(2)      . . . . ?
C21_4  C26_4  O27_4  C10_4  -47(2)     . . . . ?
C25_4  C26_4  O27_4  C10_4  129.9(17)  . . . . ?
C23_4  C22_4  O28_4  C18_4  -131.7(18) . . . . ?
C21_4  C22_4  O28_4  C18_4  48(2)      . . . . ?
C17_4  C18_4  O28_4  C22_4  134.0(17)  . . . . ?
C19_4  C18_4  O28_4  C22_4  -44(2)     . . . . ?
C24_4  C25_4  C30_4  C31_4  49(2)      . . . . ?
C26_4  C25_4  C30_4  C31_4  -131.2(19) . . . . ?
C24_4  C25_4  C30_4  C35_4  -129.1(19) . . . . ?
C26_4  C25_4  C30_4  C35_4  51(2)      . . . . ?
C35_4  C30_4  C31_4  C32_4  -2(2)      . . . . ?
C25_4  C30_4  C31_4  C32_4  179.8(18)  . . . . ?
C30_4  C31_4  C32_4  C33_4  0(2)       . . . . ?
C31_4  C32_4  C33_4  N34_4  -1(2)      . . . . ?
C32_4  C33_4  N34_4  C35_4  4(3)       . . . . ?
C32_4  C33_4  N34_4  Pd5_1  179.2(15)  . . . . ?
C33_4  N34_4  C35_4  C30_4  -7(3)      . . . . ?
Pd5_1  N34_4  C35_4  C30_4  178.3(13)  . . . . ?
C31_4  C30_4  C35_4  N34_4  5(3)       . . . . ?
C25_4  C30_4  C35_4  N34_4  -176.2(16) . . . . ?
C16_4  C17_4  C36_4  C41_4  -133(2)    . . . . ?
C18_4  C17_4  C36_4  C41_4  48(2)      . . . . ?
C16_4  C17_4  C36_4  C37_4  45(3)      . . . . ?
C18_4  C17_4  C36_4  C37_4  -134.8(19) . . . . ?
C41_4  C36_4  C37_4  C38_4  -2(3)      . . . . ?
C17_4  C36_4  C37_4  C38_4  -179.8(18) . . . . ?
C36_4  C37_4  C38_4  C39_4  3(2)       . . . . ?
C37_4  C38_4  C39_4  N40_4  -3(2)      . . . . ?
C38_4  C39_4  N40_4  C41_4  2(3)       . . . . ?
C38_4  C39_4  N40_4  Pd2_1  179.5(16)  . . . . ?
C39_4  N40_4  C41_4  C36_4  -1(4)      . . . . ?
Pd2_1  N40_4  C41_4  C36_4  -178.8(16) . . . . ?
C37_4  C36_4  C41_4  N40_4  1(3)       . . . . ?
C17_4  C36_4  C41_4  N40_4  179(2)     . . . . ?
C6_5   N1_5   C2_5   C3_5   3(3)       . . . . ?
Pd1_1  N1_5   C2_5   C3_5   177(2)     . . . . ?
N1_5   C2_5   C3_5   C4_5   1(4)       . . . . ?
C2_5   C3_5   C4_5   C5_5   -5(4)      . . . . ?
C3_5   C4_5   C5_5   C6_5   6(3)       . . . . ?
C3_5   C4_5   C5_5   C7_5   -172(2)    . . . . ?
C2_5   N1_5   C6_5   C5_5   -1(2)      . . . . ?
Pd1_1  N1_5   C6_5   C5_5   -176.4(13) . . . . ?
C4_5   C5_5   C6_5   N1_5   -3(2)      . . . . ?
C7_5   C5_5   C6_5   N1_5   175.0(17)  . . . . ?
C4_5   C5_5   C7_5   C8_5   43(3)      . . . . ?
C6_5   C5_5   C7_5   C8_5   -135(2)    . . . . ?
C4_5   C5_5   C7_5   C12_5  -136(2)    . . . . ?
C6_5   C5_5   C7_5   C12_5  46(2)      . . . . ?
C12_5  C7_5   C8_5   C9_5   2(3)       . . . . ?
C5_5   C7_5   C8_5   C9_5   -177(2)    . . . . ?
C7_5   C8_5   C9_5   C10_5  -6(4)      . . . . ?
C8_5   C9_5   C10_5  O27_5  179(2)     . . . . ?
C8_5   C9_5   C10_5  C11_5  3(3)       . . . . ?
C9_5   C10_5  C11_5  C12_5  3(2)       . . . . ?
O27_5  C10_5  C11_5  C12_5  -172.7(17) . . . . ?
C9_5   C10_5  C11_5  P20_5  176.6(17)  . . . . ?
O27_5  C10_5  C11_5  P20_5  1(2)       . . . . ?
C10_5  C11_5  C12_5  O13_5  165.0(17)  . . . . ?
P20_5  C11_5  C12_5  O13_5  -8(2)      . . . . ?
C10_5  C11_5  C12_5  C7_5   -7(2)      . . . . ?
P20_5  C11_5  C12_5  C7_5   179.8(14)  . . . . ?
C8_5   C7_5   C12_5  C11_5  4(2)       . . . . ?
C5_5   C7_5   C12_5  C11_5  -176.5(16) . . . . ?
C8_5   C7_5   C12_5  O13_5  -168.2(19) . . . . ?
C5_5   C7_5   C12_5  O13_5  11(2)      . . . . ?
C11_5  C12_5  O13_5  C14_5  -36(2)     . . . . ?
C7_5   C12_5  O13_5  C14_5  136.0(15)  . . . . ?
C12_5  O13_5  C14_5  C19_5  38(2)      . . . . ?
C12_5  O13_5  C14_5  C15_5  -139.1(17) . . . . ?
C19_5  C14_5  C15_5  C16_5  -8(3)      . . . . ?
O13_5  C14_5  C15_5  C16_5  169.5(19)  . . . . ?
C14_5  C15_5  C16_5  C17_5  8(3)       . . . . ?
C15_5  C16_5  C17_5  C18_5  -8(3)      . . . . ?
C15_5  C16_5  C17_5  C36_5  175.9(18)  . . . . ?
C16_5  C17_5  C18_5  O28_5  -169.4(16) . . . . ?
C36_5  C17_5  C18_5  O28_5  7(2)       . . . . ?
C16_5  C17_5  C18_5  C19_5  8(2)       . . . . ?
C36_5  C17_5  C18_5  C19_5  -175.7(13) . . . . ?
O13_5  C14_5  C19_5  C18_5  -168.6(15) . . . . ?
C15_5  C14_5  C19_5  C18_5  9(2)       . . . . ?
O13_5  C14_5  C19_5  P20_5  5(2)       . . . . ?
C15_5  C14_5  C19_5  P20_5  -177.4(15) . . . . ?
O28_5  C18_5  C19_5  C14_5  168.6(14)  . . . . ?
C17_5  C18_5  C19_5  C14_5  -8.6(19)   . . . . ?
O28_5  C18_5  C19_5  P20_5  -5.4(18)   . . . . ?
C17_5  C18_5  C19_5  P20_5  177.4(11)  . . . . ?
C12_5  C11_5  P20_5  O29_5  -84.7(18)  . . . . ?
C10_5  C11_5  P20_5  O29_5  101.7(16)  . . . . ?
C12_5  C11_5  P20_5  C21_5  136.5(15)  . . . . ?
C10_5  C11_5  P20_5  C21_5  -37.0(15)  . . . . ?
C12_5  C11_5  P20_5  C19_5  41.0(15)   . . . . ?
C10_5  C11_5  P20_5  C19_5  -132.5(14) . . . . ?
C14_5  C19_5  P20_5  O29_5  93.2(14)   . . . . ?
C18_5  C19_5  P20_5  O29_5  -92.6(14)  . . . . ?
C14_5  C19_5  P20_5  C21_5  -135.8(13) . . . . ?
C18_5  C19_5  P20_5  C21_5  38.4(13)   . . . . ?
C14_5  C19_5  P20_5  C11_5  -39.5(13)  . . . . ?
C18_5  C19_5  P20_5  C11_5  134.7(12)  . . . . ?
O29_5  P20_5  C21_5  C22_5  87.8(17)   . . . . ?
C11_5  P20_5  C21_5  C22_5  -132.4(14) . . . . ?
C19_5  P20_5  C21_5  C22_5  -37.4(14)  . . . . ?
O29_5  P20_5  C21_5  C26_5  -98.3(16)  . . . . ?
C11_5  P20_5  C21_5  C26_5  41.5(15)   . . . . ?
C19_5  P20_5  C21_5  C26_5  136.5(14)  . . . . ?
C26_5  C21_5  C22_5  C23_5  6(2)       . . . . ?
P20_5  C21_5  C22_5  C23_5  180.0(16)  . . . . ?
C26_5  C21_5  C22_5  O28_5  -171.5(15) . . . . ?
P20_5  C21_5  C22_5  O28_5  3(2)       . . . . ?
O28_5  C22_5  C23_5  C24_5  176.6(18)  . . . . ?
C21_5  C22_5  C23_5  C24_5  -1(3)      . . . . ?
C22_5  C23_5  C24_5  C25_5  0(3)       . . . . ?
C23_5  C24_5  C25_5  C26_5  -5(3)      . . . . ?
C23_5  C24_5  C25_5  C30_5  175.5(17)  . . . . ?
C24_5  C25_5  C26_5  O27_5  -167.3(17) . . . . ?
C30_5  C25_5  C26_5  O27_5  13(2)      . . . . ?
C24_5  C25_5  C26_5  C21_5  10(2)      . . . . ?
C30_5  C25_5  C26_5  C21_5  -169.6(15) . . . . ?
C22_5  C21_5  C26_5  C25_5  -11(2)     . . . . ?
P20_5  C21_5  C26_5  C25_5  174.8(14)  . . . . ?
C22_5  C21_5  C26_5  O27_5  166.9(16)  . . . . ?
P20_5  C21_5  C26_5  O27_5  -7(2)      . . . . ?
C25_5  C26_5  O27_5  C10_5  135.8(17)  . . . . ?
C21_5  C26_5  O27_5  C10_5  -42(2)     . . . . ?
C9_5   C10_5  O27_5  C26_5  -128(2)    . . . . ?
C11_5  C10_5  O27_5  C26_5  47(2)      . . . . ?
C23_5  C22_5  O28_5  C18_5  -134.9(19) . . . . ?
C21_5  C22_5  O28_5  C18_5  42(2)      . . . . ?
C19_5  C18_5  O28_5  C22_5  -41(2)     . . . . ?
C17_5  C18_5  O28_5  C22_5  135.7(16)  . . . . ?
C26_5  C25_5  C30_5  C35_5  43(2)      . . . . ?
C24_5  C25_5  C30_5  C35_5  -137.3(16) . . . . ?
C26_5  C25_5  C30_5  C31_5  -136.1(16) . . . . ?
C24_5  C25_5  C30_5  C31_5  44(2)      . . . . ?
C35_5  C30_5  C31_5  C32_5  7(2)       . . . . ?
C25_5  C30_5  C31_5  C32_5  -174.4(14) . . . . ?
C30_5  C31_5  C32_5  C33_5  -2.2(19)   . . . . ?
C31_5  C32_5  C33_5  N34_5  -3(2)      . . . . ?
C32_5  C33_5  N34_5  C35_5  4(3)       . . . . ?
C32_5  C33_5  N34_5  Pd2_1  -179.9(13) . . . . ?
C33_5  N34_5  C35_5  C30_5  1(2)       . . . . ?
Pd2_1  N34_5  C35_5  C30_5  -175.0(12) . . . . ?
C31_5  C30_5  C35_5  N34_5  -6(2)      . . . . ?
C25_5  C30_5  C35_5  N34_5  174.7(15)  . . . . ?
C16_5  C17_5  C36_5  C37_5  41(2)      . . . . ?
C18_5  C17_5  C36_5  C37_5  -135.4(17) . . . . ?
C16_5  C17_5  C36_5  C41_5  -137.6(18) . . . . ?
C18_5  C17_5  C36_5  C41_5  46(2)      . . . . ?
C41_5  C36_5  C37_5  C38_5  0(2)       . . . . ?
C17_5  C36_5  C37_5  C38_5  -178.2(16) . . . . ?
C36_5  C37_5  C38_5  C39_5  -1(2)      . . . . ?
C37_5  C38_5  C39_5  N40_5  -1(2)      . . . . ?
C38_5  C39_5  N40_5  C41_5  4(3)       . . . . ?
C38_5  C39_5  N40_5  Pd3_1  172.6(14)  . . . . ?
C39_5  N40_5  C41_5  C36_5  -4(2)      . . . . ?
Pd3_1  N40_5  C41_5  C36_5  -173.5(12) . . . . ?
C37_5  C36_5  C41_5  N40_5  2(2)       . . . . ?
C17_5  C36_5  C41_5  N40_5  -179.1(15) . . . . ?
C6_6   N1_6   C2_6   C3_6   10(3)      . . . . ?
Pd6_1  N1_6   C2_6   C3_6   -178.6(17) . . . . ?
N1_6   C2_6   C3_6   C4_6   -11(3)     . . . . ?
C2_6   C3_6   C4_6   C5_6   5(3)       . . . . ?
C3_6   C4_6   C5_6   C6_6   2(2)       . . . . ?
C3_6   C4_6   C5_6   C7_6   -175.7(17) . . . . ?
C2_6   N1_6   C6_6   C5_6   -3(2)      . . . . ?
Pd6_1  N1_6   C6_6   C5_6   -174.3(11) . . . . ?
C4_6   C5_6   C6_6   N1_6   -2.8(18)   . . . . ?
C7_6   C5_6   C6_6   N1_6   174.5(15)  . . . . ?
C6_6   C5_6   C7_6   C8_6   -143.5(18) . . . . ?
C4_6   C5_6   C7_6   C8_6   34(2)      . . . . ?
C6_6   C5_6   C7_6   C12_6  41.6(19)   . . . . ?
C4_6   C5_6   C7_6   C12_6  -141.3(16) . . . . ?
C12_6  C7_6   C8_6   C9_6   -8(3)      . . . . ?
C5_6   C7_6   C8_6   C9_6   177(2)     . . . . ?
C7_6   C8_6   C9_6   C10_6  2(3)       . . . . ?
C8_6   C9_6   C10_6  O27_6  172.6(19)  . . . . ?
C8_6   C9_6   C10_6  C11_6  2(3)       . . . . ?
C9_6   C10_6  C11_6  C12_6  0(2)       . . . . ?
O27_6  C10_6  C11_6  C12_6  -170.6(15) . . . . ?
C9_6   C10_6  C11_6  P20_6  174.7(15)  . . . . ?
O27_6  C10_6  C11_6  P20_6  4(2)       . . . . ?
C10_6  C11_6  C12_6  O13_6  166.4(15)  . . . . ?
P20_6  C11_6  C12_6  O13_6  -8(2)      . . . . ?
C10_6  C11_6  C12_6  C7_6   -5(2)      . . . . ?
P20_6  C11_6  C12_6  C7_6   179.9(12)  . . . . ?
C8_6   C7_6   C12_6  C11_6  9(2)       . . . . ?
C5_6   C7_6   C12_6  C11_6  -175.7(14) . . . . ?
C8_6   C7_6   C12_6  O13_6  -162.7(18) . . . . ?
C5_6   C7_6   C12_6  O13_6  12(2)      . . . . ?
C11_6  C12_6  O13_6  C14_6  -37(2)     . . . . ?
C7_6   C12_6  O13_6  C14_6  135.0(16)  . . . . ?
C12_6  O13_6  C14_6  C15_6  -136(2)    . . . . ?
C12_6  O13_6  C14_6  C19_6  40(2)      . . . . ?
O13_6  C14_6  C15_6  C16_6  -175(2)    . . . . ?
C19_6  C14_6  C15_6  C16_6  8(3)       . . . . ?
C14_6  C15_6  C16_6  C17_6  -14(4)     . . . . ?
C15_6  C16_6  C17_6  C18_6  7(3)       . . . . ?
C15_6  C16_6  C17_6  C36_6  -174(2)    . . . . ?
C16_6  C17_6  C18_6  O28_6  -171.3(17) . . . . ?
C36_6  C17_6  C18_6  O28_6  9(2)       . . . . ?
C16_6  C17_6  C18_6  C19_6  7(2)       . . . . ?
C36_6  C17_6  C18_6  C19_6  -173.1(15) . . . . ?
O28_6  C18_6  C19_6  C14_6  166.3(16)  . . . . ?
C17_6  C18_6  C19_6  C14_6  -12(2)     . . . . ?
O28_6  C18_6  C19_6  P20_6  -9(2)      . . . . ?
C17_6  C18_6  C19_6  P20_6  172.7(14)  . . . . ?
C15_6  C14_6  C19_6  C18_6  4(2)       . . . . ?
O13_6  C14_6  C19_6  C18_6  -171.9(17) . . . . ?
C15_6  C14_6  C19_6  P20_6  179.8(18)  . . . . ?
O13_6  C14_6  C19_6  P20_6  4(2)       . . . . ?
C18_6  C19_6  P20_6  O29_6  -92.2(15)  . . . . ?
C14_6  C19_6  P20_6  O29_6  92.2(14)   . . . . ?
C18_6  C19_6  P20_6  C21_6  42.3(14)   . . . . ?
C14_6  C19_6  P20_6  C21_6  -133.3(13) . . . . ?
C18_6  C19_6  P20_6  C11_6  138.8(13)  . . . . ?
C14_6  C19_6  P20_6  C11_6  -36.9(14)  . . . . ?
C12_6  C11_6  P20_6  O29_6  -88.4(14)  . . . . ?
C10_6  C11_6  P20_6  O29_6  96.9(14)   . . . . ?
C12_6  C11_6  P20_6  C19_6  40.9(13)   . . . . ?
C10_6  C11_6  P20_6  C19_6  -133.9(12) . . . . ?
C12_6  C11_6  P20_6  C21_6  135.3(12)  . . . . ?
C10_6  C11_6  P20_6  C21_6  -39.4(12)  . . . . ?
O29_6  P20_6  C21_6  C26_6  -92.8(14)  . . . . ?
C19_6  P20_6  C21_6  C26_6  135.3(12)  . . . . ?
C11_6  P20_6  C21_6  C26_6  40.8(12)   . . . . ?
O29_6  P20_6  C21_6  C22_6  93.8(14)   . . . . ?
C19_6  P20_6  C21_6  C22_6  -38.1(12)  . . . . ?
C11_6  P20_6  C21_6  C22_6  -132.6(11) . . . . ?
C26_6  C21_6  C22_6  C23_6  10.1(19)   . . . . ?
P20_6  C21_6  C22_6  C23_6  -176.3(13) . . . . ?
C26_6  C21_6  C22_6  O28_6  -172.8(12) . . . . ?
P20_6  C21_6  C22_6  O28_6  0.8(17)    . . . . ?
O28_6  C22_6  C23_6  C24_6  173.0(15)  . . . . ?
C21_6  C22_6  C23_6  C24_6  -10(2)     . . . . ?
C22_6  C23_6  C24_6  C25_6  9(2)       . . . . ?
C23_6  C24_6  C25_6  C26_6  -9(2)      . . . . ?
C23_6  C24_6  C25_6  C30_6  174.7(15)  . . . . ?
C22_6  C21_6  C26_6  O27_6  168.4(13)  . . . . ?
P20_6  C21_6  C26_6  O27_6  -5.2(18)   . . . . ?
C22_6  C21_6  C26_6  C25_6  -9.6(18)   . . . . ?
P20_6  C21_6  C26_6  C25_6  176.7(11)  . . . . ?
C24_6  C25_6  C26_6  C21_6  9(2)       . . . . ?
C30_6  C25_6  C26_6  C21_6  -174.2(13) . . . . ?
C24_6  C25_6  C26_6  O27_6  -169.0(14) . . . . ?
C30_6  C25_6  C26_6  O27_6  7.7(18)    . . . . ?
C9_6   C10_6  O27_6  C26_6  -129.7(18) . . . . ?
C11_6  C10_6  O27_6  C26_6  41(2)      . . . . ?
C21_6  C26_6  O27_6  C10_6  -41(2)     . . . . ?
C25_6  C26_6  O27_6  C10_6  136.8(15)  . . . . ?
C23_6  C22_6  O28_6  C18_6  -137.8(16) . . . . ?
C21_6  C22_6  O28_6  C18_6  45.1(18)   . . . . ?
C17_6  C18_6  O28_6  C22_6  137.2(15)  . . . . ?
C19_6  C18_6  O28_6  C22_6  -41(2)     . . . . ?
C24_6  C25_6  C30_6  C35_6  -135.9(18) . . . . ?
C26_6  C25_6  C30_6  C35_6  48(2)      . . . . ?
C24_6  C25_6  C30_6  C31_6  46(2)      . . . . ?
C26_6  C25_6  C30_6  C31_6  -130.7(19) . . . . ?
C35_6  C30_6  C31_6  C32_6  0(3)       . . . . ?
C25_6  C30_6  C31_6  C32_6  178.6(18)  . . . . ?
C30_6  C31_6  C32_6  C33_6  -1(2)      . . . . ?
C31_6  C32_6  C33_6  N34_6  -2(2)      . . . . ?
C32_6  C33_6  N34_6  C35_6  5(3)       . . . . ?
C32_6  C33_6  N34_6  Pd3_1  176.8(17)  . . . . ?
C33_6  N34_6  C35_6  C30_6  -6(3)      . . . . ?
Pd3_1  N34_6  C35_6  C30_6  -178.1(15) . . . . ?
C31_6  C30_6  C35_6  N34_6  3(3)       . . . . ?
C25_6  C30_6  C35_6  N34_6  -174.8(18) . . . . ?
C16_6  C17_6  C36_6  C41_6  -138.8(17) . . . . ?
C18_6  C17_6  C36_6  C41_6  41(2)      . . . . ?
C16_6  C17_6  C36_6  C37_6  36(2)      . . . . ?
C18_6  C17_6  C36_6  C37_6  -144.8(17) . . . . ?
C41_6  C36_6  C37_6  C38_6  0(2)       . . . . ?
C17_6  C36_6  C37_6  C38_6  -174.8(15) . . . . ?
C36_6  C37_6  C38_6  C39_6  -1.4(19)   . . . . ?
C37_6  C38_6  C39_6  N40_6  1(2)       . . . . ?
C38_6  C39_6  N40_6  C41_6  1(3)       . . . . ?
C38_6  C39_6  N40_6  Pd2_1  172.4(15)  . . . . ?
C39_6  N40_6  C41_6  C36_6  -3(3)      . . . . ?
Pd2_1  N40_6  C41_6  C36_6  -174.5(13) . . . . ?
C37_6  C36_6  C41_6  N40_6  3(3)       . . . . ?
C17_6  C36_6  C41_6  N40_6  177.1(18)  . . . . ?
C6_7   N1_7   C2_7   C3_7   2(4)       . . . . ?
Pd6_1  N1_7   C2_7   C3_7   -179(2)    . . . . ?
N1_7   C2_7   C3_7   C4_7   0(5)       . . . . ?
C2_7   C3_7   C4_7   C5_7   -2(5)      . . . . ?
C3_7   C4_7   C5_7   C6_7   2(4)       . . . . ?
C3_7   C4_7   C5_7   C7_7   -179(3)    . . . . ?
C2_7   N1_7   C6_7   C5_7   -2(2)      . . . . ?
Pd6_1  N1_7   C6_7   C5_7   179.1(11)  . . . . ?
C4_7   C5_7   C6_7   N1_7   0(2)       . . . . ?
C7_7   C5_7   C6_7   N1_7   -179.0(15) . . . . ?
C6_7   C5_7   C7_7   C8_7   -135.3(18) . . . . ?
C4_7   C5_7   C7_7   C8_7   46(3)      . . . . ?
C6_7   C5_7   C7_7   C12_7  45(2)      . . . . ?
C4_7   C5_7   C7_7   C12_7  -134(2)    . . . . ?
C12_7  C7_7   C8_7   C9_7   -3(3)      . . . . ?
C5_7   C7_7   C8_7   C9_7   177.5(18)  . . . . ?
C7_7   C8_7   C9_7   C10_7  -3(3)      . . . . ?
C8_7   C9_7   C10_7  O27_7  -179.0(16) . . . . ?
C8_7   C9_7   C10_7  C11_7  4(2)       . . . . ?
C9_7   C10_7  C11_7  C12_7  1(2)       . . . . ?
O27_7  C10_7  C11_7  C12_7  -176.3(14) . . . . ?
C9_7   C10_7  C11_7  P20_7  178.4(14)  . . . . ?
O27_7  C10_7  C11_7  P20_7  1.3(19)    . . . . ?
C8_7   C7_7   C12_7  O13_7  -168.0(17) . . . . ?
C5_7   C7_7   C12_7  O13_7  12(2)      . . . . ?
C8_7   C7_7   C12_7  C11_7  8(2)       . . . . ?
C5_7   C7_7   C12_7  C11_7  -172.4(15) . . . . ?
C10_7  C11_7  C12_7  C7_7   -7(2)      . . . . ?
P20_7  C11_7  C12_7  C7_7   175.2(14)  . . . . ?
C10_7  C11_7  C12_7  O13_7  168.7(15)  . . . . ?
P20_7  C11_7  C12_7  O13_7  -9(2)      . . . . ?
C7_7   C12_7  O13_7  C14_7  134.5(17)  . . . . ?
C11_7  C12_7  O13_7  C14_7  -42(2)     . . . . ?
C12_7  O13_7  C14_7  C15_7  -131(2)    . . . . ?
C12_7  O13_7  C14_7  C19_7  49(2)      . . . . ?
O13_7  C14_7  C15_7  C16_7  -172(2)    . . . . ?
C19_7  C14_7  C15_7  C16_7  8(3)       . . . . ?
C14_7  C15_7  C16_7  C17_7  -14(4)     . . . . ?
C15_7  C16_7  C17_7  C18_7  7(4)       . . . . ?
C15_7  C16_7  C17_7  C36_7  -175(3)    . . . . ?
C16_7  C17_7  C18_7  O28_7  -171(2)    . . . . ?
C36_7  C17_7  C18_7  O28_7  11(3)      . . . . ?
C16_7  C17_7  C18_7  C19_7  5(2)       . . . . ?
C36_7  C17_7  C18_7  C19_7  -173.1(17) . . . . ?
C15_7  C14_7  C19_7  C18_7  3(3)       . . . . ?
O13_7  C14_7  C19_7  C18_7  -176.0(18) . . . . ?
C15_7  C14_7  C19_7  P20_7  176.7(19)  . . . . ?
O13_7  C14_7  C19_7  P20_7  -3(2)      . . . . ?
O28_7  C18_7  C19_7  C14_7  166.1(18)  . . . . ?
C17_7  C18_7  C19_7  C14_7  -10(2)     . . . . ?
O28_7  C18_7  C19_7  P20_7  -7(2)      . . . . ?
C17_7  C18_7  C19_7  P20_7  176.3(15)  . . . . ?
C14_7  C19_7  P20_7  O29_7  92.4(18)   . . . . ?
C18_7  C19_7  P20_7  O29_7  -94.2(18)  . . . . ?
C14_7  C19_7  P20_7  C21_7  -131.0(14) . . . . ?
C18_7  C19_7  P20_7  C21_7  42.4(15)   . . . . ?
C14_7  C19_7  P20_7  C11_7  -38.1(15)  . . . . ?
C18_7  C19_7  P20_7  C11_7  135.3(14)  . . . . ?
C12_7  C11_7  P20_7  O29_7  -91.1(18)  . . . . ?
C10_7  C11_7  P20_7  O29_7  91.3(18)   . . . . ?
C12_7  C11_7  P20_7  C19_7  44.0(14)   . . . . ?
C10_7  C11_7  P20_7  C19_7  -133.6(14) . . . . ?
C12_7  C11_7  P20_7  C21_7  138.6(14)  . . . . ?
C10_7  C11_7  P20_7  C21_7  -39.0(14)  . . . . ?
O29_7  P20_7  C21_7  C26_7  -84.0(18)  . . . . ?
C19_7  P20_7  C21_7  C26_7  138.2(14)  . . . . ?
C11_7  P20_7  C21_7  C26_7  42.7(15)   . . . . ?
O29_7  P20_7  C21_7  C22_7  97.8(17)   . . . . ?
C19_7  P20_7  C21_7  C22_7  -40.0(15)  . . . . ?
C11_7  P20_7  C21_7  C22_7  -135.5(14) . . . . ?
C26_7  C21_7  C22_7  C23_7  6(2)       . . . . ?
P20_7  C21_7  C22_7  C23_7  -175.4(16) . . . . ?
C26_7  C21_7  C22_7  O28_7  -175.5(17) . . . . ?
P20_7  C21_7  C22_7  O28_7  3(2)       . . . . ?
O28_7  C22_7  C23_7  C24_7  176.5(19)  . . . . ?
C21_7  C22_7  C23_7  C24_7  -5(3)      . . . . ?
C22_7  C23_7  C24_7  C25_7  4(3)       . . . . ?
C23_7  C24_7  C25_7  C26_7  -4(3)      . . . . ?
C23_7  C24_7  C25_7  C30_7  174.8(18)  . . . . ?
C22_7  C21_7  C26_7  O27_7  169.7(17)  . . . . ?
P20_7  C21_7  C26_7  O27_7  -8(2)      . . . . ?
C22_7  C21_7  C26_7  C25_7  -6(2)      . . . . ?
P20_7  C21_7  C26_7  C25_7  176.0(14)  . . . . ?
C24_7  C25_7  C26_7  O27_7  -171.0(17) . . . . ?
C30_7  C25_7  C26_7  O27_7  11(2)      . . . . ?
C24_7  C25_7  C26_7  C21_7  5(2)       . . . . ?
C30_7  C25_7  C26_7  C21_7  -173.9(15) . . . . ?
C21_7  C26_7  O27_7  C10_7  -43(2)     . . . . ?
C25_7  C26_7  O27_7  C10_7  132.2(16)  . . . . ?
C9_7   C10_7  O27_7  C26_7  -130.9(17) . . . . ?
C11_7  C10_7  O27_7  C26_7  46.1(19)   . . . . ?
C17_7  C18_7  O28_7  C22_7  132.4(19)  . . . . ?
C19_7  C18_7  O28_7  C22_7  -44(2)     . . . . ?
C23_7  C22_7  O28_7  C18_7  -135(2)    . . . . ?
C21_7  C22_7  O28_7  C18_7  46(2)      . . . . ?
C24_7  C25_7  C30_7  C31_7  47(2)      . . . . ?
C26_7  C25_7  C30_7  C31_7  -134.3(17) . . . . ?
C24_7  C25_7  C30_7  C35_7  -129.6(19) . . . . ?
C26_7  C25_7  C30_7  C35_7  49(2)      . . . . ?
C35_7  C30_7  C31_7  C32_7  1(2)       . . . . ?
C25_7  C30_7  C31_7  C32_7  -176.3(16) . . . . ?
C30_7  C31_7  C32_7  C33_7  -2(2)      . . . . ?
C31_7  C32_7  C33_7  N34_7  7(2)       . . . . ?
C32_7  C33_7  N34_7  C35_7  -9(3)      . . . . ?
C32_7  C33_7  N34_7  Pd5_1  -179.9(14) . . . . ?
C33_7  N34_7  C35_7  C30_7  8(3)       . . . . ?
Pd5_1  N34_7  C35_7  C30_7  179.1(13)  . . . . ?
C31_7  C30_7  C35_7  N34_7  -4(3)      . . . . ?
C25_7  C30_7  C35_7  N34_7  173.1(16)  . . . . ?
C16_7  C17_7  C36_7  C37_7  41(3)      . . . . ?
C18_7  C17_7  C36_7  C37_7  -141(2)    . . . . ?
C16_7  C17_7  C36_7  C41_7  -134(2)    . . . . ?
C18_7  C17_7  C36_7  C41_7  44(2)      . . . . ?
C41_7  C36_7  C37_7  C38_7  -5(3)      . . . . ?
C17_7  C36_7  C37_7  C38_7  -180(2)    . . . . ?
C36_7  C37_7  C38_7  C39_7  3(2)       . . . . ?
C37_7  C38_7  C39_7  N40_7  3(2)       . . . . ?
C38_7  C39_7  N40_7  C41_7  -6(3)      . . . . ?
C38_7  C39_7  N40_7  Pd4_1  172.5(17)  . . . . ?
C39_7  N40_7  C41_7  C36_7  3(3)       . . . . ?
Pd4_1  N40_7  C41_7  C36_7  -175.2(16) . . . . ?
C37_7  C36_7  C41_7  N40_7  2(3)       . . . . ?
C17_7  C36_7  C41_7  N40_7  177(2)     . . . . ?
C6_8   N1_8   C2_8   C3_8   -3(3)      . . . . ?
Pd6_1  N1_8   C2_8   C3_8   180.0(18)  . . . . ?
N1_8   C2_8   C3_8   C4_8   7(3)       . . . . ?
C2_8   C3_8   C4_8   C5_8   -9(3)      . . . . ?
C3_8   C4_8   C5_8   C6_8   8(2)       . . . . ?
C3_8   C4_8   C5_8   C7_8   -172.2(18) . . . . ?
C2_8   N1_8   C6_8   C5_8   0(2)       . . . . ?
Pd6_1  N1_8   C6_8   C5_8   177.9(14)  . . . . ?
C4_8   C5_8   C6_8   N1_8   -3(2)      . . . . ?
C7_8   C5_8   C6_8   N1_8   176.7(16)  . . . . ?
C4_8   C5_8   C7_8   C8_8   45(2)      . . . . ?
C6_8   C5_8   C7_8   C8_8   -135.0(18) . . . . ?
C4_8   C5_8   C7_8   C12_8  -137.8(17) . . . . ?
C6_8   C5_8   C7_8   C12_8  42(2)      . . . . ?
C12_8  C7_8   C8_8   C9_8   2(3)       . . . . ?
C5_8   C7_8   C8_8   C9_8   180(2)     . . . . ?
C7_8   C8_8   C9_8   C10_8  -6(3)      . . . . ?
C8_8   C9_8   C10_8  O27_8  -176(2)    . . . . ?
C8_8   C9_8   C10_8  C11_8  4(3)       . . . . ?
C9_8   C10_8  C11_8  C12_8  3(2)       . . . . ?
O27_8  C10_8  C11_8  C12_8  -177.9(17) . . . . ?
C9_8   C10_8  C11_8  P20_8  179.7(17)  . . . . ?
O27_8  C10_8  C11_8  P20_8  -1(2)      . . . . ?
C10_8  C11_8  C12_8  C7_8   -8(2)      . . . . ?
P20_8  C11_8  C12_8  C7_8   175.8(15)  . . . . ?
C10_8  C11_8  C12_8  O13_8  170.4(16)  . . . . ?
P20_8  C11_8  C12_8  O13_8  -6(2)      . . . . ?
C8_8   C7_8   C12_8  C11_8  5(2)       . . . . ?
C5_8   C7_8   C12_8  C11_8  -172.5(16) . . . . ?
C8_8   C7_8   C12_8  O13_8  -172.8(18) . . . . ?
C5_8   C7_8   C12_8  O13_8  10(2)      . . . . ?
C11_8  C12_8  O13_8  C14_8  -46(2)     . . . . ?
C7_8   C12_8  O13_8  C14_8  132.0(16)  . . . . ?
C12_8  O13_8  C14_8  C15_8  -129.0(18) . . . . ?
C12_8  O13_8  C14_8  C19_8  52(2)      . . . . ?
O13_8  C14_8  C15_8  C16_8  179.1(18)  . . . . ?
C19_8  C14_8  C15_8  C16_8  -2(3)      . . . . ?
C14_8  C15_8  C16_8  C17_8  3(3)       . . . . ?
C15_8  C16_8  C17_8  C18_8  -6(3)      . . . . ?
C15_8  C16_8  C17_8  C36_8  177(2)     . . . . ?
C16_8  C17_8  C18_8  C19_8  8(2)       . . . . ?
C36_8  C17_8  C18_8  C19_8  -175.3(15) . . . . ?
C16_8  C17_8  C18_8  O28_8  -165.6(18) . . . . ?
C36_8  C17_8  C18_8  O28_8  11(2)      . . . . ?
O28_8  C18_8  C19_8  C14_8  166.3(16)  . . . . ?
C17_8  C18_8  C19_8  C14_8  -7(2)      . . . . ?
O28_8  C18_8  C19_8  P20_8  -9(2)      . . . . ?
C17_8  C18_8  C19_8  P20_8  178.1(14)  . . . . ?
C15_8  C14_8  C19_8  C18_8  4(2)       . . . . ?
O13_8  C14_8  C19_8  C18_8  -177.1(15) . . . . ?
C15_8  C14_8  C19_8  P20_8  179.1(15)  . . . . ?
O13_8  C14_8  C19_8  P20_8  -1.9(19)   . . . . ?
C12_8  C11_8  P20_8  O29_8  -92.7(17)  . . . . ?
C10_8  C11_8  P20_8  O29_8  90.7(17)   . . . . ?
C12_8  C11_8  P20_8  C19_8  44.4(16)   . . . . ?
C10_8  C11_8  P20_8  C19_8  -132.2(14) . . . . ?
C12_8  C11_8  P20_8  C21_8  138.4(15)  . . . . ?
C10_8  C11_8  P20_8  C21_8  -38.2(15)  . . . . ?
C18_8  C19_8  P20_8  O29_8  -84.4(17)  . . . . ?
C14_8  C19_8  P20_8  O29_8  100.6(15)  . . . . ?
C18_8  C19_8  P20_8  C11_8  136.4(15)  . . . . ?
C14_8  C19_8  P20_8  C11_8  -38.7(14)  . . . . ?
C18_8  C19_8  P20_8  C21_8  40.0(15)   . . . . ?
C14_8  C19_8  P20_8  C21_8  -135.1(13) . . . . ?
O29_8  P20_8  C21_8  C22_8  92.6(16)   . . . . ?
C11_8  P20_8  C21_8  C22_8  -131.8(14) . . . . ?
C19_8  P20_8  C21_8  C22_8  -36.6(15)  . . . . ?
O29_8  P20_8  C21_8  C26_8  -92.8(16)  . . . . ?
C11_8  P20_8  C21_8  C26_8  42.7(14)   . . . . ?
C19_8  P20_8  C21_8  C26_8  138.0(13)  . . . . ?
C26_8  C21_8  C22_8  O28_8  -171.8(16) . . . . ?
P20_8  C21_8  C22_8  O28_8  3(2)       . . . . ?
C26_8  C21_8  C22_8  C23_8  7(2)       . . . . ?
P20_8  C21_8  C22_8  C23_8  -178.4(17) . . . . ?
O28_8  C22_8  C23_8  C24_8  171(2)     . . . . ?
C21_8  C22_8  C23_8  C24_8  -8(3)      . . . . ?
C22_8  C23_8  C24_8  C25_8  8(4)       . . . . ?
C23_8  C24_8  C25_8  C26_8  -7(3)      . . . . ?
C23_8  C24_8  C25_8  C30_8  169(2)     . . . . ?
C22_8  C21_8  C26_8  O27_8  165.9(16)  . . . . ?
P20_8  C21_8  C26_8  O27_8  -8.5(19)   . . . . ?
C22_8  C21_8  C26_8  C25_8  -6(2)      . . . . ?
P20_8  C21_8  C26_8  C25_8  179.1(13)  . . . . ?
C24_8  C25_8  C26_8  O27_8  -166.2(19) . . . . ?
C30_8  C25_8  C26_8  O27_8  17(2)      . . . . ?
C24_8  C25_8  C26_8  C21_8  6(2)       . . . . ?
C30_8  C25_8  C26_8  C21_8  -170.6(14) . . . . ?
C9_8   C10_8  O27_8  C26_8  -134.3(18) . . . . ?
C11_8  C10_8  O27_8  C26_8  47(2)      . . . . ?
C21_8  C26_8  O27_8  C10_8  -41(2)     . . . . ?
C25_8  C26_8  O27_8  C10_8  131.5(16)  . . . . ?
C23_8  C22_8  O28_8  C18_8  -138(2)    . . . . ?
C21_8  C22_8  O28_8  C18_8  41(2)      . . . . ?
C19_8  C18_8  O28_8  C22_8  -39(2)     . . . . ?
C17_8  C18_8  O28_8  C22_8  134.7(17)  . . . . ?
C24_8  C25_8  C30_8  C31_8  47(3)      . . . . ?
C26_8  C25_8  C30_8  C31_8  -136.8(19) . . . . ?
C24_8  C25_8  C30_8  C35_8  -132(2)    . . . . ?
C26_8  C25_8  C30_8  C35_8  44(2)      . . . . ?
C35_8  C30_8  C31_8  C32_8  3(3)       . . . . ?
C25_8  C30_8  C31_8  C32_8  -175.6(18) . . . . ?
C30_8  C31_8  C32_8  C33_8  -2(2)      . . . . ?
C31_8  C32_8  C33_8  N34_8  -1(2)      . . . . ?
C32_8  C33_8  N34_8  C35_8  2(3)       . . . . ?
C32_8  C33_8  N34_8  Pd2_1  -177.2(16) . . . . ?
C33_8  N34_8  C35_8  C30_8  0(3)       . . . . ?
Pd2_1  N34_8  C35_8  C30_8  179.3(13)  . . . . ?
C31_8  C30_8  C35_8  N34_8  -3(3)      . . . . ?
C25_8  C30_8  C35_8  N34_8  176.2(17)  . . . . ?
C16_8  C17_8  C36_8  C41_8  -140(2)    . . . . ?
C18_8  C17_8  C36_8  C41_8  44(2)      . . . . ?
C16_8  C17_8  C36_8  C37_8  39(2)      . . . . ?
C18_8  C17_8  C36_8  C37_8  -137.9(19) . . . . ?
C41_8  C36_8  C37_8  C38_8  5(3)       . . . . ?
C17_8  C36_8  C37_8  C38_8  -173.3(18) . . . . ?
C36_8  C37_8  C38_8  C39_8  -4(2)      . . . . ?
C37_8  C38_8  C39_8  N40_8  2(2)       . . . . ?
C38_8  C39_8  N40_8  C41_8  -1(3)      . . . . ?
C38_8  C39_8  N40_8  Pd5_1  177.1(15)  . . . . ?
C39_8  N40_8  C41_8  C36_8  3(3)       . . . . ?
Pd5_1  N40_8  C41_8  C36_8  -175.9(13) . . . . ?
C37_8  C36_8  C41_8  N40_8  -5(3)      . . . . ?
C17_8  C36_8  C41_8  N40_8  173.9(17)  . . . . ?
C6_9   N1_9   C2_9   C3_9   -3(5)      . . . . ?
Pd6_1  N1_9   C2_9   C3_9   -177(3)    . . . . ?
N1_9   C2_9   C3_9   C4_9   7(7)       . . . . ?
C2_9   C3_9   C4_9   C5_9   -10(6)     . . . . ?
C3_9   C4_9   C5_9   C6_9   8(4)       . . . . ?
C3_9   C4_9   C5_9   C7_9   -174(3)    . . . . ?
C2_9   N1_9   C6_9   C5_9   1(3)       . . . . ?
Pd6_1  N1_9   C6_9   C5_9   175.7(16)  . . . . ?
C4_9   C5_9   C6_9   N1_9   -4(2)      . . . . ?
C7_9   C5_9   C6_9   N1_9   178(2)     . . . . ?
C4_9   C5_9   C7_9   C12_9  -124(2)    . . . . ?
C6_9   C5_9   C7_9   C12_9  54(2)      . . . . ?
C4_9   C5_9   C7_9   C8_9   56(3)      . . . . ?
C6_9   C5_9   C7_9   C8_9   -127(2)    . . . . ?
C12_9  C7_9   C8_9   C9_9   4(3)       . . . . ?
C5_9   C7_9   C8_9   C9_9   -176(2)    . . . . ?
C7_9   C8_9   C9_9   C10_9  -7(3)      . . . . ?
C8_9   C9_9   C10_9  O27_9  -179(2)    . . . . ?
C8_9   C9_9   C10_9  C11_9  5(3)       . . . . ?
C9_9   C10_9  C11_9  C12_9  1(2)       . . . . ?
O27_9  C10_9  C11_9  C12_9  -174.9(17) . . . . ?
C9_9   C10_9  C11_9  P20_9  178.6(17)  . . . . ?
O27_9  C10_9  C11_9  P20_9  3(2)       . . . . ?
C8_9   C7_9   C12_9  O13_9  -173.4(18) . . . . ?
C5_9   C7_9   C12_9  O13_9  6(2)       . . . . ?
C8_9   C7_9   C12_9  C11_9  2(2)       . . . . ?
C5_9   C7_9   C12_9  C11_9  -177.9(15) . . . . ?
C10_9  C11_9  C12_9  O13_9  170.9(17)  . . . . ?
P20_9  C11_9  C12_9  O13_9  -7(2)      . . . . ?
C10_9  C11_9  C12_9  C7_9   -5(2)      . . . . ?
P20_9  C11_9  C12_9  C7_9   177.2(13)  . . . . ?
C7_9   C12_9  O13_9  C14_9  136.2(16)  . . . . ?
C11_9  C12_9  O13_9  C14_9  -40(2)     . . . . ?
C12_9  O13_9  C14_9  C19_9  43(2)      . . . . ?
C12_9  O13_9  C14_9  C15_9  -134.1(17) . . . . ?
C19_9  C14_9  C15_9  C16_9  1(3)       . . . . ?
O13_9  C14_9  C15_9  C16_9  178.1(19)  . . . . ?
C14_9  C15_9  C16_9  C17_9  0(3)       . . . . ?
C15_9  C16_9  C17_9  C18_9  -4(3)      . . . . ?
C15_9  C16_9  C17_9  C36_9  175(2)     . . . . ?
C16_9  C17_9  C18_9  O28_9  -168.4(19) . . . . ?
C36_9  C17_9  C18_9  O28_9  13(2)      . . . . ?
C16_9  C17_9  C18_9  C19_9  9(2)       . . . . ?
C36_9  C17_9  C18_9  C19_9  -170.4(14) . . . . ?
C15_9  C14_9  C19_9  C18_9  4(2)       . . . . ?
O13_9  C14_9  C19_9  C18_9  -173.0(15) . . . . ?
C15_9  C14_9  C19_9  P20_9  179.0(14)  . . . . ?
O13_9  C14_9  C19_9  P20_9  2(2)       . . . . ?
O28_9  C18_9  C19_9  C14_9  167.9(16)  . . . . ?
C17_9  C18_9  C19_9  C14_9  -9(2)      . . . . ?
O28_9  C18_9  C19_9  P20_9  -7(2)      . . . . ?
C17_9  C18_9  C19_9  P20_9  176.1(13)  . . . . ?
C14_9  C19_9  P20_9  O29_9  94.9(15)   . . . . ?
C18_9  C19_9  P20_9  O29_9  -90.0(15)  . . . . ?
C14_9  C19_9  P20_9  C21_9  -133.5(13) . . . . ?
C18_9  C19_9  P20_9  C21_9  41.6(13)   . . . . ?
C14_9  C19_9  P20_9  C11_9  -38.8(13)  . . . . ?
C18_9  C19_9  P20_9  C11_9  136.3(12)  . . . . ?
C12_9  C11_9  P20_9  O29_9  -94.7(15)  . . . . ?
C10_9  C11_9  P20_9  O29_9  87.2(16)   . . . . ?
C12_9  C11_9  P20_9  C19_9  41.4(14)   . . . . ?
C10_9  C11_9  P20_9  C19_9  -136.7(14) . . . . ?
C12_9  C11_9  P20_9  C21_9  139.6(13)  . . . . ?
C10_9  C11_9  P20_9  C21_9  -38.5(14)  . . . . ?
O29_9  P20_9  C21_9  C26_9  -89.3(15)  . . . . ?
C19_9  P20_9  C21_9  C26_9  134.2(13)  . . . . ?
C11_9  P20_9  C21_9  C26_9  39.4(13)   . . . . ?
O29_9  P20_9  C21_9  C22_9  98.2(14)   . . . . ?
C19_9  P20_9  C21_9  C22_9  -38.3(13)  . . . . ?
C11_9  P20_9  C21_9  C22_9  -133.1(12) . . . . ?
C26_9  C21_9  C22_9  C23_9  0(2)       . . . . ?
P20_9  C21_9  C22_9  C23_9  172.3(14)  . . . . ?
C26_9  C21_9  C22_9  O28_9  -173.1(15) . . . . ?
P20_9  C21_9  C22_9  O28_9  -0.6(19)   . . . . ?
O28_9  C22_9  C23_9  C24_9  -179.4(19) . . . . ?
C21_9  C22_9  C23_9  C24_9  8(3)       . . . . ?
C22_9  C23_9  C24_9  C25_9  -11(3)     . . . . ?
C23_9  C24_9  C25_9  C26_9  6(3)       . . . . ?
C23_9  C24_9  C25_9  C30_9  -179(2)    . . . . ?
C22_9  C21_9  C26_9  O27_9  168.4(15)  . . . . ?
P20_9  C21_9  C26_9  O27_9  -3.8(19)   . . . . ?
C22_9  C21_9  C26_9  C25_9  -4.8(19)   . . . . ?
P20_9  C21_9  C26_9  C25_9  -177.0(12) . . . . ?
C24_9  C25_9  C26_9  O27_9  -170.8(17) . . . . ?
C30_9  C25_9  C26_9  O27_9  14(2)      . . . . ?
C24_9  C25_9  C26_9  C21_9  2(2)       . . . . ?
C30_9  C25_9  C26_9  C21_9  -173.5(14) . . . . ?
C21_9  C26_9  O27_9  C10_9  -45(2)     . . . . ?
C25_9  C26_9  O27_9  C10_9  127.8(16)  . . . . ?
C9_9   C10_9  O27_9  C26_9  -130(2)    . . . . ?
C11_9  C10_9  O27_9  C26_9  45(2)      . . . . ?
C23_9  C22_9  O28_9  C18_9  -125.6(19) . . . . ?
C21_9  C22_9  O28_9  C18_9  47(2)      . . . . ?
C17_9  C18_9  O28_9  C22_9  133.9(18)  . . . . ?
C19_9  C18_9  O28_9  C22_9  -43(2)     . . . . ?
C24_9  C25_9  C30_9  C35_9  -133(2)    . . . . ?
C26_9  C25_9  C30_9  C35_9  42(2)      . . . . ?
C24_9  C25_9  C30_9  C31_9  50(2)      . . . . ?
C26_9  C25_9  C30_9  C31_9  -134.7(17) . . . . ?
C35_9  C30_9  C31_9  C32_9  -1(2)      . . . . ?
C25_9  C30_9  C31_9  C32_9  176.4(17)  . . . . ?
C30_9  C31_9  C32_9  C33_9  1(2)       . . . . ?
C31_9  C32_9  C33_9  N34_9  2(3)       . . . . ?
C32_9  C33_9  N34_9  C35_9  -5(3)      . . . . ?
C32_9  C33_9  N34_9  Pd4_1  -177.0(16) . . . . ?
C33_9  N34_9  C35_9  C30_9  5(3)       . . . . ?
Pd4_1  N34_9  C35_9  C30_9  177.7(14)  . . . . ?
C31_9  C30_9  C35_9  N34_9  -3(3)      . . . . ?
C25_9  C30_9  C35_9  N34_9  -179.8(17) . . . . ?
C16_9  C17_9  C36_9  C37_9  40(2)      . . . . ?
C18_9  C17_9  C36_9  C37_9  -141.2(16) . . . . ?
C16_9  C17_9  C36_9  C41_9  -139(2)    . . . . ?
C18_9  C17_9  C36_9  C41_9  40(2)      . . . . ?
C41_9  C36_9  C37_9  C38_9  1(2)       . . . . ?
C17_9  C36_9  C37_9  C38_9  -177.4(15) . . . . ?
C36_9  C37_9  C38_9  C39_9  -1.1(19)   . . . . ?
C37_9  C38_9  C39_9  N40_9  -1(2)      . . . . ?
C38_9  C39_9  N40_9  C41_9  3(3)       . . . . ?
C38_9  C39_9  N40_9  Pd3_1  174.6(13)  . . . . ?
C39_9  N40_9  C41_9  C36_9  -3(3)      . . . . ?
Pd3_1  N40_9  C41_9  C36_9  -174.7(14) . . . . ?
C37_9  C36_9  C41_9  N40_9  1(3)       . . . . ?
C17_9  C36_9  C41_9  N40_9  179.5(18)  . . . . ?
C6_11  N1_11  C2_11  C3_11  -7(3)      . . . . ?
Pd1_10 N1_11  C2_11  C3_11  173.3(19)  . . . . ?
N1_11  C2_11  C3_11  C4_11  10(4)      . . . . ?
C2_11  C3_11  C4_11  C5_11  -8(4)      . . . . ?
C3_11  C4_11  C5_11  C6_11  4(3)       . . . . ?
C3_11  C4_11  C5_11  C7_11  -177(2)    . . . . ?
C2_11  N1_11  C6_11  C5_11  3(2)       . . . . ?
Pd1_10 N1_11  C6_11  C5_11  -177.5(12) . . . . ?
C4_11  C5_11  C6_11  N1_11  -1.5(19)   . . . . ?
C7_11  C5_11  C6_11  N1_11  179.3(15)  . . . . ?
C4_11  C5_11  C7_11  C8_11  44(2)      . . . . ?
C6_11  C5_11  C7_11  C8_11  -137.1(17) . . . . ?
C4_11  C5_11  C7_11  C12_11 -136.6(18) . . . . ?
C6_11  C5_11  C7_11  C12_11 43(2)      . . . . ?
C12_11 C7_11  C8_11  C9_11  -3(3)      . . . . ?
C5_11  C7_11  C8_11  C9_11  177.1(19)  . . . . ?
C7_11  C8_11  C9_11  C10_11 3(3)       . . . . ?
C8_11  C9_11  C10_11 O27_11 174(2)     . . . . ?
C8_11  C9_11  C10_11 C11_11 -3(3)      . . . . ?
C9_11  C10_11 C11_11 C12_11 3(2)       . . . . ?
O27_11 C10_11 C11_11 C12_11 -174.2(16) . . . . ?
C9_11  C10_11 C11_11 P20_11 179.3(17)  . . . . ?
O27_11 C10_11 C11_11 P20_11 2(2)       . . . . ?
C8_11  C7_11  C12_11 O13_11 -167.4(17) . . . . ?
C5_11  C7_11  C12_11 O13_11 13(2)      . . . . ?
C8_11  C7_11  C12_11 C11_11 2(2)       . . . . ?
C5_11  C7_11  C12_11 C11_11 -177.2(15) . . . . ?
C10_11 C11_11 C12_11 O13_11 167.7(15)  . . . . ?
P20_11 C11_11 C12_11 O13_11 -8.9(19)   . . . . ?
C10_11 C11_11 C12_11 C7_11  -2(2)      . . . . ?
P20_11 C11_11 C12_11 C7_11  -179.0(13) . . . . ?
C7_11  C12_11 O13_11 C14_11 129.9(17)  . . . . ?
C11_11 C12_11 O13_11 C14_11 -41(2)     . . . . ?
C12_11 O13_11 C14_11 C15_11 -134(2)    . . . . ?
C12_11 O13_11 C14_11 C19_11 44(2)      . . . . ?
O13_11 C14_11 C15_11 C16_11 174(2)     . . . . ?
C19_11 C14_11 C15_11 C16_11 -4(3)      . . . . ?
C14_11 C15_11 C16_11 C17_11 3(4)       . . . . ?
C15_11 C16_11 C17_11 C18_11 -4(3)      . . . . ?
C15_11 C16_11 C17_11 C36_11 174(2)     . . . . ?
C16_11 C17_11 C18_11 C19_11 6(2)       . . . . ?
C36_11 C17_11 C18_11 C19_11 -172.4(15) . . . . ?
C16_11 C17_11 C18_11 O28_11 -168.8(17) . . . . ?
C36_11 C17_11 C18_11 O28_11 13(2)      . . . . ?
O28_11 C18_11 C19_11 C14_11 167.7(16)  . . . . ?
C17_11 C18_11 C19_11 C14_11 -7(2)      . . . . ?
O28_11 C18_11 C19_11 P20_11 -5.9(19)   . . . . ?
C17_11 C18_11 C19_11 P20_11 179.2(13)  . . . . ?
C15_11 C14_11 C19_11 C18_11 7(2)       . . . . ?
O13_11 C14_11 C19_11 C18_11 -171.5(17) . . . . ?
C15_11 C14_11 C19_11 P20_11 -179.6(18) . . . . ?
O13_11 C14_11 C19_11 P20_11 2(2)       . . . . ?
C12_11 C11_11 P20_11 O29_11 -90.4(15)  . . . . ?
C10_11 C11_11 P20_11 O29_11 93.2(15)   . . . . ?
C12_11 C11_11 P20_11 C21_11 137.3(14)  . . . . ?
C10_11 C11_11 P20_11 C21_11 -39.0(14)  . . . . ?
C12_11 C11_11 P20_11 C19_11 42.2(14)   . . . . ?
C10_11 C11_11 P20_11 C19_11 -134.2(13) . . . . ?
C18_11 C19_11 P20_11 O29_11 -91.3(15)  . . . . ?
C14_11 C19_11 P20_11 O29_11 94.9(14)   . . . . ?
C18_11 C19_11 P20_11 C11_11 135.5(13)  . . . . ?
C14_11 C19_11 P20_11 C11_11 -38.3(14)  . . . . ?
C18_11 C19_11 P20_11 C21_11 40.2(14)   . . . . ?
C14_11 C19_11 P20_11 C21_11 -133.6(13) . . . . ?
O29_11 P20_11 C21_11 C22_11 96.0(15)   . . . . ?
C11_11 P20_11 C21_11 C22_11 -131.8(13) . . . . ?
C19_11 P20_11 C21_11 C22_11 -35.0(14)  . . . . ?
O29_11 P20_11 C21_11 C26_11 -90.1(15)  . . . . ?
C11_11 P20_11 C21_11 C26_11 42.2(14)   . . . . ?
C19_11 P20_11 C21_11 C26_11 139.0(13)  . . . . ?
C26_11 C21_11 C22_11 C23_11 5(2)       . . . . ?
P20_11 C21_11 C22_11 C23_11 178.7(16)  . . . . ?
C26_11 C21_11 C22_11 O28_11 -177.3(15) . . . . ?
P20_11 C21_11 C22_11 O28_11 -3.2(19)   . . . . ?
O28_11 C22_11 C23_11 C24_11 179.1(17)  . . . . ?
C21_11 C22_11 C23_11 C24_11 -3(3)      . . . . ?
C22_11 C23_11 C24_11 C25_11 4(3)       . . . . ?
C23_11 C24_11 C25_11 C26_11 -7(3)      . . . . ?
C23_11 C24_11 C25_11 C30_11 175.6(17)  . . . . ?
C24_11 C25_11 C26_11 O27_11 -164.0(17) . . . . ?
C30_11 C25_11 C26_11 O27_11 14(2)      . . . . ?
C24_11 C25_11 C26_11 C21_11 9(2)       . . . . ?
C30_11 C25_11 C26_11 C21_11 -173.6(15) . . . . ?
C22_11 C21_11 C26_11 O27_11 165.0(16)  . . . . ?
P20_11 C21_11 C26_11 O27_11 -9(2)      . . . . ?
C22_11 C21_11 C26_11 C25_11 -8(2)      . . . . ?
P20_11 C21_11 C26_11 C25_11 178.2(14)  . . . . ?
C9_11  C10_11 O27_11 C26_11 -133(2)    . . . . ?
C11_11 C10_11 O27_11 C26_11 44(2)      . . . . ?
C25_11 C26_11 O27_11 C10_11 132.3(17)  . . . . ?
C21_11 C26_11 O27_11 C10_11 -41(2)     . . . . ?
C23_11 C22_11 O28_11 C18_11 -131.6(18) . . . . ?
C21_11 C22_11 O28_11 C18_11 50(2)      . . . . ?
C19_11 C18_11 O28_11 C22_11 -45(2)     . . . . ?
C17_11 C18_11 O28_11 C22_11 130.0(17)  . . . . ?
C24_11 C25_11 C30_11 C35_11 -139.6(19) . . . . ?
C26_11 C25_11 C30_11 C35_11 43(2)      . . . . ?
C24_11 C25_11 C30_11 C31_11 37(2)      . . . . ?
C26_11 C25_11 C30_11 C31_11 -140.9(19) . . . . ?
C35_11 C30_11 C31_11 C32_11 -3(2)      . . . . ?
C25_11 C30_11 C31_11 C32_11 -179.8(16) . . . . ?
C30_11 C31_11 C32_11 C33_11 3(2)       . . . . ?
C31_11 C32_11 C33_11 N34_11 3(2)       . . . . ?
C32_11 C33_11 N34_11 C35_11 -9(3)      . . . . ?
C32_11 C33_11 N34_11 Pd6_10 177.9(13)  . . . . ?
C33_11 N34_11 C35_11 C30_11 9(3)       . . . . ?
Pd6_10 N34_11 C35_11 C30_11 -178.2(15) . . . . ?
C31_11 C30_11 C35_11 N34_11 -2(3)      . . . . ?
C25_11 C30_11 C35_11 N34_11 174.1(19)  . . . . ?
C16_11 C17_11 C36_11 C41_11 -136(2)    . . . . ?
C18_11 C17_11 C36_11 C41_11 42(2)      . . . . ?
C16_11 C17_11 C36_11 C37_11 45(2)      . . . . ?
C18_11 C17_11 C36_11 C37_11 -137(2)    . . . . ?
C41_11 C36_11 C37_11 C38_11 1(3)       . . . . ?
C17_11 C36_11 C37_11 C38_11 -179.6(19) . . . . ?
C36_11 C37_11 C38_11 C39_11 -1(2)      . . . . ?
C37_11 C38_11 C39_11 N40_11 0(2)       . . . . ?
C38_11 C39_11 N40_11 C41_11 1(3)       . . . . ?
C38_11 C39_11 N40_11 Pd4_10 -179.9(16) . . . . ?
C39_11 N40_11 C41_11 C36_11 -1(3)      . . . . ?
Pd4_10 N40_11 C41_11 C36_11 179.9(15)  . . . . ?
C37_11 C36_11 C41_11 N40_11 0(3)       . . . . ?
C17_11 C36_11 C41_11 N40_11 -179.1(19) . . . . ?
C6_12  N1_12  C2_12  C3_12  -3(3)      . . . . ?
Pd6_10 N1_12  C2_12  C3_12  177.1(18)  . . . . ?
N1_12  C2_12  C3_12  C4_12  -2(4)      . . . . ?
C2_12  C3_12  C4_12  C5_12  8(3)       . . . . ?
C3_12  C4_12  C5_12  C6_12  -8(3)      . . . . ?
C3_12  C4_12  C5_12  C7_12  176(2)     . . . . ?
C2_12  N1_12  C6_12  C5_12  3(2)       . . . . ?
Pd6_10 N1_12  C6_12  C5_12  -177.1(11) . . . . ?
C4_12  C5_12  C6_12  N1_12  2.1(19)    . . . . ?
C7_12  C5_12  C6_12  N1_12  178.0(15)  . . . . ?
C6_12  C5_12  C7_12  C8_12  -137.2(18) . . . . ?
C4_12  C5_12  C7_12  C8_12  39(2)      . . . . ?
C6_12  C5_12  C7_12  C12_12 40(2)      . . . . ?
C4_12  C5_12  C7_12  C12_12 -143.9(19) . . . . ?
C12_12 C7_12  C8_12  C9_12  -2(3)      . . . . ?
C5_12  C7_12  C8_12  C9_12  176(2)     . . . . ?
C7_12  C8_12  C9_12  C10_12 2(3)       . . . . ?
C8_12  C9_12  C10_12 O27_12 172(2)     . . . . ?
C8_12  C9_12  C10_12 C11_12 -4(3)      . . . . ?
C9_12  C10_12 C11_12 C12_12 6(2)       . . . . ?
O27_12 C10_12 C11_12 C12_12 -170.0(18) . . . . ?
C9_12  C10_12 C11_12 P20_12 178.2(18)  . . . . ?
O27_12 C10_12 C11_12 P20_12 3(2)       . . . . ?
C8_12  C7_12  C12_12 C11_12 3(2)       . . . . ?
C5_12  C7_12  C12_12 C11_12 -174.2(17) . . . . ?
C8_12  C7_12  C12_12 O13_12 -172.4(19) . . . . ?
C5_12  C7_12  C12_12 O13_12 10(2)      . . . . ?
C10_12 C11_12 C12_12 C7_12  -5(2)      . . . . ?
P20_12 C11_12 C12_12 C7_12  -177.9(16) . . . . ?
C10_12 C11_12 C12_12 O13_12 170.5(18)  . . . . ?
P20_12 C11_12 C12_12 O13_12 -2(2)      . . . . ?
C7_12  C12_12 O13_12 C14_12 131.9(18)  . . . . ?
C11_12 C12_12 O13_12 C14_12 -44(2)     . . . . ?
C12_12 O13_12 C14_12 C15_12 -135.4(19) . . . . ?
C12_12 O13_12 C14_12 C19_12 45(2)      . . . . ?
O13_12 C14_12 C15_12 C16_12 173(2)     . . . . ?
C19_12 C14_12 C15_12 C16_12 -7(3)      . . . . ?
C14_12 C15_12 C16_12 C17_12 9(4)       . . . . ?
C15_12 C16_12 C17_12 C18_12 -10(3)     . . . . ?
C15_12 C16_12 C17_12 C36_12 170(2)     . . . . ?
C16_12 C17_12 C18_12 O28_12 -167.9(19) . . . . ?
C36_12 C17_12 C18_12 O28_12 12(2)      . . . . ?
C16_12 C17_12 C18_12 C19_12 10(2)      . . . . ?
C36_12 C17_12 C18_12 C19_12 -170.4(15) . . . . ?
C15_12 C14_12 C19_12 C18_12 8(2)       . . . . ?
O13_12 C14_12 C19_12 C18_12 -172.2(15) . . . . ?
C15_12 C14_12 C19_12 P20_12 -177.4(15) . . . . ?
O13_12 C14_12 C19_12 P20_12 2.2(18)    . . . . ?
O28_12 C18_12 C19_12 C14_12 168.4(15)  . . . . ?
C17_12 C18_12 C19_12 C14_12 -9(2)      . . . . ?
O28_12 C18_12 C19_12 P20_12 -6(2)      . . . . ?
C17_12 C18_12 C19_12 P20_12 176.7(13)  . . . . ?
C12_12 C11_12 P20_12 O29_12 -92.9(18)  . . . . ?
C10_12 C11_12 P20_12 O29_12 94.8(18)   . . . . ?
C12_12 C11_12 P20_12 C21_12 135.0(15)  . . . . ?
C10_12 C11_12 P20_12 C21_12 -37.3(15)  . . . . ?
C12_12 C11_12 P20_12 C19_12 39.9(16)   . . . . ?
C10_12 C11_12 P20_12 C19_12 -132.4(14) . . . . ?
C14_12 C19_12 P20_12 O29_12 94.4(14)   . . . . ?
C18_12 C19_12 P20_12 O29_12 -91.1(16)  . . . . ?
C14_12 C19_12 P20_12 C11_12 -38.8(13)  . . . . ?
C18_12 C19_12 P20_12 C11_12 135.6(13)  . . . . ?
C14_12 C19_12 P20_12 C21_12 -135.7(12) . . . . ?
C18_12 C19_12 P20_12 C21_12 38.7(14)   . . . . ?
O29_12 P20_12 C21_12 C26_12 -95.1(16)  . . . . ?
C11_12 P20_12 C21_12 C26_12 38.0(15)   . . . . ?
C19_12 P20_12 C21_12 C26_12 134.7(14)  . . . . ?
O29_12 P20_12 C21_12 C22_12 95.1(16)   . . . . ?
C11_12 P20_12 C21_12 C22_12 -131.8(14) . . . . ?
C19_12 P20_12 C21_12 C22_12 -35.1(15)  . . . . ?
C26_12 C21_12 C22_12 O28_12 -171.6(18) . . . . ?
P20_12 C21_12 C22_12 O28_12 -2(2)      . . . . ?
C26_12 C21_12 C22_12 C23_12 1(2)       . . . . ?
P20_12 C21_12 C22_12 C23_12 170.5(16)  . . . . ?
O28_12 C22_12 C23_12 C24_12 -175.6(17) . . . . ?
C21_12 C22_12 C23_12 C24_12 12(3)      . . . . ?
C22_12 C23_12 C24_12 C25_12 -17(3)     . . . . ?
C23_12 C24_12 C25_12 C26_12 8(3)       . . . . ?
C23_12 C24_12 C25_12 C30_12 -174.0(18) . . . . ?
C22_12 C21_12 C26_12 O27_12 165.8(18)  . . . . ?
P20_12 C21_12 C26_12 O27_12 -4(2)      . . . . ?
C22_12 C21_12 C26_12 C25_12 -10(2)     . . . . ?
P20_12 C21_12 C26_12 C25_12 -179.9(14) . . . . ?
C24_12 C25_12 C26_12 C21_12 6(2)       . . . . ?
C30_12 C25_12 C26_12 C21_12 -172.3(16) . . . . ?
C24_12 C25_12 C26_12 O27_12 -170.7(17) . . . . ?
C30_12 C25_12 C26_12 O27_12 12(2)      . . . . ?
C21_12 C26_12 O27_12 C10_12 -42(2)     . . . . ?
C25_12 C26_12 O27_12 C10_12 134.0(18)  . . . . ?
C9_12  C10_12 O27_12 C26_12 -134(2)    . . . . ?
C11_12 C10_12 O27_12 C26_12 42(2)      . . . . ?
C23_12 C22_12 O28_12 C18_12 -125.9(19) . . . . ?
C21_12 C22_12 O28_12 C18_12 47(2)      . . . . ?
C17_12 C18_12 O28_12 C22_12 135.0(18)  . . . . ?
C19_12 C18_12 O28_12 C22_12 -42(2)     . . . . ?
C24_12 C25_12 C30_12 C35_12 -132(2)    . . . . ?
C26_12 C25_12 C30_12 C35_12 46(2)      . . . . ?
C24_12 C25_12 C30_12 C31_12 44(2)      . . . . ?
C26_12 C25_12 C30_12 C31_12 -138.8(19) . . . . ?
C35_12 C30_12 C31_12 C32_12 -3(3)      . . . . ?
C25_12 C30_12 C31_12 C32_12 -178.2(18) . . . . ?
C30_12 C31_12 C32_12 C33_12 1(2)       . . . . ?
C31_12 C32_12 C33_12 N34_12 3(2)       . . . . ?
C32_12 C33_12 N34_12 C35_12 -4(3)      . . . . ?
C32_12 C33_12 N34_12 Pd3_10 179.4(14)  . . . . ?
C33_12 N34_12 C35_12 C30_12 3(3)       . . . . ?
Pd3_10 N34_12 C35_12 C30_12 178.9(14)  . . . . ?
C31_12 C30_12 C35_12 N34_12 1(3)       . . . . ?
C25_12 C30_12 C35_12 N34_12 176.5(18)  . . . . ?
C16_12 C17_12 C36_12 C41_12 -141(2)    . . . . ?
C18_12 C17_12 C36_12 C41_12 39(2)      . . . . ?
C16_12 C17_12 C36_12 C37_12 41(2)      . . . . ?
C18_12 C17_12 C36_12 C37_12 -138.8(18) . . . . ?
C41_12 C36_12 C37_12 C38_12 4(2)       . . . . ?
C17_12 C36_12 C37_12 C38_12 -178.5(16) . . . . ?
C36_12 C37_12 C38_12 C39_12 1(2)       . . . . ?
C37_12 C38_12 C39_12 N40_12 -4(2)      . . . . ?
C38_12 C39_12 N40_12 C41_12 2(2)       . . . . ?
C38_12 C39_12 N40_12 Pd4_10 177.7(13)  . . . . ?
C39_12 N40_12 C41_12 C36_12 3(2)       . . . . ?
Pd4_10 N40_12 C41_12 C36_12 -172.8(12) . . . . ?
C37_12 C36_12 C41_12 N40_12 -6(2)      . . . . ?
C17_12 C36_12 C41_12 N40_12 176.7(16)  . . . . ?
C6_13  N1_13  C2_13  C3_13  8(4)       . . . . ?
Pd6_10 N1_13  C2_13  C3_13  178(2)     . . . . ?
N1_13  C2_13  C3_13  C4_13  -7(5)      . . . . ?
C2_13  C3_13  C4_13  C5_13  2(4)       . . . . ?
C3_13  C4_13  C5_13  C6_13  1(3)       . . . . ?
C3_13  C4_13  C5_13  C7_13  -180(2)    . . . . ?
C2_13  N1_13  C6_13  C5_13  -4(2)      . . . . ?
Pd6_10 N1_13  C6_13  C5_13  -173.9(12) . . . . ?
C4_13  C5_13  C6_13  N1_13  -1(2)      . . . . ?
C7_13  C5_13  C6_13  N1_13  -179.5(16) . . . . ?
C6_13  C5_13  C7_13  C8_13  -136.9(18) . . . . ?
C4_13  C5_13  C7_13  C8_13  44(2)      . . . . ?
C6_13  C5_13  C7_13  C12_13 45(2)      . . . . ?
C4_13  C5_13  C7_13  C12_13 -134.2(18) . . . . ?
C12_13 C7_13  C8_13  C9_13  -9(3)      . . . . ?
C5_13  C7_13  C8_13  C9_13  172.6(19)  . . . . ?
C7_13  C8_13  C9_13  C10_13 6(3)       . . . . ?
C8_13  C9_13  C10_13 O27_13 176.7(18)  . . . . ?
C8_13  C9_13  C10_13 C11_13 -4(3)      . . . . ?
C9_13  C10_13 C11_13 C12_13 6(2)       . . . . ?
O27_13 C10_13 C11_13 C12_13 -175.4(13) . . . . ?
C9_13  C10_13 C11_13 P20_13 175.8(15)  . . . . ?
O27_13 C10_13 C11_13 P20_13 -5.2(17)   . . . . ?
C10_13 C11_13 C12_13 O13_13 167.0(14)  . . . . ?
P20_13 C11_13 C12_13 O13_13 -3.0(18)   . . . . ?
C10_13 C11_13 C12_13 C7_13  -8.3(19)   . . . . ?
P20_13 C11_13 C12_13 C7_13  -178.4(12) . . . . ?
C8_13  C7_13  C12_13 O13_13 -165.6(16) . . . . ?
C5_13  C7_13  C12_13 O13_13 13(2)      . . . . ?
C8_13  C7_13  C12_13 C11_13 10(2)      . . . . ?
C5_13  C7_13  C12_13 C11_13 -171.7(14) . . . . ?
C11_13 C12_13 O13_13 C14_13 -41(2)     . . . . ?
C7_13  C12_13 O13_13 C14_13 134.7(16)  . . . . ?
C12_13 O13_13 C14_13 C15_13 -137.9(18) . . . . ?
C12_13 O13_13 C14_13 C19_13 40(2)      . . . . ?
C19_13 C14_13 C15_13 C16_13 1(3)       . . . . ?
O13_13 C14_13 C15_13 C16_13 179.7(17)  . . . . ?
C14_13 C15_13 C16_13 C17_13 -1(3)      . . . . ?
C15_13 C16_13 C17_13 C18_13 -6(2)      . . . . ?
C15_13 C16_13 C17_13 C36_13 175.9(16)  . . . . ?
C16_13 C17_13 C18_13 O28_13 -167.0(17) . . . . ?
C36_13 C17_13 C18_13 O28_13 11(2)      . . . . ?
C16_13 C17_13 C18_13 C19_13 12(2)      . . . . ?
C36_13 C17_13 C18_13 C19_13 -170.4(14) . . . . ?
C15_13 C14_13 C19_13 C18_13 5(2)       . . . . ?
O13_13 C14_13 C19_13 C18_13 -173.5(16) . . . . ?
C15_13 C14_13 C19_13 P20_13 -177.6(16) . . . . ?
O13_13 C14_13 C19_13 P20_13 4(2)       . . . . ?
O28_13 C18_13 C19_13 C14_13 167.6(16)  . . . . ?
C17_13 C18_13 C19_13 C14_13 -11(2)     . . . . ?
O28_13 C18_13 C19_13 P20_13 -10(2)     . . . . ?
C17_13 C18_13 C19_13 P20_13 171.2(12)  . . . . ?
C14_13 C19_13 P20_13 O29_13 92.9(16)   . . . . ?
C18_13 C19_13 P20_13 O29_13 -89.4(15)  . . . . ?
C14_13 C19_13 P20_13 C11_13 -38.2(14)  . . . . ?
C18_13 C19_13 P20_13 C11_13 139.6(12)  . . . . ?
C14_13 C19_13 P20_13 C21_13 -136.4(14) . . . . ?
C18_13 C19_13 P20_13 C21_13 41.3(13)   . . . . ?
C12_13 C11_13 P20_13 O29_13 -93.2(14)  . . . . ?
C10_13 C11_13 P20_13 O29_13 96.6(14)   . . . . ?
C12_13 C11_13 P20_13 C19_13 38.0(13)   . . . . ?
C10_13 C11_13 P20_13 C19_13 -132.2(12) . . . . ?
C12_13 C11_13 P20_13 C21_13 133.2(12)  . . . . ?
C10_13 C11_13 P20_13 C21_13 -37.0(13)  . . . . ?
O29_13 P20_13 C21_13 C22_13 94.0(16)   . . . . ?
C19_13 P20_13 C21_13 C22_13 -36.2(15)  . . . . ?
C11_13 P20_13 C21_13 C22_13 -133.0(14) . . . . ?
O29_13 P20_13 C21_13 C26_13 -90.9(15)  . . . . ?
C19_13 P20_13 C21_13 C26_13 138.9(13)  . . . . ?
C11_13 P20_13 C21_13 C26_13 42.1(13)   . . . . ?
C26_13 C21_13 C22_13 C23_13 3(2)       . . . . ?
P20_13 C21_13 C22_13 C23_13 177.4(17)  . . . . ?
C26_13 C21_13 C22_13 O28_13 -177.0(16) . . . . ?
P20_13 C21_13 C22_13 O28_13 -2(2)      . . . . ?
C21_13 C22_13 C23_13 C24_13 5(3)       . . . . ?
O28_13 C22_13 C23_13 C24_13 -175(2)    . . . . ?
C22_13 C23_13 C24_13 C25_13 -8(4)      . . . . ?
C23_13 C24_13 C25_13 C26_13 2(3)       . . . . ?
C23_13 C24_13 C25_13 C30_13 -177(2)    . . . . ?
C24_13 C25_13 C26_13 O27_13 -170.5(18) . . . . ?
C30_13 C25_13 C26_13 O27_13 9(2)       . . . . ?
C24_13 C25_13 C26_13 C21_13 6(2)       . . . . ?
C30_13 C25_13 C26_13 C21_13 -174.9(14) . . . . ?
C22_13 C21_13 C26_13 O27_13 168.1(16)  . . . . ?
P20_13 C21_13 C26_13 O27_13 -7.0(19)   . . . . ?
C22_13 C21_13 C26_13 C25_13 -8(2)      . . . . ?
P20_13 C21_13 C26_13 C25_13 176.4(13)  . . . . ?
C9_13  C10_13 O27_13 C26_13 -129.0(18) . . . . ?
C11_13 C10_13 O27_13 C26_13 52.0(19)   . . . . ?
C25_13 C26_13 O27_13 C10_13 131.3(16)  . . . . ?
C21_13 C26_13 O27_13 C10_13 -45(2)     . . . . ?
C17_13 C18_13 O28_13 C22_13 139.3(16)  . . . . ?
C19_13 C18_13 O28_13 C22_13 -39(2)     . . . . ?
C23_13 C22_13 O28_13 C18_13 -133.6(19) . . . . ?
C21_13 C22_13 O28_13 C18_13 46(2)      . . . . ?
C24_13 C25_13 C30_13 C31_13 51(2)      . . . . ?
C26_13 C25_13 C30_13 C31_13 -128.4(18) . . . . ?
C24_13 C25_13 C30_13 C35_13 -135(2)    . . . . ?
C26_13 C25_13 C30_13 C35_13 46(2)      . . . . ?
C35_13 C30_13 C31_13 C32_13 5(2)       . . . . ?
C25_13 C30_13 C31_13 C32_13 179.4(17)  . . . . ?
C30_13 C31_13 C32_13 C33_13 -1(2)      . . . . ?
C31_13 C32_13 C33_13 N34_13 1(2)       . . . . ?
C32_13 C33_13 N34_13 C35_13 -5(3)      . . . . ?
C32_13 C33_13 N34_13 Pd5_10 -179.2(15) . . . . ?
C33_13 N34_13 C35_13 C30_13 9(3)       . . . . ?
Pd5_10 N34_13 C35_13 C30_13 -176.3(15) . . . . ?
C31_13 C30_13 C35_13 N34_13 -9(3)      . . . . ?
C25_13 C30_13 C35_13 N34_13 176.1(19)  . . . . ?
C16_13 C17_13 C36_13 C41_13 -132.7(17) . . . . ?
C18_13 C17_13 C36_13 C41_13 49(2)      . . . . ?
C16_13 C17_13 C36_13 C37_13 45(2)      . . . . ?
C18_13 C17_13 C36_13 C37_13 -133.2(17) . . . . ?
C41_13 C36_13 C37_13 C38_13 4(2)       . . . . ?
C17_13 C36_13 C37_13 C38_13 -173.0(16) . . . . ?
C36_13 C37_13 C38_13 C39_13 -3(2)      . . . . ?
C37_13 C38_13 C39_13 N40_13 0(2)       . . . . ?
C38_13 C39_13 N40_13 C41_13 1(3)       . . . . ?
C38_13 C39_13 N40_13 Pd3_10 178.3(13)  . . . . ?
C39_13 N40_13 C41_13 C36_13 0(2)       . . . . ?
Pd3_10 N40_13 C41_13 C36_13 -176.8(12) . . . . ?
C37_13 C36_13 C41_13 N40_13 -3(2)      . . . . ?
C17_13 C36_13 C41_13 N40_13 174.4(15)  . . . . ?
C6_14  N1_14  C2_14  C3_14  -15(3)     . . . . ?
Pd6_10 N1_14  C2_14  C3_14  169(2)     . . . . ?
N1_14  C2_14  C3_14  C4_14  17(4)      . . . . ?
C2_14  C3_14  C4_14  C5_14  -10(4)     . . . . ?
C3_14  C4_14  C5_14  C6_14  2(3)       . . . . ?
C3_14  C4_14  C5_14  C7_14  -173(2)    . . . . ?
C2_14  N1_14  C6_14  C5_14  6(2)       . . . . ?
Pd6_10 N1_14  C6_14  C5_14  -178.4(12) . . . . ?
C4_14  C5_14  C6_14  N1_14  0(2)       . . . . ?
C7_14  C5_14  C6_14  N1_14  175.2(16)  . . . . ?
C6_14  C5_14  C7_14  C8_14  -136(2)    . . . . ?
C4_14  C5_14  C7_14  C8_14  39(3)      . . . . ?
C6_14  C5_14  C7_14  C12_14 47(2)      . . . . ?
C4_14  C5_14  C7_14  C12_14 -138(2)    . . . . ?
C12_14 C7_14  C8_14  C9_14  -11(3)     . . . . ?
C5_14  C7_14  C8_14  C9_14  171(2)     . . . . ?
C7_14  C8_14  C9_14  C10_14 7(4)       . . . . ?
C8_14  C9_14  C10_14 C11_14 -2(3)      . . . . ?
C8_14  C9_14  C10_14 O27_14 171(2)     . . . . ?
C9_14  C10_14 C11_14 C12_14 2(2)       . . . . ?
O27_14 C10_14 C11_14 C12_14 -170.7(17) . . . . ?
C9_14  C10_14 C11_14 P20_14 175.6(18)  . . . . ?
O27_14 C10_14 C11_14 P20_14 3(2)       . . . . ?
C10_14 C11_14 C12_14 O13_14 170.7(19)  . . . . ?
P20_14 C11_14 C12_14 O13_14 -3(2)      . . . . ?
C10_14 C11_14 C12_14 C7_14  -7(2)      . . . . ?
P20_14 C11_14 C12_14 C7_14  179.5(15)  . . . . ?
C8_14  C7_14  C12_14 C11_14 12(2)      . . . . ?
C5_14  C7_14  C12_14 C11_14 -171.0(16) . . . . ?
C8_14  C7_14  C12_14 O13_14 -166(2)    . . . . ?
C5_14  C7_14  C12_14 O13_14 11(2)      . . . . ?
C11_14 C12_14 O13_14 C14_14 -47(3)     . . . . ?
C7_14  C12_14 O13_14 C14_14 131(2)     . . . . ?
C12_14 O13_14 C14_14 C15_14 -137(3)    . . . . ?
C12_14 O13_14 C14_14 C19_14 45(3)      . . . . ?
O13_14 C14_14 C15_14 C16_14 -172(3)    . . . . ?
C19_14 C14_14 C15_14 C16_14 6(4)       . . . . ?
C14_14 C15_14 C16_14 C17_14 -16(5)     . . . . ?
C15_14 C16_14 C17_14 C18_14 11(4)      . . . . ?
C15_14 C16_14 C17_14 C36_14 -168(3)    . . . . ?
C16_14 C17_14 C18_14 O28_14 -174(2)    . . . . ?
C36_14 C17_14 C18_14 O28_14 5(3)       . . . . ?
C16_14 C17_14 C18_14 C19_14 4(3)       . . . . ?
C36_14 C17_14 C18_14 C19_14 -177.1(17) . . . . ?
C15_14 C14_14 C19_14 C18_14 9(3)       . . . . ?
O13_14 C14_14 C19_14 C18_14 -173.3(18) . . . . ?
C15_14 C14_14 C19_14 P20_14 -175(2)    . . . . ?
O13_14 C14_14 C19_14 P20_14 3(2)       . . . . ?
O28_14 C18_14 C19_14 C14_14 164.0(19)  . . . . ?
C17_14 C18_14 C19_14 C14_14 -14(2)     . . . . ?
O28_14 C18_14 C19_14 P20_14 -12(2)     . . . . ?
C17_14 C18_14 C19_14 P20_14 169.8(15)  . . . . ?
C12_14 C11_14 P20_14 O29_14 -96.5(18)  . . . . ?
C10_14 C11_14 P20_14 O29_14 90.0(17)   . . . . ?
C12_14 C11_14 P20_14 C21_14 133.3(15)  . . . . ?
C10_14 C11_14 P20_14 C21_14 -40.3(15)  . . . . ?
C12_14 C11_14 P20_14 C19_14 38.6(15)   . . . . ?
C10_14 C11_14 P20_14 C19_14 -134.9(15) . . . . ?
C14_14 C19_14 P20_14 O29_14 101.3(16)  . . . . ?
C18_14 C19_14 P20_14 O29_14 -82.2(16)  . . . . ?
C14_14 C19_14 P20_14 C11_14 -38.1(15)  . . . . ?
C18_14 C19_14 P20_14 C11_14 138.3(14)  . . . . ?
C14_14 C19_14 P20_14 C21_14 -133.6(14) . . . . ?
C18_14 C19_14 P20_14 C21_14 42.8(15)   . . . . ?
O29_14 P20_14 C21_14 C26_14 -95.8(16)  . . . . ?
C11_14 P20_14 C21_14 C26_14 41.4(16)   . . . . ?
C19_14 P20_14 C21_14 C26_14 136.6(15)  . . . . ?
O29_14 P20_14 C21_14 C22_14 89.8(16)   . . . . ?
C11_14 P20_14 C21_14 C22_14 -133.0(15) . . . . ?
C19_14 P20_14 C21_14 C22_14 -37.8(16)  . . . . ?
C26_14 C21_14 C22_14 C23_14 5(2)       . . . . ?
P20_14 C21_14 C22_14 C23_14 178.9(17)  . . . . ?
C26_14 C21_14 C22_14 O28_14 -171.8(19) . . . . ?
P20_14 C21_14 C22_14 O28_14 2(2)       . . . . ?
O28_14 C22_14 C23_14 C24_14 176(2)     . . . . ?
C21_14 C22_14 C23_14 C24_14 -1(3)      . . . . ?
C22_14 C23_14 C24_14 C25_14 -1(3)      . . . . ?
C23_14 C24_14 C25_14 C26_14 -2(3)      . . . . ?
C23_14 C24_14 C25_14 C30_14 179.4(19)  . . . . ?
C22_14 C21_14 C26_14 O27_14 169.3(19)  . . . . ?
P20_14 C21_14 C26_14 O27_14 -5(2)      . . . . ?
C22_14 C21_14 C26_14 C25_14 -8(2)      . . . . ?
P20_14 C21_14 C26_14 C25_14 178.3(15)  . . . . ?
C24_14 C25_14 C26_14 C21_14 6(2)       . . . . ?
C30_14 C25_14 C26_14 C21_14 -175.3(16) . . . . ?
C24_14 C25_14 C26_14 O27_14 -171.0(18) . . . . ?
C30_14 C25_14 C26_14 O27_14 8(2)       . . . . ?
C21_14 C26_14 O27_14 C10_14 -43(2)     . . . . ?
C25_14 C26_14 O27_14 C10_14 134.0(17)  . . . . ?
C9_14  C10_14 O27_14 C26_14 -129(2)    . . . . ?
C11_14 C10_14 O27_14 C26_14 44(2)      . . . . ?
C23_14 C22_14 O28_14 C18_14 -135(2)    . . . . ?
C21_14 C22_14 O28_14 C18_14 42(3)      . . . . ?
C19_14 C18_14 O28_14 C22_14 -36(3)     . . . . ?
C17_14 C18_14 O28_14 C22_14 142(2)     . . . . ?
C24_14 C25_14 C30_14 C35_14 -121(2)    . . . . ?
C26_14 C25_14 C30_14 C35_14 60(2)      . . . . ?
C24_14 C25_14 C30_14 C31_14 53(3)      . . . . ?
C26_14 C25_14 C30_14 C31_14 -125(2)    . . . . ?
C35_14 C30_14 C31_14 C32_14 -2(3)      . . . . ?
C25_14 C30_14 C31_14 C32_14 -176.3(19) . . . . ?
C30_14 C31_14 C32_14 C33_14 -1(2)      . . . . ?
C31_14 C32_14 C33_14 N34_14 0(2)       . . . . ?
C32_14 C33_14 N34_14 C35_14 6(3)       . . . . ?
C32_14 C33_14 N34_14 Pd1_10 -176.5(16) . . . . ?
C33_14 N34_14 C35_14 C30_14 -9(3)      . . . . ?
Pd1_10 N34_14 C35_14 C30_14 172.8(14)  . . . . ?
C31_14 C30_14 C35_14 N34_14 7(3)       . . . . ?
C25_14 C30_14 C35_14 N34_14 -178.0(17) . . . . ?
C16_14 C17_14 C36_14 C41_14 -120(3)    . . . . ?
C18_14 C17_14 C36_14 C41_14 61(2)      . . . . ?
C16_14 C17_14 C36_14 C37_14 59(3)      . . . . ?
C18_14 C17_14 C36_14 C37_14 -120(2)    . . . . ?
C41_14 C36_14 C37_14 C38_14 1(3)       . . . . ?
C17_14 C36_14 C37_14 C38_14 -178.3(19) . . . . ?
C36_14 C37_14 C38_14 C39_14 -2(2)      . . . . ?
C37_14 C38_14 C39_14 N40_14 0(2)       . . . . ?
C38_14 C39_14 N40_14 C41_14 3(3)       . . . . ?
C38_14 C39_14 N40_14 Pd5_10 -178.5(16) . . . . ?
C39_14 N40_14 C41_14 C36_14 -5(4)      . . . . ?
Pd5_10 N40_14 C41_14 C36_14 177.1(18)  . . . . ?
C37_14 C36_14 C41_14 N40_14 2(3)       . . . . ?
C17_14 C36_14 C41_14 N40_14 -178(2)    . . . . ?
C6_15  N1_15  C2_15  C3_15  -6(3)      . . . . ?
Pd5_10 N1_15  C2_15  C3_15  174(2)     . . . . ?
N1_15  C2_15  C3_15  C4_15  6(4)       . . . . ?
C2_15  C3_15  C4_15  C5_15  -4(4)      . . . . ?
C3_15  C4_15  C5_15  C6_15  1(3)       . . . . ?
C3_15  C4_15  C5_15  C7_15  -177(2)    . . . . ?
C2_15  N1_15  C6_15  C5_15  3(2)       . . . . ?
Pd5_10 N1_15  C6_15  C5_15  -177.5(13) . . . . ?
C4_15  C5_15  C6_15  N1_15  -1(2)      . . . . ?
C7_15  C5_15  C6_15  N1_15  177.7(17)  . . . . ?
C6_15  C5_15  C7_15  C8_15  -139.7(18) . . . . ?
C4_15  C5_15  C7_15  C8_15  39(2)      . . . . ?
C6_15  C5_15  C7_15  C12_15 42(2)      . . . . ?
C4_15  C5_15  C7_15  C12_15 -139.4(18) . . . . ?
C12_15 C7_15  C8_15  C9_15  -9(3)      . . . . ?
C5_15  C7_15  C8_15  C9_15  173.4(19)  . . . . ?
C7_15  C8_15  C9_15  C10_15 8(3)       . . . . ?
C8_15  C9_15  C10_15 O27_15 175.4(18)  . . . . ?
C8_15  C9_15  C10_15 C11_15 -7(3)      . . . . ?
C9_15  C10_15 C11_15 C12_15 6(2)       . . . . ?
O27_15 C10_15 C11_15 C12_15 -176.0(15) . . . . ?
C9_15  C10_15 C11_15 P20_15 -179.3(15) . . . . ?
O27_15 C10_15 C11_15 P20_15 -1.4(19)   . . . . ?
C8_15  C7_15  C12_15 O13_15 -166.1(17) . . . . ?
C5_15  C7_15  C12_15 O13_15 12(2)      . . . . ?
C8_15  C7_15  C12_15 C11_15 8(2)       . . . . ?
C5_15  C7_15  C12_15 C11_15 -174.0(15) . . . . ?
C10_15 C11_15 C12_15 C7_15  -7(2)      . . . . ?
P20_15 C11_15 C12_15 C7_15  178.7(14)  . . . . ?
C10_15 C11_15 C12_15 O13_15 167.5(15)  . . . . ?
P20_15 C11_15 C12_15 O13_15 -7.0(19)   . . . . ?
C7_15  C12_15 O13_15 C14_15 133.8(16)  . . . . ?
C11_15 C12_15 O13_15 C14_15 -41(2)     . . . . ?
C12_15 O13_15 C14_15 C15_15 -128.1(16) . . . . ?
C12_15 O13_15 C14_15 C19_15 45(2)      . . . . ?
C19_15 C14_15 C15_15 C16_15 5(2)       . . . . ?
O13_15 C14_15 C15_15 C16_15 178.5(15)  . . . . ?
C14_15 C15_15 C16_15 C17_15 -5(3)      . . . . ?
C15_15 C16_15 C17_15 C18_15 0(2)       . . . . ?
C15_15 C16_15 C17_15 C36_15 -178.0(16) . . . . ?
C16_15 C17_15 C18_15 O28_15 -167.9(15) . . . . ?
C36_15 C17_15 C18_15 O28_15 10(2)      . . . . ?
C16_15 C17_15 C18_15 C19_15 5(2)       . . . . ?
C36_15 C17_15 C18_15 C19_15 -176.8(13) . . . . ?
C15_15 C14_15 C19_15 C18_15 -1(2)      . . . . ?
O13_15 C14_15 C19_15 C18_15 -173.5(14) . . . . ?
C15_15 C14_15 C19_15 P20_15 172.9(14)  . . . . ?
O13_15 C14_15 C19_15 P20_15 0(2)       . . . . ?
O28_15 C18_15 C19_15 C14_15 168.2(15)  . . . . ?
C17_15 C18_15 C19_15 C14_15 -5(2)      . . . . ?
O28_15 C18_15 C19_15 P20_15 -5.4(18)   . . . . ?
C17_15 C18_15 C19_15 P20_15 -178.5(12) . . . . ?
C14_15 C19_15 P20_15 O29_15 94.4(17)   . . . . ?
C18_15 C19_15 P20_15 O29_15 -92.2(17)  . . . . ?
C14_15 C19_15 P20_15 C11_15 -36.9(14)  . . . . ?
C18_15 C19_15 P20_15 C11_15 136.4(13)  . . . . ?
C14_15 C19_15 P20_15 C21_15 -133.4(14) . . . . ?
C18_15 C19_15 P20_15 C21_15 40.0(14)   . . . . ?
C12_15 C11_15 P20_15 O29_15 -91.6(15)  . . . . ?
C10_15 C11_15 P20_15 O29_15 94.0(15)   . . . . ?
C12_15 C11_15 P20_15 C19_15 40.2(14)   . . . . ?
C10_15 C11_15 P20_15 C19_15 -134.2(13) . . . . ?
C12_15 C11_15 P20_15 C21_15 138.4(13)  . . . . ?
C10_15 C11_15 P20_15 C21_15 -36.0(14)  . . . . ?
O29_15 P20_15 C21_15 C22_15 93.1(15)   . . . . ?
C19_15 P20_15 C21_15 C22_15 -40.3(13)  . . . . ?
C11_15 P20_15 C21_15 C22_15 -136.1(12) . . . . ?
O29_15 P20_15 C21_15 C26_15 -93.4(16)  . . . . ?
C19_15 P20_15 C21_15 C26_15 133.3(13)  . . . . ?
C11_15 P20_15 C21_15 C26_15 37.4(14)   . . . . ?
C26_15 C21_15 C22_15 C23_15 11(2)      . . . . ?
P20_15 C21_15 C22_15 C23_15 -175.4(17) . . . . ?
C26_15 C21_15 C22_15 O28_15 -167.3(14) . . . . ?
P20_15 C21_15 C22_15 O28_15 6.4(18)    . . . . ?
O28_15 C22_15 C23_15 C24_15 161(2)     . . . . ?
C21_15 C22_15 C23_15 C24_15 -17(3)     . . . . ?
C22_15 C23_15 C24_15 C25_15 20(3)      . . . . ?
C23_15 C24_15 C25_15 C26_15 -15(2)     . . . . ?
C23_15 C24_15 C25_15 C30_15 166.5(18)  . . . . ?
C24_15 C25_15 C26_15 O27_15 -172.2(14) . . . . ?
C30_15 C25_15 C26_15 O27_15 7(2)       . . . . ?
C24_15 C25_15 C26_15 C21_15 9.4(19)    . . . . ?
C30_15 C25_15 C26_15 C21_15 -171.8(13) . . . . ?
C22_15 C21_15 C26_15 O27_15 174.0(14)  . . . . ?
P20_15 C21_15 C26_15 O27_15 0.6(18)    . . . . ?
C22_15 C21_15 C26_15 C25_15 -8(2)      . . . . ?
P20_15 C21_15 C26_15 C25_15 179.0(12)  . . . . ?
C25_15 C26_15 O27_15 C10_15 131.2(14)  . . . . ?
C21_15 C26_15 O27_15 C10_15 -50.3(17)  . . . . ?
C9_15  C10_15 O27_15 C26_15 -131.1(18) . . . . ?
C11_15 C10_15 O27_15 C26_15 51.0(19)   . . . . ?
C23_15 C22_15 O28_15 C18_15 -137(2)    . . . . ?
C21_15 C22_15 O28_15 C18_15 41(2)      . . . . ?
C19_15 C18_15 O28_15 C22_15 -41(2)     . . . . ?
C17_15 C18_15 O28_15 C22_15 131.8(16)  . . . . ?
C24_15 C25_15 C30_15 C35_15 -137.7(16) . . . . ?
C26_15 C25_15 C30_15 C35_15 44(2)      . . . . ?
C24_15 C25_15 C30_15 C31_15 42(2)      . . . . ?
C26_15 C25_15 C30_15 C31_15 -136.5(17) . . . . ?
C35_15 C30_15 C31_15 C32_15 1(2)       . . . . ?
C25_15 C30_15 C31_15 C32_15 -179.0(17) . . . . ?
C30_15 C31_15 C32_15 C33_15 0(2)       . . . . ?
C31_15 C32_15 C33_15 N34_15 -2(2)      . . . . ?
C32_15 C33_15 N34_15 C35_15 2(3)       . . . . ?
C32_15 C33_15 N34_15 Pd1_10 175.8(15)  . . . . ?
C33_15 N34_15 C35_15 C30_15 -1(3)      . . . . ?
Pd1_10 N34_15 C35_15 C30_15 -174.6(12) . . . . ?
C31_15 C30_15 C35_15 N34_15 -1(2)      . . . . ?
C25_15 C30_15 C35_15 N34_15 179.2(15)  . . . . ?
C16_15 C17_15 C36_15 C37_15 41(2)      . . . . ?
C18_15 C17_15 C36_15 C37_15 -136.8(16) . . . . ?
C16_15 C17_15 C36_15 C41_15 -141.5(18) . . . . ?
C18_15 C17_15 C36_15 C41_15 40.4(19)   . . . . ?
C41_15 C36_15 C37_15 C38_15 4(2)       . . . . ?
C17_15 C36_15 C37_15 C38_15 -178.3(15) . . . . ?
C36_15 C37_15 C38_15 C39_15 -1(2)      . . . . ?
C37_15 C38_15 C39_15 N40_15 -1(2)      . . . . ?
C38_15 C39_15 N40_15 C41_15 0(3)       . . . . ?
C38_15 C39_15 N40_15 Pd2_10 -178.8(13) . . . . ?
C39_15 N40_15 C41_15 C36_15 3(3)       . . . . ?
Pd2_10 N40_15 C41_15 C36_15 -177.8(13) . . . . ?
C37_15 C36_15 C41_15 N40_15 -6(3)      . . . . ?
C17_15 C36_15 C41_15 N40_15 177.0(17)  . . . . ?
C6_16  N1_16  C2_16  C3_16  7(3)       . . . . ?
Pd5_10 N1_16  C2_16  C3_16  -178(2)    . . . . ?
N1_16  C2_16  C3_16  C4_16  -3(4)      . . . . ?
C2_16  C3_16  C4_16  C5_16  -4(4)      . . . . ?
C3_16  C4_16  C5_16  C6_16  6(3)       . . . . ?
C3_16  C4_16  C5_16  C7_16  -175(2)    . . . . ?
C2_16  N1_16  C6_16  C5_16  -4(2)      . . . . ?
Pd5_10 N1_16  C6_16  C5_16  -179.6(11) . . . . ?
C4_16  C5_16  C6_16  N1_16  -1.6(18)   . . . . ?
C7_16  C5_16  C6_16  N1_16  179.2(14)  . . . . ?
C4_16  C5_16  C7_16  C8_16  46(2)      . . . . ?
C6_16  C5_16  C7_16  C8_16  -135.2(16) . . . . ?
C4_16  C5_16  C7_16  C12_16 -138.8(18) . . . . ?
C6_16  C5_16  C7_16  C12_16 40(2)      . . . . ?
C12_16 C7_16  C8_16  C9_16  -6(2)      . . . . ?
C5_16  C7_16  C8_16  C9_16  170.1(18)  . . . . ?
C7_16  C8_16  C9_16  C10_16 5(3)       . . . . ?
C8_16  C9_16  C10_16 C11_16 -4(3)      . . . . ?
C8_16  C9_16  C10_16 O27_16 172.6(19)  . . . . ?
C9_16  C10_16 C11_16 C12_16 4(2)       . . . . ?
O27_16 C10_16 C11_16 C12_16 -172.7(17) . . . . ?
C9_16  C10_16 C11_16 P20_16 178.1(17)  . . . . ?
O27_16 C10_16 C11_16 P20_16 1(2)       . . . . ?
C8_16  C7_16  C12_16 O13_16 -171.3(16) . . . . ?
C5_16  C7_16  C12_16 O13_16 13(2)      . . . . ?
C8_16  C7_16  C12_16 C11_16 5(2)       . . . . ?
C5_16  C7_16  C12_16 C11_16 -171.0(14) . . . . ?
C10_16 C11_16 C12_16 O13_16 171.9(16)  . . . . ?
P20_16 C11_16 C12_16 O13_16 -2.2(19)   . . . . ?
C10_16 C11_16 C12_16 C7_16  -4(2)      . . . . ?
P20_16 C11_16 C12_16 C7_16  -178.4(13) . . . . ?
C7_16  C12_16 O13_16 C14_16 131.2(16)  . . . . ?
C11_16 C12_16 O13_16 C14_16 -45(2)     . . . . ?
C12_16 O13_16 C14_16 C15_16 -129.8(18) . . . . ?
C12_16 O13_16 C14_16 C19_16 43(2)      . . . . ?
O13_16 C14_16 C15_16 C16_16 170.0(19)  . . . . ?
C19_16 C14_16 C15_16 C16_16 -3(3)      . . . . ?
C14_16 C15_16 C16_16 C17_16 6(3)       . . . . ?
C15_16 C16_16 C17_16 C18_16 -9(3)      . . . . ?
C15_16 C16_16 C17_16 C36_16 171(2)     . . . . ?
C16_16 C17_16 C18_16 C19_16 8(2)       . . . . ?
C36_16 C17_16 C18_16 C19_16 -171.1(16) . . . . ?
C16_16 C17_16 C18_16 O28_16 -170.8(19) . . . . ?
C36_16 C17_16 C18_16 O28_16 10(2)      . . . . ?
O28_16 C18_16 C19_16 C14_16 173.7(18)  . . . . ?
C17_16 C18_16 C19_16 C14_16 -5(2)      . . . . ?
O28_16 C18_16 C19_16 P20_16 -3(2)      . . . . ?
C17_16 C18_16 C19_16 P20_16 177.7(15)  . . . . ?
C15_16 C14_16 C19_16 C18_16 3(2)       . . . . ?
O13_16 C14_16 C19_16 C18_16 -170.0(17) . . . . ?
C15_16 C14_16 C19_16 P20_16 179.7(17)  . . . . ?
O13_16 C14_16 C19_16 P20_16 7(2)       . . . . ?
C18_16 C19_16 P20_16 O29_16 -90.9(17)  . . . . ?
C14_16 C19_16 P20_16 O29_16 92.1(16)   . . . . ?
C18_16 C19_16 P20_16 C21_16 37.8(16)   . . . . ?
C14_16 C19_16 P20_16 C21_16 -139.2(14) . . . . ?
C18_16 C19_16 P20_16 C11_16 134.0(15)  . . . . ?
C14_16 C19_16 P20_16 C11_16 -43.0(15)  . . . . ?
C10_16 C11_16 P20_16 O29_16 89.6(17)   . . . . ?
C12_16 C11_16 P20_16 O29_16 -96.0(15)  . . . . ?
C10_16 C11_16 P20_16 C19_16 -134.1(14) . . . . ?
C12_16 C11_16 P20_16 C19_16 40.2(14)   . . . . ?
C10_16 C11_16 P20_16 C21_16 -39.0(15)  . . . . ?
C12_16 C11_16 P20_16 C21_16 135.4(13)  . . . . ?
O29_16 P20_16 C21_16 C22_16 97.0(15)   . . . . ?
C19_16 P20_16 C21_16 C22_16 -35.6(14)  . . . . ?
C11_16 P20_16 C21_16 C22_16 -131.7(14) . . . . ?
O29_16 P20_16 C21_16 C26_16 -90.0(14)  . . . . ?
C19_16 P20_16 C21_16 C26_16 137.4(13)  . . . . ?
C11_16 P20_16 C21_16 C26_16 41.3(13)   . . . . ?
C26_16 C21_16 C22_16 C23_16 9(2)       . . . . ?
P20_16 C21_16 C22_16 C23_16 -178.3(17) . . . . ?
C26_16 C21_16 C22_16 O28_16 -171.8(16) . . . . ?
P20_16 C21_16 C22_16 O28_16 1(2)       . . . . ?
O28_16 C22_16 C23_16 C24_16 178(2)     . . . . ?
C21_16 C22_16 C23_16 C24_16 -3(3)      . . . . ?
C22_16 C23_16 C24_16 C25_16 0(3)       . . . . ?
C23_16 C24_16 C25_16 C26_16 -3(3)      . . . . ?
C23_16 C24_16 C25_16 C30_16 179.1(19)  . . . . ?
C24_16 C25_16 C26_16 O27_16 -169.3(16) . . . . ?
C30_16 C25_16 C26_16 O27_16 9(2)       . . . . ?
C24_16 C25_16 C26_16 C21_16 9(2)       . . . . ?
C30_16 C25_16 C26_16 C21_16 -173.3(13) . . . . ?
C22_16 C21_16 C26_16 O27_16 166.0(15)  . . . . ?
P20_16 C21_16 C26_16 O27_16 -6.9(19)   . . . . ?
C22_16 C21_16 C26_16 C25_16 -12(2)     . . . . ?
P20_16 C21_16 C26_16 C25_16 175.2(12)  . . . . ?
C25_16 C26_16 O27_16 C10_16 136.4(17)  . . . . ?
C21_16 C26_16 O27_16 C10_16 -41(2)     . . . . ?
C11_16 C10_16 O27_16 C26_16 45(2)      . . . . ?
C9_16  C10_16 O27_16 C26_16 -132(2)    . . . . ?
C19_16 C18_16 O28_16 C22_16 -43(2)     . . . . ?
C17_16 C18_16 O28_16 C22_16 136.0(18)  . . . . ?
C23_16 C22_16 O28_16 C18_16 -137(2)    . . . . ?
C21_16 C22_16 O28_16 C18_16 44(2)      . . . . ?
C24_16 C25_16 C30_16 C31_16 31(2)      . . . . ?
C26_16 C25_16 C30_16 C31_16 -146.7(17) . . . . ?
C24_16 C25_16 C30_16 C35_16 -142.0(16) . . . . ?
C26_16 C25_16 C30_16 C35_16 39.9(19)   . . . . ?
C35_16 C30_16 C31_16 C32_16 -7(2)      . . . . ?
C25_16 C30_16 C31_16 C32_16 179.2(16)  . . . . ?
C30_16 C31_16 C32_16 C33_16 3(2)       . . . . ?
C31_16 C32_16 C33_16 N34_16 4(2)       . . . . ?
C32_16 C33_16 N34_16 C35_16 -5(3)      . . . . ?
C32_16 C33_16 N34_16 Pd2_10 167.3(16)  . . . . ?
C33_16 N34_16 C35_16 C30_16 0(3)       . . . . ?
Pd2_10 N34_16 C35_16 C30_16 -172.2(12) . . . . ?
C31_16 C30_16 C35_16 N34_16 6(2)       . . . . ?
C25_16 C30_16 C35_16 N34_16 179.5(16)  . . . . ?
C16_16 C17_16 C36_16 C37_16 39(2)      . . . . ?
C18_16 C17_16 C36_16 C37_16 -142.0(19) . . . . ?
C16_16 C17_16 C36_16 C41_16 -143(2)    . . . . ?
C18_16 C17_16 C36_16 C41_16 36(2)      . . . . ?
C41_16 C36_16 C37_16 C38_16 2(2)       . . . . ?
C17_16 C36_16 C37_16 C38_16 -179.1(17) . . . . ?
C36_16 C37_16 C38_16 C39_16 -1(2)      . . . . ?
C37_16 C38_16 C39_16 N40_16 1(2)       . . . . ?
C38_16 C39_16 N40_16 C41_16 -3(3)      . . . . ?
C38_16 C39_16 N40_16 Pd3_10 175.2(14)  . . . . ?
C39_16 N40_16 C41_16 C36_16 5(3)       . . . . ?
Pd3_10 N40_16 C41_16 C36_16 -173.3(14) . . . . ?
C37_16 C36_16 C41_16 N40_16 -5(3)      . . . . ?
C17_16 C36_16 C41_16 N40_16 176.9(17)  . . . . ?
C6_17  N1_17  C2_17  C3_17  -10(3)     . . . . ?
Pd2_10 N1_17  C2_17  C3_17  168(2)     . . . . ?
N1_17  C2_17  C3_17  C4_17  16(4)      . . . . ?
C2_17  C3_17  C4_17  C5_17  -15(4)     . . . . ?
C3_17  C4_17  C5_17  C6_17  8(3)       . . . . ?
C3_17  C4_17  C5_17  C7_17  -168(3)    . . . . ?
C2_17  N1_17  C6_17  C5_17  2(2)       . . . . ?
Pd2_10 N1_17  C6_17  C5_17  -175.8(12) . . . . ?
C4_17  C5_17  C6_17  N1_17  -1(2)      . . . . ?
C7_17  C5_17  C6_17  N1_17  174.2(16)  . . . . ?
C6_17  C5_17  C7_17  C8_17  -137.0(18) . . . . ?
C4_17  C5_17  C7_17  C8_17  38(3)      . . . . ?
C6_17  C5_17  C7_17  C12_17 40(2)      . . . . ?
C4_17  C5_17  C7_17  C12_17 -145(2)    . . . . ?
C12_17 C7_17  C8_17  C9_17  -4(3)      . . . . ?
C5_17  C7_17  C8_17  C9_17  173.2(19)  . . . . ?
C7_17  C8_17  C9_17  C10_17 1(3)       . . . . ?
C8_17  C9_17  C10_17 O27_17 175.1(18)  . . . . ?
C8_17  C9_17  C10_17 C11_17 -1(3)      . . . . ?
O27_17 C10_17 C11_17 C12_17 -171.0(15) . . . . ?
C9_17  C10_17 C11_17 C12_17 5(2)       . . . . ?
O27_17 C10_17 C11_17 P20_17 4(2)       . . . . ?
C9_17  C10_17 C11_17 P20_17 -180.0(15) . . . . ?
C8_17  C7_17  C12_17 O13_17 -166.6(16) . . . . ?
C5_17  C7_17  C12_17 O13_17 16(2)      . . . . ?
C8_17  C7_17  C12_17 C11_17 7(2)       . . . . ?
C5_17  C7_17  C12_17 C11_17 -169.7(14) . . . . ?
C10_17 C11_17 C12_17 C7_17  -8(2)      . . . . ?
P20_17 C11_17 C12_17 C7_17  176.8(13)  . . . . ?
C10_17 C11_17 C12_17 O13_17 165.8(15)  . . . . ?
P20_17 C11_17 C12_17 O13_17 -9.0(18)   . . . . ?
C7_17  C12_17 O13_17 C14_17 135.8(16)  . . . . ?
C11_17 C12_17 O13_17 C14_17 -38(2)     . . . . ?
C12_17 O13_17 C14_17 C19_17 47(2)      . . . . ?
C12_17 O13_17 C14_17 C15_17 -132.3(17) . . . . ?
C19_17 C14_17 C15_17 C16_17 3(3)       . . . . ?
O13_17 C14_17 C15_17 C16_17 -177.7(17) . . . . ?
C14_17 C15_17 C16_17 C17_17 -6(3)      . . . . ?
C15_17 C16_17 C17_17 C18_17 1(2)       . . . . ?
C15_17 C16_17 C17_17 C36_17 -179.8(16) . . . . ?
C16_17 C17_17 C18_17 O28_17 -173.6(16) . . . . ?
C36_17 C17_17 C18_17 O28_17 7(2)       . . . . ?
C16_17 C17_17 C18_17 C19_17 7(2)       . . . . ?
C36_17 C17_17 C18_17 C19_17 -172.7(14) . . . . ?
C15_17 C14_17 C19_17 C18_17 5(2)       . . . . ?
O13_17 C14_17 C19_17 C18_17 -174.6(15) . . . . ?
C15_17 C14_17 C19_17 P20_17 175.2(14)  . . . . ?
O13_17 C14_17 C19_17 P20_17 -3.9(19)   . . . . ?
O28_17 C18_17 C19_17 C14_17 170.4(15)  . . . . ?
C17_17 C18_17 C19_17 C14_17 -10(2)     . . . . ?
O28_17 C18_17 C19_17 P20_17 -0.3(18)   . . . . ?
C17_17 C18_17 C19_17 P20_17 179.6(12)  . . . . ?
C14_17 C19_17 P20_17 O29_17 97.0(15)   . . . . ?
C18_17 C19_17 P20_17 O29_17 -92.2(14)  . . . . ?
C14_17 C19_17 P20_17 C21_17 -131.9(13) . . . . ?
C18_17 C19_17 P20_17 C21_17 39.0(13)   . . . . ?
C14_17 C19_17 P20_17 C11_17 -34.8(13)  . . . . ?
C18_17 C19_17 P20_17 C11_17 136.0(12)  . . . . ?
C12_17 C11_17 P20_17 O29_17 -88.5(14)  . . . . ?
C10_17 C11_17 P20_17 O29_17 96.5(14)   . . . . ?
C12_17 C11_17 P20_17 C19_17 40.9(13)   . . . . ?
C10_17 C11_17 P20_17 C19_17 -134.0(12) . . . . ?
C12_17 C11_17 P20_17 C21_17 137.2(12)  . . . . ?
C10_17 C11_17 P20_17 C21_17 -37.7(13)  . . . . ?
O29_17 P20_17 C21_17 C26_17 -97.5(15)  . . . . ?
C19_17 P20_17 C21_17 C26_17 133.9(13)  . . . . ?
C11_17 P20_17 C21_17 C26_17 36.7(14)   . . . . ?
O29_17 P20_17 C21_17 C22_17 88.3(16)   . . . . ?
C19_17 P20_17 C21_17 C22_17 -40.4(14)  . . . . ?
C11_17 P20_17 C21_17 C22_17 -137.6(14) . . . . ?
C26_17 C21_17 C22_17 C23_17 3(2)       . . . . ?
P20_17 C21_17 C22_17 C23_17 177.3(16)  . . . . ?
C26_17 C21_17 C22_17 O28_17 -172.5(15) . . . . ?
P20_17 C21_17 C22_17 O28_17 2(2)       . . . . ?
O28_17 C22_17 C23_17 C24_17 170.9(19)  . . . . ?
C21_17 C22_17 C23_17 C24_17 -4(3)      . . . . ?
C22_17 C23_17 C24_17 C25_17 9(3)       . . . . ?
C23_17 C24_17 C25_17 C26_17 -11(3)     . . . . ?
C23_17 C24_17 C25_17 C30_17 172.4(19)  . . . . ?
C24_17 C25_17 C26_17 O27_17 -168.9(18) . . . . ?
C30_17 C25_17 C26_17 O27_17 8(2)       . . . . ?
C24_17 C25_17 C26_17 C21_17 9(2)       . . . . ?
C30_17 C25_17 C26_17 C21_17 -174.1(15) . . . . ?
C22_17 C21_17 C26_17 O27_17 172.5(16)  . . . . ?
P20_17 C21_17 C26_17 O27_17 -2(2)      . . . . ?
C22_17 C21_17 C26_17 C25_17 -5(2)      . . . . ?
P20_17 C21_17 C26_17 C25_17 -179.8(14) . . . . ?
C9_17  C10_17 O27_17 C26_17 -134.9(18) . . . . ?
C11_17 C10_17 O27_17 C26_17 41(2)      . . . . ?
C25_17 C26_17 O27_17 C10_17 135.3(16)  . . . . ?
C21_17 C26_17 O27_17 C10_17 -43(2)     . . . . ?
C23_17 C22_17 O28_17 C18_17 -125.4(18) . . . . ?
C21_17 C22_17 O28_17 C18_17 49.9(19)   . . . . ?
C17_17 C18_17 O28_17 C22_17 129.1(16)  . . . . ?
C19_17 C18_17 O28_17 C22_17 -51.0(18)  . . . . ?
C24_17 C25_17 C30_17 C35_17 -143(2)    . . . . ?
C26_17 C25_17 C30_17 C35_17 41(2)      . . . . ?
C24_17 C25_17 C30_17 C31_17 39(3)      . . . . ?
C26_17 C25_17 C30_17 C31_17 -138(2)    . . . . ?
C35_17 C30_17 C31_17 C32_17 0(3)       . . . . ?
C25_17 C30_17 C31_17 C32_17 178.1(19)  . . . . ?
C30_17 C31_17 C32_17 C33_17 0(2)       . . . . ?
C31_17 C32_17 C33_17 N34_17 3(2)       . . . . ?
C32_17 C33_17 N34_17 C35_17 -5(3)      . . . . ?
C32_17 C33_17 N34_17 Pd4_10 173.9(16)  . . . . ?
C33_17 N34_17 C35_17 C30_17 5(3)       . . . . ?
Pd4_10 N34_17 C35_17 C30_17 -174.4(15) . . . . ?
C31_17 C30_17 C35_17 N34_17 -2(3)      . . . . ?
C25_17 C30_17 C35_17 N34_17 179.6(18)  . . . . ?
C16_17 C17_17 C36_17 C37_17 45(2)      . . . . ?
C18_17 C17_17 C36_17 C37_17 -136.0(18) . . . . ?
C16_17 C17_17 C36_17 C41_17 -135.3(17) . . . . ?
C18_17 C17_17 C36_17 C41_17 44(2)      . . . . ?
C41_17 C36_17 C37_17 C38_17 1(2)       . . . . ?
C17_17 C36_17 C37_17 C38_17 -179.1(16) . . . . ?
C36_17 C37_17 C38_17 C39_17 -1(2)      . . . . ?
C37_17 C38_17 C39_17 N40_17 3(2)       . . . . ?
C38_17 C39_17 N40_17 C41_17 -5(3)      . . . . ?
C38_17 C39_17 N40_17 Pd3_10 -177.6(13) . . . . ?
C39_17 N40_17 C41_17 C36_17 5(3)       . . . . ?
Pd3_10 N40_17 C41_17 C36_17 178.0(13)  . . . . ?
C37_17 C36_17 C41_17 N40_17 -3(3)      . . . . ?
C17_17 C36_17 C41_17 N40_17 176.8(17)  . . . . ?
C6_18  N1_18  C2_18  C3_18  2(4)       . . . . ?
Pd2_10 N1_18  C2_18  C3_18  168(2)     . . . . ?
N1_18  C2_18  C3_18  C4_18  6(4)       . . . . ?
C2_18  C3_18  C4_18  C5_18  -12(4)     . . . . ?
C3_18  C4_18  C5_18  C6_18  10(3)      . . . . ?
C3_18  C4_18  C5_18  C7_18  -171(2)    . . . . ?
C2_18  N1_18  C6_18  C5_18  -4(2)      . . . . ?
Pd2_10 N1_18  C6_18  C5_18  -170.4(12) . . . . ?
C4_18  C5_18  C6_18  N1_18  -2(2)      . . . . ?
C7_18  C5_18  C6_18  N1_18  178.9(15)  . . . . ?
C4_18  C5_18  C7_18  C8_18  35(2)      . . . . ?
C6_18  C5_18  C7_18  C8_18  -145.7(17) . . . . ?
C4_18  C5_18  C7_18  C12_18 -144.7(19) . . . . ?
C6_18  C5_18  C7_18  C12_18 34.1(19)   . . . . ?
C12_18 C7_18  C8_18  C9_18  -3(3)      . . . . ?
C5_18  C7_18  C8_18  C9_18  176.9(17)  . . . . ?
C7_18  C8_18  C9_18  C10_18 -5(3)      . . . . ?
C8_18  C9_18  C10_18 O27_18 -178.2(19) . . . . ?
C8_18  C9_18  C10_18 C11_18 5(3)       . . . . ?
C9_18  C10_18 C11_18 C12_18 3(2)       . . . . ?
O27_18 C10_18 C11_18 C12_18 -173.8(16) . . . . ?
C9_18  C10_18 C11_18 P20_18 176.8(14)  . . . . ?
O27_18 C10_18 C11_18 P20_18 0(2)       . . . . ?
C10_18 C11_18 C12_18 O13_18 164.4(16)  . . . . ?
P20_18 C11_18 C12_18 O13_18 -10(2)     . . . . ?
C10_18 C11_18 C12_18 C7_18  -11(2)     . . . . ?
P20_18 C11_18 C12_18 C7_18  175.1(13)  . . . . ?
C8_18  C7_18  C12_18 O13_18 -164.8(17) . . . . ?
C5_18  C7_18  C12_18 O13_18 15(2)      . . . . ?
C8_18  C7_18  C12_18 C11_18 11(2)      . . . . ?
C5_18  C7_18  C12_18 C11_18 -169.3(14) . . . . ?
C11_18 C12_18 O13_18 C14_18 -34(2)     . . . . ?
C7_18  C12_18 O13_18 C14_18 141.0(17)  . . . . ?
C12_18 O13_18 C14_18 C15_18 -140(2)    . . . . ?
C12_18 O13_18 C14_18 C19_18 37(2)      . . . . ?
C19_18 C14_18 C15_18 C16_18 -11(3)     . . . . ?
O13_18 C14_18 C15_18 C16_18 166(2)     . . . . ?
C14_18 C15_18 C16_18 C17_18 10(4)      . . . . ?
C15_18 C16_18 C17_18 C18_18 -7(3)      . . . . ?
C15_18 C16_18 C17_18 C36_18 171(2)     . . . . ?
C16_18 C17_18 C18_18 C19_18 5(2)       . . . . ?
C36_18 C17_18 C18_18 C19_18 -172.9(16) . . . . ?
C16_18 C17_18 C18_18 O28_18 -168.6(17) . . . . ?
C36_18 C17_18 C18_18 O28_18 14(2)      . . . . ?
C15_18 C14_18 C19_18 C18_18 9(2)       . . . . ?
O13_18 C14_18 C19_18 C18_18 -168.3(16) . . . . ?
C15_18 C14_18 C19_18 P20_18 -178.2(18) . . . . ?
O13_18 C14_18 C19_18 P20_18 4(2)       . . . . ?
C17_18 C18_18 C19_18 C14_18 -6(2)      . . . . ?
O28_18 C18_18 C19_18 C14_18 167.4(16)  . . . . ?
C17_18 C18_18 C19_18 P20_18 -178.4(14) . . . . ?
O28_18 C18_18 C19_18 P20_18 -5(2)      . . . . ?
C10_18 C11_18 P20_18 O29_18 94.4(15)   . . . . ?
C12_18 C11_18 P20_18 O29_18 -91.5(15)  . . . . ?
C10_18 C11_18 P20_18 C21_18 -37.4(14)  . . . . ?
C12_18 C11_18 P20_18 C21_18 136.8(13)  . . . . ?
C10_18 C11_18 P20_18 C19_18 -134.4(14) . . . . ?
C12_18 C11_18 P20_18 C19_18 39.8(14)   . . . . ?
C14_18 C19_18 P20_18 O29_18 95.8(15)   . . . . ?
C18_18 C19_18 P20_18 O29_18 -91.6(15)  . . . . ?
C14_18 C19_18 P20_18 C11_18 -36.7(14)  . . . . ?
C18_18 C19_18 P20_18 C11_18 135.8(14)  . . . . ?
C14_18 C19_18 P20_18 C21_18 -133.1(13) . . . . ?
C18_18 C19_18 P20_18 C21_18 39.4(15)   . . . . ?
O29_18 P20_18 C21_18 C26_18 -90.7(16)  . . . . ?
C11_18 P20_18 C21_18 C26_18 41.6(15)   . . . . ?
C19_18 P20_18 C21_18 C26_18 139.0(15)  . . . . ?
O29_18 P20_18 C21_18 C22_18 94.2(15)   . . . . ?
C11_18 P20_18 C21_18 C22_18 -133.5(14) . . . . ?
C19_18 P20_18 C21_18 C22_18 -36.1(15)  . . . . ?
C26_18 C21_18 C22_18 C23_18 0(2)       . . . . ?
P20_18 C21_18 C22_18 C23_18 175.5(18)  . . . . ?
C26_18 C21_18 C22_18 O28_18 -175.9(18) . . . . ?
P20_18 C21_18 C22_18 O28_18 -1(2)      . . . . ?
O28_18 C22_18 C23_18 C24_18 176(2)     . . . . ?
C21_18 C22_18 C23_18 C24_18 -1(3)      . . . . ?
C22_18 C23_18 C24_18 C25_18 7(4)       . . . . ?
C23_18 C24_18 C25_18 C26_18 -13(3)     . . . . ?
C23_18 C24_18 C25_18 C30_18 170(2)     . . . . ?
C22_18 C21_18 C26_18 O27_18 166.6(18)  . . . . ?
P20_18 C21_18 C26_18 O27_18 -8(2)      . . . . ?
C22_18 C21_18 C26_18 C25_18 -6(2)      . . . . ?
P20_18 C21_18 C26_18 C25_18 178.6(15)  . . . . ?
C24_18 C25_18 C26_18 C21_18 12(3)      . . . . ?
C30_18 C25_18 C26_18 C21_18 -169.9(18) . . . . ?
C24_18 C25_18 C26_18 O27_18 -160(2)    . . . . ?
C30_18 C25_18 C26_18 O27_18 17(2)      . . . . ?
C9_18  C10_18 O27_18 C26_18 -131.7(18) . . . . ?
C11_18 C10_18 O27_18 C26_18 45(2)      . . . . ?
C21_18 C26_18 O27_18 C10_18 -40(2)     . . . . ?
C25_18 C26_18 O27_18 C10_18 133.1(18)  . . . . ?
C23_18 C22_18 O28_18 C18_18 -128(2)    . . . . ?
C21_18 C22_18 O28_18 C18_18 48(2)      . . . . ?
C17_18 C18_18 O28_18 C22_18 129.0(17)  . . . . ?
C19_18 C18_18 O28_18 C22_18 -45(2)     . . . . ?
C24_18 C25_18 C30_18 C31_18 35(3)      . . . . ?
C26_18 C25_18 C30_18 C31_18 -142(2)    . . . . ?
C24_18 C25_18 C30_18 C35_18 -142(2)    . . . . ?
C26_18 C25_18 C30_18 C35_18 41(3)      . . . . ?
C35_18 C30_18 C31_18 C32_18 -3(3)      . . . . ?
C25_18 C30_18 C31_18 C32_18 -179.8(19) . . . . ?
C30_18 C31_18 C32_18 C33_18 -1(2)      . . . . ?
C31_18 C32_18 C33_18 N34_18 2(2)       . . . . ?
C32_18 C33_18 N34_18 C35_18 0(3)       . . . . ?
C32_18 C33_18 N34_18 Pd1_10 174.1(16)  . . . . ?
C33_18 N34_18 C35_18 C30_18 -4(4)      . . . . ?
Pd1_10 N34_18 C35_18 C30_18 -178.3(17) . . . . ?
C31_18 C30_18 C35_18 N34_18 5(3)       . . . . ?
C25_18 C30_18 C35_18 N34_18 -177(2)    . . . . ?
C18_18 C17_18 C36_18 C41_18 46(2)      . . . . ?
C16_18 C17_18 C36_18 C41_18 -131(2)    . . . . ?
C18_18 C17_18 C36_18 C37_18 -136.7(19) . . . . ?
C16_18 C17_18 C36_18 C37_18 46(2)      . . . . ?
C41_18 C36_18 C37_18 C38_18 -2(3)      . . . . ?
C17_18 C36_18 C37_18 C38_18 -179.2(18) . . . . ?
C36_18 C37_18 C38_18 C39_18 3(2)       . . . . ?
C37_18 C38_18 C39_18 N40_18 0(2)       . . . . ?
C38_18 C39_18 N40_18 C41_18 -4(3)      . . . . ?
C38_18 C39_18 N40_18 Pd4_10 -174.4(15) . . . . ?
C39_18 N40_18 C41_18 C36_18 5(3)       . . . . ?
Pd4_10 N40_18 C41_18 C36_18 176.1(15)  . . . . ?
C37_18 C36_18 C41_18 N40_18 -2(3)      . . . . ?
C17_18 C36_18 C41_18 N40_18 175.2(19)  . . . . ?

_platon_squeeze_void_probe_radius 1.20
_platon_squeeze_details           ''

loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1  0.096 -0.084 0.002 25998 11104 ' '
2  0.414 0.032  0.829 16    13    ' '
3  0.605 0.050  0.536 15    15    ' '
4  0.896 0.087  0.039 15    12    ' '
5  0.087 0.104  0.289 15    12    ' '
6  0.250 0.186  0.120 9     2     ' '
7  0.268 0.199  0.994 12    -2    ' '
8  0.687 0.302  0.815 138   50    ' '
9  0.285 0.228  0.558 23    3     ' '
10 0.644 0.239  0.315 7     4     ' '
11 0.302 0.313  0.065 138   50    ' '
12 0.814 0.250  0.870 9     2     ' '
13 0.801 0.268  0.744 12    -2    ' '
14 0.772 0.285  0.308 23    3     ' '
15 0.713 0.276  0.884 7     3     ' '
16 0.276 0.287  0.134 7     3     ' '
17 0.239 0.356  0.565 7     4     ' '
18 0.529 0.388  0.384 7     2     ' '
19 0.050 0.395  0.786 16    15    ' '
20 0.968 0.414  0.579 16    13    ' '
21 0.533 0.449  0.075 15    10    ' '
22 0.449 0.467  0.325 15    10    ' '
23 0.389 0.471  0.634 7     2     ' '
24 0.611 0.529  0.134 7     2     ' '
25 0.551 0.533  0.825 15    10    ' '
26 0.467 0.551  0.575 15    9     ' '
27 0.032 0.585  0.079 16    13    ' '
28 0.950 0.605  0.286 15    15    ' '
29 0.698 0.686  0.565 139   49    ' '
30 0.471 0.611  0.884 7     2     ' '
31 0.313 0.698  0.315 138   50    ' '
32 0.761 0.644  0.065 7     4     ' '
33 0.228 0.715  0.808 23    3     ' '
34 0.724 0.713  0.634 7     3     ' '
35 0.287 0.724  0.384 7     3     ' '
36 0.199 0.732  0.244 12    -2    ' '
37 0.186 0.750  0.370 9     2     ' '
38 0.715 0.772  0.058 23    3     ' '
39 0.356 0.761  0.815 7     4     ' '
40 0.732 0.801  0.494 12    -2    ' '
41 0.750 0.814  0.620 9     2     ' '
42 0.913 0.896  0.789 16    12    ' '
43 0.104 0.913  0.539 15    12    ' '
44 0.395 0.950  0.036 16    16    ' '
45 0.586 0.968  0.329 16    12    ' '

