data_cu_ch_szw_1_1230_0m
_audit_creation_date               2026-01-10
_audit_creation_method
;
Olex2 1.5
(compiled 2025.07.13 svn.rb7424aed for OlexSys, GUI svn.r7314)
;
_shelx_SHELXL_version_number       '2025/1'
_audit_contact_author_address      ?
_audit_contact_author_email        ?
_audit_contact_author_name         ''
_audit_contact_author_phone        ?
_publ_contact_author_id_orcid      ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_chemical_name_common              ?
_chemical_name_systematic          ?
_chemical_formula_moiety           'C26 H12 F6 N4'
_chemical_formula_sum              'C26 H12 F6 N4'
_chemical_formula_weight           494.40
_chemical_absolute_configuration   ad
_chemical_melting_point            ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'F' 'F' 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system        'trigonal'
_space_group_IT_number             144
_space_group_name_H-M_alt          'P 31'
_space_group_name_Hall             'P 31'
loop_
  _space_group_symop_operation_xyz
 'x, y, z'
 '-y, x-y, z+1/3'
 '-x+y, -x, z+2/3'

_cell_length_a                     32.2457(9)
_cell_length_b                     32.2457(9)
_cell_length_c                     15.7465(7)
_cell_angle_alpha                  90
_cell_angle_beta                   90
_cell_angle_gamma                  120
_cell_volume                       14179.4(10)
_cell_formula_units_Z              27
_cell_measurement_reflns_used      9782
_cell_measurement_temperature      200.00
_cell_measurement_theta_max        69.74
_cell_measurement_theta_min        3.16
_shelx_estimated_absorpt_T_max     0.914
_shelx_estimated_absorpt_T_min     0.865
_exptl_absorpt_coefficient_mu      1.147
_exptl_absorpt_correction_T_max    0.7533
_exptl_absorpt_correction_T_min    0.3830
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1634 before and 0.1040 after correction.
The Ratio of minimum to maximum transmission is 0.5084.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details     ?
_exptl_crystal_colour              ?
_exptl_crystal_density_diffrn      1.563
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      ?
_exptl_crystal_description         block
_exptl_crystal_F_000               6750
_exptl_crystal_size_max            0.13
_exptl_crystal_size_mid            0.11
_exptl_crystal_size_min            0.08
_exptl_transmission_factor_max     ?
_exptl_transmission_factor_min     ?
_diffrn_reflns_av_R_equivalents    0.1146
_diffrn_reflns_av_unetI/netI       0.1071
_diffrn_reflns_Laue_measured_fraction_full  0.997
_diffrn_reflns_Laue_measured_fraction_max  0.992
_diffrn_reflns_limit_h_max         39
_diffrn_reflns_limit_h_min         -39
_diffrn_reflns_limit_k_max         39
_diffrn_reflns_limit_k_min         -39
_diffrn_reflns_limit_l_max         14
_diffrn_reflns_limit_l_min         -19
_diffrn_reflns_number              127801
_diffrn_reflns_point_group_measured_fraction_full  0.927
_diffrn_reflns_point_group_measured_fraction_max  0.917
_diffrn_reflns_theta_full          67.679
_diffrn_reflns_theta_max           70.369
_diffrn_reflns_theta_min           2.741
_diffrn_ambient_temperature        200.00
_diffrn_detector                   CPAD
_diffrn_detector_area_resol_mean   7.41
_diffrn_detector_type              'Bruker PHOTON III'
_diffrn_measured_fraction_theta_full  0.997
_diffrn_measured_fraction_theta_max  0.992
_diffrn_measurement_device         'four-circle diffractometer'
_diffrn_measurement_device_type    'Bruker D8 VENTURE dual wavelength Mo/Cu'
_diffrn_measurement_method         'ω and φ scans'
_diffrn_radiation_monochromator    'Helios Multi-layer Optic'
_diffrn_radiation_probe            X-ray
_diffrn_radiation_type             CuK\a
_diffrn_radiation_wavelength       1.54178
_diffrn_source                     'microfocus sealed X-ray tube'
_diffrn_source_current             1.1
_diffrn_source_power               0.05500000000000001
_diffrn_source_type                'Incoatec I\ms DIAMOND'
_diffrn_source_voltage             50.0
_diffrn_standards_number           0
_reflns_Friedel_coverage           0.849
_reflns_Friedel_fraction_full      0.856
_reflns_Friedel_fraction_max       0.842
_reflns_number_gt                  20986
_reflns_number_total               33091
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression       'I > 2σ(I)'
_computing_cell_refinement         'SAINT V8.41 (Bruker, 2024)'
_computing_data_collection         'APEX6 V2024.9-1 (Bruker, 2025)'
_computing_data_reduction          'SAINT V8.41 (Bruker, 2024)'
_computing_molecular_graphics      'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement    'SHELXL 2025/1 (Sheldrick, 2015)'
_computing_structure_solution      'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max           0.454
_refine_diff_density_min           -0.354
_refine_diff_density_rms           0.064
_refine_ls_abs_structure_details
;
 Flack x determined using 6556 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack     0.11(7)
_refine_ls_extinction_coef         .
_refine_ls_extinction_method       none
_refine_ls_goodness_of_fit_ref     1.127
_refine_ls_hydrogen_treatment      constr
_refine_ls_matrix_type             full
_refine_ls_number_parameters       2917
_refine_ls_number_reflns           33091
_refine_ls_number_restraints       6859
_refine_ls_R_factor_all            0.1519
_refine_ls_R_factor_gt             0.1101
_refine_ls_restrained_S_all        1.190
_refine_ls_shift/su_max            0.003
_refine_ls_shift/su_mean           0.000
_refine_ls_structure_factor_coef   Fsqd
_refine_ls_weighting_details      
 'w=1/[σ²(Fo²)+(0.1200P)²+15.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme        calc
_refine_ls_wR_factor_gt            0.2877
_refine_ls_wR_factor_ref           0.3213
_refine_special_details            ?
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2. Restrained distances
 C21_1-N4_1 \\sim N4_1-C17_1 \\sim C8_1-N1_1 \\sim N1_1-C5_1
 C21_2-N4_2 \\sim N4_2-C17_2 \\sim C8_2-N1_2 \\sim N1_2-C5_2
 C21_3-N4_3 \\sim N4_3-C17_3 \\sim C8_3-N1_3 \\sim N1_3-C5_3
 C21_4-N4_4 \\sim N4_4-C17_4 \\sim C8_4-N1_4 \\sim N1_4-C5_4
 C21_5-N4_5 \\sim N4_5-C17_5 \\sim C8_5-N1_5 \\sim N1_5-C5_5
 C21_6-N4_6 \\sim N4_6-C17_6 \\sim C8_6-N1_6 \\sim N1_6-C5_6
 C21_7-N4_7 \\sim N4_7-C17_7 \\sim C8_7-N1_7 \\sim N1_7-C5_7
 C21_8-N4_8 \\sim N4_8-C17_8 \\sim C8_8-N1_8 \\sim N1_8-C5_8
 C21_9-N4_9 \\sim N4_9-C17_9 \\sim C8_9-N1_9 \\sim N1_9-C5_9
 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
F1_1 \\sim F2_1 \\sim F3_1 \\sim F4_1 \\sim F5_1 \\sim F6_1 \\sim N1_1 \\sim
N2_1 \\sim N3_1 \\sim N4_1 \\sim C1_1 \\sim C2_1 \\sim C3_1 \\sim C4_1 \\sim
C5_1 \\sim C6_1 \\sim C7_1 \\sim C8_1 \\sim C9_1 \\sim C10_1 \\sim C11_1 \\sim
C12_1 \\sim C13_1 \\sim C14_1 \\sim C15_1 \\sim C16_1 \\sim C17_1 \\sim C18_1
\\sim C19_1 \\sim C20_1 \\sim C21_1 \\sim C22_1 \\sim C23_1 \\sim C24_1 \\sim
C25_1 \\sim C26_1 \\sim F1_2 \\sim F2_2 \\sim F3_2 \\sim F4_2 \\sim F5_2 \\sim
F6_2 \\sim N1_2 \\sim N2_2 \\sim N3_2 \\sim N4_2 \\sim C1_2 \\sim C2_2 \\sim
C3_2 \\sim C4_2 \\sim C5_2 \\sim C6_2 \\sim C7_2 \\sim C8_2 \\sim C9_2 \\sim
C10_2 \\sim C11_2 \\sim C12_2 \\sim C13_2 \\sim C14_2 \\sim C15_2 \\sim C16_2
\\sim C17_2 \\sim C18_2 \\sim C19_2 \\sim C20_2 \\sim C21_2 \\sim C22_2 \\sim
C23_2 \\sim C24_2 \\sim C25_2 \\sim C26_2 \\sim F1_3 \\sim F2_3 \\sim F3_3
\\sim F4_3 \\sim F5_3 \\sim F6_3 \\sim N1_3 \\sim N2_3 \\sim N3_3 \\sim N4_3
\\sim C1_3 \\sim C2_3 \\sim C3_3 \\sim C4_3 \\sim C5_3 \\sim C6_3 \\sim C7_3
\\sim C8_3 \\sim C9_3 \\sim C10_3 \\sim C11_3 \\sim C12_3 \\sim C13_3 \\sim
C14_3 \\sim C15_3 \\sim C16_3 \\sim C17_3 \\sim C18_3 \\sim C19_3 \\sim C20_3
\\sim C21_3 \\sim C22_3 \\sim C23_3 \\sim C24_3 \\sim C25_3 \\sim C26_3 \\sim
F1_4 \\sim F2_4 \\sim F3_4 \\sim F4_4 \\sim F5_4 \\sim F6_4 \\sim N1_4 \\sim
N2_4 \\sim N3_4 \\sim N4_4 \\sim C1_4 \\sim C2_4 \\sim C3_4 \\sim C4_4 \\sim
C5_4 \\sim C6_4 \\sim C7_4 \\sim C8_4 \\sim C9_4 \\sim C10_4 \\sim C11_4 \\sim
C12_4 \\sim C13_4 \\sim C14_4 \\sim C15_4 \\sim C16_4 \\sim C17_4 \\sim C18_4
\\sim C19_4 \\sim C20_4 \\sim C21_4 \\sim C22_4 \\sim C23_4 \\sim C24_4 \\sim
C25_4 \\sim C26_4 \\sim F1_5 \\sim F2_5 \\sim F3_5 \\sim F4_5 \\sim F5_5 \\sim
F6_5 \\sim N1_5 \\sim N2_5 \\sim N3_5 \\sim N4_5 \\sim C1_5 \\sim C2_5 \\sim
C3_5 \\sim C4_5 \\sim C5_5 \\sim C6_5 \\sim C7_5 \\sim C8_5 \\sim C9_5 \\sim
C10_5 \\sim C11_5 \\sim C12_5 \\sim C13_5 \\sim C14_5 \\sim C15_5 \\sim C16_5
\\sim C17_5 \\sim C18_5 \\sim C19_5 \\sim C20_5 \\sim C21_5 \\sim C22_5 \\sim
C23_5 \\sim C24_5 \\sim C25_5 \\sim C26_5 \\sim F1_6 \\sim F2_6 \\sim F3_6
\\sim F4_6 \\sim F5_6 \\sim F6_6 \\sim N1_6 \\sim N2_6 \\sim N3_6 \\sim N4_6
\\sim C1_6 \\sim C2_6 \\sim C3_6 \\sim C4_6 \\sim C5_6 \\sim C6_6 \\sim C7_6
\\sim C8_6 \\sim C9_6 \\sim C10_6 \\sim C11_6 \\sim C12_6 \\sim C13_6 \\sim
C14_6 \\sim C15_6 \\sim C16_6 \\sim C17_6 \\sim C18_6 \\sim C19_6 \\sim C20_6
\\sim C21_6 \\sim C22_6 \\sim C23_6 \\sim C24_6 \\sim C25_6 \\sim C26_6 \\sim
F1_7 \\sim F2_7 \\sim F3_7 \\sim F4_7 \\sim F5_7 \\sim F6_7 \\sim N1_7 \\sim
N2_7 \\sim N3_7 \\sim N4_7 \\sim C1_7 \\sim C2_7 \\sim C3_7 \\sim C4_7 \\sim
C5_7 \\sim C6_7 \\sim C7_7 \\sim C8_7 \\sim C9_7 \\sim C10_7 \\sim C11_7 \\sim
C12_7 \\sim C13_7 \\sim C14_7 \\sim C15_7 \\sim C16_7 \\sim C17_7 \\sim C18_7
\\sim C19_7 \\sim C20_7 \\sim C21_7 \\sim C22_7 \\sim C23_7 \\sim C24_7 \\sim
C25_7 \\sim C26_7 \\sim F1_8 \\sim F2_8 \\sim F3_8 \\sim F4_8 \\sim F5_8 \\sim
F6_8 \\sim N1_8 \\sim N2_8 \\sim N3_8 \\sim N4_8 \\sim C1_8 \\sim C2_8 \\sim
C3_8 \\sim C4_8 \\sim C5_8 \\sim C6_8 \\sim C7_8 \\sim C8_8 \\sim C9_8 \\sim
C10_8 \\sim C11_8 \\sim C12_8 \\sim C13_8 \\sim C14_8 \\sim C15_8 \\sim C16_8
\\sim C17_8 \\sim C18_8 \\sim C19_8 \\sim C20_8 \\sim C21_8 \\sim C22_8 \\sim
C23_8 \\sim C24_8 \\sim C25_8 \\sim C26_8 \\sim F1_9 \\sim F2_9 \\sim F3_9
\\sim F4_9 \\sim F5_9 \\sim F6_9 \\sim N1_9 \\sim N2_9 \\sim N3_9 \\sim N4_9
\\sim C1_9 \\sim C2_9 \\sim C3_9 \\sim C4_9 \\sim C5_9 \\sim C6_9 \\sim C7_9
\\sim C8_9 \\sim C9_9 \\sim C10_9 \\sim C11_9 \\sim C12_9 \\sim C13_9 \\sim
C14_9 \\sim C15_9 \\sim C16_9 \\sim C17_9 \\sim C18_9 \\sim C19_9 \\sim C20_9
\\sim C21_9 \\sim C22_9 \\sim C23_9 \\sim C24_9 \\sim C25_9 \\sim C26_9: within
2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
4. Same fragment restrains
{F1_2, F2_2, F3_2, F4_2, F5_2, F6_2, N1_2, N2_2, N3_2, N4_2, C1_2, C2_2, C3_2,
C4_2, C5_2, C6_2, C7_2, C8_2, C9_2, C10_2, C11_2, C12_2, C13_2, C14_2, C15_2,
C16_2, C17_2, C18_2, C19_2, C20_2, C21_2, C22_2, C23_2, C24_2, C25_2, C26_2}
{F1_3, F2_3, F3_3, F4_3, F5_3, F6_3, N1_3, N2_3, N3_3, N4_3, C1_3, C2_3, C3_3,
C4_3, C5_3, C6_3, C7_3, C8_3, C9_3, C10_3, C11_3, C12_3, C13_3, C14_3, C15_3,
C16_3, C17_3, C18_3, C19_3, C20_3, C21_3, C22_3, C23_3, C24_3, C25_3, C26_3}
{F1_4, F2_4, F3_4, F4_4, F5_4, F6_4, N1_4, N2_4, N3_4, N4_4, C1_4, C2_4, C3_4,
C4_4, C5_4, C6_4, C7_4, C8_4, C9_4, C10_4, C11_4, C12_4, C13_4, C14_4, C15_4,
C16_4, C17_4, C18_4, C19_4, C20_4, C21_4, C22_4, C23_4, C24_4, C25_4, C26_4}
{F1_5, F2_5, F3_5, F4_5, F5_5, F6_5, N1_5, N2_5, N3_5, N4_5, C1_5, C2_5, C3_5,
C4_5, C5_5, C6_5, C7_5, C8_5, C9_5, C10_5, C11_5, C12_5, C13_5, C14_5, C15_5,
C16_5, C17_5, C18_5, C19_5, C20_5, C21_5, C22_5, C23_5, C24_5, C25_5, C26_5}
{F1_6, F2_6, F3_6, F4_6, F5_6, F6_6, N1_6, N2_6, N3_6, N4_6, C1_6, C2_6, C3_6,
C4_6, C5_6, C6_6, C7_6, C8_6, C9_6, C10_6, C11_6, C12_6, C13_6, C14_6, C15_6,
C16_6, C17_6, C18_6, C19_6, C20_6, C21_6, C22_6, C23_6, C24_6, C25_6, C26_6}
{F1_7, F2_7, F3_7, F4_7, F5_7, F6_7, N1_7, N2_7, N3_7, N4_7, C1_7, C2_7, C3_7,
C4_7, C5_7, C6_7, C7_7, C8_7, C9_7, C10_7, C11_7, C12_7, C13_7, C14_7, C15_7,
C16_7, C17_7, C18_7, C19_7, C20_7, C21_7, C22_7, C23_7, C24_7, C25_7, C26_7}
{F1_8, F2_8, F3_8, F4_8, F5_8, F6_8, N1_8, N2_8, N3_8, N4_8, C1_8, C2_8, C3_8,
C4_8, C5_8, C6_8, C7_8, C8_8, C9_8, C10_8, C11_8, C12_8, C13_8, C14_8, C15_8,
C16_8, C17_8, C18_8, C19_8, C20_8, C21_8, C22_8, C23_8, C24_8, C25_8, C26_8}
{F1_9, F2_9, F3_9, F4_9, F5_9, F6_9, N1_9, N2_9, N3_9, N4_9, C1_9, C2_9, C3_9,
C4_9, C5_9, C6_9, C7_9, C8_9, C9_9, C10_9, C11_9, C12_9, C13_9, C14_9, C15_9,
C16_9, C17_9, C18_9, C19_9, C20_9, C21_9, C22_9, C23_9, C24_9, C25_9, C26_9}
as
{F1_1, F2_1, F3_1, F4_1, F5_1, F6_1, N1_1, N2_1, N3_1, N4_1, C1_1, C2_1, C3_1,
C4_1, C5_1, C6_1, C7_1, C8_1, C9_1, C10_1, C11_1, C12_1, C13_1, C14_1, C15_1,
C16_1, C17_1, C18_1, C19_1, C20_1, C21_1, C22_1, C23_1, C24_1, C25_1, C26_1}
sigma for 1-2: 0.01 1-3: 0.02
5.a Aromatic/amide H refined with riding coordinates:
 C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C15(H15), C16(H16), C18(H18),
 C19(H19), C22(H22), C23(H23), C25(H25), C3(H3), C6(H6), C7(H7), C9(H9),
 C10(H10), C15(H15), C16(H16), C18(H18), C19(H19), C22(H22), C23(H23), C25(H25),
  C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C15(H15), C16(H16), C18(H18),
 C19(H19), C22(H22), C23(H23), C25(H25), C3(H3), C6(H6), C7(H7), C9(H9),
 C10(H10), C15(H15), C16(H16), C18(H18), C19(H19), C22(H22), C23(H23), C25(H25),
  C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C15(H15), C16(H16), C18(H18),
 C19(H19), C22(H22), C23(H23), C25(H25), C3(H3), C6(H6), C7(H7), C9(H9),
 C10(H10), C15(H15), C16(H16), C18(H18), C19(H19), C22(H22), C23(H23), C25(H25),
  C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C15(H15), C16(H16), C18(H18),
 C19(H19), C22(H22), C23(H23), C25(H25), C3(H3), C6(H6), C7(H7), C9(H9),
 C10(H10), C15(H15), C16(H16), C18(H18), C19(H19), C22(H22), C23(H23), C25(H25),
  C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C15(H15), C16(H16), C18(H18),
 C19(H19), C22(H22), C23(H23), C25(H25)
;
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary       dual
_atom_sites_solution_secondary     ?
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 F1_1 F 0.2901(3) 0.2922(2) 0.2413(5) 0.102(2) Uani 1 1 d D U . . .
 F2_1 F 0.3215(3) 0.2540(3) 0.2000(7) 0.131(3) Uani 1 1 d D U . . .
 F3_1 F 0.2850(4) 0.2759(4) 0.1113(6) 0.175(5) Uani 1 1 d D U . . .
 F4_1 F 0.1218(2) 0.1428(3) 0.4376(8) 0.149(4) Uani 1 1 d D U . . .
 F5_1 F 0.1470(3) 0.2171(2) 0.4256(5) 0.092(2) Uani 1 1 d D U . . .
 F6_1 F 0.1429(4) 0.1868(5) 0.5468(6) 0.155(4) Uani 1 1 d D U . . .
 N1_1 N 0.1167(4) 0.0807(4) 0.2520(10) 0.157(6) Uani 1 1 d D U . . .
 N2_1 N 0.1886(3) 0.0878(3) 0.2874(7) 0.104(3) Uani 1 1 d D U . . .
 N3_1 N 0.2813(3) 0.1479(2) 0.3816(5) 0.070(2) Uani 1 1 d D U . . .
 N4_1 N 0.3403(3) 0.2227(3) 0.4160(6) 0.082(3) Uani 1 1 d D U . . .
 C1_1 C 0.2820(3) 0.2570(3) 0.1862(6) 0.082(3) Uani 1 1 d D U . . .
 C2_1 C 0.2371(3) 0.2116(3) 0.2017(7) 0.068(2) Uani 1 1 d D U . . .
 C3_1 C 0.2395(3) 0.1730(3) 0.2318(7) 0.066(2) Uani 1 1 d D U . . .
 H3_1 H 0.269552 0.174660 0.239238 0.079 Uiso 1 1 calc R U . . .
 C4_1 C 0.1969(3) 0.1313(3) 0.2513(8) 0.101(4) Uani 1 1 d D U . . .
 C5_1 C 0.1519(4) 0.1267(4) 0.2367(11) 0.134(5) Uani 1 1 d D U . . .
 C6_1 C 0.1513(4) 0.1669(5) 0.2043(12) 0.134(5) Uani 1 1 d D U . . .
 H6_1 H 0.121400 0.164922 0.193264 0.161 Uiso 1 1 calc R U . . .
 C7_1 C 0.1927(3) 0.2091(4) 0.1883(10) 0.105(4) Uani 1 1 d D U . . .
 H7_1 H 0.191508 0.236220 0.168249 0.126 Uiso 1 1 calc R U . . .
 C8_1 C 0.1386(4) 0.0574(4) 0.2799(12) 0.140(6) Uani 1 1 d D U . . .
 C9_1 C 0.1191(5) 0.0071(4) 0.2956(13) 0.149(7) Uani 1 1 d D U . . .
 H9_1 H 0.085470 -0.014312 0.295288 0.179 Uiso 1 1 calc R U . . .
 C10_1 C 0.1497(5) -0.0088(5) 0.3108(12) 0.149(7) Uani 1 1 d D U . . .
 H10_1 H 0.137006 -0.042367 0.315048 0.179 Uiso 1 1 calc R U . . .
 C11_1 C 0.2000(4) 0.0214(3) 0.3209(10) 0.119(4) Uani 1 1 d D U . . .
 C12_1 C 0.2185(4) 0.0720(3) 0.3227(9) 0.093(3) Uani 1 1 d D U . . .
 C13_1 C 0.2643(3) 0.1015(3) 0.3536(8) 0.083(3) Uani 1 1 d D U . . .
 C14_1 C 0.2966(4) 0.0833(4) 0.3564(9) 0.102(3) Uani 1 1 d D U . . .
 C15_1 C 0.3460(4) 0.1173(4) 0.3665(10) 0.103(4) Uani 1 1 d D U . . .
 H15_1 H 0.367956 0.105797 0.363660 0.124 Uiso 1 1 calc R U . . .
 C16_1 C 0.3637(4) 0.1635(4) 0.3793(9) 0.100(3) Uani 1 1 d D U . . .
 H16_1 H 0.397233 0.184973 0.381519 0.120 Uiso 1 1 calc R U . . .
 C17_1 C 0.3303(3) 0.1800(3) 0.3899(8) 0.078(3) Uani 1 1 d D U . . .
 C18_1 C 0.2781(5) 0.0339(4) 0.3502(11) 0.117(4) Uani 1 1 d D U . . .
 H18_1 H 0.298755 0.020981 0.355056 0.141 Uiso 1 1 calc R U . . .
 C19_1 C 0.2311(5) 0.0048(4) 0.3376(10) 0.110(4) Uani 1 1 d D U . . .
 H19_1 H 0.218741 -0.028832 0.340082 0.132 Uiso 1 1 calc R U . . .
 C20_1 C 0.2587(2) 0.1724(3) 0.4101(6) 0.0512(19) Uani 1 1 d D U . . .
 C21_1 C 0.2968(3) 0.2189(3) 0.4278(7) 0.066(2) Uani 1 1 d D U . . .
 C22_1 C 0.2880(3) 0.2542(3) 0.4576(7) 0.075(3) Uani 1 1 d D U . . .
 H22_1 H 0.313458 0.285983 0.466648 0.090 Uiso 1 1 calc R U . . .
 C23_1 C 0.2422(3) 0.2421(3) 0.4735(8) 0.079(3) Uani 1 1 d D U . . .
 H23_1 H 0.235454 0.265175 0.496938 0.095 Uiso 1 1 calc R U . . .
 C24_1 C 0.2044(3) 0.1957(3) 0.4558(7) 0.064(2) Uani 1 1 d D U . . .
 C25_1 C 0.2110(3) 0.1593(3) 0.4273(6) 0.053(2) Uani 1 1 d D U . . .
 H25_1 H 0.185261 0.127506 0.419719 0.064 Uiso 1 1 calc R U . . .
 C26_1 C 0.1552(3) 0.1866(4) 0.4673(7) 0.095(3) Uani 1 1 d D U . . .
 F1_2 F 0.3353(3) 0.0381(3) -0.0839(6) 0.131(3) Uani 1 1 d D U . . .
 F2_2 F 0.2605(3) -0.0007(3) -0.0987(7) 0.118(3) Uani 1 1 d D U . . .
 F3_2 F 0.3051(4) 0.0237(4) -0.2069(6) 0.167(5) Uani 1 1 d D U . . .
 F4_2 F 0.3611(2) 0.2217(2) 0.0713(5) 0.090(2) Uani 1 1 d D U . . .
 F5_2 F 0.41199(18) 0.1984(2) 0.0778(5) 0.0830(19) Uani 1 1 d D U . . .
 F6_2 F 0.3859(3) 0.2111(2) 0.1902(4) 0.101(2) Uani 1 1 d D U . . .
 N1_2 N 0.2938(4) 0.2074(3) -0.1131(7) 0.117(4) Uani 1 1 d D U . . .
 N2_2 N 0.2320(3) 0.1419(2) -0.0531(5) 0.071(2) Uani 1 1 d D U . . .
 N3_2 N 0.2041(2) 0.0592(2) 0.0664(5) 0.0607(19) Uani 1 1 d D U . . .
 N4_2 N 0.2216(3) 0.0032(2) 0.1129(7) 0.082(3) Uani 1 1 d D U . . .
 C1_2 C 0.3001(3) 0.0372(3) -0.1314(7) 0.092(3) Uani 1 1 d D U . . .
 C2_2 C 0.2991(3) 0.0829(3) -0.1297(8) 0.084(3) Uani 1 1 d D U . . .
 C3_2 C 0.2609(3) 0.0842(3) -0.0946(6) 0.057(2) Uani 1 1 d D U . . .
 H3_2 H 0.233690 0.055761 -0.074915 0.068 Uiso 1 1 calc R U . . .
 C4_2 C 0.2632(3) 0.1281(3) -0.0886(6) 0.065(3) Uani 1 1 d D U . . .
 C5_2 C 0.3024(4) 0.1707(3) -0.1197(8) 0.096(4) Uani 1 1 d D U . . .
 C6_2 C 0.3401(4) 0.1681(4) -0.1582(8) 0.102(4) Uani 1 1 d D U . . .
 H6_2 H 0.366103 0.195913 -0.182484 0.122 Uiso 1 1 calc R U . . .
 C7_2 C 0.3394(4) 0.1251(4) -0.1610(9) 0.102(4) Uani 1 1 d D U . . .
 H7_2 H 0.365874 0.123682 -0.183839 0.123 Uiso 1 1 calc R U . . .
 C8_2 C 0.2521(4) 0.1908(3) -0.0734(8) 0.099(3) Uani 1 1 d D U . . .
 C9_2 C 0.2226(5) 0.2120(4) -0.0632(10) 0.115(4) Uani 1 1 d D U . . .
 H9_2 H 0.234698 0.244737 -0.076758 0.138 Uiso 1 1 calc R U . . .
 C10_2 C 0.1776(5) 0.1851(4) -0.0343(11) 0.115(4) Uani 1 1 d D U . . .
 H10_2 H 0.158394 0.199653 -0.028446 0.138 Uiso 1 1 calc R U . . .
 C11_2 C 0.1572(4) 0.1358(4) -0.0119(9) 0.097(3) Uani 1 1 d D U . . .
 C12_2 C 0.1886(3) 0.1169(3) -0.0095(7) 0.082(3) Uani 1 1 d D U . . .
 C13_2 C 0.1734(3) 0.0740(3) 0.0334(8) 0.079(3) Uani 1 1 d D U . . .
 C14_2 C 0.1239(3) 0.0437(4) 0.0474(9) 0.098(3) Uani 1 1 d D U . . .
 C15_2 C 0.1076(4) -0.0051(4) 0.0683(10) 0.111(4) Uani 1 1 d D U . . .
 H15_2 H 0.074119 -0.026631 0.071398 0.133 Uiso 1 1 calc R U . . .
 C16_2 C 0.1370(3) -0.0221(4) 0.0837(10) 0.106(4) Uani 1 1 d D U . . .
 H16_2 H 0.125019 -0.055336 0.092846 0.127 Uiso 1 1 calc R U . . .
 C17_2 C 0.1871(3) 0.0112(3) 0.0860(8) 0.083(3) Uani 1 1 d D U . . .
 C18_2 C 0.0929(4) 0.0622(5) 0.0372(11) 0.115(4) Uani 1 1 d D U . . .
 H18_2 H 0.059469 0.042114 0.046403 0.138 Uiso 1 1 calc R U . . .
 C19_2 C 0.1100(4) 0.1078(5) 0.0148(11) 0.113(4) Uani 1 1 d D U . . .
 H19_2 H 0.089727 0.121361 0.017014 0.136 Uiso 1 1 calc R U . . .
 C20_2 C 0.2524(2) 0.0835(2) 0.0893(6) 0.056(2) Uani 1 1 d D U . . .
 C21_2 C 0.2615(2) 0.0475(2) 0.1156(7) 0.059(2) Uani 1 1 d D U . . .
 C22_2 C 0.3081(3) 0.0593(3) 0.1374(7) 0.063(2) Uani 1 1 d D U . . .
 H22_2 H 0.315495 0.035121 0.152306 0.075 Uiso 1 1 calc R U . . .
 C23_2 C 0.3425(3) 0.1060(2) 0.1366(7) 0.056(2) Uani 1 1 d D U . . .
 H23_2 H 0.374308 0.114579 0.151361 0.067 Uiso 1 1 calc R U . . .
 C24_2 C 0.3325(2) 0.1425(2) 0.1145(6) 0.0465(18) Uani 1 1 d D U . . .
 C25_2 C 0.2872(2) 0.1317(2) 0.0897(6) 0.0500(19) Uani 1 1 d D U . . .
 H25_2 H 0.280159 0.155899 0.073656 0.060 Uiso 1 1 calc R U . . .
 C26_2 C 0.3717(3) 0.1922(2) 0.1140(5) 0.062(2) Uani 1 1 d D U . . .
 F1_3 F 0.4902(3) 0.5605(2) 0.4327(5) 0.103(2) Uani 1 1 d D U . . .
 F2_3 F 0.4508(3) 0.4868(3) 0.4560(8) 0.141(4) Uani 1 1 d D U . . .
 F3_3 F 0.4816(5) 0.5350(5) 0.5591(6) 0.168(4) Uani 1 1 d D U . . .
 F4_3 F 0.66370(19) 0.5803(2) 0.2659(5) 0.0829(19) Uani 1 1 d D U . . .
 F5_3 F 0.6407(2) 0.6313(2) 0.2645(5) 0.086(2) Uani 1 1 d D U . . .
 F6_3 F 0.6515(3) 0.6049(3) 0.1495(4) 0.097(2) Uani 1 1 d D U . . .
 N1_3 N 0.6543(3) 0.5111(3) 0.4437(7) 0.090(3) Uani 1 1 d D U . . .
 N2_3 N 0.5856(2) 0.4507(2) 0.3883(5) 0.0587(18) Uani 1 1 d D U . . .
 N3_3 N 0.4983(2) 0.4248(2) 0.2794(5) 0.0590(19) Uani 1 1 d D U . . .
 N4_3 N 0.4426(3) 0.4445(3) 0.2407(7) 0.086(3) Uani 1 1 d D U . . .
 C1_3 C 0.4905(3) 0.5267(3) 0.4824(6) 0.092(3) Uani 1 1 d D U . . .
 C2_3 C 0.5348(3) 0.5240(3) 0.4748(6) 0.069(2) Uani 1 1 d D U . . .
 C3_3 C 0.5322(3) 0.4839(3) 0.4382(6) 0.052(2) Uani 1 1 d D U . . .
 H3_3 H 0.502303 0.457543 0.421088 0.062 Uiso 1 1 calc R U . . .
 C4_3 C 0.5743(3) 0.4831(3) 0.4272(6) 0.055(2) Uani 1 1 d D U . . .
 C5_3 C 0.6183(3) 0.5209(3) 0.4551(7) 0.072(3) Uani 1 1 d D U . . .
 C6_3 C 0.6199(4) 0.5610(4) 0.4920(8) 0.095(4) Uani 1 1 d D U . . .
 H6_3 H 0.649407 0.586603 0.512258 0.114 Uiso 1 1 calc R U . . .
 C7_3 C 0.5786(4) 0.5631(4) 0.4989(8) 0.089(3) Uani 1 1 d D U . . .
 H7_3 H 0.579791 0.591277 0.520058 0.106 Uiso 1 1 calc R U . . .
 C8_3 C 0.6340(3) 0.4683(3) 0.4070(7) 0.075(3) Uani 1 1 d D U . . .
 C9_3 C 0.6544(3) 0.4389(4) 0.3878(8) 0.085(3) Uani 1 1 d D U . . .
 H9_3 H 0.688002 0.451386 0.390331 0.102 Uiso 1 1 calc R U . . .
 C10_3 C 0.6248(3) 0.3933(4) 0.3664(8) 0.084(3) Uani 1 1 d D U . . .
 H10_3 H 0.637142 0.372059 0.364897 0.101 Uiso 1 1 calc R U . . .
 C11_3 C 0.5754(3) 0.3749(3) 0.3455(7) 0.076(3) Uani 1 1 d D U . . .
 C12_3 C 0.5573(3) 0.4070(3) 0.3463(6) 0.061(2) Uani 1 1 d D U . . .
 C13_3 C 0.5138(3) 0.3937(2) 0.3069(7) 0.063(2) Uani 1 1 d D U . . .
 C14_3 C 0.4813(3) 0.3442(3) 0.2949(9) 0.085(3) Uani 1 1 d D U . . .
 C15_3 C 0.4328(4) 0.3298(3) 0.2754(10) 0.103(4) Uani 1 1 d D U . . .
 H15_3 H 0.411013 0.296528 0.267925 0.124 Uiso 1 1 calc R U . . .
 C16_3 C 0.4159(4) 0.3597(3) 0.2671(10) 0.106(4) Uani 1 1 d D U . . .
 H16_3 H 0.382601 0.348255 0.260846 0.127 Uiso 1 1 calc R U . . .
 C17_3 C 0.4501(3) 0.4100(3) 0.2678(9) 0.087(3) Uani 1 1 d D U . . .
 C18_3 C 0.4987(4) 0.3121(3) 0.3028(9) 0.091(3) Uani 1 1 d D U . . .
 H18_3 H 0.477587 0.278884 0.294079 0.109 Uiso 1 1 calc R U . . .
 C19_3 C 0.5445(4) 0.3278(3) 0.3225(8) 0.084(3) Uani 1 1 d D U . . .
 H19_3 H 0.556176 0.305997 0.320726 0.101 Uiso 1 1 calc R U . . .
 C20_3 C 0.5231(2) 0.4734(2) 0.2573(6) 0.053(2) Uani 1 1 d D U . . .
 C21_3 C 0.4869(2) 0.4839(2) 0.2351(7) 0.062(2) Uani 1 1 d D U . . .
 C22_3 C 0.5001(3) 0.5303(3) 0.2100(7) 0.063(2) Uani 1 1 d D U . . .
 H22_3 H 0.476496 0.538281 0.194114 0.076 Uiso 1 1 calc R U . . .
 C23_3 C 0.5474(3) 0.5641(3) 0.2086(6) 0.052(2) Uani 1 1 d D U . . .
 H23_3 H 0.556555 0.596044 0.193595 0.063 Uiso 1 1 calc R U . . .
 C24_3 C 0.5833(2) 0.5529(2) 0.2289(5) 0.0460(17) Uani 1 1 d D U . . .
 C25_3 C 0.5716(3) 0.5068(2) 0.2496(5) 0.0473(18) Uani 1 1 d D U . . .
 H25_3 H 0.595460 0.498182 0.258129 0.057 Uiso 1 1 calc R U . . .
 C26_3 C 0.6335(3) 0.5914(3) 0.2261(5) 0.062(2) Uani 1 1 d D U . . .
 F1_4 F 0.2953(3) 0.6308(2) 0.2430(6) 0.111(3) Uani 1 1 d D U . . .
 F2_4 F 0.3325(2) 0.5915(2) 0.2396(7) 0.117(3) Uani 1 1 d D U . . .
 F3_4 F 0.3107(4) 0.6104(3) 0.1257(5) 0.134(3) Uani 1 1 d D U . . .
 F4_4 F 0.1111(2) 0.4764(2) 0.4098(5) 0.100(2) Uani 1 1 d D U . . .
 F5_4 F 0.1375(2) 0.5511(2) 0.4069(5) 0.087(2) Uani 1 1 d D U . . .
 F6_4 F 0.1239(3) 0.5147(3) 0.5238(5) 0.113(3) Uani 1 1 d D U . . .
 N1_4 N 0.1228(3) 0.4196(3) 0.2276(7) 0.095(3) Uani 1 1 d D U . . .
 N2_4 N 0.1891(3) 0.4226(3) 0.2842(5) 0.079(3) Uani 1 1 d D U . . .
 N3_4 N 0.2730(3) 0.4783(3) 0.4047(6) 0.075(2) Uani 1 1 d D U . . .
 N4_4 N 0.3301(3) 0.5532(3) 0.4456(7) 0.092(3) Uani 1 1 d D U . . .
 C1_4 C 0.2961(3) 0.5942(3) 0.2028(6) 0.090(3) Uani 1 1 d D U . . .
 C2_4 C 0.2493(3) 0.5492(3) 0.2068(6) 0.065(2) Uani 1 1 d D U . . .
 C3_4 C 0.2470(3) 0.5094(2) 0.2426(5) 0.0506(19) Uani 1 1 d D U . . .
 H3_4 H 0.275208 0.510078 0.262282 0.061 Uiso 1 1 calc R U . . .
 C4_4 C 0.2030(3) 0.4683(3) 0.2494(6) 0.062(2) Uani 1 1 d D U . . .
 C5_4 C 0.1612(3) 0.4644(3) 0.2147(7) 0.086(3) Uani 1 1 d D U . . .
 C6_4 C 0.1643(4) 0.5053(4) 0.1782(8) 0.094(3) Uani 1 1 d D U . . .
 H6_4 H 0.136503 0.504043 0.155239 0.113 Uiso 1 1 calc R U . . .
 C7_4 C 0.2075(3) 0.5473(4) 0.1754(7) 0.082(3) Uani 1 1 d D U . . .
 H7_4 H 0.209126 0.575203 0.151949 0.098 Uiso 1 1 calc R U . . .
 C8_4 C 0.1407(3) 0.3946(3) 0.2626(8) 0.098(4) Uani 1 1 d D U . . .
 C9_4 C 0.1182(5) 0.3437(4) 0.2755(10) 0.121(5) Uani 1 1 d D U . . .
 H9_4 H 0.084979 0.323105 0.264996 0.146 Uiso 1 1 calc R U . . .
 C10_4 C 0.1460(5) 0.3266(4) 0.3030(10) 0.127(5) Uani 1 1 d D U . . .
 H10_4 H 0.132142 0.292796 0.305487 0.152 Uiso 1 1 calc R U . . .
 C11_4 C 0.1948(4) 0.3548(3) 0.3290(9) 0.107(4) Uani 1 1 d D U . . .
 C12_4 C 0.2151(3) 0.4054(3) 0.3295(6) 0.072(3) Uani 1 1 d D U . . .
 C13_4 C 0.2572(4) 0.4331(3) 0.3733(7) 0.082(3) Uani 1 1 d D U . . .
 C14_4 C 0.2870(4) 0.4129(3) 0.3909(9) 0.097(3) Uani 1 1 d D U . . .
 C15_4 C 0.3356(4) 0.4462(4) 0.4100(10) 0.107(4) Uani 1 1 d D U . . .
 H15_4 H 0.356497 0.433587 0.415441 0.129 Uiso 1 1 calc R U . . .
 C16_4 C 0.3549(4) 0.4932(4) 0.4211(10) 0.112(4) Uani 1 1 d D U . . .
 H16_4 H 0.388431 0.514118 0.426293 0.135 Uiso 1 1 calc R U . . .
 C17_4 C 0.3210(3) 0.5099(4) 0.4245(8) 0.086(3) Uani 1 1 d D U . . .
 C18_4 C 0.2685(5) 0.3641(4) 0.3768(10) 0.114(4) Uani 1 1 d D U . . .
 H18_4 H 0.288706 0.350750 0.384623 0.137 Uiso 1 1 calc R U . . .
 C19_4 C 0.2232(5) 0.3356(4) 0.3526(10) 0.109(4) Uani 1 1 d D U . . .
 H19_4 H 0.210312 0.301892 0.351475 0.131 Uiso 1 1 calc R U . . .
 C20_4 C 0.2494(3) 0.5030(3) 0.4260(6) 0.063(2) Uani 1 1 d D U . . .
 C21_4 C 0.2860(3) 0.5494(3) 0.4475(7) 0.072(2) Uani 1 1 d D U . . .
 C22_4 C 0.2753(3) 0.5854(4) 0.4666(8) 0.083(3) Uani 1 1 d D U . . .
 H22_4 H 0.299933 0.617073 0.478899 0.100 Uiso 1 1 calc R U . . .
 C23_4 C 0.2282(3) 0.5734(3) 0.4671(8) 0.076(3) Uani 1 1 d D U . . .
 H23_4 H 0.219873 0.597169 0.479623 0.091 Uiso 1 1 calc R U . . .
 C24_4 C 0.1917(2) 0.5259(3) 0.4491(6) 0.058(2) Uani 1 1 d D U . . .
 C25_4 C 0.2010(3) 0.4901(3) 0.4263(6) 0.056(2) Uani 1 1 d D U . . .
 H25_4 H 0.176286 0.458780 0.411859 0.067 Uiso 1 1 calc R U . . .
 C26_4 C 0.1422(3) 0.5170(3) 0.4481(6) 0.068(3) Uani 1 1 d D U . . .
 F1_5 F 0.4434(2) 0.2499(2) 0.7427(5) 0.106(3) Uani 1 1 d D U . . .
 F2_5 F 0.5181(2) 0.2923(2) 0.7628(6) 0.100(2) Uani 1 1 d D U . . .
 F3_5 F 0.4714(4) 0.2654(3) 0.8697(6) 0.132(3) Uani 1 1 d D U . . .
 F4_5 F 0.4148(2) 0.4155(2) 0.5903(6) 0.113(3) Uani 1 1 d D U . . .
 F5_5 F 0.3677(2) 0.3405(2) 0.5868(6) 0.107(3) Uani 1 1 d D U . . .
 F6_5 F 0.3918(3) 0.3782(3) 0.4723(5) 0.124(3) Uani 1 1 d D U . . .
 N1_5 N 0.4609(4) 0.4483(3) 0.7960(8) 0.114(3) Uani 1 1 d D U . . .
 N2_5 N 0.5316(3) 0.4577(2) 0.7448(6) 0.084(3) Uani 1 1 d D U . . .
 N3_5 N 0.5746(2) 0.4188(2) 0.6201(5) 0.0613(19) Uani 1 1 d D U . . .
 N4_5 N 0.5667(3) 0.3519(3) 0.5565(6) 0.081(2) Uani 1 1 d D U . . .
 C1_5 C 0.4762(3) 0.2842(3) 0.7934(6) 0.073(3) Uani 1 1 d D U . . .
 C2_5 C 0.4728(3) 0.3282(3) 0.7940(7) 0.069(2) Uani 1 1 d D U . . .
 C3_5 C 0.5112(3) 0.3714(3) 0.7707(6) 0.054(2) Uani 1 1 d D U . . .
 H3_5 H 0.541617 0.375017 0.758093 0.065 Uiso 1 1 calc R U . . .
 C4_5 C 0.5027(3) 0.4096(3) 0.7667(7) 0.073(2) Uani 1 1 d D U . . .
 C5_5 C 0.4603(4) 0.4059(3) 0.7989(8) 0.095(3) Uani 1 1 d D U . . .
 C6_5 C 0.4220(4) 0.3613(4) 0.8204(10) 0.110(4) Uani 1 1 d D U . . .
 H6_5 H 0.392052 0.358023 0.835931 0.132 Uiso 1 1 calc R U . . .
 C7_5 C 0.4280(4) 0.3223(4) 0.8190(9) 0.097(3) Uani 1 1 d D U . . .
 H7_5 H 0.402411 0.291666 0.834656 0.117 Uiso 1 1 calc R U . . .
 C8_5 C 0.5043(4) 0.4795(3) 0.7682(9) 0.100(3) Uani 1 1 d D U . . .
 C9_5 C 0.5273(5) 0.5303(4) 0.7658(10) 0.121(4) Uani 1 1 d D U . . .
 H9_5 H 0.509943 0.546221 0.778332 0.145 Uiso 1 1 calc R U . . .
 C10_5 C 0.5735(5) 0.5551(4) 0.7457(9) 0.120(5) Uani 1 1 d D U . . .
 H10_5 H 0.588890 0.589087 0.747658 0.144 Uiso 1 1 calc R U . . .
 C11_5 C 0.6016(4) 0.5341(3) 0.7212(8) 0.124(5) Uani 1 1 d D U . . .
 C12_5 C 0.5770(3) 0.4835(3) 0.7083(6) 0.089(3) Uani 1 1 d D U . . .
 C13_5 C 0.5989(3) 0.4633(3) 0.6608(6) 0.084(3) Uani 1 1 d D U . . .
 C14_5 C 0.6496(3) 0.4887(4) 0.6550(9) 0.116(5) Uani 1 1 d D U . . .
 C15_5 C 0.6717(4) 0.4624(5) 0.6252(9) 0.122(5) Uani 1 1 d D U . . .
 H15_5 H 0.705705 0.478668 0.623477 0.147 Uiso 1 1 calc R U . . .
 C16_5 C 0.6481(3) 0.4166(5) 0.5996(9) 0.112(4) Uani 1 1 d D U . . .
 H16_5 H 0.664865 0.400501 0.584236 0.134 Uiso 1 1 calc R U . . .
 C17_5 C 0.5968(3) 0.3926(4) 0.5959(8) 0.086(3) Uani 1 1 d D U . . .
 C18_5 C 0.6737(4) 0.5380(4) 0.6742(11) 0.139(6) Uani 1 1 d D U . . .
 H18_5 H 0.707380 0.556558 0.666114 0.166 Uiso 1 1 calc R U . . .
 C19_5 C 0.6497(4) 0.5590(5) 0.7037(11) 0.155(7) Uani 1 1 d D U . . .
 H19_5 H 0.666752 0.592609 0.712823 0.186 Uiso 1 1 calc R U . . .
 C20_5 C 0.5282(2) 0.3930(3) 0.5882(6) 0.0501(19) Uani 1 1 d D U . . .
 C21_5 C 0.5237(3) 0.3504(3) 0.5545(6) 0.064(2) Uani 1 1 d D U . . .
 C22_5 C 0.4804(3) 0.3164(3) 0.5191(7) 0.073(3) Uani 1 1 d D U . . .
 H22_5 H 0.476833 0.287616 0.495728 0.088 Uiso 1 1 calc R U . . .
 C23_5 C 0.4433(3) 0.3250(3) 0.5184(8) 0.074(3) Uani 1 1 d D U . . .
 H23_5 H 0.413530 0.301832 0.494778 0.089 Uiso 1 1 calc R U . . .
 C24_5 C 0.4481(2) 0.3679(2) 0.5523(6) 0.056(2) Uani 1 1 d D U . . .
 C25_5 C 0.4906(2) 0.4022(2) 0.5869(5) 0.0432(17) Uani 1 1 d D U . . .
 H25_5 H 0.494171 0.431225 0.609013 0.052 Uiso 1 1 calc R U . . .
 C26_5 C 0.4069(3) 0.3756(3) 0.5494(6) 0.078(3) Uani 1 1 d D U . . .
 F1_6 F 0.1152(3) -0.0744(2) 0.7568(5) 0.099(2) Uani 1 1 d D U . . .
 F2_6 F 0.1907(2) -0.0294(3) 0.7645(6) 0.109(3) Uani 1 1 d D U . . .
 F3_6 F 0.1487(4) -0.0503(3) 0.8759(6) 0.132(3) Uani 1 1 d D U . . .
 F4_6 F 0.0730(3) 0.0767(2) 0.5769(8) 0.140(4) Uani 1 1 d D U . . .
 F5_6 F 0.0293(2) 0.0016(2) 0.5935(5) 0.098(2) Uani 1 1 d D U . . .
 F6_6 F 0.0456(3) 0.0297(5) 0.4707(6) 0.168(5) Uani 1 1 d D U . . .
 N1_6 N 0.1326(4) 0.1265(3) 0.7770(8) 0.105(3) Uani 1 1 d D U . . .
 N2_6 N 0.1998(3) 0.1323(2) 0.7184(6) 0.082(3) Uani 1 1 d D U . . .
 N3_6 N 0.2374(2) 0.0854(3) 0.5958(6) 0.079(2) Uani 1 1 d D U . . .
 N4_6 N 0.2255(3) 0.0129(4) 0.5530(8) 0.104(3) Uani 1 1 d D U . . .
 C1_6 C 0.1497(3) -0.0360(3) 0.7981(6) 0.076(3) Uani 1 1 d D U . . .
 C2_6 C 0.1443(3) 0.0068(3) 0.7907(6) 0.061(2) Uani 1 1 d D U . . .
 C3_6 C 0.1803(3) 0.0484(2) 0.7559(6) 0.052(2) Uani 1 1 d D U . . .
 H3_6 H 0.209579 0.051174 0.737073 0.062 Uiso 1 1 calc R U . . .
 C4_6 C 0.1714(3) 0.0858(3) 0.7500(6) 0.065(2) Uani 1 1 d D U . . .
 C5_6 C 0.1288(4) 0.0827(3) 0.7789(8) 0.090(3) Uani 1 1 d D U . . .
 C6_6 C 0.0937(4) 0.0406(4) 0.8169(9) 0.096(3) Uani 1 1 d D U . . .
 H6_6 H 0.065298 0.038342 0.839216 0.115 Uiso 1 1 calc R U . . .
 C7_6 C 0.1016(3) 0.0026(4) 0.8210(9) 0.082(3) Uani 1 1 d D U . . .
 H7_6 H 0.077725 -0.026837 0.844729 0.099 Uiso 1 1 calc R U . . .
 C8_6 C 0.1737(4) 0.1552(3) 0.7383(9) 0.103(3) Uani 1 1 d D U . . .
 C9_6 C 0.1970(5) 0.2064(4) 0.7284(11) 0.135(5) Uani 1 1 d D U . . .
 H9_6 H 0.180465 0.223448 0.738007 0.162 Uiso 1 1 calc R U . . .
 C10_6 C 0.2430(5) 0.2287(4) 0.7050(11) 0.136(6) Uani 1 1 d D U . . .
 H10_6 H 0.259857 0.262753 0.705662 0.163 Uiso 1 1 calc R U . . .
 C11_6 C 0.2690(4) 0.2059(3) 0.6791(10) 0.129(5) Uani 1 1 d D U . . .
 C12_6 C 0.2434(3) 0.1552(3) 0.6736(7) 0.093(4) Uani 1 1 d D U . . .
 C13_6 C 0.2625(3) 0.1314(3) 0.6290(7) 0.100(4) Uani 1 1 d D U . . .
 C14_6 C 0.3135(3) 0.1557(4) 0.6181(9) 0.128(5) Uani 1 1 d D U . . .
 C15_6 C 0.3329(4) 0.1260(5) 0.5944(11) 0.133(5) Uani 1 1 d D U . . .
 H15_6 H 0.366807 0.141345 0.591061 0.159 Uiso 1 1 calc R U . . .
 C16_6 C 0.3088(4) 0.0792(5) 0.5766(10) 0.129(5) Uani 1 1 d D U . . .
 H16_6 H 0.324807 0.061871 0.564620 0.155 Uiso 1 1 calc R U . . .
 C17_6 C 0.2578(3) 0.0568(4) 0.5765(8) 0.096(3) Uani 1 1 d D U . . .
 C18_6 C 0.3383(5) 0.2052(4) 0.6310(11) 0.156(7) Uani 1 1 d D U . . .
 H18_6 H 0.371559 0.222364 0.618739 0.187 Uiso 1 1 calc R U . . .
 C19_6 C 0.3177(4) 0.2299(4) 0.6598(11) 0.152(7) Uani 1 1 d D U . . .
 H19_6 H 0.336275 0.263622 0.666916 0.182 Uiso 1 1 calc R U . . .
 C20_6 C 0.1895(2) 0.0571(3) 0.5742(6) 0.061(2) Uani 1 1 d D U . . .
 C21_6 C 0.1831(3) 0.0125(3) 0.5500(8) 0.081(3) Uani 1 1 d D U . . .
 C22_6 C 0.1376(3) -0.0251(4) 0.5288(9) 0.092(3) Uani 1 1 d D U . . .
 H22_6 H 0.132718 -0.056114 0.516450 0.110 Uiso 1 1 calc R U . . .
 C23_6 C 0.1008(4) -0.0162(3) 0.5264(8) 0.079(3) Uani 1 1 d D U . . .
 H23_6 H 0.069957 -0.040962 0.509709 0.095 Uiso 1 1 calc R U . . .
 C24_6 C 0.1075(3) 0.0290(3) 0.5483(7) 0.070(3) Uani 1 1 d D U . . .
 C25_6 C 0.1516(3) 0.0665(3) 0.5702(7) 0.061(2) Uani 1 1 d D U . . .
 H25_6 H 0.156147 0.097438 0.582121 0.073 Uiso 1 1 calc R U . . .
 C26_6 C 0.0648(3) 0.0345(3) 0.5470(7) 0.093(4) Uani 1 1 d D U . . .
 F1_7 F 0.1146(3) 0.2591(2) 0.7620(5) 0.097(2) Uani 1 1 d D U . . .
 F2_7 F 0.1870(3) 0.3072(3) 0.7935(8) 0.155(4) Uani 1 1 d D U . . .
 F3_7 F 0.1333(5) 0.2809(4) 0.8891(6) 0.158(4) Uani 1 1 d D U . . .
 F4_7 F 0.0794(2) 0.4065(2) 0.5398(7) 0.123(3) Uani 1 1 d D U . . .
 F5_7 F 0.0367(2) 0.3347(2) 0.5715(4) 0.0841(19) Uani 1 1 d D U . . .
 F6_7 F 0.0573(3) 0.3535(4) 0.4433(5) 0.146(4) Uani 1 1 d D U . . .
 N1_7 N 0.1139(3) 0.4520(3) 0.7506(7) 0.084(3) Uani 1 1 d D U . . .
 N2_7 N 0.1875(2) 0.4625(2) 0.7183(6) 0.074(2) Uani 1 1 d D U . . .
 N3_7 N 0.2398(2) 0.4210(3) 0.6233(6) 0.082(3) Uani 1 1 d D U . . .
 N4_7 N 0.2372(3) 0.3513(4) 0.5894(8) 0.120(4) Uani 1 1 d D U . . .
 C1_7 C 0.1424(4) 0.2974(3) 0.8121(7) 0.101(4) Uani 1 1 d D U . . .
 C2_7 C 0.1345(3) 0.3383(3) 0.7974(7) 0.072(3) Uani 1 1 d D U . . .
 C3_7 C 0.1715(3) 0.3804(3) 0.7675(6) 0.058(2) Uani 1 1 d D U . . .
 H3_7 H 0.202718 0.385015 0.758820 0.070 Uiso 1 1 calc R U . . .
 C4_7 C 0.1602(3) 0.4161(3) 0.7506(6) 0.063(2) Uani 1 1 d D U . . .
 C5_7 C 0.1152(3) 0.4111(3) 0.7664(7) 0.074(3) Uani 1 1 d D U . . .
 C6_7 C 0.0785(3) 0.3668(3) 0.7925(7) 0.079(3) Uani 1 1 d D U . . .
 H6_7 H 0.046886 0.361455 0.799223 0.095 Uiso 1 1 calc R U . . .
 C7_7 C 0.0880(3) 0.3308(4) 0.8086(7) 0.076(3) Uani 1 1 d D U . . .
 H7_7 H 0.063112 0.300557 0.827463 0.091 Uiso 1 1 calc R U . . .
 C8_7 C 0.1579(3) 0.4830(3) 0.7244(8) 0.088(3) Uani 1 1 d D U . . .
 C9_7 C 0.1789(4) 0.5335(3) 0.7108(11) 0.114(4) Uani 1 1 d D U . . .
 H9_7 H 0.159779 0.548328 0.710895 0.136 Uiso 1 1 calc R U . . .
 C10_7 C 0.2260(4) 0.5590(4) 0.6981(12) 0.122(5) Uani 1 1 d D U . . .
 H10_7 H 0.240215 0.592705 0.692374 0.146 Uiso 1 1 calc R U . . .
 C11_7 C 0.2565(4) 0.5388(3) 0.6924(11) 0.116(4) Uani 1 1 d D U . . .
 C12_7 C 0.2347(3) 0.4884(3) 0.6893(8) 0.083(3) Uani 1 1 d D U . . .
 C13_7 C 0.2599(3) 0.4667(3) 0.6593(7) 0.086(3) Uani 1 1 d D U . . .
 C14_7 C 0.3104(3) 0.4958(4) 0.6572(9) 0.109(4) Uani 1 1 d D U . . .
 C15_7 C 0.3352(4) 0.4700(5) 0.6442(11) 0.124(5) Uani 1 1 d D U . . .
 H15_7 H 0.369203 0.487961 0.647238 0.149 Uiso 1 1 calc R U . . .
 C16_7 C 0.3156(3) 0.4235(5) 0.6282(11) 0.119(4) Uani 1 1 d D U . . .
 H16_7 H 0.334713 0.408626 0.625738 0.143 Uiso 1 1 calc R U . . .
 C17_7 C 0.2649(3) 0.3962(4) 0.6146(9) 0.107(4) Uani 1 1 d D U . . .
 C18_7 C 0.3319(4) 0.5456(4) 0.6663(11) 0.115(5) Uani 1 1 d D U . . .
 H18_7 H 0.365477 0.565117 0.658922 0.138 Uiso 1 1 calc R U . . .
 C19_7 C 0.3058(4) 0.5662(4) 0.6850(12) 0.137(6) Uani 1 1 d D U . . .
 H19_7 H 0.321240 0.599845 0.693388 0.164 Uiso 1 1 calc R U . . .
 C20_7 C 0.1945(3) 0.3902(3) 0.5898(6) 0.067(2) Uani 1 1 d D U . . .
 C21_7 C 0.1940(3) 0.3474(4) 0.5704(8) 0.091(3) Uani 1 1 d D U . . .
 C22_7 C 0.1522(4) 0.3086(4) 0.5381(9) 0.105(4) Uani 1 1 d D U . . .
 H22_7 H 0.150909 0.279024 0.526246 0.126 Uiso 1 1 calc R U . . .
 C23_7 C 0.1132(4) 0.3139(4) 0.5237(8) 0.091(3) Uani 1 1 d D U . . .
 H23_7 H 0.084051 0.287392 0.504229 0.109 Uiso 1 1 calc R U . . .
 C24_7 C 0.1160(3) 0.3587(3) 0.5377(6) 0.063(2) Uani 1 1 d D U . . .
 C25_7 C 0.1567(2) 0.3975(3) 0.5687(6) 0.057(2) Uani 1 1 d D U . . .
 H25_7 H 0.158904 0.427807 0.575495 0.068 Uiso 1 1 calc R U . . .
 C26_7 C 0.0732(3) 0.3631(3) 0.5219(6) 0.069(3) Uani 1 1 d D U . . .
 F1_8 F 0.4819(3) 0.2241(2) 0.4299(5) 0.099(2) Uani 1 1 d D U . . .
 F2_8 F 0.4511(3) 0.1533(3) 0.4717(7) 0.128(3) Uani 1 1 d D U . . .
 F3_8 F 0.4865(4) 0.2119(4) 0.5612(5) 0.145(4) Uani 1 1 d D U . . .
 F4_8 F 0.6578(2) 0.2453(3) 0.2291(6) 0.107(3) Uani 1 1 d D U . . .
 F5_8 F 0.6317(2) 0.29389(19) 0.2450(4) 0.0793(18) Uani 1 1 d D U . . .
 F6_8 F 0.6349(3) 0.2689(3) 0.1235(5) 0.123(3) Uani 1 1 d D U . . .
 N1_8 N 0.6615(3) 0.1992(4) 0.4273(9) 0.127(4) Uani 1 1 d D U . . .
 N2_8 N 0.5933(3) 0.1303(3) 0.3942(6) 0.087(3) Uani 1 1 d D U . . .
 N3_8 N 0.5003(2) 0.0896(2) 0.2949(5) 0.0616(19) Uani 1 1 d D U . . .
 N4_8 N 0.4389(3) 0.1014(3) 0.2574(6) 0.078(3) Uani 1 1 d D U . . .
 C1_8 C 0.4898(4) 0.1969(3) 0.4855(6) 0.089(3) Uani 1 1 d D U . . .
 C2_8 C 0.5361(3) 0.1986(3) 0.4713(7) 0.076(3) Uani 1 1 d D U . . .
 C3_8 C 0.5358(3) 0.1582(3) 0.4428(6) 0.060(2) Uani 1 1 d D U . . .
 H3_8 H 0.506808 0.128903 0.434455 0.071 Uiso 1 1 calc R U . . .
 C4_8 C 0.5799(3) 0.1625(3) 0.4268(6) 0.064(2) Uani 1 1 d D U . . .
 C5_8 C 0.6234(3) 0.2058(4) 0.4367(8) 0.100(4) Uani 1 1 d D U . . .
 C6_8 C 0.6219(4) 0.2459(4) 0.4670(9) 0.110(5) Uani 1 1 d D U . . .
 H6_8 H 0.650777 0.275055 0.477680 0.132 Uiso 1 1 calc R U . . .
 C7_8 C 0.5789(4) 0.2426(4) 0.4811(9) 0.105(4) Uani 1 1 d D U . . .
 H7_8 H 0.577643 0.270300 0.497804 0.126 Uiso 1 1 calc R U . . .
 C8_8 C 0.6439(3) 0.1552(4) 0.3972(11) 0.118(4) Uani 1 1 d D U . . .
 C9_8 C 0.6681(5) 0.1284(5) 0.3850(14) 0.147(5) Uani 1 1 d D U . . .
 H9_8 H 0.701992 0.143588 0.382750 0.177 Uiso 1 1 calc R U . . .
 C10_8 C 0.6402(5) 0.0811(5) 0.3769(13) 0.144(5) Uani 1 1 d D U . . .
 H10_8 H 0.655657 0.062559 0.377393 0.173 Uiso 1 1 calc R U . . .
 C11_8 C 0.5896(4) 0.0560(4) 0.3676(11) 0.123(4) Uani 1 1 d D U . . .
 C12_8 C 0.5664(3) 0.0837(3) 0.3627(8) 0.094(3) Uani 1 1 d D U . . .
 C13_8 C 0.5209(3) 0.0640(3) 0.3282(7) 0.082(3) Uani 1 1 d D U . . .
 C14_8 C 0.4925(4) 0.0133(3) 0.3268(8) 0.105(4) Uani 1 1 d D U . . .
 C15_8 C 0.4421(4) -0.0062(4) 0.3123(9) 0.113(4) Uani 1 1 d D U . . .
 H15_8 H 0.422453 -0.040033 0.313122 0.136 Uiso 1 1 calc R U . . .
 C16_8 C 0.4207(4) 0.0195(3) 0.2978(9) 0.102(4) Uani 1 1 d D U . . .
 H16_8 H 0.386829 0.004737 0.294929 0.122 Uiso 1 1 calc R U . . .
 C17_8 C 0.4508(3) 0.0703(3) 0.2868(7) 0.071(3) Uani 1 1 d D U . . .
 C18_8 C 0.5148(5) -0.0141(4) 0.3401(10) 0.130(5) Uani 1 1 d D U . . .
 H18_8 H 0.496494 -0.047989 0.335917 0.155 Uiso 1 1 calc R U . . .
 C19_8 C 0.5615(5) 0.0070(4) 0.3585(11) 0.126(4) Uani 1 1 d D U . . .
 H19_8 H 0.575762 -0.012343 0.365698 0.151 Uiso 1 1 calc R U . . .
 C20_8 C 0.5204(2) 0.1360(2) 0.2620(5) 0.0469(18) Uani 1 1 d D U . . .
 C21_8 C 0.4812(3) 0.1421(3) 0.2420(6) 0.063(2) Uani 1 1 d D U . . .
 C22_8 C 0.4894(3) 0.1859(3) 0.2110(6) 0.063(2) Uani 1 1 d D U . . .
 H22_8 H 0.463499 0.191278 0.199945 0.076 Uiso 1 1 calc R U . . .
 C23_8 C 0.5353(3) 0.2208(3) 0.1968(7) 0.063(2) Uani 1 1 d D U . . .
 H23_8 H 0.541391 0.250726 0.174493 0.076 Uiso 1 1 calc R U . . .
 C24_8 C 0.5742(3) 0.2139(3) 0.2144(6) 0.057(2) Uani 1 1 d D U . . .
 C25_8 C 0.5673(3) 0.1711(2) 0.2458(6) 0.0508(19) Uani 1 1 d D U . . .
 H25_8 H 0.593344 0.165894 0.255911 0.061 Uiso 1 1 calc R U . . .
 C26_8 C 0.6229(3) 0.2545(3) 0.2028(6) 0.076(3) Uani 1 1 d D U . . .
 F1_9 F 0.2577(3) 0.3319(3) -0.0775(7) 0.134(4) Uani 1 1 d D U . . .
 F2_9 F 0.3312(2) 0.3589(2) -0.0646(5) 0.097(2) Uani 1 1 d D U . . .
 F3_9 F 0.3008(4) 0.3460(4) -0.1868(6) 0.153(4) Uani 1 1 d D U . . .
 F4_9 F 0.3668(2) 0.5551(2) 0.1068(6) 0.109(3) Uani 1 1 d D U . . .
 F5_9 F 0.4086(2) 0.5210(3) 0.1019(5) 0.097(2) Uani 1 1 d D U . . .
 F6_9 F 0.3855(3) 0.5324(3) 0.2215(5) 0.124(3) Uani 1 1 d D U . . .
 N1_9 N 0.3282(3) 0.5491(3) -0.1084(8) 0.095(3) Uani 1 1 d D U . . .
 N2_9 N 0.2547(2) 0.4902(3) -0.0665(6) 0.070(2) Uani 1 1 d D U . . .
 N3_9 N 0.2036(2) 0.4062(2) 0.0510(5) 0.0567(18) Uani 1 1 d D U . . .
 N4_9 N 0.2051(3) 0.3429(3) 0.1112(7) 0.095(3) Uani 1 1 d D U . . .
 C1_9 C 0.2995(3) 0.3636(3) -0.1128(7) 0.089(3) Uani 1 1 d D U . . .
 C2_9 C 0.3072(3) 0.4128(3) -0.1128(7) 0.068(2) Uani 1 1 d D U . . .
 C3_9 C 0.2705(3) 0.4211(3) -0.0919(6) 0.060(2) Uani 1 1 d D U . . .
 H3_9 H 0.239095 0.395697 -0.079785 0.072 Uiso 1 1 calc R U . . .
 C4_9 C 0.2818(3) 0.4688(3) -0.0896(7) 0.066(2) Uani 1 1 d D U . . .
 C5_9 C 0.3275(3) 0.5070(3) -0.1094(8) 0.080(3) Uani 1 1 d D U . . .
 C6_9 C 0.3636(3) 0.4973(4) -0.1333(9) 0.085(3) Uani 1 1 d D U . . .
 H6_9 H 0.394297 0.522393 -0.149725 0.102 Uiso 1 1 calc R U . . .
 C7_9 C 0.3535(3) 0.4509(3) -0.1326(9) 0.087(3) Uani 1 1 d D U . . .
 H7_9 H 0.378179 0.443951 -0.145609 0.104 Uiso 1 1 calc R U . . .
 C8_9 C 0.2847(3) 0.5391(3) -0.0847(10) 0.098(3) Uani 1 1 d D U . . .
 C9_9 C 0.2640(4) 0.5693(4) -0.0831(11) 0.114(4) Uani 1 1 d D U . . .
 H9_9 H 0.283324 0.602994 -0.089506 0.137 Uiso 1 1 calc R U . . .
 C10_9 C 0.2165(4) 0.5487(4) -0.0724(11) 0.111(4) Uani 1 1 d D U . . .
 H10_9 H 0.202164 0.567945 -0.080534 0.134 Uiso 1 1 calc R U . . .
 C11_9 C 0.1861(3) 0.5000(4) -0.0497(9) 0.090(3) Uani 1 1 d D U . . .
 C12_9 C 0.2079(3) 0.4717(3) -0.0353(7) 0.070(2) Uani 1 1 d D U . . .
 C13_9 C 0.1824(3) 0.4288(3) 0.0093(6) 0.062(2) Uani 1 1 d D U . . .
 C14_9 C 0.1319(3) 0.4065(4) 0.0123(8) 0.086(3) Uani 1 1 d D U . . .
 C15_9 C 0.1064(4) 0.3574(4) 0.0376(9) 0.098(4) Uani 1 1 d D U . . .
 H15_9 H 0.072362 0.341479 0.037179 0.118 Uiso 1 1 calc R U . . .
 C16_9 C 0.1270(3) 0.3322(4) 0.0617(9) 0.103(4) Uani 1 1 d D U . . .
 H16_9 H 0.108448 0.298650 0.071451 0.123 Uiso 1 1 calc R U . . .
 C17_9 C 0.1780(3) 0.3573(3) 0.0724(8) 0.085(3) Uani 1 1 d D U . . .
 C18_9 C 0.1107(3) 0.4338(4) -0.0107(8) 0.090(3) Uani 1 1 d D U . . .
 H18_9 H 0.076808 0.419560 -0.008802 0.108 Uiso 1 1 calc R U . . .
 C19_9 C 0.1374(4) 0.4796(4) -0.0352(10) 0.100(3) Uani 1 1 d D U . . .
 H19_9 H 0.122556 0.498497 -0.042722 0.121 Uiso 1 1 calc R U . . .
 C20_9 C 0.2490(2) 0.4229(2) 0.0851(6) 0.0518(19) Uani 1 1 d D U . . .
 C21_9 C 0.2486(3) 0.3828(3) 0.1217(8) 0.077(3) Uani 1 1 d D U . . .
 C22_9 C 0.2895(3) 0.3883(3) 0.1609(8) 0.082(3) Uani 1 1 d D U . . .
 H22_9 H 0.289608 0.361539 0.186181 0.098 Uiso 1 1 calc R U . . .
 C23_9 C 0.3292(3) 0.4319(3) 0.1629(7) 0.073(3) Uani 1 1 d D U . . .
 H23_9 H 0.358241 0.435320 0.184880 0.087 Uiso 1 1 calc R U . . .
 C24_9 C 0.3281(2) 0.4727(3) 0.1325(6) 0.058(2) Uani 1 1 d D U . . .
 C25_9 C 0.2879(2) 0.4688(2) 0.0950(6) 0.0482(18) Uani 1 1 d D U . . .
 H25_9 H 0.286711 0.496210 0.076576 0.058 Uiso 1 1 calc R U . . .
 C26_9 C 0.3715(3) 0.5193(3) 0.1415(6) 0.081(3) Uani 1 1 d D U . . .


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 F1_1 C1_1 1.345(9) . ?
 F2_1 C1_1 1.344(9) . ?
 F3_1 C1_1 1.309(9) . ?
 F4_1 C26_1 1.362(10) . ?
 F5_1 C26_1 1.319(9) . ?
 F6_1 C26_1 1.315(9) . ?
 N1_1 C5_1 1.364(9) . ?
 N1_1 C8_1 1.335(9) . ?
 N2_1 C4_1 1.410(9) . ?
 N2_1 C8_1 1.412(10) . ?
 N2_1 C12_1 1.410(9) . ?
 N3_1 C13_1 1.382(8) . ?
 N3_1 C17_1 1.397(9) . ?
 N3_1 C20_1 1.388(8) . ?
 N4_1 C17_1 1.314(8) . ?
 N4_1 C21_1 1.359(8) . ?
 C1_1 C2_1 1.476(9) . ?
 C2_1 C3_1 1.371(9) . ?
 C2_1 C7_1 1.405(10) . ?
 C3_1 H3_1 0.9500 . ?
 C3_1 C4_1 1.395(9) . ?
 C4_1 C5_1 1.400(10) . ?
 C5_1 C6_1 1.404(11) . ?
 C6_1 H6_1 0.9500 . ?
 C6_1 C7_1 1.371(11) . ?
 C7_1 H7_1 0.9500 . ?
 C8_1 C9_1 1.440(11) . ?
 C9_1 H9_1 0.9500 . ?
 C9_1 C10_1 1.341(12) . ?
 C10_1 H10_1 0.9500 . ?
 C10_1 C11_1 1.422(12) . ?
 C11_1 C12_1 1.429(10) . ?
 C11_1 C19_1 1.380(11) . ?
 C12_1 C13_1 1.386(10) . ?
 C13_1 C14_1 1.432(9) . ?
 C14_1 C15_1 1.419(11) . ?
 C14_1 C18_1 1.397(11) . ?
 C15_1 H15_1 0.9500 . ?
 C15_1 C16_1 1.319(11) . ?
 C16_1 H16_1 0.9500 . ?
 C16_1 C17_1 1.428(10) . ?
 C18_1 H18_1 0.9500 . ?
 C18_1 C19_1 1.338(12) . ?
 C19_1 H19_1 0.9500 . ?
 C20_1 C21_1 1.411(9) . ?
 C20_1 C25_1 1.403(8) . ?
 C21_1 C22_1 1.386(9) . ?
 C22_1 H22_1 0.9500 . ?
 C22_1 C23_1 1.348(10) . ?
 C23_1 H23_1 0.9500 . ?
 C23_1 C24_1 1.406(9) . ?
 C24_1 C25_1 1.372(8) . ?
 C24_1 C26_1 1.470(9) . ?
 C25_1 H25_1 0.9500 . ?
 F1_2 C1_2 1.347(9) . ?
 F2_2 C1_2 1.351(9) . ?
 F3_2 C1_2 1.304(10) . ?
 F4_2 C26_2 1.341(8) . ?
 F5_2 C26_2 1.342(8) . ?
 F6_2 C26_2 1.319(9) . ?
 N1_2 C5_2 1.347(9) . ?
 N1_2 C8_2 1.331(9) . ?
 N2_2 C4_2 1.402(9) . ?
 N2_2 C8_2 1.409(9) . ?
 N2_2 C12_2 1.397(9) . ?
 N3_2 C13_2 1.396(8) . ?
 N3_2 C17_2 1.393(9) . ?
 N3_2 C20_2 1.396(7) . ?
 N4_2 C17_2 1.330(8) . ?
 N4_2 C21_2 1.364(7) . ?
 C1_2 C2_2 1.490(10) . ?
 C2_2 C3_2 1.369(9) . ?
 C2_2 C7_2 1.419(9) . ?
 C3_2 H3_2 0.9500 . ?
 C3_2 C4_2 1.386(8) . ?
 C4_2 C5_2 1.409(9) . ?
 C5_2 C6_2 1.398(10) . ?
 C6_2 H6_2 0.9500 . ?
 C6_2 C7_2 1.374(11) . ?
 C7_2 H7_2 0.9500 . ?
 C8_2 C9_2 1.430(10) . ?
 C9_2 H9_2 0.9500 . ?
 C9_2 C10_2 1.343(11) . ?
 C10_2 H10_2 0.9500 . ?
 C10_2 C11_2 1.428(11) . ?
 C11_2 C12_2 1.419(9) . ?
 C11_2 C19_2 1.391(11) . ?
 C12_2 C13_2 1.390(10) . ?
 C13_2 C14_2 1.411(9) . ?
 C14_2 C15_2 1.427(11) . ?
 C14_2 C18_2 1.408(10) . ?
 C15_2 H15_2 0.9500 . ?
 C15_2 C16_2 1.334(11) . ?
 C16_2 H16_2 0.9500 . ?
 C16_2 C17_2 1.423(9) . ?
 C18_2 H18_2 0.9500 . ?
 C18_2 C19_2 1.335(11) . ?
 C19_2 H19_2 0.9500 . ?
 C20_2 C21_2 1.393(8) . ?
 C20_2 C25_2 1.391(8) . ?
 C21_2 C22_2 1.397(8) . ?
 C22_2 H22_2 0.9500 . ?
 C22_2 C23_2 1.354(9) . ?
 C23_2 H23_2 0.9500 . ?
 C23_2 C24_2 1.408(8) . ?
 C24_2 C25_2 1.378(8) . ?
 C24_2 C26_2 1.463(8) . ?
 C25_2 H25_2 0.9500 . ?
 F1_3 C1_3 1.346(9) . ?
 F2_3 C1_3 1.348(10) . ?
 F3_3 C1_3 1.301(10) . ?
 F4_3 C26_3 1.346(8) . ?
 F5_3 C26_3 1.335(8) . ?
 F6_3 C26_3 1.315(8) . ?
 N1_3 C5_3 1.360(8) . ?
 N1_3 C8_3 1.328(8) . ?
 N2_3 C4_3 1.407(8) . ?
 N2_3 C8_3 1.399(8) . ?
 N2_3 C12_3 1.403(8) . ?
 N3_3 C13_3 1.392(8) . ?
 N3_3 C17_3 1.392(9) . ?
 N3_3 C20_3 1.402(7) . ?
 N4_3 C17_3 1.323(8) . ?
 N4_3 C21_3 1.359(8) . ?
 C1_3 C2_3 1.478(9) . ?
 C2_3 C3_3 1.381(8) . ?
 C2_3 C7_3 1.395(10) . ?
 C3_3 H3_3 0.9500 . ?
 C3_3 C4_3 1.383(8) . ?
 C4_3 C5_3 1.400(9) . ?
 C5_3 C6_3 1.394(10) . ?
 C6_3 H6_3 0.9500 . ?
 C6_3 C7_3 1.374(10) . ?
 C7_3 H7_3 0.9500 . ?
 C8_3 C9_3 1.431(10) . ?
 C9_3 H9_3 0.9500 . ?
 C9_3 C10_3 1.333(11) . ?
 C10_3 H10_3 0.9500 . ?
 C10_3 C11_3 1.432(10) . ?
 C11_3 C12_3 1.420(9) . ?
 C11_3 C19_3 1.385(10) . ?
 C12_3 C13_3 1.392(9) . ?
 C13_3 C14_3 1.419(9) . ?
 C14_3 C15_3 1.426(10) . ?
 C14_3 C18_3 1.405(10) . ?
 C15_3 H15_3 0.9500 . ?
 C15_3 C16_3 1.331(11) . ?
 C16_3 H16_3 0.9500 . ?
 C16_3 C17_3 1.435(9) . ?
 C18_3 H18_3 0.9500 . ?
 C18_3 C19_3 1.336(11) . ?
 C19_3 H19_3 0.9500 . ?
 C20_3 C21_3 1.410(8) . ?
 C20_3 C25_3 1.391(8) . ?
 C21_3 C22_3 1.394(8) . ?
 C22_3 H22_3 0.9500 . ?
 C22_3 C23_3 1.361(9) . ?
 C23_3 H23_3 0.9500 . ?
 C23_3 C24_3 1.410(8) . ?
 C24_3 C25_3 1.377(8) . ?
 C24_3 C26_3 1.469(8) . ?
 C25_3 H25_3 0.9500 . ?
 F1_4 C1_4 1.349(9) . ?
 F2_4 C1_4 1.352(9) . ?
 F3_4 C1_4 1.312(9) . ?
 F4_4 C26_4 1.331(9) . ?
 F5_4 C26_4 1.349(8) . ?
 F6_4 C26_4 1.317(9) . ?
 N1_4 C5_4 1.367(8) . ?
 N1_4 C8_4 1.324(9) . ?
 N2_4 C4_4 1.418(8) . ?
 N2_4 C8_4 1.398(9) . ?
 N2_4 C12_4 1.411(9) . ?
 N3_4 C13_4 1.373(9) . ?
 N3_4 C17_4 1.397(9) . ?
 N3_4 C20_4 1.392(8) . ?
 N4_4 C17_4 1.319(8) . ?
 N4_4 C21_4 1.365(8) . ?
 C1_4 C2_4 1.482(9) . ?
 C2_4 C3_4 1.370(8) . ?
 C2_4 C7_4 1.408(9) . ?
 C3_4 H3_4 0.9500 . ?
 C3_4 C4_4 1.380(8) . ?
 C4_4 C5_4 1.398(9) . ?
 C5_4 C6_4 1.396(10) . ?
 C6_4 H6_4 0.9500 . ?
 C6_4 C7_4 1.374(10) . ?
 C7_4 H7_4 0.9500 . ?
 C8_4 C9_4 1.440(10) . ?
 C9_4 H9_4 0.9500 . ?
 C9_4 C10_4 1.339(12) . ?
 C10_4 H10_4 0.9500 . ?
 C10_4 C11_4 1.426(11) . ?
 C11_4 C12_4 1.422(9) . ?
 C11_4 C19_4 1.389(11) . ?
 C12_4 C13_4 1.379(10) . ?
 C13_4 C14_4 1.429(9) . ?
 C14_4 C15_4 1.420(11) . ?
 C14_4 C18_4 1.396(10) . ?
 C15_4 H15_4 0.9500 . ?
 C15_4 C16_4 1.331(11) . ?
 C16_4 H16_4 0.9500 . ?
 C16_4 C17_4 1.439(10) . ?
 C18_4 H18_4 0.9500 . ?
 C18_4 C19_4 1.334(11) . ?
 C19_4 H19_4 0.9500 . ?
 C20_4 C21_4 1.407(9) . ?
 C20_4 C25_4 1.400(8) . ?
 C21_4 C22_4 1.398(9) . ?
 C22_4 H22_4 0.9500 . ?
 C22_4 C23_4 1.367(9) . ?
 C23_4 H23_4 0.9500 . ?
 C23_4 C24_4 1.418(9) . ?
 C24_4 C25_4 1.379(8) . ?
 C24_4 C26_4 1.471(9) . ?
 C25_4 H25_4 0.9500 . ?
 F1_5 C1_5 1.345(9) . ?
 F2_5 C1_5 1.332(9) . ?
 F3_5 C1_5 1.320(9) . ?
 F4_5 C26_5 1.344(9) . ?
 F5_5 C26_5 1.341(8) . ?
 F6_5 C26_5 1.326(9) . ?
 N1_5 C5_5 1.358(8) . ?
 N1_5 C8_5 1.324(9) . ?
 N2_5 C4_5 1.396(9) . ?
 N2_5 C8_5 1.421(9) . ?
 N2_5 C12_5 1.395(9) . ?
 N3_5 C13_5 1.401(9) . ?
 N3_5 C17_5 1.405(9) . ?
 N3_5 C20_5 1.394(8) . ?
 N4_5 C17_5 1.331(9) . ?
 N4_5 C21_5 1.363(8) . ?
 C1_5 C2_5 1.478(9) . ?
 C2_5 C3_5 1.373(9) . ?
 C2_5 C7_5 1.416(9) . ?
 C3_5 H3_5 0.9500 . ?
 C3_5 C4_5 1.391(8) . ?
 C4_5 C5_5 1.405(9) . ?
 C5_5 C6_5 1.390(10) . ?
 C6_5 H6_5 0.9500 . ?
 C6_5 C7_5 1.363(10) . ?
 C7_5 H7_5 0.9500 . ?
 C8_5 C9_5 1.421(10) . ?
 C9_5 H9_5 0.9500 . ?
 C9_5 C10_5 1.331(12) . ?
 C10_5 H10_5 0.9500 . ?
 C10_5 C11_5 1.429(11) . ?
 C11_5 C12_5 1.428(10) . ?
 C11_5 C19_5 1.372(11) . ?
 C12_5 C13_5 1.395(10) . ?
 C13_5 C14_5 1.419(10) . ?
 C14_5 C15_5 1.432(11) . ?
 C14_5 C18_5 1.409(11) . ?
 C15_5 H15_5 0.9500 . ?
 C15_5 C16_5 1.342(11) . ?
 C16_5 H16_5 0.9500 . ?
 C16_5 C17_5 1.434(10) . ?
 C18_5 H18_5 0.9500 . ?
 C18_5 C19_5 1.341(12) . ?
 C19_5 H19_5 0.9500 . ?
 C20_5 C21_5 1.409(8) . ?
 C20_5 C25_5 1.384(8) . ?
 C21_5 C22_5 1.391(9) . ?
 C22_5 H22_5 0.9500 . ?
 C22_5 C23_5 1.356(9) . ?
 C23_5 H23_5 0.9500 . ?
 C23_5 C24_5 1.416(8) . ?
 C24_5 C25_5 1.373(8) . ?
 C24_5 C26_5 1.468(8) . ?
 C25_5 H25_5 0.9500 . ?
 F1_6 C1_6 1.346(9) . ?
 F2_6 C1_6 1.338(9) . ?
 F3_6 C1_6 1.302(9) . ?
 F4_6 C26_6 1.337(9) . ?
 F5_6 C26_6 1.327(9) . ?
 F6_6 C26_6 1.324(10) . ?
 N1_6 C5_6 1.355(8) . ?
 N1_6 C8_6 1.327(9) . ?
 N2_6 C4_6 1.400(8) . ?
 N2_6 C8_6 1.405(9) . ?
 N2_6 C12_6 1.409(9) . ?
 N3_6 C13_6 1.386(9) . ?
 N3_6 C17_6 1.410(9) . ?
 N3_6 C20_6 1.387(8) . ?
 N4_6 C17_6 1.323(9) . ?
 N4_6 C21_6 1.365(8) . ?
 C1_6 C2_6 1.480(9) . ?
 C2_6 C3_6 1.374(8) . ?
 C2_6 C7_6 1.402(9) . ?
 C3_6 H3_6 0.9500 . ?
 C3_6 C4_6 1.376(9) . ?
 C4_6 C5_6 1.400(9) . ?
 C5_6 C6_6 1.395(10) . ?
 C6_6 H6_6 0.9500 . ?
 C6_6 C7_6 1.369(10) . ?
 C7_6 H7_6 0.9500 . ?
 C8_6 C9_6 1.439(10) . ?
 C9_6 H9_6 0.9500 . ?
 C9_6 C10_6 1.338(12) . ?
 C10_6 H10_6 0.9500 . ?
 C10_6 C11_6 1.423(12) . ?
 C11_6 C12_6 1.418(10) . ?
 C11_6 C19_6 1.394(11) . ?
 C12_6 C13_6 1.391(10) . ?
 C13_6 C14_6 1.433(10) . ?
 C14_6 C15_6 1.431(11) . ?
 C14_6 C18_6 1.396(11) . ?
 C15_6 H15_6 0.9500 . ?
 C15_6 C16_6 1.337(11) . ?
 C16_6 H16_6 0.9500 . ?
 C16_6 C17_6 1.429(10) . ?
 C18_6 H18_6 0.9500 . ?
 C18_6 C19_6 1.345(12) . ?
 C19_6 H19_6 0.9500 . ?
 C20_6 C21_6 1.400(9) . ?
 C20_6 C25_6 1.400(8) . ?
 C21_6 C22_6 1.397(9) . ?
 C22_6 H22_6 0.9500 . ?
 C22_6 C23_6 1.354(10) . ?
 C23_6 H23_6 0.9500 . ?
 C23_6 C24_6 1.407(9) . ?
 C24_6 C25_6 1.372(9) . ?
 C24_6 C26_6 1.472(9) . ?
 C25_6 H25_6 0.9500 . ?
 F1_7 C1_7 1.356(10) . ?
 F2_7 C1_7 1.342(10) . ?
 F3_7 C1_7 1.296(10) . ?
 F4_7 C26_7 1.344(9) . ?
 F5_7 C26_7 1.325(8) . ?
 F6_7 C26_7 1.316(9) . ?
 N1_7 C5_7 1.362(8) . ?
 N1_7 C8_7 1.329(9) . ?
 N2_7 C4_7 1.398(8) . ?
 N2_7 C8_7 1.410(9) . ?
 N2_7 C12_7 1.398(9) . ?
 N3_7 C13_7 1.401(9) . ?
 N3_7 C17_7 1.399(9) . ?
 N3_7 C20_7 1.395(8) . ?
 N4_7 C17_7 1.327(9) . ?
 N4_7 C21_7 1.365(8) . ?
 C1_7 C2_7 1.482(10) . ?
 C2_7 C3_7 1.368(9) . ?
 C2_7 C7_7 1.404(9) . ?
 C3_7 H3_7 0.9500 . ?
 C3_7 C4_7 1.397(9) . ?
 C4_7 C5_7 1.400(9) . ?
 C5_7 C6_7 1.388(10) . ?
 C6_7 H6_7 0.9500 . ?
 C6_7 C7_7 1.363(10) . ?
 C7_7 H7_7 0.9500 . ?
 C8_7 C9_7 1.431(10) . ?
 C9_7 H9_7 0.9500 . ?
 C9_7 C10_7 1.334(11) . ?
 C10_7 H10_7 0.9500 . ?
 C10_7 C11_7 1.426(11) . ?
 C11_7 C12_7 1.413(10) . ?
 C11_7 C19_7 1.384(11) . ?
 C12_7 C13_7 1.392(10) . ?
 C13_7 C14_7 1.416(9) . ?
 C14_7 C15_7 1.429(11) . ?
 C14_7 C18_7 1.404(11) . ?
 C15_7 H15_7 0.9500 . ?
 C15_7 C16_7 1.330(11) . ?
 C16_7 H16_7 0.9500 . ?
 C16_7 C17_7 1.434(10) . ?
 C18_7 H18_7 0.9500 . ?
 C18_7 C19_7 1.338(12) . ?
 C19_7 H19_7 0.9500 . ?
 C20_7 C21_7 1.408(9) . ?
 C20_7 C25_7 1.393(8) . ?
 C21_7 C22_7 1.398(10) . ?
 C22_7 H22_7 0.9500 . ?
 C22_7 C23_7 1.372(10) . ?
 C23_7 H23_7 0.9500 . ?
 C23_7 C24_7 1.419(9) . ?
 C24_7 C25_7 1.372(8) . ?
 C24_7 C26_7 1.476(9) . ?
 C25_7 H25_7 0.9500 . ?
 F1_8 C1_8 1.351(9) . ?
 F2_8 C1_8 1.351(9) . ?
 F3_8 C1_8 1.310(9) . ?
 F4_8 C26_8 1.363(9) . ?
 F5_8 C26_8 1.331(8) . ?
 F6_8 C26_8 1.321(9) . ?
 N1_8 C5_8 1.354(9) . ?
 N1_8 C8_8 1.325(9) . ?
 N2_8 C4_8 1.407(9) . ?
 N2_8 C8_8 1.415(9) . ?
 N2_8 C12_8 1.397(9) . ?
 N3_8 C13_8 1.395(8) . ?
 N3_8 C17_8 1.399(9) . ?
 N3_8 C20_8 1.397(8) . ?
 N4_8 C17_8 1.325(8) . ?
 N4_8 C21_8 1.360(8) . ?
 C1_8 C2_8 1.483(10) . ?
 C2_8 C3_8 1.372(9) . ?
 C2_8 C7_8 1.410(10) . ?
 C3_8 H3_8 0.9500 . ?
 C3_8 C4_8 1.381(9) . ?
 C4_8 C5_8 1.410(10) . ?
 C5_8 C6_8 1.401(10) . ?
 C6_8 H6_8 0.9500 . ?
 C6_8 C7_8 1.356(11) . ?
 C7_8 H7_8 0.9500 . ?
 C8_8 C9_8 1.435(11) . ?
 C9_8 H9_8 0.9500 . ?
 C9_8 C10_8 1.334(12) . ?
 C10_8 H10_8 0.9500 . ?
 C10_8 C11_8 1.423(11) . ?
 C11_8 C12_8 1.425(10) . ?
 C11_8 C19_8 1.379(11) . ?
 C12_8 C13_8 1.386(10) . ?
 C13_8 C14_8 1.420(10) . ?
 C14_8 C15_8 1.438(11) . ?
 C14_8 C18_8 1.404(11) . ?
 C15_8 H15_8 0.9500 . ?
 C15_8 C16_8 1.337(11) . ?
 C16_8 H16_8 0.9500 . ?
 C16_8 C17_8 1.436(9) . ?
 C18_8 H18_8 0.9500 . ?
 C18_8 C19_8 1.338(12) . ?
 C19_8 H19_8 0.9500 . ?
 C20_8 C21_8 1.409(9) . ?
 C20_8 C25_8 1.387(8) . ?
 C21_8 C22_8 1.389(9) . ?
 C22_8 H22_8 0.9500 . ?
 C22_8 C23_8 1.359(9) . ?
 C23_8 H23_8 0.9500 . ?
 C23_8 C24_8 1.406(9) . ?
 C24_8 C25_8 1.374(8) . ?
 C24_8 C26_8 1.471(9) . ?
 C25_8 H25_8 0.9500 . ?
 F1_9 C1_9 1.339(9) . ?
 F2_9 C1_9 1.342(9) . ?
 F3_9 C1_9 1.306(10) . ?
 F4_9 C26_9 1.351(9) . ?
 F5_9 C26_9 1.325(8) . ?
 F6_9 C26_9 1.334(9) . ?
 N1_9 C5_9 1.348(8) . ?
 N1_9 C8_9 1.327(8) . ?
 N2_9 C4_9 1.406(8) . ?
 N2_9 C8_9 1.406(9) . ?
 N2_9 C12_9 1.405(8) . ?
 N3_9 C13_9 1.389(8) . ?
 N3_9 C17_9 1.404(9) . ?
 N3_9 C20_9 1.391(8) . ?
 N4_9 C17_9 1.326(8) . ?
 N4_9 C21_9 1.360(8) . ?
 C1_9 C2_9 1.479(9) . ?
 C2_9 C3_9 1.380(8) . ?
 C2_9 C7_9 1.413(9) . ?
 C3_9 H3_9 0.9500 . ?
 C3_9 C4_9 1.392(9) . ?
 C4_9 C5_9 1.404(9) . ?
 C5_9 C6_9 1.396(9) . ?
 C6_9 H6_9 0.9500 . ?
 C6_9 C7_9 1.363(10) . ?
 C7_9 H7_9 0.9500 . ?
 C8_9 C9_9 1.430(10) . ?
 C9_9 H9_9 0.9500 . ?
 C9_9 C10_9 1.341(11) . ?
 C10_9 H10_9 0.9500 . ?
 C10_9 C11_9 1.419(11) . ?
 C11_9 C12_9 1.418(9) . ?
 C11_9 C19_9 1.388(10) . ?
 C12_9 C13_9 1.395(9) . ?
 C13_9 C14_9 1.415(9) . ?
 C14_9 C15_9 1.429(11) . ?
 C14_9 C18_9 1.406(10) . ?
 C15_9 H15_9 0.9500 . ?
 C15_9 C16_9 1.337(11) . ?
 C16_9 H16_9 0.9500 . ?
 C16_9 C17_9 1.436(10) . ?
 C18_9 H18_9 0.9500 . ?
 C18_9 C19_9 1.342(11) . ?
 C19_9 H19_9 0.9500 . ?
 C20_9 C21_9 1.408(9) . ?
 C20_9 C25_9 1.390(8) . ?
 C21_9 C22_9 1.388(9) . ?
 C22_9 H22_9 0.9500 . ?
 C22_9 C23_9 1.348(10) . ?
 C23_9 H23_9 0.9500 . ?
 C23_9 C24_9 1.417(9) . ?
 C24_9 C25_9 1.372(8) . ?
 C24_9 C26_9 1.462(9) . ?
 C25_9 H25_9 0.9500 . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 C8_1 N1_1 C5_1 106.4(9) . . ?
 C4_1 N2_1 C8_1 103.8(7) . . ?
 C12_1 N2_1 C4_1 134.1(8) . . ?
 C12_1 N2_1 C8_1 122.1(8) . . ?
 C13_1 N3_1 C17_1 121.3(7) . . ?
 C13_1 N3_1 C20_1 133.0(7) . . ?
 C20_1 N3_1 C17_1 105.7(6) . . ?
 C17_1 N4_1 C21_1 104.3(7) . . ?
 F1_1 C1_1 C2_1 114.1(8) . . ?
 F2_1 C1_1 F1_1 99.4(8) . . ?
 F2_1 C1_1 C2_1 113.5(7) . . ?
 F3_1 C1_1 F1_1 104.5(8) . . ?
 F3_1 C1_1 F2_1 109.2(10) . . ?
 F3_1 C1_1 C2_1 114.7(9) . . ?
 C3_1 C2_1 C1_1 118.9(7) . . ?
 C3_1 C2_1 C7_1 121.2(8) . . ?
 C7_1 C2_1 C1_1 119.9(8) . . ?
 C2_1 C3_1 H3_1 120.8 . . ?
 C2_1 C3_1 C4_1 118.4(8) . . ?
 C4_1 C3_1 H3_1 120.8 . . ?
 C3_1 C4_1 N2_1 130.8(8) . . ?
 C3_1 C4_1 C5_1 122.4(8) . . ?
 C5_1 C4_1 N2_1 106.8(7) . . ?
 N1_1 C5_1 C4_1 110.0(8) . . ?
 N1_1 C5_1 C6_1 132.9(10) . . ?
 C4_1 C5_1 C6_1 117.0(8) . . ?
 C5_1 C6_1 H6_1 119.1 . . ?
 C7_1 C6_1 C5_1 121.8(10) . . ?
 C7_1 C6_1 H6_1 119.1 . . ?
 C2_1 C7_1 H7_1 120.4 . . ?
 C6_1 C7_1 C2_1 119.3(10) . . ?
 C6_1 C7_1 H7_1 120.4 . . ?
 N1_1 C8_1 N2_1 112.3(8) . . ?
 N1_1 C8_1 C9_1 129.4(10) . . ?
 N2_1 C8_1 C9_1 118.1(9) . . ?
 C8_1 C9_1 H9_1 121.0 . . ?
 C10_1 C9_1 C8_1 118.0(11) . . ?
 C10_1 C9_1 H9_1 121.0 . . ?
 C9_1 C10_1 H10_1 117.8 . . ?
 C9_1 C10_1 C11_1 124.3(12) . . ?
 C11_1 C10_1 H10_1 117.8 . . ?
 C10_1 C11_1 C12_1 117.7(10) . . ?
 C19_1 C11_1 C10_1 123.9(10) . . ?
 C19_1 C11_1 C12_1 118.0(9) . . ?
 N2_1 C12_1 C11_1 115.8(8) . . ?
 C13_1 C12_1 N2_1 125.1(7) . . ?
 C13_1 C12_1 C11_1 119.0(8) . . ?
 N3_1 C13_1 C12_1 124.5(7) . . ?
 N3_1 C13_1 C14_1 117.3(8) . . ?
 C12_1 C13_1 C14_1 118.2(8) . . ?
 C15_1 C14_1 C13_1 117.0(8) . . ?
 C18_1 C14_1 C13_1 118.8(9) . . ?
 C18_1 C14_1 C15_1 124.3(9) . . ?
 C14_1 C15_1 H15_1 117.5 . . ?
 C16_1 C15_1 C14_1 125.0(9) . . ?
 C16_1 C15_1 H15_1 117.5 . . ?
 C15_1 C16_1 H16_1 121.4 . . ?
 C15_1 C16_1 C17_1 117.2(10) . . ?
 C17_1 C16_1 H16_1 121.4 . . ?
 N3_1 C17_1 C16_1 120.0(8) . . ?
 N4_1 C17_1 N3_1 113.4(7) . . ?
 N4_1 C17_1 C16_1 126.2(8) . . ?
 C14_1 C18_1 H18_1 120.0 . . ?
 C19_1 C18_1 C14_1 120.0(10) . . ?
 C19_1 C18_1 H18_1 120.0 . . ?
 C11_1 C19_1 H19_1 118.6 . . ?
 C18_1 C19_1 C11_1 122.9(10) . . ?
 C18_1 C19_1 H19_1 118.5 . . ?
 N3_1 C20_1 C21_1 104.1(6) . . ?
 N3_1 C20_1 C25_1 134.2(7) . . ?
 C25_1 C20_1 C21_1 121.5(6) . . ?
 N4_1 C21_1 C20_1 112.3(7) . . ?
 N4_1 C21_1 C22_1 126.8(8) . . ?
 C22_1 C21_1 C20_1 120.9(7) . . ?
 C21_1 C22_1 H22_1 121.0 . . ?
 C23_1 C22_1 C21_1 117.9(8) . . ?
 C23_1 C22_1 H22_1 121.0 . . ?
 C22_1 C23_1 H23_1 119.5 . . ?
 C22_1 C23_1 C24_1 121.0(8) . . ?
 C24_1 C23_1 H23_1 119.5 . . ?
 C23_1 C24_1 C26_1 117.7(7) . . ?
 C25_1 C24_1 C23_1 123.4(7) . . ?
 C25_1 C24_1 C26_1 118.9(7) . . ?
 C20_1 C25_1 H25_1 122.5 . . ?
 C24_1 C25_1 C20_1 115.0(7) . . ?
 C24_1 C25_1 H25_1 122.5 . . ?
 F4_1 C26_1 C24_1 112.5(7) . . ?
 F5_1 C26_1 F4_1 104.6(8) . . ?
 F5_1 C26_1 C24_1 112.9(7) . . ?
 F6_1 C26_1 F4_1 104.3(9) . . ?
 F6_1 C26_1 F5_1 107.1(8) . . ?
 F6_1 C26_1 C24_1 114.6(9) . . ?
 C8_2 N1_2 C5_2 107.1(8) . . ?
 C4_2 N2_2 C8_2 105.3(7) . . ?
 C12_2 N2_2 C4_2 133.0(7) . . ?
 C12_2 N2_2 C8_2 121.7(7) . . ?
 C17_2 N3_2 C13_2 120.6(6) . . ?
 C17_2 N3_2 C20_2 105.9(6) . . ?
 C20_2 N3_2 C13_2 133.4(7) . . ?
 C17_2 N4_2 C21_2 104.5(6) . . ?
 F1_2 C1_2 F2_2 102.4(8) . . ?
 F1_2 C1_2 C2_2 113.7(8) . . ?
 F2_2 C1_2 C2_2 114.1(7) . . ?
 F3_2 C1_2 F1_2 105.7(9) . . ?
 F3_2 C1_2 F2_2 105.4(9) . . ?
 F3_2 C1_2 C2_2 114.4(10) . . ?
 C3_2 C2_2 C1_2 120.1(7) . . ?
 C3_2 C2_2 C7_2 121.0(8) . . ?
 C7_2 C2_2 C1_2 118.8(8) . . ?
 C2_2 C3_2 H3_2 120.9 . . ?
 C2_2 C3_2 C4_2 118.1(7) . . ?
 C4_2 C3_2 H3_2 120.9 . . ?
 N2_2 C4_2 C5_2 105.5(7) . . ?
 C3_2 C4_2 N2_2 132.3(7) . . ?
 C3_2 C4_2 C5_2 122.3(7) . . ?
 N1_2 C5_2 C4_2 110.5(8) . . ?
 N1_2 C5_2 C6_2 130.7(8) . . ?
 C6_2 C5_2 C4_2 118.5(8) . . ?
 C5_2 C6_2 H6_2 120.1 . . ?
 C7_2 C6_2 C5_2 119.8(8) . . ?
 C7_2 C6_2 H6_2 120.1 . . ?
 C2_2 C7_2 H7_2 119.9 . . ?
 C6_2 C7_2 C2_2 120.2(9) . . ?
 C6_2 C7_2 H7_2 119.9 . . ?
 N1_2 C8_2 N2_2 111.2(7) . . ?
 N1_2 C8_2 C9_2 130.0(9) . . ?
 N2_2 C8_2 C9_2 117.7(8) . . ?
 C8_2 C9_2 H9_2 120.3 . . ?
 C10_2 C9_2 C8_2 119.5(9) . . ?
 C10_2 C9_2 H9_2 120.3 . . ?
 C9_2 C10_2 H10_2 118.4 . . ?
 C9_2 C10_2 C11_2 123.3(10) . . ?
 C11_2 C10_2 H10_2 118.4 . . ?
 C12_2 C11_2 C10_2 117.1(9) . . ?
 C19_2 C11_2 C10_2 122.7(9) . . ?
 C19_2 C11_2 C12_2 119.9(9) . . ?
 N2_2 C12_2 C11_2 117.5(8) . . ?
 C13_2 C12_2 N2_2 124.5(7) . . ?
 C13_2 C12_2 C11_2 117.9(8) . . ?
 N3_2 C13_2 C14_2 117.1(7) . . ?
 C12_2 C13_2 N3_2 124.3(7) . . ?
 C12_2 C13_2 C14_2 118.6(7) . . ?
 C13_2 C14_2 C15_2 117.6(8) . . ?
 C18_2 C14_2 C13_2 119.1(9) . . ?
 C18_2 C14_2 C15_2 123.2(9) . . ?
 C14_2 C15_2 H15_2 118.3 . . ?
 C16_2 C15_2 C14_2 123.5(9) . . ?
 C16_2 C15_2 H15_2 118.3 . . ?
 C15_2 C16_2 H16_2 121.2 . . ?
 C15_2 C16_2 C17_2 117.7(10) . . ?
 C17_2 C16_2 H16_2 121.2 . . ?
 N3_2 C17_2 C16_2 120.1(8) . . ?
 N4_2 C17_2 N3_2 112.5(6) . . ?
 N4_2 C17_2 C16_2 127.1(8) . . ?
 C14_2 C18_2 H18_2 119.7 . . ?
 C19_2 C18_2 C14_2 120.5(10) . . ?
 C19_2 C18_2 H18_2 119.7 . . ?
 C11_2 C19_2 H19_2 119.7 . . ?
 C18_2 C19_2 C11_2 120.6(10) . . ?
 C18_2 C19_2 H19_2 119.7 . . ?
 C21_2 C20_2 N3_2 104.6(6) . . ?
 C25_2 C20_2 N3_2 132.8(7) . . ?
 C25_2 C20_2 C21_2 122.7(6) . . ?
 N4_2 C21_2 C20_2 112.4(6) . . ?
 N4_2 C21_2 C22_2 128.0(7) . . ?
 C20_2 C21_2 C22_2 119.6(6) . . ?
 C21_2 C22_2 H22_2 121.0 . . ?
 C23_2 C22_2 C21_2 118.0(7) . . ?
 C23_2 C22_2 H22_2 121.0 . . ?
 C22_2 C23_2 H23_2 118.9 . . ?
 C22_2 C23_2 C24_2 122.1(7) . . ?
 C24_2 C23_2 H23_2 118.9 . . ?
 C23_2 C24_2 C26_2 118.9(6) . . ?
 C25_2 C24_2 C23_2 120.9(6) . . ?
 C25_2 C24_2 C26_2 120.0(6) . . ?
 C20_2 C25_2 H25_2 121.8 . . ?
 C24_2 C25_2 C20_2 116.5(6) . . ?
 C24_2 C25_2 H25_2 121.8 . . ?
 F4_2 C26_2 F5_2 104.7(7) . . ?
 F4_2 C26_2 C24_2 113.2(6) . . ?
 F5_2 C26_2 C24_2 113.9(6) . . ?
 F6_2 C26_2 F4_2 106.4(7) . . ?
 F6_2 C26_2 F5_2 103.3(7) . . ?
 F6_2 C26_2 C24_2 114.3(7) . . ?
 C8_3 N1_3 C5_3 105.4(7) . . ?
 C8_3 N2_3 C4_3 104.9(6) . . ?
 C8_3 N2_3 C12_3 122.6(6) . . ?
 C12_3 N2_3 C4_3 132.2(6) . . ?
 C13_3 N3_3 C20_3 132.3(6) . . ?
 C17_3 N3_3 C13_3 122.4(6) . . ?
 C17_3 N3_3 C20_3 105.3(5) . . ?
 C17_3 N4_3 C21_3 104.9(6) . . ?
 F1_3 C1_3 F2_3 101.9(8) . . ?
 F1_3 C1_3 C2_3 113.5(8) . . ?
 F2_3 C1_3 C2_3 113.7(7) . . ?
 F3_3 C1_3 F1_3 106.3(8) . . ?
 F3_3 C1_3 F2_3 106.4(10) . . ?
 F3_3 C1_3 C2_3 113.9(9) . . ?
 C3_3 C2_3 C1_3 118.7(7) . . ?
 C3_3 C2_3 C7_3 121.4(8) . . ?
 C7_3 C2_3 C1_3 119.8(8) . . ?
 C2_3 C3_3 H3_3 121.0 . . ?
 C2_3 C3_3 C4_3 117.9(7) . . ?
 C4_3 C3_3 H3_3 121.0 . . ?
 C3_3 C4_3 N2_3 133.5(7) . . ?
 C3_3 C4_3 C5_3 121.5(7) . . ?
 C5_3 C4_3 N2_3 104.9(6) . . ?
 N1_3 C5_3 C4_3 111.5(7) . . ?
 N1_3 C5_3 C6_3 129.1(8) . . ?
 C6_3 C5_3 C4_3 119.3(7) . . ?
 C5_3 C6_3 H6_3 120.3 . . ?
 C7_3 C6_3 C5_3 119.4(8) . . ?
 C7_3 C6_3 H6_3 120.3 . . ?
 C2_3 C7_3 H7_3 119.9 . . ?
 C6_3 C7_3 C2_3 120.2(9) . . ?
 C6_3 C7_3 H7_3 119.9 . . ?
 N1_3 C8_3 N2_3 112.5(6) . . ?
 N1_3 C8_3 C9_3 129.0(8) . . ?
 N2_3 C8_3 C9_3 118.5(7) . . ?
 C8_3 C9_3 H9_3 121.0 . . ?
 C10_3 C9_3 C8_3 118.1(8) . . ?
 C10_3 C9_3 H9_3 121.0 . . ?
 C9_3 C10_3 H10_3 118.3 . . ?
 C9_3 C10_3 C11_3 123.3(8) . . ?
 C11_3 C10_3 H10_3 118.3 . . ?
 C12_3 C11_3 C10_3 118.2(7) . . ?
 C19_3 C11_3 C10_3 123.8(8) . . ?
 C19_3 C11_3 C12_3 118.0(8) . . ?
 N2_3 C12_3 C11_3 116.0(7) . . ?
 C13_3 C12_3 N2_3 124.6(6) . . ?
 C13_3 C12_3 C11_3 119.4(7) . . ?
 N3_3 C13_3 C14_3 116.1(7) . . ?
 C12_3 C13_3 N3_3 125.9(6) . . ?
 C12_3 C13_3 C14_3 117.9(6) . . ?
 C13_3 C14_3 C15_3 117.9(7) . . ?
 C18_3 C14_3 C13_3 118.4(8) . . ?
 C18_3 C14_3 C15_3 123.7(8) . . ?
 C14_3 C15_3 H15_3 117.8 . . ?
 C16_3 C15_3 C14_3 124.4(8) . . ?
 C16_3 C15_3 H15_3 117.8 . . ?
 C15_3 C16_3 H16_3 121.4 . . ?
 C15_3 C16_3 C17_3 117.2(9) . . ?
 C17_3 C16_3 H16_3 121.4 . . ?
 N3_3 C17_3 C16_3 118.9(8) . . ?
 N4_3 C17_3 N3_3 113.5(6) . . ?
 N4_3 C17_3 C16_3 126.0(8) . . ?
 C14_3 C18_3 H18_3 119.5 . . ?
 C19_3 C18_3 C14_3 120.9(8) . . ?
 C19_3 C18_3 H18_3 119.5 . . ?
 C11_3 C19_3 H19_3 119.0 . . ?
 C18_3 C19_3 C11_3 121.9(8) . . ?
 C18_3 C19_3 H19_3 119.0 . . ?
 N3_3 C20_3 C21_3 104.6(5) . . ?
 C25_3 C20_3 N3_3 132.7(6) . . ?
 C25_3 C20_3 C21_3 122.5(6) . . ?
 N4_3 C21_3 C20_3 111.7(6) . . ?
 N4_3 C21_3 C22_3 129.4(7) . . ?
 C22_3 C21_3 C20_3 118.9(6) . . ?
 C21_3 C22_3 H22_3 120.6 . . ?
 C23_3 C22_3 C21_3 118.7(7) . . ?
 C23_3 C22_3 H22_3 120.6 . . ?
 C22_3 C23_3 H23_3 119.1 . . ?
 C22_3 C23_3 C24_3 121.8(7) . . ?
 C24_3 C23_3 H23_3 119.1 . . ?
 C23_3 C24_3 C26_3 118.4(6) . . ?
 C25_3 C24_3 C23_3 120.8(6) . . ?
 C25_3 C24_3 C26_3 120.7(6) . . ?
 C20_3 C25_3 H25_3 121.6 . . ?
 C24_3 C25_3 C20_3 116.8(6) . . ?
 C24_3 C25_3 H25_3 121.6 . . ?
 F4_3 C26_3 C24_3 113.6(6) . . ?
 F5_3 C26_3 F4_3 104.2(7) . . ?
 F5_3 C26_3 C24_3 112.9(6) . . ?
 F6_3 C26_3 F4_3 105.0(7) . . ?
 F6_3 C26_3 F5_3 105.1(7) . . ?
 F6_3 C26_3 C24_3 115.1(7) . . ?
 C8_4 N1_4 C5_4 105.3(7) . . ?
 C8_4 N2_4 C4_4 104.3(7) . . ?
 C8_4 N2_4 C12_4 124.0(7) . . ?
 C12_4 N2_4 C4_4 131.7(7) . . ?
 C13_4 N3_4 C17_4 122.9(7) . . ?
 C13_4 N3_4 C20_4 132.5(8) . . ?
 C20_4 N3_4 C17_4 104.6(6) . . ?
 C17_4 N4_4 C21_4 104.0(7) . . ?
 F1_4 C1_4 F2_4 104.6(8) . . ?
 F1_4 C1_4 C2_4 112.4(7) . . ?
 F2_4 C1_4 C2_4 114.2(7) . . ?
 F3_4 C1_4 F1_4 104.3(8) . . ?
 F3_4 C1_4 F2_4 105.7(8) . . ?
 F3_4 C1_4 C2_4 114.6(9) . . ?
 C3_4 C2_4 C1_4 119.1(7) . . ?
 C3_4 C2_4 C7_4 120.1(7) . . ?
 C7_4 C2_4 C1_4 120.8(7) . . ?
 C2_4 C3_4 H3_4 120.7 . . ?
 C2_4 C3_4 C4_4 118.6(7) . . ?
 C4_4 C3_4 H3_4 120.7 . . ?
 C3_4 C4_4 N2_4 131.8(7) . . ?
 C3_4 C4_4 C5_4 122.7(7) . . ?
 C5_4 C4_4 N2_4 105.5(6) . . ?
 N1_4 C5_4 C4_4 111.2(7) . . ?
 N1_4 C5_4 C6_4 131.1(9) . . ?
 C6_4 C5_4 C4_4 117.6(7) . . ?
 C5_4 C6_4 H6_4 119.9 . . ?
 C7_4 C6_4 C5_4 120.2(8) . . ?
 C7_4 C6_4 H6_4 119.9 . . ?
 C2_4 C7_4 H7_4 119.7 . . ?
 C6_4 C7_4 C2_4 120.5(8) . . ?
 C6_4 C7_4 H7_4 119.7 . . ?
 N1_4 C8_4 N2_4 113.2(7) . . ?
 N1_4 C8_4 C9_4 128.9(9) . . ?
 N2_4 C8_4 C9_4 117.8(9) . . ?
 C8_4 C9_4 H9_4 121.5 . . ?
 C10_4 C9_4 C8_4 117.0(11) . . ?
 C10_4 C9_4 H9_4 121.5 . . ?
 C9_4 C10_4 H10_4 117.2 . . ?
 C9_4 C10_4 C11_4 125.7(10) . . ?
 C11_4 C10_4 H10_4 117.2 . . ?
 C12_4 C11_4 C10_4 117.5(9) . . ?
 C19_4 C11_4 C10_4 123.8(9) . . ?
 C19_4 C11_4 C12_4 118.8(9) . . ?
 N2_4 C12_4 C11_4 115.2(8) . . ?
 C13_4 C12_4 N2_4 125.7(7) . . ?
 C13_4 C12_4 C11_4 119.0(8) . . ?
 N3_4 C13_4 C12_4 126.2(7) . . ?
 N3_4 C13_4 C14_4 115.7(7) . . ?
 C12_4 C13_4 C14_4 118.0(7) . . ?
 C15_4 C14_4 C13_4 115.9(8) . . ?
 C18_4 C14_4 C13_4 118.6(9) . . ?
 C18_4 C14_4 C15_4 124.9(9) . . ?
 C14_4 C15_4 H15_4 116.6 . . ?
 C16_4 C15_4 C14_4 126.8(10) . . ?
 C16_4 C15_4 H15_4 116.6 . . ?
 C15_4 C16_4 H16_4 122.6 . . ?
 C15_4 C16_4 C17_4 114.8(10) . . ?
 C17_4 C16_4 H16_4 122.6 . . ?
 N3_4 C17_4 C16_4 119.3(8) . . ?
 N4_4 C17_4 N3_4 114.0(7) . . ?
 N4_4 C17_4 C16_4 126.7(8) . . ?
 C14_4 C18_4 H18_4 119.2 . . ?
 C19_4 C18_4 C14_4 121.6(10) . . ?
 C19_4 C18_4 H18_4 119.2 . . ?
 C11_4 C19_4 H19_4 119.7 . . ?
 C18_4 C19_4 C11_4 120.6(9) . . ?
 C18_4 C19_4 H19_4 119.7 . . ?
 N3_4 C20_4 C21_4 105.0(6) . . ?
 N3_4 C20_4 C25_4 132.7(7) . . ?
 C25_4 C20_4 C21_4 122.2(6) . . ?
 N4_4 C21_4 C20_4 111.9(7) . . ?
 N4_4 C21_4 C22_4 127.5(8) . . ?
 C22_4 C21_4 C20_4 120.6(7) . . ?
 C21_4 C22_4 H22_4 121.0 . . ?
 C23_4 C22_4 C21_4 117.9(8) . . ?
 C23_4 C22_4 H22_4 121.0 . . ?
 C22_4 C23_4 H23_4 119.7 . . ?
 C22_4 C23_4 C24_4 120.6(8) . . ?
 C24_4 C23_4 H23_4 119.7 . . ?
 C23_4 C24_4 C26_4 116.6(6) . . ?
 C25_4 C24_4 C23_4 123.1(7) . . ?
 C25_4 C24_4 C26_4 120.1(6) . . ?
 C20_4 C25_4 H25_4 122.3 . . ?
 C24_4 C25_4 C20_4 115.5(7) . . ?
 C24_4 C25_4 H25_4 122.3 . . ?
 F4_4 C26_4 F5_4 104.3(7) . . ?
 F4_4 C26_4 C24_4 114.1(6) . . ?
 F5_4 C26_4 C24_4 113.4(7) . . ?
 F6_4 C26_4 F4_4 105.0(7) . . ?
 F6_4 C26_4 F5_4 104.5(7) . . ?
 F6_4 C26_4 C24_4 114.4(8) . . ?
 C8_5 N1_5 C5_5 104.7(8) . . ?
 C4_5 N2_5 C8_5 104.5(7) . . ?
 C12_5 N2_5 C4_5 133.0(7) . . ?
 C12_5 N2_5 C8_5 122.5(7) . . ?
 C13_5 N3_5 C17_5 123.2(6) . . ?
 C20_5 N3_5 C13_5 131.3(6) . . ?
 C20_5 N3_5 C17_5 105.2(6) . . ?
 C17_5 N4_5 C21_5 105.8(7) . . ?
 F1_5 C1_5 C2_5 112.7(7) . . ?
 F2_5 C1_5 F1_5 104.6(8) . . ?
 F2_5 C1_5 C2_5 111.6(6) . . ?
 F3_5 C1_5 F1_5 107.5(8) . . ?
 F3_5 C1_5 F2_5 107.1(8) . . ?
 F3_5 C1_5 C2_5 112.8(8) . . ?
 C3_5 C2_5 C1_5 120.7(7) . . ?
 C3_5 C2_5 C7_5 123.5(7) . . ?
 C7_5 C2_5 C1_5 115.8(7) . . ?
 C2_5 C3_5 H3_5 122.1 . . ?
 C2_5 C3_5 C4_5 115.7(7) . . ?
 C4_5 C3_5 H3_5 122.1 . . ?
 N2_5 C4_5 C5_5 105.4(6) . . ?
 C3_5 C4_5 N2_5 132.6(8) . . ?
 C3_5 C4_5 C5_5 121.5(7) . . ?
 N1_5 C5_5 C4_5 112.2(8) . . ?
 N1_5 C5_5 C6_5 127.5(9) . . ?
 C6_5 C5_5 C4_5 119.9(7) . . ?
 C5_5 C6_5 H6_5 120.4 . . ?
 C7_5 C6_5 C5_5 119.3(9) . . ?
 C7_5 C6_5 H6_5 120.4 . . ?
 C2_5 C7_5 H7_5 120.5 . . ?
 C6_5 C7_5 C2_5 119.1(9) . . ?
 C6_5 C7_5 H7_5 120.5 . . ?
 N1_5 C8_5 N2_5 113.0(7) . . ?
 N1_5 C8_5 C9_5 128.9(9) . . ?
 N2_5 C8_5 C9_5 117.9(9) . . ?
 C8_5 C9_5 H9_5 120.6 . . ?
 C10_5 C9_5 C8_5 118.8(10) . . ?
 C10_5 C9_5 H9_5 120.6 . . ?
 C9_5 C10_5 H10_5 117.9 . . ?
 C9_5 C10_5 C11_5 124.3(10) . . ?
 C11_5 C10_5 H10_5 117.9 . . ?
 C12_5 C11_5 C10_5 117.3(9) . . ?
 C19_5 C11_5 C10_5 125.1(10) . . ?
 C19_5 C11_5 C12_5 117.4(10) . . ?
 N2_5 C12_5 C11_5 116.1(8) . . ?
 N2_5 C12_5 C13_5 124.7(7) . . ?
 C13_5 C12_5 C11_5 119.2(8) . . ?
 N3_5 C13_5 C14_5 117.1(8) . . ?
 C12_5 C13_5 N3_5 124.7(7) . . ?
 C12_5 C13_5 C14_5 118.2(8) . . ?
 C13_5 C14_5 C15_5 116.7(8) . . ?
 C18_5 C14_5 C13_5 117.7(9) . . ?
 C18_5 C14_5 C15_5 125.5(10) . . ?
 C14_5 C15_5 H15_5 117.5 . . ?
 C16_5 C15_5 C14_5 125.0(10) . . ?
 C16_5 C15_5 H15_5 117.5 . . ?
 C15_5 C16_5 H16_5 120.9 . . ?
 C15_5 C16_5 C17_5 118.3(10) . . ?
 C17_5 C16_5 H16_5 120.9 . . ?
 N3_5 C17_5 C16_5 117.4(8) . . ?
 N4_5 C17_5 N3_5 112.3(6) . . ?
 N4_5 C17_5 C16_5 128.8(9) . . ?
 C14_5 C18_5 H18_5 119.6 . . ?
 C19_5 C18_5 C14_5 120.7(11) . . ?
 C19_5 C18_5 H18_5 119.6 . . ?
 C11_5 C19_5 H19_5 118.5 . . ?
 C18_5 C19_5 C11_5 123.0(11) . . ?
 C18_5 C19_5 H19_5 118.5 . . ?
 N3_5 C20_5 C21_5 105.8(6) . . ?
 C25_5 C20_5 N3_5 132.2(6) . . ?
 C25_5 C20_5 C21_5 122.0(6) . . ?
 N4_5 C21_5 C20_5 110.5(6) . . ?
 N4_5 C21_5 C22_5 129.8(7) . . ?
 C22_5 C21_5 C20_5 119.5(6) . . ?
 C21_5 C22_5 H22_5 120.6 . . ?
 C23_5 C22_5 C21_5 118.8(7) . . ?
 C23_5 C22_5 H22_5 120.6 . . ?
 C22_5 C23_5 H23_5 119.3 . . ?
 C22_5 C23_5 C24_5 121.4(7) . . ?
 C24_5 C23_5 H23_5 119.3 . . ?
 C23_5 C24_5 C26_5 119.2(7) . . ?
 C25_5 C24_5 C23_5 120.9(6) . . ?
 C25_5 C24_5 C26_5 119.9(6) . . ?
 C20_5 C25_5 H25_5 121.3 . . ?
 C24_5 C25_5 C20_5 117.4(6) . . ?
 C24_5 C25_5 H25_5 121.3 . . ?
 F4_5 C26_5 C24_5 113.2(6) . . ?
 F5_5 C26_5 F4_5 104.2(8) . . ?
 F5_5 C26_5 C24_5 113.1(7) . . ?
 F6_5 C26_5 F4_5 106.2(8) . . ?
 F6_5 C26_5 F5_5 103.5(7) . . ?
 F6_5 C26_5 C24_5 115.6(8) . . ?
 C8_6 N1_6 C5_6 106.0(7) . . ?
 C4_6 N2_6 C8_6 104.0(6) . . ?
 C4_6 N2_6 C12_6 133.4(7) . . ?
 C8_6 N2_6 C12_6 122.6(7) . . ?
 C13_6 N3_6 C17_6 124.4(7) . . ?
 C13_6 N3_6 C20_6 131.3(7) . . ?
 C20_6 N3_6 C17_6 104.3(6) . . ?
 C17_6 N4_6 C21_6 105.5(8) . . ?
 F1_6 C1_6 C2_6 113.0(7) . . ?
 F2_6 C1_6 F1_6 104.6(8) . . ?
 F2_6 C1_6 C2_6 112.7(7) . . ?
 F3_6 C1_6 F1_6 105.5(8) . . ?
 F3_6 C1_6 F2_6 106.1(9) . . ?
 F3_6 C1_6 C2_6 114.2(8) . . ?
 C3_6 C2_6 C1_6 120.5(7) . . ?
 C3_6 C2_6 C7_6 122.6(7) . . ?
 C7_6 C2_6 C1_6 116.9(7) . . ?
 C2_6 C3_6 H3_6 122.0 . . ?
 C2_6 C3_6 C4_6 116.0(7) . . ?
 C4_6 C3_6 H3_6 122.0 . . ?
 N2_6 C4_6 C5_6 106.6(6) . . ?
 C3_6 C4_6 N2_6 130.6(7) . . ?
 C3_6 C4_6 C5_6 122.9(7) . . ?
 N1_6 C5_6 C4_6 110.2(7) . . ?
 N1_6 C5_6 C6_6 129.0(8) . . ?
 C6_6 C5_6 C4_6 119.9(7) . . ?
 C5_6 C6_6 H6_6 121.1 . . ?
 C7_6 C6_6 C5_6 117.9(8) . . ?
 C7_6 C6_6 H6_6 121.1 . . ?
 C2_6 C7_6 H7_6 119.6 . . ?
 C6_6 C7_6 C2_6 120.7(8) . . ?
 C6_6 C7_6 H7_6 119.6 . . ?
 N1_6 C8_6 N2_6 112.7(7) . . ?
 N1_6 C8_6 C9_6 128.0(9) . . ?
 N2_6 C8_6 C9_6 118.3(9) . . ?
 C8_6 C9_6 H9_6 121.7 . . ?
 C10_6 C9_6 C8_6 116.7(11) . . ?
 C10_6 C9_6 H9_6 121.7 . . ?
 C9_6 C10_6 H10_6 117.2 . . ?
 C9_6 C10_6 C11_6 125.5(10) . . ?
 C11_6 C10_6 H10_6 117.2 . . ?
 C12_6 C11_6 C10_6 117.5(9) . . ?
 C19_6 C11_6 C10_6 124.4(10) . . ?
 C19_6 C11_6 C12_6 118.1(10) . . ?
 N2_6 C12_6 C11_6 115.2(8) . . ?
 C13_6 C12_6 N2_6 124.4(7) . . ?
 C13_6 C12_6 C11_6 120.3(8) . . ?
 N3_6 C13_6 C12_6 126.6(7) . . ?
 N3_6 C13_6 C14_6 116.0(8) . . ?
 C12_6 C13_6 C14_6 117.4(8) . . ?
 C15_6 C14_6 C13_6 115.4(9) . . ?
 C18_6 C14_6 C13_6 117.0(10) . . ?
 C18_6 C14_6 C15_6 127.6(10) . . ?
 C14_6 C15_6 H15_6 116.2 . . ?
 C16_6 C15_6 C14_6 127.5(10) . . ?
 C16_6 C15_6 H15_6 116.2 . . ?
 C15_6 C16_6 H16_6 121.8 . . ?
 C15_6 C16_6 C17_6 116.3(10) . . ?
 C17_6 C16_6 H16_6 121.8 . . ?
 N3_6 C17_6 C16_6 117.7(9) . . ?
 N4_6 C17_6 N3_6 112.7(7) . . ?
 N4_6 C17_6 C16_6 129.2(9) . . ?
 C14_6 C18_6 H18_6 118.1 . . ?
 C19_6 C18_6 C14_6 123.7(11) . . ?
 C19_6 C18_6 H18_6 118.1 . . ?
 C11_6 C19_6 H19_6 120.1 . . ?
 C18_6 C19_6 C11_6 119.8(11) . . ?
 C18_6 C19_6 H19_6 120.1 . . ?
 N3_6 C20_6 C21_6 106.7(6) . . ?
 N3_6 C20_6 C25_6 132.3(7) . . ?
 C25_6 C20_6 C21_6 120.9(7) . . ?
 N4_6 C21_6 C20_6 110.5(7) . . ?
 N4_6 C21_6 C22_6 128.9(8) . . ?
 C22_6 C21_6 C20_6 120.6(7) . . ?
 C21_6 C22_6 H22_6 120.9 . . ?
 C23_6 C22_6 C21_6 118.1(9) . . ?
 C23_6 C22_6 H22_6 120.9 . . ?
 C22_6 C23_6 H23_6 119.4 . . ?
 C22_6 C23_6 C24_6 121.1(8) . . ?
 C24_6 C23_6 H23_6 119.4 . . ?
 C23_6 C24_6 C26_6 116.9(7) . . ?
 C25_6 C24_6 C23_6 122.0(7) . . ?
 C25_6 C24_6 C26_6 121.1(7) . . ?
 C20_6 C25_6 H25_6 121.6 . . ?
 C24_6 C25_6 C20_6 116.8(7) . . ?
 C24_6 C25_6 H25_6 121.6 . . ?
 F4_6 C26_6 C24_6 113.3(7) . . ?
 F5_6 C26_6 F4_6 105.8(8) . . ?
 F5_6 C26_6 C24_6 112.5(8) . . ?
 F6_6 C26_6 F4_6 106.3(9) . . ?
 F6_6 C26_6 F5_6 103.9(8) . . ?
 F6_6 C26_6 C24_6 114.2(9) . . ?
 C8_7 N1_7 C5_7 104.3(7) . . ?
 C4_7 N2_7 C8_7 105.5(6) . . ?
 C4_7 N2_7 C12_7 132.3(7) . . ?
 C12_7 N2_7 C8_7 122.1(7) . . ?
 C17_7 N3_7 C13_7 123.1(7) . . ?
 C20_7 N3_7 C13_7 132.1(7) . . ?
 C20_7 N3_7 C17_7 104.8(7) . . ?
 C17_7 N4_7 C21_7 105.5(8) . . ?
 F1_7 C1_7 C2_7 112.8(8) . . ?
 F2_7 C1_7 F1_7 103.4(9) . . ?
 F2_7 C1_7 C2_7 113.4(8) . . ?
 F3_7 C1_7 F1_7 105.1(9) . . ?
 F3_7 C1_7 F2_7 107.3(10) . . ?
 F3_7 C1_7 C2_7 113.9(9) . . ?
 C3_7 C2_7 C1_7 118.9(7) . . ?
 C3_7 C2_7 C7_7 122.7(7) . . ?
 C7_7 C2_7 C1_7 118.2(8) . . ?
 C2_7 C3_7 H3_7 122.4 . . ?
 C2_7 C3_7 C4_7 115.2(7) . . ?
 C4_7 C3_7 H3_7 122.4 . . ?
 N2_7 C4_7 C5_7 104.4(6) . . ?
 C3_7 C4_7 N2_7 131.9(7) . . ?
 C3_7 C4_7 C5_7 123.7(7) . . ?
 N1_7 C5_7 C4_7 112.9(7) . . ?
 N1_7 C5_7 C6_7 128.9(8) . . ?
 C6_7 C5_7 C4_7 118.2(7) . . ?
 C5_7 C6_7 H6_7 120.3 . . ?
 C7_7 C6_7 C5_7 119.5(8) . . ?
 C7_7 C6_7 H6_7 120.3 . . ?
 C2_7 C7_7 H7_7 119.8 . . ?
 C6_7 C7_7 C2_7 120.5(8) . . ?
 C6_7 C7_7 H7_7 119.8 . . ?
 N1_7 C8_7 N2_7 112.7(7) . . ?
 N1_7 C8_7 C9_7 128.5(8) . . ?
 N2_7 C8_7 C9_7 118.5(8) . . ?
 C8_7 C9_7 H9_7 121.0 . . ?
 C10_7 C9_7 C8_7 117.9(10) . . ?
 C10_7 C9_7 H9_7 121.0 . . ?
 C9_7 C10_7 H10_7 117.9 . . ?
 C9_7 C10_7 C11_7 124.2(10) . . ?
 C11_7 C10_7 H10_7 117.9 . . ?
 C12_7 C11_7 C10_7 117.8(9) . . ?
 C19_7 C11_7 C10_7 123.2(10) . . ?
 C19_7 C11_7 C12_7 118.9(10) . . ?
 N2_7 C12_7 C11_7 116.3(8) . . ?
 C13_7 C12_7 N2_7 123.0(7) . . ?
 C13_7 C12_7 C11_7 120.7(8) . . ?
 N3_7 C13_7 C14_7 117.4(8) . . ?
 C12_7 C13_7 N3_7 126.0(7) . . ?
 C12_7 C13_7 C14_7 116.3(8) . . ?
 C13_7 C14_7 C15_7 114.4(9) . . ?
 C18_7 C14_7 C13_7 120.1(9) . . ?
 C18_7 C14_7 C15_7 125.6(9) . . ?
 C14_7 C15_7 H15_7 116.7 . . ?
 C16_7 C15_7 C14_7 126.6(10) . . ?
 C16_7 C15_7 H15_7 116.7 . . ?
 C15_7 C16_7 H16_7 120.9 . . ?
 C15_7 C16_7 C17_7 118.2(10) . . ?
 C17_7 C16_7 H16_7 120.9 . . ?
 N3_7 C17_7 C16_7 116.4(9) . . ?
 N4_7 C17_7 N3_7 112.7(7) . . ?
 N4_7 C17_7 C16_7 130.8(9) . . ?
 C14_7 C18_7 H18_7 119.4 . . ?
 C19_7 C18_7 C14_7 121.2(10) . . ?
 C19_7 C18_7 H18_7 119.4 . . ?
 C11_7 C19_7 H19_7 119.7 . . ?
 C18_7 C19_7 C11_7 120.5(11) . . ?
 C18_7 C19_7 H19_7 119.7 . . ?
 N3_7 C20_7 C21_7 105.9(6) . . ?
 C25_7 C20_7 N3_7 131.6(8) . . ?
 C25_7 C20_7 C21_7 122.2(7) . . ?
 N4_7 C21_7 C20_7 110.4(7) . . ?
 N4_7 C21_7 C22_7 130.1(9) . . ?
 C22_7 C21_7 C20_7 119.4(7) . . ?
 C21_7 C22_7 H22_7 120.6 . . ?
 C23_7 C22_7 C21_7 118.8(9) . . ?
 C23_7 C22_7 H22_7 120.6 . . ?
 C22_7 C23_7 H23_7 119.8 . . ?
 C22_7 C23_7 C24_7 120.4(9) . . ?
 C24_7 C23_7 H23_7 119.8 . . ?
 C23_7 C24_7 C26_7 118.9(7) . . ?
 C25_7 C24_7 C23_7 122.0(7) . . ?
 C25_7 C24_7 C26_7 119.1(7) . . ?
 C20_7 C25_7 H25_7 121.6 . . ?
 C24_7 C25_7 C20_7 116.7(7) . . ?
 C24_7 C25_7 H25_7 121.6 . . ?
 F4_7 C26_7 C24_7 113.9(7) . . ?
 F5_7 C26_7 F4_7 102.2(7) . . ?
 F5_7 C26_7 C24_7 112.7(7) . . ?
 F6_7 C26_7 F4_7 106.1(9) . . ?
 F6_7 C26_7 F5_7 106.5(7) . . ?
 F6_7 C26_7 C24_7 114.3(8) . . ?
 C8_8 N1_8 C5_8 105.9(8) . . ?
 C4_8 N2_8 C8_8 105.2(7) . . ?
 C12_8 N2_8 C4_8 132.0(7) . . ?
 C12_8 N2_8 C8_8 122.8(8) . . ?
 C13_8 N3_8 C17_8 123.0(7) . . ?
 C13_8 N3_8 C20_8 132.0(7) . . ?
 C20_8 N3_8 C17_8 105.0(6) . . ?
 C17_8 N4_8 C21_8 105.2(7) . . ?
 F1_8 C1_8 F2_8 101.2(8) . . ?
 F1_8 C1_8 C2_8 113.1(8) . . ?
 F2_8 C1_8 C2_8 113.7(7) . . ?
 F3_8 C1_8 F1_8 105.9(8) . . ?
 F3_8 C1_8 F2_8 109.2(9) . . ?
 F3_8 C1_8 C2_8 112.9(9) . . ?
 C3_8 C2_8 C1_8 119.0(7) . . ?
 C3_8 C2_8 C7_8 122.0(8) . . ?
 C7_8 C2_8 C1_8 118.8(8) . . ?
 C2_8 C3_8 H3_8 121.7 . . ?
 C2_8 C3_8 C4_8 116.6(8) . . ?
 C4_8 C3_8 H3_8 121.7 . . ?
 N2_8 C4_8 C5_8 104.5(7) . . ?
 C3_8 C4_8 N2_8 132.4(7) . . ?
 C3_8 C4_8 C5_8 122.9(7) . . ?
 N1_8 C5_8 C4_8 111.3(8) . . ?
 N1_8 C5_8 C6_8 129.4(9) . . ?
 C6_8 C5_8 C4_8 118.4(8) . . ?
 C5_8 C6_8 H6_8 120.3 . . ?
 C7_8 C6_8 C5_8 119.4(9) . . ?
 C7_8 C6_8 H6_8 120.3 . . ?
 C2_8 C7_8 H7_8 119.7 . . ?
 C6_8 C7_8 C2_8 120.6(10) . . ?
 C6_8 C7_8 H7_8 119.7 . . ?
 N1_8 C8_8 N2_8 111.9(8) . . ?
 N1_8 C8_8 C9_8 128.5(10) . . ?
 N2_8 C8_8 C9_8 118.2(9) . . ?
 C8_8 C9_8 H9_8 121.8 . . ?
 C10_8 C9_8 C8_8 116.4(11) . . ?
 C10_8 C9_8 H9_8 121.8 . . ?
 C9_8 C10_8 H10_8 117.1 . . ?
 C9_8 C10_8 C11_8 125.8(11) . . ?
 C11_8 C10_8 H10_8 117.1 . . ?
 C10_8 C11_8 C12_8 117.5(9) . . ?
 C19_8 C11_8 C10_8 124.9(9) . . ?
 C19_8 C11_8 C12_8 117.5(9) . . ?
 N2_8 C12_8 C11_8 114.7(8) . . ?
 C13_8 C12_8 N2_8 125.3(7) . . ?
 C13_8 C12_8 C11_8 120.1(8) . . ?
 N3_8 C13_8 C14_8 117.0(8) . . ?
 C12_8 C13_8 N3_8 125.7(7) . . ?
 C12_8 C13_8 C14_8 117.2(8) . . ?
 C13_8 C14_8 C15_8 116.1(8) . . ?
 C18_8 C14_8 C13_8 119.0(9) . . ?
 C18_8 C14_8 C15_8 124.8(9) . . ?
 C14_8 C15_8 H15_8 117.3 . . ?
 C16_8 C15_8 C14_8 125.3(9) . . ?
 C16_8 C15_8 H15_8 117.3 . . ?
 C15_8 C16_8 H16_8 121.2 . . ?
 C15_8 C16_8 C17_8 117.6(10) . . ?
 C17_8 C16_8 H16_8 121.2 . . ?
 N3_8 C17_8 C16_8 117.8(8) . . ?
 N4_8 C17_8 N3_8 113.1(6) . . ?
 N4_8 C17_8 C16_8 128.2(8) . . ?
 C14_8 C18_8 H18_8 119.6 . . ?
 C19_8 C18_8 C14_8 120.8(11) . . ?
 C19_8 C18_8 H18_8 119.6 . . ?
 C11_8 C19_8 H19_8 118.9 . . ?
 C18_8 C19_8 C11_8 122.2(10) . . ?
 C18_8 C19_8 H19_8 118.9 . . ?
 N3_8 C20_8 C21_8 105.3(6) . . ?
 C25_8 C20_8 N3_8 132.5(6) . . ?
 C25_8 C20_8 C21_8 122.2(6) . . ?
 N4_8 C21_8 C20_8 111.3(6) . . ?
 N4_8 C21_8 C22_8 129.3(7) . . ?
 C22_8 C21_8 C20_8 119.5(6) . . ?
 C21_8 C22_8 H22_8 120.8 . . ?
 C23_8 C22_8 C21_8 118.4(7) . . ?
 C23_8 C22_8 H22_8 120.8 . . ?
 C22_8 C23_8 H23_8 119.2 . . ?
 C22_8 C23_8 C24_8 121.6(7) . . ?
 C24_8 C23_8 H23_8 119.2 . . ?
 C23_8 C24_8 C26_8 118.3(7) . . ?
 C25_8 C24_8 C23_8 121.4(7) . . ?
 C25_8 C24_8 C26_8 120.3(7) . . ?
 C20_8 C25_8 H25_8 121.6 . . ?
 C24_8 C25_8 C20_8 116.7(7) . . ?
 C24_8 C25_8 H25_8 121.6 . . ?
 F4_8 C26_8 C24_8 113.5(7) . . ?
 F5_8 C26_8 F4_8 104.5(7) . . ?
 F5_8 C26_8 C24_8 114.3(7) . . ?
 F6_8 C26_8 F4_8 103.6(8) . . ?
 F6_8 C26_8 F5_8 104.6(8) . . ?
 F6_8 C26_8 C24_8 115.1(8) . . ?
 C8_9 N1_9 C5_9 106.1(7) . . ?
 C8_9 N2_9 C4_9 104.4(6) . . ?
 C12_9 N2_9 C4_9 133.0(7) . . ?
 C12_9 N2_9 C8_9 122.6(7) . . ?
 C13_9 N3_9 C17_9 122.4(6) . . ?
 C13_9 N3_9 C20_9 132.7(6) . . ?
 C20_9 N3_9 C17_9 104.8(6) . . ?
 C17_9 N4_9 C21_9 105.7(7) . . ?
 F1_9 C1_9 F2_9 102.2(8) . . ?
 F1_9 C1_9 C2_9 112.7(7) . . ?
 F2_9 C1_9 C2_9 113.1(8) . . ?
 F3_9 C1_9 F1_9 106.1(9) . . ?
 F3_9 C1_9 F2_9 105.3(8) . . ?
 F3_9 C1_9 C2_9 116.2(9) . . ?
 C3_9 C2_9 C1_9 120.6(7) . . ?
 C3_9 C2_9 C7_9 121.4(7) . . ?
 C7_9 C2_9 C1_9 118.0(7) . . ?
 C2_9 C3_9 H3_9 121.8 . . ?
 C2_9 C3_9 C4_9 116.4(7) . . ?
 C4_9 C3_9 H3_9 121.8 . . ?
 C3_9 C4_9 N2_9 131.6(7) . . ?
 C3_9 C4_9 C5_9 122.8(7) . . ?
 C5_9 C4_9 N2_9 105.5(6) . . ?
 N1_9 C5_9 C4_9 111.1(7) . . ?
 N1_9 C5_9 C6_9 129.2(8) . . ?
 C6_9 C5_9 C4_9 119.4(7) . . ?
 C5_9 C6_9 H6_9 120.8 . . ?
 C7_9 C6_9 C5_9 118.4(8) . . ?
 C7_9 C6_9 H6_9 120.8 . . ?
 C2_9 C7_9 H7_9 119.2 . . ?
 C6_9 C7_9 C2_9 121.5(8) . . ?
 C6_9 C7_9 H7_9 119.2 . . ?
 N1_9 C8_9 N2_9 112.4(7) . . ?
 N1_9 C8_9 C9_9 129.6(8) . . ?
 N2_9 C8_9 C9_9 117.7(8) . . ?
 C8_9 C9_9 H9_9 120.9 . . ?
 C10_9 C9_9 C8_9 118.1(10) . . ?
 C10_9 C9_9 H9_9 120.9 . . ?
 C9_9 C10_9 H10_9 117.8 . . ?
 C9_9 C10_9 C11_9 124.4(9) . . ?
 C11_9 C10_9 H10_9 117.8 . . ?
 C12_9 C11_9 C10_9 117.6(8) . . ?
 C19_9 C11_9 C10_9 123.8(9) . . ?
 C19_9 C11_9 C12_9 118.5(8) . . ?
 N2_9 C12_9 C11_9 116.2(7) . . ?
 C13_9 C12_9 N2_9 124.9(7) . . ?
 C13_9 C12_9 C11_9 118.9(7) . . ?
 N3_9 C13_9 C12_9 124.0(6) . . ?
 N3_9 C13_9 C14_9 117.4(7) . . ?
 C12_9 C13_9 C14_9 118.6(7) . . ?
 C13_9 C14_9 C15_9 116.8(8) . . ?
 C18_9 C14_9 C13_9 118.0(8) . . ?
 C18_9 C14_9 C15_9 125.1(8) . . ?
 C14_9 C15_9 H15_9 117.7 . . ?
 C16_9 C15_9 C14_9 124.6(9) . . ?
 C16_9 C15_9 H15_9 117.7 . . ?
 C15_9 C16_9 H16_9 121.1 . . ?
 C15_9 C16_9 C17_9 117.9(9) . . ?
 C17_9 C16_9 H16_9 121.1 . . ?
 N3_9 C17_9 C16_9 118.0(8) . . ?
 N4_9 C17_9 N3_9 112.7(6) . . ?
 N4_9 C17_9 C16_9 128.6(8) . . ?
 C14_9 C18_9 H18_9 119.4 . . ?
 C19_9 C18_9 C14_9 121.3(9) . . ?
 C19_9 C18_9 H18_9 119.4 . . ?
 C11_9 C19_9 H19_9 119.4 . . ?
 C18_9 C19_9 C11_9 121.3(9) . . ?
 C18_9 C19_9 H19_9 119.4 . . ?
 N3_9 C20_9 C21_9 106.1(6) . . ?
 C25_9 C20_9 N3_9 132.2(6) . . ?
 C25_9 C20_9 C21_9 121.3(6) . . ?
 N4_9 C21_9 C20_9 110.6(7) . . ?
 N4_9 C21_9 C22_9 129.8(8) . . ?
 C22_9 C21_9 C20_9 119.6(7) . . ?
 C21_9 C22_9 H22_9 120.4 . . ?
 C23_9 C22_9 C21_9 119.3(8) . . ?
 C23_9 C22_9 H22_9 120.4 . . ?
 C22_9 C23_9 H23_9 119.7 . . ?
 C22_9 C23_9 C24_9 120.6(8) . . ?
 C24_9 C23_9 H23_9 119.7 . . ?
 C23_9 C24_9 C26_9 117.8(7) . . ?
 C25_9 C24_9 C23_9 121.5(7) . . ?
 C25_9 C24_9 C26_9 120.7(7) . . ?
 C20_9 C25_9 H25_9 121.5 . . ?
 C24_9 C25_9 C20_9 117.0(6) . . ?
 C24_9 C25_9 H25_9 121.5 . . ?
 F4_9 C26_9 C24_9 112.5(7) . . ?
 F5_9 C26_9 F4_9 105.0(8) . . ?
 F5_9 C26_9 F6_9 106.0(7) . . ?
 F5_9 C26_9 C24_9 112.1(7) . . ?
 F6_9 C26_9 F4_9 106.0(8) . . ?
 F6_9 C26_9 C24_9 114.6(8) . . ?

loop_
  _geom_torsion_atom_site_label_1
  _geom_torsion_atom_site_label_2
  _geom_torsion_atom_site_label_3
  _geom_torsion_atom_site_label_4
  _geom_torsion
  _geom_torsion_site_symmetry_1
  _geom_torsion_site_symmetry_2
  _geom_torsion_site_symmetry_3
  _geom_torsion_site_symmetry_4
  _geom_torsion_publ_flag
 F1_1 C1_1 C2_1 C3_1 -109.7(11) . . . . ?
 F1_1 C1_1 C2_1 C7_1 68.2(14) . . . . ?
 F2_1 C1_1 C2_1 C3_1 3.3(14) . . . . ?
 F2_1 C1_1 C2_1 C7_1 -178.8(12) . . . . ?
 F3_1 C1_1 C2_1 C3_1 129.7(12) . . . . ?
 F3_1 C1_1 C2_1 C7_1 -52.4(15) . . . . ?
 N1_1 C5_1 C6_1 C7_1 -174.5(19) . . . . ?
 N1_1 C8_1 C9_1 C10_1 170(2) . . . . ?
 N2_1 C4_1 C5_1 N1_1 -7.7(18) . . . . ?
 N2_1 C4_1 C5_1 C6_1 177.0(16) . . . . ?
 N2_1 C8_1 C9_1 C10_1 -5(3) . . . . ?
 N2_1 C12_1 C13_1 N3_1 23(2) . . . . ?
 N2_1 C12_1 C13_1 C14_1 -156.0(13) . . . . ?
 N3_1 C13_1 C14_1 C15_1 -15.7(19) . . . . ?
 N3_1 C13_1 C14_1 C18_1 163.5(13) . . . . ?
 N3_1 C20_1 C21_1 N4_1 -3.4(12) . . . . ?
 N3_1 C20_1 C21_1 C22_1 179.6(10) . . . . ?
 N3_1 C20_1 C25_1 C24_1 179.6(10) . . . . ?
 N4_1 C21_1 C22_1 C23_1 -173.1(11) . . . . ?
 C1_1 C2_1 C3_1 C4_1 176.1(10) . . . . ?
 C1_1 C2_1 C7_1 C6_1 -178.9(14) . . . . ?
 C2_1 C3_1 C4_1 N2_1 -175.7(13) . . . . ?
 C2_1 C3_1 C4_1 C5_1 4(2) . . . . ?
 C3_1 C2_1 C7_1 C6_1 -1(2) . . . . ?
 C3_1 C4_1 C5_1 N1_1 172.9(14) . . . . ?
 C3_1 C4_1 C5_1 C6_1 -2(2) . . . . ?
 C4_1 N2_1 C8_1 N1_1 -7(2) . . . . ?
 C4_1 N2_1 C8_1 C9_1 168.0(16) . . . . ?
 C4_1 N2_1 C12_1 C11_1 -155.4(15) . . . . ?
 C4_1 N2_1 C12_1 C13_1 21(2) . . . . ?
 C4_1 C5_1 C6_1 C7_1 -1(3) . . . . ?
 C5_1 N1_1 C8_1 N2_1 3(2) . . . . ?
 C5_1 N1_1 C8_1 C9_1 -172(2) . . . . ?
 C5_1 C6_1 C7_1 C2_1 2(3) . . . . ?
 C7_1 C2_1 C3_1 C4_1 -1.8(18) . . . . ?
 C8_1 N1_1 C5_1 C4_1 3(2) . . . . ?
 C8_1 N1_1 C5_1 C6_1 177(2) . . . . ?
 C8_1 N2_1 C4_1 C3_1 -171.9(15) . . . . ?
 C8_1 N2_1 C4_1 C5_1 8.6(16) . . . . ?
 C8_1 N2_1 C12_1 C11_1 23(2) . . . . ?
 C8_1 N2_1 C12_1 C13_1 -161.1(14) . . . . ?
 C8_1 C9_1 C10_1 C11_1 7(3) . . . . ?
 C9_1 C10_1 C11_1 C12_1 6(3) . . . . ?
 C9_1 C10_1 C11_1 C19_1 179(2) . . . . ?
 C10_1 C11_1 C12_1 N2_1 -20(2) . . . . ?
 C10_1 C11_1 C12_1 C13_1 163.6(15) . . . . ?
 C10_1 C11_1 C19_1 C18_1 -177.2(17) . . . . ?
 C11_1 C12_1 C13_1 N3_1 -160.4(13) . . . . ?
 C11_1 C12_1 C13_1 C14_1 20(2) . . . . ?
 C12_1 N2_1 C4_1 C3_1 6(3) . . . . ?
 C12_1 N2_1 C4_1 C5_1 -173.2(15) . . . . ?
 C12_1 N2_1 C8_1 N1_1 174.3(15) . . . . ?
 C12_1 N2_1 C8_1 C9_1 -10(2) . . . . ?
 C12_1 C11_1 C19_1 C18_1 -4(3) . . . . ?
 C12_1 C13_1 C14_1 C15_1 163.7(13) . . . . ?
 C12_1 C13_1 C14_1 C18_1 -17(2) . . . . ?
 C13_1 N3_1 C17_1 N4_1 179.0(10) . . . . ?
 C13_1 N3_1 C17_1 C16_1 -7.7(17) . . . . ?
 C13_1 N3_1 C20_1 C21_1 -179.2(11) . . . . ?
 C13_1 N3_1 C20_1 C25_1 5.4(19) . . . . ?
 C13_1 C14_1 C15_1 C16_1 5(2) . . . . ?
 C13_1 C14_1 C18_1 C19_1 3(2) . . . . ?
 C14_1 C15_1 C16_1 C17_1 5(2) . . . . ?
 C14_1 C18_1 C19_1 C11_1 7(3) . . . . ?
 C15_1 C14_1 C18_1 C19_1 -177.4(16) . . . . ?
 C15_1 C16_1 C17_1 N3_1 -4(2) . . . . ?
 C15_1 C16_1 C17_1 N4_1 168.8(13) . . . . ?
 C17_1 N3_1 C13_1 C12_1 -162.2(12) . . . . ?
 C17_1 N3_1 C13_1 C14_1 17.3(16) . . . . ?
 C17_1 N3_1 C20_1 C21_1 4.0(10) . . . . ?
 C17_1 N3_1 C20_1 C25_1 -171.4(11) . . . . ?
 C17_1 N4_1 C21_1 C20_1 1.2(13) . . . . ?
 C17_1 N4_1 C21_1 C22_1 178.0(12) . . . . ?
 C18_1 C14_1 C15_1 C16_1 -174.1(16) . . . . ?
 C19_1 C11_1 C12_1 N2_1 166.5(14) . . . . ?
 C19_1 C11_1 C12_1 C13_1 -10(2) . . . . ?
 C20_1 N3_1 C13_1 C12_1 21(2) . . . . ?
 C20_1 N3_1 C13_1 C14_1 -159.1(11) . . . . ?
 C20_1 N3_1 C17_1 N4_1 -3.7(13) . . . . ?
 C20_1 N3_1 C17_1 C16_1 169.5(11) . . . . ?
 C20_1 C21_1 C22_1 C23_1 3.5(17) . . . . ?
 C21_1 N4_1 C17_1 N3_1 1.6(13) . . . . ?
 C21_1 N4_1 C17_1 C16_1 -171.2(12) . . . . ?
 C21_1 C20_1 C25_1 C24_1 4.8(14) . . . . ?
 C21_1 C22_1 C23_1 C24_1 -3.5(18) . . . . ?
 C22_1 C23_1 C24_1 C25_1 4.5(18) . . . . ?
 C22_1 C23_1 C24_1 C26_1 -174.4(11) . . . . ?
 C23_1 C24_1 C25_1 C20_1 -4.9(15) . . . . ?
 C23_1 C24_1 C26_1 F4_1 171.6(10) . . . . ?
 C23_1 C24_1 C26_1 F5_1 53.6(13) . . . . ?
 C23_1 C24_1 C26_1 F6_1 -69.4(13) . . . . ?
 C25_1 C20_1 C21_1 N4_1 172.8(9) . . . . ?
 C25_1 C20_1 C21_1 C22_1 -4.3(15) . . . . ?
 C25_1 C24_1 C26_1 F4_1 -7.3(13) . . . . ?
 C25_1 C24_1 C26_1 F5_1 -125.3(10) . . . . ?
 C25_1 C24_1 C26_1 F6_1 111.6(11) . . . . ?
 C26_1 C24_1 C25_1 C20_1 173.9(9) . . . . ?
 F1_2 C1_2 C2_2 C3_2 -115.0(12) . . . . ?
 F1_2 C1_2 C2_2 C7_2 61.8(15) . . . . ?
 F2_2 C1_2 C2_2 C3_2 2.0(15) . . . . ?
 F2_2 C1_2 C2_2 C7_2 178.8(11) . . . . ?
 F3_2 C1_2 C2_2 C3_2 123.4(12) . . . . ?
 F3_2 C1_2 C2_2 C7_2 -59.8(15) . . . . ?
 N1_2 C5_2 C6_2 C7_2 -176.1(14) . . . . ?
 N1_2 C8_2 C9_2 C10_2 167.7(16) . . . . ?
 N2_2 C4_2 C5_2 N1_2 -6.7(14) . . . . ?
 N2_2 C4_2 C5_2 C6_2 179.3(11) . . . . ?
 N2_2 C8_2 C9_2 C10_2 1(2) . . . . ?
 N2_2 C12_2 C13_2 N3_2 25(2) . . . . ?
 N2_2 C12_2 C13_2 C14_2 -156.8(12) . . . . ?
 N3_2 C13_2 C14_2 C15_2 -20(2) . . . . ?
 N3_2 C13_2 C14_2 C18_2 162.4(13) . . . . ?
 N3_2 C20_2 C21_2 N4_2 -2.1(13) . . . . ?
 N3_2 C20_2 C21_2 C22_2 175.4(10) . . . . ?
 N3_2 C20_2 C25_2 C24_2 -178.0(10) . . . . ?
 N4_2 C21_2 C22_2 C23_2 -179.3(11) . . . . ?
 C1_2 C2_2 C3_2 C4_2 175.2(10) . . . . ?
 C1_2 C2_2 C7_2 C6_2 -178.3(12) . . . . ?
 C2_2 C3_2 C4_2 N2_2 -176.5(11) . . . . ?
 C2_2 C3_2 C4_2 C5_2 2.1(16) . . . . ?
 C3_2 C2_2 C7_2 C6_2 -2(2) . . . . ?
 C3_2 C4_2 C5_2 N1_2 174.4(10) . . . . ?
 C3_2 C4_2 C5_2 C6_2 0.4(18) . . . . ?
 C4_2 N2_2 C8_2 N1_2 -3.9(14) . . . . ?
 C4_2 N2_2 C8_2 C9_2 165.5(12) . . . . ?
 C4_2 N2_2 C12_2 C11_2 -155.2(12) . . . . ?
 C4_2 N2_2 C12_2 C13_2 22(2) . . . . ?
 C4_2 C5_2 C6_2 C7_2 -3(2) . . . . ?
 C5_2 N1_2 C8_2 N2_2 -0.2(16) . . . . ?
 C5_2 N1_2 C8_2 C9_2 -168.0(14) . . . . ?
 C5_2 C6_2 C7_2 C2_2 4(2) . . . . ?
 C7_2 C2_2 C3_2 C4_2 -1.5(17) . . . . ?
 C8_2 N1_2 C5_2 C4_2 4.3(16) . . . . ?
 C8_2 N1_2 C5_2 C6_2 177.4(14) . . . . ?
 C8_2 N2_2 C4_2 C3_2 -175.1(11) . . . . ?
 C8_2 N2_2 C4_2 C5_2 6.2(12) . . . . ?
 C8_2 N2_2 C12_2 C11_2 21.6(17) . . . . ?
 C8_2 N2_2 C12_2 C13_2 -160.8(12) . . . . ?
 C8_2 C9_2 C10_2 C11_2 1(3) . . . . ?
 C9_2 C10_2 C11_2 C12_2 9(2) . . . . ?
 C9_2 C10_2 C11_2 C19_2 -177.3(17) . . . . ?
 C10_2 C11_2 C12_2 N2_2 -19.3(19) . . . . ?
 C10_2 C11_2 C12_2 C13_2 162.9(13) . . . . ?
 C10_2 C11_2 C19_2 C18_2 -178.2(17) . . . . ?
 C11_2 C12_2 C13_2 N3_2 -157.0(12) . . . . ?
 C11_2 C12_2 C13_2 C14_2 20.8(19) . . . . ?
 C12_2 N2_2 C4_2 C3_2 2(2) . . . . ?
 C12_2 N2_2 C4_2 C5_2 -176.7(11) . . . . ?
 C12_2 N2_2 C8_2 N1_2 178.5(11) . . . . ?
 C12_2 N2_2 C8_2 C9_2 -12.0(18) . . . . ?
 C12_2 C11_2 C19_2 C18_2 -5(3) . . . . ?
 C12_2 C13_2 C14_2 C15_2 162.1(14) . . . . ?
 C12_2 C13_2 C14_2 C18_2 -16(2) . . . . ?
 C13_2 N3_2 C17_2 N4_2 177.0(11) . . . . ?
 C13_2 N3_2 C17_2 C16_2 -8.7(18) . . . . ?
 C13_2 N3_2 C20_2 C21_2 -178.2(11) . . . . ?
 C13_2 N3_2 C20_2 C25_2 2(2) . . . . ?
 C13_2 C14_2 C15_2 C16_2 7(2) . . . . ?
 C13_2 C14_2 C18_2 C19_2 0(2) . . . . ?
 C14_2 C15_2 C16_2 C17_2 5(2) . . . . ?
 C14_2 C18_2 C19_2 C11_2 10(3) . . . . ?
 C15_2 C14_2 C18_2 C19_2 -177.7(17) . . . . ?
 C15_2 C16_2 C17_2 N3_2 -5(2) . . . . ?
 C15_2 C16_2 C17_2 N4_2 168.8(15) . . . . ?
 C17_2 N3_2 C13_2 C12_2 -161.2(12) . . . . ?
 C17_2 N3_2 C13_2 C14_2 20.9(17) . . . . ?
 C17_2 N3_2 C20_2 C21_2 4.0(12) . . . . ?
 C17_2 N3_2 C20_2 C25_2 -175.6(11) . . . . ?
 C17_2 N4_2 C21_2 C20_2 -0.8(14) . . . . ?
 C17_2 N4_2 C21_2 C22_2 -178.1(12) . . . . ?
 C18_2 C14_2 C15_2 C16_2 -175.2(16) . . . . ?
 C19_2 C11_2 C12_2 N2_2 166.6(13) . . . . ?
 C19_2 C11_2 C12_2 C13_2 -11(2) . . . . ?
 C20_2 N3_2 C13_2 C12_2 21(2) . . . . ?
 C20_2 N3_2 C13_2 C14_2 -156.6(12) . . . . ?
 C20_2 N3_2 C17_2 N4_2 -4.9(14) . . . . ?
 C20_2 N3_2 C17_2 C16_2 169.4(12) . . . . ?
 C20_2 C21_2 C22_2 C23_2 3.6(16) . . . . ?
 C21_2 N4_2 C17_2 N3_2 3.6(15) . . . . ?
 C21_2 N4_2 C17_2 C16_2 -170.3(14) . . . . ?
 C21_2 C20_2 C25_2 C24_2 2.4(15) . . . . ?
 C21_2 C22_2 C23_2 C24_2 -0.1(16) . . . . ?
 C22_2 C23_2 C24_2 C25_2 -2.3(15) . . . . ?
 C22_2 C23_2 C24_2 C26_2 -179.2(10) . . . . ?
 C23_2 C24_2 C25_2 C20_2 1.1(14) . . . . ?
 C23_2 C24_2 C26_2 F4_2 163.3(8) . . . . ?
 C23_2 C24_2 C26_2 F5_2 43.8(11) . . . . ?
 C23_2 C24_2 C26_2 F6_2 -74.7(10) . . . . ?
 C25_2 C20_2 C21_2 N4_2 177.6(10) . . . . ?
 C25_2 C20_2 C21_2 C22_2 -4.9(16) . . . . ?
 C25_2 C24_2 C26_2 F4_2 -13.6(12) . . . . ?
 C25_2 C24_2 C26_2 F5_2 -133.1(9) . . . . ?
 C25_2 C24_2 C26_2 F6_2 108.4(10) . . . . ?
 C26_2 C24_2 C25_2 C20_2 178.0(8) . . . . ?
 F1_3 C1_3 C2_3 C3_3 -112.2(10) . . . . ?
 F1_3 C1_3 C2_3 C7_3 63.2(13) . . . . ?
 F2_3 C1_3 C2_3 C3_3 3.8(13) . . . . ?
 F2_3 C1_3 C2_3 C7_3 179.2(11) . . . . ?
 F3_3 C1_3 C2_3 C3_3 125.9(11) . . . . ?
 F3_3 C1_3 C2_3 C7_3 -58.7(14) . . . . ?
 N1_3 C5_3 C6_3 C7_3 -178.5(12) . . . . ?
 N1_3 C8_3 C9_3 C10_3 166.8(13) . . . . ?
 N2_3 C4_3 C5_3 N1_3 -6.4(12) . . . . ?
 N2_3 C4_3 C5_3 C6_3 175.8(10) . . . . ?
 N2_3 C8_3 C9_3 C10_3 -10.9(17) . . . . ?
 N2_3 C12_3 C13_3 N3_3 21.2(17) . . . . ?
 N2_3 C12_3 C13_3 C14_3 -157.2(11) . . . . ?
 N3_3 C13_3 C14_3 C15_3 -14.4(18) . . . . ?
 N3_3 C13_3 C14_3 C18_3 165.5(11) . . . . ?
 N3_3 C20_3 C21_3 N4_3 -1.4(12) . . . . ?
 N3_3 C20_3 C21_3 C22_3 179.8(9) . . . . ?
 N3_3 C20_3 C25_3 C24_3 -177.9(9) . . . . ?
 N4_3 C21_3 C22_3 C23_3 -179.3(11) . . . . ?
 C1_3 C2_3 C3_3 C4_3 176.4(8) . . . . ?
 C1_3 C2_3 C7_3 C6_3 -179.9(11) . . . . ?
 C2_3 C3_3 C4_3 N2_3 -175.2(10) . . . . ?
 C2_3 C3_3 C4_3 C5_3 2.5(14) . . . . ?
 C3_3 C2_3 C7_3 C6_3 -4.6(18) . . . . ?
 C3_3 C4_3 C5_3 N1_3 175.3(9) . . . . ?
 C3_3 C4_3 C5_3 C6_3 -2.4(16) . . . . ?
 C4_3 N2_3 C8_3 N1_3 -8.0(12) . . . . ?
 C4_3 N2_3 C8_3 C9_3 170.0(10) . . . . ?
 C4_3 N2_3 C12_3 C11_3 -155.1(10) . . . . ?
 C4_3 N2_3 C12_3 C13_3 24.6(16) . . . . ?
 C4_3 C5_3 C6_3 C7_3 -1.2(19) . . . . ?
 C5_3 N1_3 C8_3 N2_3 4.1(13) . . . . ?
 C5_3 N1_3 C8_3 C9_3 -173.7(12) . . . . ?
 C5_3 C6_3 C7_3 C2_3 5(2) . . . . ?
 C7_3 C2_3 C3_3 C4_3 1.0(15) . . . . ?
 C8_3 N1_3 C5_3 C4_3 1.6(13) . . . . ?
 C8_3 N1_3 C5_3 C6_3 179.1(13) . . . . ?
 C8_3 N2_3 C4_3 C3_3 -173.7(10) . . . . ?
 C8_3 N2_3 C4_3 C5_3 8.3(10) . . . . ?
 C8_3 N2_3 C12_3 C11_3 17.9(14) . . . . ?
 C8_3 N2_3 C12_3 C13_3 -162.4(10) . . . . ?
 C8_3 C9_3 C10_3 C11_3 12.6(19) . . . . ?
 C9_3 C10_3 C11_3 C12_3 1.2(19) . . . . ?
 C9_3 C10_3 C11_3 C19_3 179.5(13) . . . . ?
 C10_3 C11_3 C12_3 N2_3 -16.0(15) . . . . ?
 C10_3 C11_3 C12_3 C13_3 164.3(11) . . . . ?
 C10_3 C11_3 C19_3 C18_3 -179.5(13) . . . . ?
 C11_3 C12_3 C13_3 N3_3 -159.2(10) . . . . ?
 C11_3 C12_3 C13_3 C14_3 22.5(16) . . . . ?
 C12_3 N2_3 C4_3 C3_3 0.2(18) . . . . ?
 C12_3 N2_3 C4_3 C5_3 -177.8(10) . . . . ?
 C12_3 N2_3 C8_3 N1_3 177.3(9) . . . . ?
 C12_3 N2_3 C8_3 C9_3 -4.6(15) . . . . ?
 C12_3 C11_3 C19_3 C18_3 -1.1(19) . . . . ?
 C12_3 C13_3 C14_3 C15_3 164.1(12) . . . . ?
 C12_3 C13_3 C14_3 C18_3 -16.0(18) . . . . ?
 C13_3 N3_3 C17_3 N4_3 -179.4(11) . . . . ?
 C13_3 N3_3 C17_3 C16_3 -13.1(18) . . . . ?
 C13_3 N3_3 C20_3 C21_3 -179.8(10) . . . . ?
 C13_3 N3_3 C20_3 C25_3 5.1(18) . . . . ?
 C13_3 C14_3 C15_3 C16_3 0(2) . . . . ?
 C13_3 C14_3 C18_3 C19_3 1(2) . . . . ?
 C14_3 C15_3 C16_3 C17_3 8(2) . . . . ?
 C14_3 C18_3 C19_3 C11_3 8(2) . . . . ?
 C15_3 C14_3 C18_3 C19_3 -179.0(15) . . . . ?
 C15_3 C16_3 C17_3 N3_3 -2(2) . . . . ?
 C15_3 C16_3 C17_3 N4_3 162.8(15) . . . . ?
 C17_3 N3_3 C13_3 C12_3 -157.4(11) . . . . ?
 C17_3 N3_3 C13_3 C14_3 20.9(16) . . . . ?
 C17_3 N3_3 C20_3 C21_3 0.8(11) . . . . ?
 C17_3 N3_3 C20_3 C25_3 -174.4(11) . . . . ?
 C17_3 N4_3 C21_3 C20_3 1.5(14) . . . . ?
 C17_3 N4_3 C21_3 C22_3 -179.9(12) . . . . ?
 C18_3 C14_3 C15_3 C16_3 -179.4(16) . . . . ?
 C19_3 C11_3 C12_3 N2_3 165.5(10) . . . . ?
 C19_3 C11_3 C12_3 C13_3 -14.1(16) . . . . ?
 C20_3 N3_3 C13_3 C12_3 23.2(18) . . . . ?
 C20_3 N3_3 C13_3 C14_3 -158.5(11) . . . . ?
 C20_3 N3_3 C17_3 N4_3 0.1(14) . . . . ?
 C20_3 N3_3 C17_3 C16_3 166.5(12) . . . . ?
 C20_3 C21_3 C22_3 C23_3 -0.7(16) . . . . ?
 C21_3 N4_3 C17_3 N3_3 -1.0(15) . . . . ?
 C21_3 N4_3 C17_3 C16_3 -166.2(14) . . . . ?
 C21_3 C20_3 C25_3 C24_3 7.7(14) . . . . ?
 C21_3 C22_3 C23_3 C24_3 2.3(15) . . . . ?
 C22_3 C23_3 C24_3 C25_3 1.1(14) . . . . ?
 C22_3 C23_3 C24_3 C26_3 -179.8(9) . . . . ?
 C23_3 C24_3 C25_3 C20_3 -6.0(13) . . . . ?
 C23_3 C24_3 C26_3 F4_3 164.5(8) . . . . ?
 C23_3 C24_3 C26_3 F5_3 46.1(11) . . . . ?
 C23_3 C24_3 C26_3 F6_3 -74.5(10) . . . . ?
 C25_3 C20_3 C21_3 N4_3 174.3(10) . . . . ?
 C25_3 C20_3 C21_3 C22_3 -4.5(15) . . . . ?
 C25_3 C24_3 C26_3 F4_3 -16.5(11) . . . . ?
 C25_3 C24_3 C26_3 F5_3 -134.8(8) . . . . ?
 C25_3 C24_3 C26_3 F6_3 104.6(9) . . . . ?
 C26_3 C24_3 C25_3 C20_3 175.0(8) . . . . ?
 F1_4 C1_4 C2_4 C3_4 -121.7(10) . . . . ?
 F1_4 C1_4 C2_4 C7_4 57.6(13) . . . . ?
 F2_4 C1_4 C2_4 C3_4 -2.8(13) . . . . ?
 F2_4 C1_4 C2_4 C7_4 176.6(10) . . . . ?
 F3_4 C1_4 C2_4 C3_4 119.4(10) . . . . ?
 F3_4 C1_4 C2_4 C7_4 -61.2(13) . . . . ?
 N1_4 C5_4 C6_4 C7_4 177.4(13) . . . . ?
 N1_4 C8_4 C9_4 C10_4 171.9(16) . . . . ?
 N2_4 C4_4 C5_4 N1_4 1.2(13) . . . . ?
 N2_4 C4_4 C5_4 C6_4 177.9(11) . . . . ?
 N2_4 C8_4 C9_4 C10_4 -4(2) . . . . ?
 N2_4 C12_4 C13_4 N3_4 23.1(19) . . . . ?
 N2_4 C12_4 C13_4 C14_4 -159.2(11) . . . . ?
 N3_4 C13_4 C14_4 C15_4 -21.9(18) . . . . ?
 N3_4 C13_4 C14_4 C18_4 166.8(13) . . . . ?
 N3_4 C20_4 C21_4 N4_4 -4.0(13) . . . . ?
 N3_4 C20_4 C21_4 C22_4 175.4(11) . . . . ?
 N3_4 C20_4 C25_4 C24_4 -177.6(11) . . . . ?
 N4_4 C21_4 C22_4 C23_4 -178.2(12) . . . . ?
 C1_4 C2_4 C3_4 C4_4 177.2(8) . . . . ?
 C1_4 C2_4 C7_4 C6_4 179.1(11) . . . . ?
 C2_4 C3_4 C4_4 N2_4 -178.5(10) . . . . ?
 C2_4 C3_4 C4_4 C5_4 5.8(15) . . . . ?
 C3_4 C2_4 C7_4 C6_4 -1.6(18) . . . . ?
 C3_4 C4_4 C5_4 N1_4 177.9(10) . . . . ?
 C3_4 C4_4 C5_4 C6_4 -5.4(17) . . . . ?
 C4_4 N2_4 C8_4 N1_4 -7.3(14) . . . . ?
 C4_4 N2_4 C8_4 C9_4 168.9(11) . . . . ?
 C4_4 N2_4 C12_4 C11_4 -159.0(11) . . . . ?
 C4_4 N2_4 C12_4 C13_4 21.5(19) . . . . ?
 C4_4 C5_4 C6_4 C7_4 2(2) . . . . ?
 C5_4 N1_4 C8_4 N2_4 8.0(15) . . . . ?
 C5_4 N1_4 C8_4 C9_4 -167.7(14) . . . . ?
 C5_4 C6_4 C7_4 C2_4 2(2) . . . . ?
 C7_4 C2_4 C3_4 C4_4 -2.1(15) . . . . ?
 C8_4 N1_4 C5_4 C4_4 -5.5(15) . . . . ?
 C8_4 N1_4 C5_4 C6_4 178.4(14) . . . . ?
 C8_4 N2_4 C4_4 C3_4 -172.9(11) . . . . ?
 C8_4 N2_4 C4_4 C5_4 3.4(12) . . . . ?
 C8_4 N2_4 C12_4 C11_4 19.7(16) . . . . ?
 C8_4 N2_4 C12_4 C13_4 -159.9(12) . . . . ?
 C8_4 C9_4 C10_4 C11_4 7(3) . . . . ?
 C9_4 C10_4 C11_4 C12_4 3(3) . . . . ?
 C9_4 C10_4 C11_4 C19_4 -176.2(17) . . . . ?
 C10_4 C11_4 C12_4 N2_4 -15.5(18) . . . . ?
 C10_4 C11_4 C12_4 C13_4 164.0(13) . . . . ?
 C10_4 C11_4 C19_4 C18_4 -179.5(17) . . . . ?
 C11_4 C12_4 C13_4 N3_4 -156.4(12) . . . . ?
 C11_4 C12_4 C13_4 C14_4 21.3(18) . . . . ?
 C12_4 N2_4 C4_4 C3_4 6.0(19) . . . . ?
 C12_4 N2_4 C4_4 C5_4 -177.7(11) . . . . ?
 C12_4 N2_4 C8_4 N1_4 173.7(11) . . . . ?
 C12_4 N2_4 C8_4 C9_4 -10.1(18) . . . . ?
 C12_4 C11_4 C19_4 C18_4 1(2) . . . . ?
 C12_4 C13_4 C14_4 C15_4 160.2(13) . . . . ?
 C12_4 C13_4 C14_4 C18_4 -11.2(19) . . . . ?
 C13_4 N3_4 C17_4 N4_4 173.5(11) . . . . ?
 C13_4 N3_4 C17_4 C16_4 -7.0(18) . . . . ?
 C13_4 N3_4 C20_4 C21_4 -174.9(11) . . . . ?
 C13_4 N3_4 C20_4 C25_4 3(2) . . . . ?
 C13_4 C14_4 C15_4 C16_4 7(2) . . . . ?
 C13_4 C14_4 C18_4 C19_4 -4(2) . . . . ?
 C14_4 C15_4 C16_4 C17_4 9(3) . . . . ?
 C14_4 C18_4 C19_4 C11_4 9(3) . . . . ?
 C15_4 C14_4 C18_4 C19_4 -174.7(16) . . . . ?
 C15_4 C16_4 C17_4 N3_4 -9(2) . . . . ?
 C15_4 C16_4 C17_4 N4_4 170.6(15) . . . . ?
 C17_4 N3_4 C13_4 C12_4 -159.6(12) . . . . ?
 C17_4 N3_4 C13_4 C14_4 22.6(17) . . . . ?
 C17_4 N3_4 C20_4 C21_4 6.7(11) . . . . ?
 C17_4 N3_4 C20_4 C25_4 -175.4(11) . . . . ?
 C17_4 N4_4 C21_4 C20_4 -0.7(14) . . . . ?
 C17_4 N4_4 C21_4 C22_4 180.0(13) . . . . ?
 C18_4 C14_4 C15_4 C16_4 177.6(16) . . . . ?
 C19_4 C11_4 C12_4 N2_4 163.8(12) . . . . ?
 C19_4 C11_4 C12_4 C13_4 -16.7(19) . . . . ?
 C20_4 N3_4 C13_4 C12_4 22(2) . . . . ?
 C20_4 N3_4 C13_4 C14_4 -155.6(11) . . . . ?
 C20_4 N3_4 C17_4 N4_4 -7.9(14) . . . . ?
 C20_4 N3_4 C17_4 C16_4 171.6(12) . . . . ?
 C20_4 C21_4 C22_4 C23_4 2.6(19) . . . . ?
 C21_4 N4_4 C17_4 N3_4 5.4(15) . . . . ?
 C21_4 N4_4 C17_4 C16_4 -174.0(14) . . . . ?
 C21_4 C20_4 C25_4 C24_4 0.0(15) . . . . ?
 C21_4 C22_4 C23_4 C24_4 0.3(19) . . . . ?
 C22_4 C23_4 C24_4 C25_4 -3.2(18) . . . . ?
 C22_4 C23_4 C24_4 C26_4 -177.8(11) . . . . ?
 C23_4 C24_4 C25_4 C20_4 3.0(15) . . . . ?
 C23_4 C24_4 C26_4 F4_4 163.2(9) . . . . ?
 C23_4 C24_4 C26_4 F5_4 43.9(12) . . . . ?
 C23_4 C24_4 C26_4 F6_4 -75.9(11) . . . . ?
 C25_4 C20_4 C21_4 N4_4 177.8(10) . . . . ?
 C25_4 C20_4 C21_4 C22_4 -2.8(17) . . . . ?
 C25_4 C24_4 C26_4 F4_4 -11.6(13) . . . . ?
 C25_4 C24_4 C26_4 F5_4 -130.9(10) . . . . ?
 C25_4 C24_4 C26_4 F6_4 109.4(10) . . . . ?
 C26_4 C24_4 C25_4 C20_4 177.4(9) . . . . ?
 F1_5 C1_5 C2_5 C3_5 -121.9(11) . . . . ?
 F1_5 C1_5 C2_5 C7_5 57.7(13) . . . . ?
 F2_5 C1_5 C2_5 C3_5 -4.5(14) . . . . ?
 F2_5 C1_5 C2_5 C7_5 175.1(11) . . . . ?
 F3_5 C1_5 C2_5 C3_5 116.2(11) . . . . ?
 F3_5 C1_5 C2_5 C7_5 -64.2(13) . . . . ?
 N1_5 C5_5 C6_5 C7_5 179.4(15) . . . . ?
 N1_5 C8_5 C9_5 C10_5 171.1(16) . . . . ?
 N2_5 C4_5 C5_5 N1_5 1.6(15) . . . . ?
 N2_5 C4_5 C5_5 C6_5 174.8(13) . . . . ?
 N2_5 C8_5 C9_5 C10_5 -3(2) . . . . ?
 N2_5 C12_5 C13_5 N3_5 21.3(17) . . . . ?
 N2_5 C12_5 C13_5 C14_5 -156.5(11) . . . . ?
 N3_5 C13_5 C14_5 C15_5 -13.6(17) . . . . ?
 N3_5 C13_5 C14_5 C18_5 162.8(12) . . . . ?
 N3_5 C20_5 C21_5 N4_5 -6.5(12) . . . . ?
 N3_5 C20_5 C21_5 C22_5 178.7(10) . . . . ?
 N3_5 C20_5 C25_5 C24_5 -177.8(10) . . . . ?
 N4_5 C21_5 C22_5 C23_5 -174.1(12) . . . . ?
 C1_5 C2_5 C3_5 C4_5 174.8(9) . . . . ?
 C1_5 C2_5 C7_5 C6_5 -179.5(13) . . . . ?
 C2_5 C3_5 C4_5 N2_5 -178.8(11) . . . . ?
 C2_5 C3_5 C4_5 C5_5 10.8(17) . . . . ?
 C3_5 C2_5 C7_5 C6_5 0(2) . . . . ?
 C3_5 C4_5 C5_5 N1_5 174.3(11) . . . . ?
 C3_5 C4_5 C5_5 C6_5 -12(2) . . . . ?
 C4_5 N2_5 C8_5 N1_5 -4.6(15) . . . . ?
 C4_5 N2_5 C8_5 C9_5 170.5(12) . . . . ?
 C4_5 N2_5 C12_5 C11_5 -159.6(11) . . . . ?
 C4_5 N2_5 C12_5 C13_5 21.0(19) . . . . ?
 C4_5 C5_5 C6_5 C7_5 7(2) . . . . ?
 C5_5 N1_5 C8_5 N2_5 5.5(17) . . . . ?
 C5_5 N1_5 C8_5 C9_5 -168.9(15) . . . . ?
 C5_5 C6_5 C7_5 C2_5 -1(2) . . . . ?
 C7_5 C2_5 C3_5 C4_5 -4.7(17) . . . . ?
 C8_5 N1_5 C5_5 C4_5 -4.3(17) . . . . ?
 C8_5 N1_5 C5_5 C6_5 -176.9(16) . . . . ?
 C8_5 N2_5 C4_5 C3_5 -169.9(12) . . . . ?
 C8_5 N2_5 C4_5 C5_5 1.7(13) . . . . ?
 C8_5 N2_5 C12_5 C11_5 20.4(16) . . . . ?
 C8_5 N2_5 C12_5 C13_5 -159.0(11) . . . . ?
 C8_5 C9_5 C10_5 C11_5 4(3) . . . . ?
 C9_5 C10_5 C11_5 C12_5 7(2) . . . . ?
 C9_5 C10_5 C11_5 C19_5 -177.1(16) . . . . ?
 C10_5 C11_5 C12_5 N2_5 -18.8(16) . . . . ?
 C10_5 C11_5 C12_5 C13_5 160.6(12) . . . . ?
 C10_5 C11_5 C19_5 C18_5 -174.3(17) . . . . ?
 C11_5 C12_5 C13_5 N3_5 -158.0(10) . . . . ?
 C11_5 C12_5 C13_5 C14_5 24.1(16) . . . . ?
 C12_5 N2_5 C4_5 C3_5 10(2) . . . . ?
 C12_5 N2_5 C4_5 C5_5 -178.4(12) . . . . ?
 C12_5 N2_5 C8_5 N1_5 175.4(11) . . . . ?
 C12_5 N2_5 C8_5 C9_5 -9.5(18) . . . . ?
 C12_5 C11_5 C19_5 C18_5 1(2) . . . . ?
 C12_5 C13_5 C14_5 C15_5 164.4(12) . . . . ?
 C12_5 C13_5 C14_5 C18_5 -19.2(18) . . . . ?
 C13_5 N3_5 C17_5 N4_5 -178.5(9) . . . . ?
 C13_5 N3_5 C17_5 C16_5 -11.4(16) . . . . ?
 C13_5 N3_5 C20_5 C21_5 -179.8(10) . . . . ?
 C13_5 N3_5 C20_5 C25_5 -1.0(17) . . . . ?
 C13_5 C14_5 C15_5 C16_5 3(2) . . . . ?
 C13_5 C14_5 C18_5 C19_5 5(2) . . . . ?
 C14_5 C15_5 C16_5 C17_5 4(2) . . . . ?
 C14_5 C18_5 C19_5 C11_5 4(3) . . . . ?
 C15_5 C14_5 C18_5 C19_5 -178.4(17) . . . . ?
 C15_5 C16_5 C17_5 N3_5 -0.4(19) . . . . ?
 C15_5 C16_5 C17_5 N4_5 164.3(13) . . . . ?
 C17_5 N3_5 C13_5 C12_5 -159.3(11) . . . . ?
 C17_5 N3_5 C13_5 C14_5 18.5(15) . . . . ?
 C17_5 N3_5 C20_5 C21_5 5.9(11) . . . . ?
 C17_5 N3_5 C20_5 C25_5 -175.2(10) . . . . ?
 C17_5 N4_5 C21_5 C20_5 4.3(13) . . . . ?
 C17_5 N4_5 C21_5 C22_5 178.4(12) . . . . ?
 C18_5 C14_5 C15_5 C16_5 -173.4(15) . . . . ?
 C19_5 C11_5 C12_5 N2_5 165.5(12) . . . . ?
 C19_5 C11_5 C12_5 C13_5 -15.1(18) . . . . ?
 C20_5 N3_5 C13_5 C12_5 27.3(17) . . . . ?
 C20_5 N3_5 C13_5 C14_5 -154.9(10) . . . . ?
 C20_5 N3_5 C17_5 N4_5 -3.7(13) . . . . ?
 C20_5 N3_5 C17_5 C16_5 163.5(10) . . . . ?
 C20_5 C21_5 C22_5 C23_5 -0.4(17) . . . . ?
 C21_5 N4_5 C17_5 N3_5 -0.3(13) . . . . ?
 C21_5 N4_5 C17_5 C16_5 -165.7(12) . . . . ?
 C21_5 C20_5 C25_5 C24_5 0.9(14) . . . . ?
 C21_5 C22_5 C23_5 C24_5 0.5(18) . . . . ?
 C22_5 C23_5 C24_5 C25_5 0.2(17) . . . . ?
 C22_5 C23_5 C24_5 C26_5 179.4(10) . . . . ?
 C23_5 C24_5 C25_5 C20_5 -0.9(14) . . . . ?
 C23_5 C24_5 C26_5 F4_5 174.4(9) . . . . ?
 C23_5 C24_5 C26_5 F5_5 56.2(13) . . . . ?
 C23_5 C24_5 C26_5 F6_5 -62.9(12) . . . . ?
 C25_5 C20_5 C21_5 N4_5 174.5(9) . . . . ?
 C25_5 C20_5 C21_5 C22_5 -0.3(15) . . . . ?
 C25_5 C24_5 C26_5 F4_5 -6.4(13) . . . . ?
 C25_5 C24_5 C26_5 F5_5 -124.5(10) . . . . ?
 C25_5 C24_5 C26_5 F6_5 116.4(10) . . . . ?
 C26_5 C24_5 C25_5 C20_5 179.9(8) . . . . ?
 F1_6 C1_6 C2_6 C3_6 -121.3(10) . . . . ?
 F1_6 C1_6 C2_6 C7_6 59.2(13) . . . . ?
 F2_6 C1_6 C2_6 C3_6 -3.0(14) . . . . ?
 F2_6 C1_6 C2_6 C7_6 177.5(10) . . . . ?
 F3_6 C1_6 C2_6 C3_6 118.2(11) . . . . ?
 F3_6 C1_6 C2_6 C7_6 -61.4(13) . . . . ?
 N1_6 C5_6 C6_6 C7_6 -170.3(15) . . . . ?
 N1_6 C8_6 C9_6 C10_6 164.7(18) . . . . ?
 N2_6 C4_6 C5_6 N1_6 -8.2(15) . . . . ?
 N2_6 C4_6 C5_6 C6_6 -177.8(13) . . . . ?
 N2_6 C8_6 C9_6 C10_6 -3(2) . . . . ?
 N2_6 C12_6 C13_6 N3_6 24(2) . . . . ?
 N2_6 C12_6 C13_6 C14_6 -154.0(12) . . . . ?
 N3_6 C13_6 C14_6 C15_6 -15.4(19) . . . . ?
 N3_6 C13_6 C14_6 C18_6 164.3(13) . . . . ?
 N3_6 C20_6 C21_6 N4_6 -2.1(13) . . . . ?
 N3_6 C20_6 C21_6 C22_6 176.5(11) . . . . ?
 N3_6 C20_6 C25_6 C24_6 -178.2(11) . . . . ?
 N4_6 C21_6 C22_6 C23_6 -176.9(13) . . . . ?
 C1_6 C2_6 C3_6 C4_6 178.5(9) . . . . ?
 C1_6 C2_6 C7_6 C6_6 179.7(12) . . . . ?
 C2_6 C3_6 C4_6 N2_6 -180.0(11) . . . . ?
 C2_6 C3_6 C4_6 C5_6 1.2(16) . . . . ?
 C3_6 C2_6 C7_6 C6_6 0(2) . . . . ?
 C3_6 C4_6 C5_6 N1_6 170.8(11) . . . . ?
 C3_6 C4_6 C5_6 C6_6 1(2) . . . . ?
 C4_6 N2_6 C8_6 N1_6 -1.1(16) . . . . ?
 C4_6 N2_6 C8_6 C9_6 168.8(13) . . . . ?
 C4_6 N2_6 C12_6 C11_6 -158.4(13) . . . . ?
 C4_6 N2_6 C12_6 C13_6 19(2) . . . . ?
 C4_6 C5_6 C6_6 C7_6 -3(2) . . . . ?
 C5_6 N1_6 C8_6 N2_6 -3.9(18) . . . . ?
 C5_6 N1_6 C8_6 C9_6 -172.5(16) . . . . ?
 C5_6 C6_6 C7_6 C2_6 2(2) . . . . ?
 C7_6 C2_6 C3_6 C4_6 -1.9(16) . . . . ?
 C8_6 N1_6 C5_6 C4_6 7.5(17) . . . . ?
 C8_6 N1_6 C5_6 C6_6 175.8(16) . . . . ?
 C8_6 N2_6 C4_6 C3_6 -173.5(12) . . . . ?
 C8_6 N2_6 C4_6 C5_6 5.5(13) . . . . ?
 C8_6 N2_6 C12_6 C11_6 24.2(18) . . . . ?
 C8_6 N2_6 C12_6 C13_6 -158.2(13) . . . . ?
 C8_6 C9_6 C10_6 C11_6 8(3) . . . . ?
 C9_6 C10_6 C11_6 C12_6 3(3) . . . . ?
 C9_6 C10_6 C11_6 C19_6 -176.0(18) . . . . ?
 C10_6 C11_6 C12_6 N2_6 -19(2) . . . . ?
 C10_6 C11_6 C12_6 C13_6 163.5(15) . . . . ?
 C10_6 C11_6 C19_6 C18_6 -176.0(19) . . . . ?
 C11_6 C12_6 C13_6 N3_6 -158.5(12) . . . . ?
 C11_6 C12_6 C13_6 C14_6 23.6(19) . . . . ?
 C12_6 N2_6 C4_6 C3_6 9(2) . . . . ?
 C12_6 N2_6 C4_6 C5_6 -172.3(12) . . . . ?
 C12_6 N2_6 C8_6 N1_6 176.9(12) . . . . ?
 C12_6 N2_6 C8_6 C9_6 -13(2) . . . . ?
 C12_6 C11_6 C19_6 C18_6 5(3) . . . . ?
 C12_6 C13_6 C14_6 C15_6 162.7(14) . . . . ?
 C12_6 C13_6 C14_6 C18_6 -17.6(19) . . . . ?
 C13_6 N3_6 C17_6 N4_6 174.1(11) . . . . ?
 C13_6 N3_6 C17_6 C16_6 -11.8(18) . . . . ?
 C13_6 N3_6 C20_6 C21_6 -175.3(11) . . . . ?
 C13_6 N3_6 C20_6 C25_6 7.7(19) . . . . ?
 C13_6 C14_6 C15_6 C16_6 4(3) . . . . ?
 C13_6 C14_6 C18_6 C19_6 6(3) . . . . ?
 C14_6 C15_6 C16_6 C17_6 4(3) . . . . ?
 C14_6 C18_6 C19_6 C11_6 1(3) . . . . ?
 C15_6 C14_6 C18_6 C19_6 -174.5(19) . . . . ?
 C15_6 C16_6 C17_6 N3_6 -1(2) . . . . ?
 C15_6 C16_6 C17_6 N4_6 172.4(16) . . . . ?
 C17_6 N3_6 C13_6 C12_6 -158.0(12) . . . . ?
 C17_6 N3_6 C13_6 C14_6 19.9(17) . . . . ?
 C17_6 N3_6 C20_6 C21_6 4.4(12) . . . . ?
 C17_6 N3_6 C20_6 C25_6 -172.5(12) . . . . ?
 C17_6 N4_6 C21_6 C20_6 -1.4(15) . . . . ?
 C17_6 N4_6 C21_6 C22_6 -179.9(14) . . . . ?
 C18_6 C14_6 C15_6 C16_6 -175.1(18) . . . . ?
 C19_6 C11_6 C12_6 N2_6 160.6(14) . . . . ?
 C19_6 C11_6 C12_6 C13_6 -17(2) . . . . ?
 C20_6 N3_6 C13_6 C12_6 22(2) . . . . ?
 C20_6 N3_6 C13_6 C14_6 -160.3(11) . . . . ?
 C20_6 N3_6 C17_6 N4_6 -5.7(14) . . . . ?
 C20_6 N3_6 C17_6 C16_6 168.4(12) . . . . ?
 C20_6 C21_6 C22_6 C23_6 5(2) . . . . ?
 C21_6 N4_6 C17_6 N3_6 4.5(16) . . . . ?
 C21_6 N4_6 C17_6 C16_6 -168.8(15) . . . . ?
 C21_6 C20_6 C25_6 C24_6 5.1(15) . . . . ?
 C21_6 C22_6 C23_6 C24_6 -3(2) . . . . ?
 C22_6 C23_6 C24_6 C25_6 2.2(19) . . . . ?
 C22_6 C23_6 C24_6 C26_6 -177.6(12) . . . . ?
 C23_6 C24_6 C25_6 C20_6 -3.2(16) . . . . ?
 C23_6 C24_6 C26_6 F4_6 173.4(10) . . . . ?
 C23_6 C24_6 C26_6 F5_6 53.4(14) . . . . ?
 C23_6 C24_6 C26_6 F6_6 -64.7(13) . . . . ?
 C25_6 C20_6 C21_6 N4_6 175.3(10) . . . . ?
 C25_6 C20_6 C21_6 C22_6 -6.1(18) . . . . ?
 C25_6 C24_6 C26_6 F4_6 -6.3(15) . . . . ?
 C25_6 C24_6 C26_6 F5_6 -126.3(11) . . . . ?
 C25_6 C24_6 C26_6 F6_6 115.6(12) . . . . ?
 C26_6 C24_6 C25_6 C20_6 176.5(9) . . . . ?
 F1_7 C1_7 C2_7 C3_7 -117.0(11) . . . . ?
 F1_7 C1_7 C2_7 C7_7 58.1(13) . . . . ?
 F2_7 C1_7 C2_7 C3_7 0.1(15) . . . . ?
 F2_7 C1_7 C2_7 C7_7 175.2(11) . . . . ?
 F3_7 C1_7 C2_7 C3_7 123.2(12) . . . . ?
 F3_7 C1_7 C2_7 C7_7 -61.7(14) . . . . ?
 N1_7 C5_7 C6_7 C7_7 -176.9(12) . . . . ?
 N1_7 C8_7 C9_7 C10_7 169.0(15) . . . . ?
 N2_7 C4_7 C5_7 N1_7 -3.6(13) . . . . ?
 N2_7 C4_7 C5_7 C6_7 174.6(10) . . . . ?
 N2_7 C8_7 C9_7 C10_7 -4(2) . . . . ?
 N2_7 C12_7 C13_7 N3_7 26.1(19) . . . . ?
 N2_7 C12_7 C13_7 C14_7 -161.0(12) . . . . ?
 N3_7 C13_7 C14_7 C15_7 -19.5(18) . . . . ?
 N3_7 C13_7 C14_7 C18_7 159.6(13) . . . . ?
 N3_7 C20_7 C21_7 N4_7 -1.0(14) . . . . ?
 N3_7 C20_7 C21_7 C22_7 177.8(12) . . . . ?
 N3_7 C20_7 C25_7 C24_7 -179.1(10) . . . . ?
 N4_7 C21_7 C22_7 C23_7 -179.5(14) . . . . ?
 C1_7 C2_7 C3_7 C4_7 176.3(9) . . . . ?
 C1_7 C2_7 C7_7 C6_7 -177.3(11) . . . . ?
 C2_7 C3_7 C4_7 N2_7 -178.3(11) . . . . ?
 C2_7 C3_7 C4_7 C5_7 3.0(15) . . . . ?
 C3_7 C2_7 C7_7 C6_7 -2.4(18) . . . . ?
 C3_7 C4_7 C5_7 N1_7 175.4(10) . . . . ?
 C3_7 C4_7 C5_7 C6_7 -6.4(16) . . . . ?
 C4_7 N2_7 C8_7 N1_7 -5.4(14) . . . . ?
 C4_7 N2_7 C8_7 C9_7 168.5(12) . . . . ?
 C4_7 N2_7 C12_7 C11_7 -155.9(12) . . . . ?
 C4_7 N2_7 C12_7 C13_7 24(2) . . . . ?
 C4_7 C5_7 C6_7 C7_7 5.2(17) . . . . ?
 C5_7 N1_7 C8_7 N2_7 3.2(14) . . . . ?
 C5_7 N1_7 C8_7 C9_7 -170.0(14) . . . . ?
 C5_7 C6_7 C7_7 C2_7 -1.1(18) . . . . ?
 C7_7 C2_7 C3_7 C4_7 1.5(16) . . . . ?
 C8_7 N1_7 C5_7 C4_7 0.3(14) . . . . ?
 C8_7 N1_7 C5_7 C6_7 -177.6(12) . . . . ?
 C8_7 N2_7 C4_7 C3_7 -173.8(11) . . . . ?
 C8_7 N2_7 C4_7 C5_7 5.1(11) . . . . ?
 C8_7 N2_7 C12_7 C11_7 19.8(17) . . . . ?
 C8_7 N2_7 C12_7 C13_7 -160.7(11) . . . . ?
 C8_7 C9_7 C10_7 C11_7 4(3) . . . . ?
 C9_7 C10_7 C11_7 C12_7 8(3) . . . . ?
 C9_7 C10_7 C11_7 C19_7 -175.4(18) . . . . ?
 C10_7 C11_7 C12_7 N2_7 -19(2) . . . . ?
 C10_7 C11_7 C12_7 C13_7 161.1(14) . . . . ?
 C10_7 C11_7 C19_7 C18_7 -169.1(18) . . . . ?
 C11_7 C12_7 C13_7 N3_7 -154.5(13) . . . . ?
 C11_7 C12_7 C13_7 C14_7 18.4(18) . . . . ?
 C12_7 N2_7 C4_7 C3_7 2(2) . . . . ?
 C12_7 N2_7 C4_7 C5_7 -178.7(11) . . . . ?
 C12_7 N2_7 C8_7 N1_7 177.9(11) . . . . ?
 C12_7 N2_7 C8_7 C9_7 -8.2(18) . . . . ?
 C12_7 C11_7 C19_7 C18_7 7(3) . . . . ?
 C12_7 C13_7 C14_7 C15_7 167.0(13) . . . . ?
 C12_7 C13_7 C14_7 C18_7 -13.9(19) . . . . ?
 C13_7 N3_7 C17_7 N4_7 171.6(12) . . . . ?
 C13_7 N3_7 C17_7 C16_7 -12.5(19) . . . . ?
 C13_7 N3_7 C20_7 C21_7 -174.6(12) . . . . ?
 C13_7 N3_7 C20_7 C25_7 12(2) . . . . ?
 C13_7 C14_7 C15_7 C16_7 5(2) . . . . ?
 C13_7 C14_7 C18_7 C19_7 6(2) . . . . ?
 C14_7 C15_7 C16_7 C17_7 6(3) . . . . ?
 C14_7 C18_7 C19_7 C11_7 -3(3) . . . . ?
 C15_7 C14_7 C18_7 C19_7 -174.6(17) . . . . ?
 C15_7 C16_7 C17_7 N3_7 -3(2) . . . . ?
 C15_7 C16_7 C17_7 N4_7 172.2(17) . . . . ?
 C17_7 N3_7 C13_7 C12_7 -162.9(12) . . . . ?
 C17_7 N3_7 C13_7 C14_7 24.3(17) . . . . ?
 C17_7 N3_7 C20_7 C21_7 5.2(12) . . . . ?
 C17_7 N3_7 C20_7 C25_7 -168.5(11) . . . . ?
 C17_7 N4_7 C21_7 C20_7 -3.9(16) . . . . ?
 C17_7 N4_7 C21_7 C22_7 177.5(15) . . . . ?
 C18_7 C14_7 C15_7 C16_7 -173.8(17) . . . . ?
 C19_7 C11_7 C12_7 N2_7 164.1(14) . . . . ?
 C19_7 C11_7 C12_7 C13_7 -15(2) . . . . ?
 C20_7 N3_7 C13_7 C12_7 17(2) . . . . ?
 C20_7 N3_7 C13_7 C14_7 -156.0(12) . . . . ?
 C20_7 N3_7 C17_7 N4_7 -8.2(15) . . . . ?
 C20_7 N3_7 C17_7 C16_7 167.7(12) . . . . ?
 C20_7 C21_7 C22_7 C23_7 2(2) . . . . ?
 C21_7 N4_7 C17_7 N3_7 7.6(17) . . . . ?
 C21_7 N4_7 C17_7 C16_7 -167.5(16) . . . . ?
 C21_7 C20_7 C25_7 C24_7 8.0(15) . . . . ?
 C21_7 C22_7 C23_7 C24_7 3(2) . . . . ?
 C22_7 C23_7 C24_7 C25_7 -2.5(19) . . . . ?
 C22_7 C23_7 C24_7 C26_7 -179.7(12) . . . . ?
 C23_7 C24_7 C25_7 C20_7 -2.9(15) . . . . ?
 C23_7 C24_7 C26_7 F4_7 177.9(10) . . . . ?
 C23_7 C24_7 C26_7 F5_7 62.0(12) . . . . ?
 C23_7 C24_7 C26_7 F6_7 -59.8(13) . . . . ?
 C25_7 C20_7 C21_7 N4_7 173.5(11) . . . . ?
 C25_7 C20_7 C21_7 C22_7 -7.7(18) . . . . ?
 C25_7 C24_7 C26_7 F4_7 0.6(13) . . . . ?
 C25_7 C24_7 C26_7 F5_7 -115.4(10) . . . . ?
 C25_7 C24_7 C26_7 F6_7 122.8(11) . . . . ?
 C26_7 C24_7 C25_7 C20_7 174.3(9) . . . . ?
 F1_8 C1_8 C2_8 C3_8 -111.9(10) . . . . ?
 F1_8 C1_8 C2_8 C7_8 63.2(13) . . . . ?
 F2_8 C1_8 C2_8 C3_8 2.9(14) . . . . ?
 F2_8 C1_8 C2_8 C7_8 177.9(11) . . . . ?
 F3_8 C1_8 C2_8 C3_8 128.0(11) . . . . ?
 F3_8 C1_8 C2_8 C7_8 -56.9(14) . . . . ?
 N1_8 C5_8 C6_8 C7_8 -171.7(15) . . . . ?
 N1_8 C8_8 C9_8 C10_8 162(2) . . . . ?
 N2_8 C4_8 C5_8 N1_8 -11.3(14) . . . . ?
 N2_8 C4_8 C5_8 C6_8 178.8(12) . . . . ?
 N2_8 C8_8 C9_8 C10_8 -4(3) . . . . ?
 N2_8 C12_8 C13_8 N3_8 21(2) . . . . ?
 N2_8 C12_8 C13_8 C14_8 -158.6(12) . . . . ?
 N3_8 C13_8 C14_8 C15_8 -15.8(16) . . . . ?
 N3_8 C13_8 C14_8 C18_8 164.8(11) . . . . ?
 N3_8 C20_8 C21_8 N4_8 -2.8(11) . . . . ?
 N3_8 C20_8 C21_8 C22_8 177.2(9) . . . . ?
 N3_8 C20_8 C25_8 C24_8 -178.5(9) . . . . ?
 N4_8 C21_8 C22_8 C23_8 -176.7(11) . . . . ?
 C1_8 C2_8 C3_8 C4_8 177.0(9) . . . . ?
 C1_8 C2_8 C7_8 C6_8 -178.7(12) . . . . ?
 C2_8 C3_8 C4_8 N2_8 -176.8(11) . . . . ?
 C2_8 C3_8 C4_8 C5_8 -1.5(15) . . . . ?
 C3_8 C2_8 C7_8 C6_8 -4(2) . . . . ?
 C3_8 C4_8 C5_8 N1_8 172.3(11) . . . . ?
 C3_8 C4_8 C5_8 C6_8 2.4(18) . . . . ?
 C4_8 N2_8 C8_8 N1_8 -0.9(17) . . . . ?
 C4_8 N2_8 C8_8 C9_8 167.0(14) . . . . ?
 C4_8 N2_8 C12_8 C11_8 -155.7(12) . . . . ?
 C4_8 N2_8 C12_8 C13_8 25(2) . . . . ?
 C4_8 C5_8 C6_8 C7_8 -4(2) . . . . ?
 C5_8 N1_8 C8_8 N2_8 -6.0(19) . . . . ?
 C5_8 N1_8 C8_8 C9_8 -172.3(17) . . . . ?
 C5_8 C6_8 C7_8 C2_8 5(2) . . . . ?
 C7_8 C2_8 C3_8 C4_8 2.1(16) . . . . ?
 C8_8 N1_8 C5_8 C4_8 10.8(17) . . . . ?
 C8_8 N1_8 C5_8 C6_8 179.3(16) . . . . ?
 C8_8 N2_8 C4_8 C3_8 -177.0(12) . . . . ?
 C8_8 N2_8 C4_8 C5_8 7.1(13) . . . . ?
 C8_8 N2_8 C12_8 C11_8 25.4(19) . . . . ?
 C8_8 N2_8 C12_8 C13_8 -154.2(13) . . . . ?
 C8_8 C9_8 C10_8 C11_8 9(3) . . . . ?
 C9_8 C10_8 C11_8 C12_8 3(3) . . . . ?
 C9_8 C10_8 C11_8 C19_8 179(2) . . . . ?
 C10_8 C11_8 C12_8 N2_8 -19(2) . . . . ?
 C10_8 C11_8 C12_8 C13_8 160.1(15) . . . . ?
 C10_8 C11_8 C19_8 C18_8 -172.0(18) . . . . ?
 C11_8 C12_8 C13_8 N3_8 -158.3(12) . . . . ?
 C11_8 C12_8 C13_8 C14_8 21.8(18) . . . . ?
 C12_8 N2_8 C4_8 C3_8 4(2) . . . . ?
 C12_8 N2_8 C4_8 C5_8 -172.0(12) . . . . ?
 C12_8 N2_8 C8_8 N1_8 178.3(13) . . . . ?
 C12_8 N2_8 C8_8 C9_8 -14(2) . . . . ?
 C12_8 C11_8 C19_8 C18_8 5(3) . . . . ?
 C12_8 C13_8 C14_8 C15_8 164.1(12) . . . . ?
 C12_8 C13_8 C14_8 C18_8 -15.3(18) . . . . ?
 C13_8 N3_8 C17_8 N4_8 177.0(9) . . . . ?
 C13_8 N3_8 C17_8 C16_8 -12.4(15) . . . . ?
 C13_8 N3_8 C20_8 C21_8 -177.3(10) . . . . ?
 C13_8 N3_8 C20_8 C25_8 5.1(17) . . . . ?
 C13_8 C14_8 C15_8 C16_8 2(2) . . . . ?
 C13_8 C14_8 C18_8 C19_8 4(2) . . . . ?
 C14_8 C15_8 C16_8 C17_8 7(2) . . . . ?
 C14_8 C18_8 C19_8 C11_8 2(3) . . . . ?
 C15_8 C14_8 C18_8 C19_8 -175.6(16) . . . . ?
 C15_8 C16_8 C17_8 N3_8 -2.2(18) . . . . ?
 C15_8 C16_8 C17_8 N4_8 166.9(13) . . . . ?
 C17_8 N3_8 C13_8 C12_8 -158.4(11) . . . . ?
 C17_8 N3_8 C13_8 C14_8 21.5(14) . . . . ?
 C17_8 N3_8 C20_8 C21_8 4.0(10) . . . . ?
 C17_8 N3_8 C20_8 C25_8 -173.6(10) . . . . ?
 C17_8 N4_8 C21_8 C20_8 0.3(12) . . . . ?
 C17_8 N4_8 C21_8 C22_8 -179.7(11) . . . . ?
 C18_8 C14_8 C15_8 C16_8 -178.5(14) . . . . ?
 C19_8 C11_8 C12_8 N2_8 163.7(14) . . . . ?
 C19_8 C11_8 C12_8 C13_8 -17(2) . . . . ?
 C20_8 N3_8 C13_8 C12_8 23.1(18) . . . . ?
 C20_8 N3_8 C13_8 C14_8 -157.0(10) . . . . ?
 C20_8 N3_8 C17_8 N4_8 -4.2(12) . . . . ?
 C20_8 N3_8 C17_8 C16_8 166.5(10) . . . . ?
 C20_8 C21_8 C22_8 C23_8 3.3(15) . . . . ?
 C21_8 N4_8 C17_8 N3_8 2.4(12) . . . . ?
 C21_8 N4_8 C17_8 C16_8 -167.0(11) . . . . ?
 C21_8 C20_8 C25_8 C24_8 4.3(13) . . . . ?
 C21_8 C22_8 C23_8 C24_8 -1.3(16) . . . . ?
 C22_8 C23_8 C24_8 C25_8 0.8(15) . . . . ?
 C22_8 C23_8 C24_8 C26_8 -175.9(9) . . . . ?
 C23_8 C24_8 C25_8 C20_8 -2.2(14) . . . . ?
 C23_8 C24_8 C26_8 F4_8 174.2(9) . . . . ?
 C23_8 C24_8 C26_8 F5_8 54.4(12) . . . . ?
 C23_8 C24_8 C26_8 F6_8 -66.7(12) . . . . ?
 C25_8 C20_8 C21_8 N4_8 175.0(9) . . . . ?
 C25_8 C20_8 C21_8 C22_8 -5.0(14) . . . . ?
 C25_8 C24_8 C26_8 F4_8 -2.5(13) . . . . ?
 C25_8 C24_8 C26_8 F5_8 -122.3(10) . . . . ?
 C25_8 C24_8 C26_8 F6_8 116.6(10) . . . . ?
 C26_8 C24_8 C25_8 C20_8 174.4(8) . . . . ?
 F1_9 C1_9 C2_9 C3_9 -10.6(14) . . . . ?
 F1_9 C1_9 C2_9 C7_9 167.7(11) . . . . ?
 F2_9 C1_9 C2_9 C3_9 -126.0(11) . . . . ?
 F2_9 C1_9 C2_9 C7_9 52.4(14) . . . . ?
 F3_9 C1_9 C2_9 C3_9 112.0(12) . . . . ?
 F3_9 C1_9 C2_9 C7_9 -69.6(14) . . . . ?
 N1_9 C5_9 C6_9 C7_9 -177.0(14) . . . . ?
 N1_9 C8_9 C9_9 C10_9 167.0(17) . . . . ?
 N2_9 C4_9 C5_9 N1_9 -6.5(14) . . . . ?
 N2_9 C4_9 C5_9 C6_9 178.6(12) . . . . ?
 N2_9 C8_9 C9_9 C10_9 -6(2) . . . . ?
 N2_9 C12_9 C13_9 N3_9 20.4(17) . . . . ?
 N2_9 C12_9 C13_9 C14_9 -159.2(11) . . . . ?
 N3_9 C13_9 C14_9 C15_9 -16.2(16) . . . . ?
 N3_9 C13_9 C14_9 C18_9 164.7(10) . . . . ?
 N3_9 C20_9 C21_9 N4_9 -0.1(13) . . . . ?
 N3_9 C20_9 C21_9 C22_9 179.7(11) . . . . ?
 N3_9 C20_9 C25_9 C24_9 179.6(10) . . . . ?
 N4_9 C21_9 C22_9 C23_9 179.3(13) . . . . ?
 C1_9 C2_9 C3_9 C4_9 176.9(10) . . . . ?
 C1_9 C2_9 C7_9 C6_9 -179.5(12) . . . . ?
 C2_9 C3_9 C4_9 N2_9 -175.8(11) . . . . ?
 C2_9 C3_9 C4_9 C5_9 1.7(16) . . . . ?
 C3_9 C2_9 C7_9 C6_9 -1(2) . . . . ?
 C3_9 C4_9 C5_9 N1_9 175.5(11) . . . . ?
 C3_9 C4_9 C5_9 C6_9 0.6(18) . . . . ?
 C4_9 N2_9 C8_9 N1_9 -6.0(15) . . . . ?
 C4_9 N2_9 C8_9 C9_9 168.3(13) . . . . ?
 C4_9 N2_9 C12_9 C11_9 -156.3(12) . . . . ?
 C4_9 N2_9 C12_9 C13_9 25.1(19) . . . . ?
 C4_9 C5_9 C6_9 C7_9 -3(2) . . . . ?
 C5_9 N1_9 C8_9 N2_9 2.0(17) . . . . ?
 C5_9 N1_9 C8_9 C9_9 -171.4(16) . . . . ?
 C5_9 C6_9 C7_9 C2_9 3(2) . . . . ?
 C7_9 C2_9 C3_9 C4_9 -1.4(16) . . . . ?
 C8_9 N1_9 C5_9 C4_9 2.9(16) . . . . ?
 C8_9 N1_9 C5_9 C6_9 177.1(15) . . . . ?
 C8_9 N2_9 C4_9 C3_9 -175.0(12) . . . . ?
 C8_9 N2_9 C4_9 C5_9 7.2(13) . . . . ?
 C8_9 N2_9 C12_9 C11_9 20.8(17) . . . . ?
 C8_9 N2_9 C12_9 C13_9 -157.8(12) . . . . ?
 C8_9 C9_9 C10_9 C11_9 10(3) . . . . ?
 C9_9 C10_9 C11_9 C12_9 2(3) . . . . ?
 C9_9 C10_9 C11_9 C19_9 177.1(17) . . . . ?
 C10_9 C11_9 C12_9 N2_9 -16.6(19) . . . . ?
 C10_9 C11_9 C12_9 C13_9 162.1(13) . . . . ?
 C10_9 C11_9 C19_9 C18_9 -177.4(15) . . . . ?
 C11_9 C12_9 C13_9 N3_9 -158.2(11) . . . . ?
 C11_9 C12_9 C13_9 C14_9 22.2(16) . . . . ?
 C12_9 N2_9 C4_9 C3_9 2(2) . . . . ?
 C12_9 N2_9 C4_9 C5_9 -175.3(11) . . . . ?
 C12_9 N2_9 C8_9 N1_9 176.2(11) . . . . ?
 C12_9 N2_9 C8_9 C9_9 -9(2) . . . . ?
 C12_9 C11_9 C19_9 C18_9 -2(2) . . . . ?
 C12_9 C13_9 C14_9 C15_9 163.4(11) . . . . ?
 C12_9 C13_9 C14_9 C18_9 -15.7(17) . . . . ?
 C13_9 N3_9 C17_9 N4_9 179.4(10) . . . . ?
 C13_9 N3_9 C17_9 C16_9 -9.3(17) . . . . ?
 C13_9 N3_9 C20_9 C21_9 178.2(10) . . . . ?
 C13_9 N3_9 C20_9 C25_9 5.6(18) . . . . ?
 C13_9 C14_9 C15_9 C16_9 3(2) . . . . ?
 C13_9 C14_9 C18_9 C19_9 0(2) . . . . ?
 C14_9 C15_9 C16_9 C17_9 7(2) . . . . ?
 C14_9 C18_9 C19_9 C11_9 9(2) . . . . ?
 C15_9 C14_9 C18_9 C19_9 -178.7(14) . . . . ?
 C15_9 C16_9 C17_9 N3_9 -5(2) . . . . ?
 C15_9 C16_9 C17_9 N4_9 165.2(15) . . . . ?
 C17_9 N3_9 C13_9 C12_9 -159.8(11) . . . . ?
 C17_9 N3_9 C13_9 C14_9 19.8(15) . . . . ?
 C17_9 N3_9 C20_9 C21_9 2.4(11) . . . . ?
 C17_9 N3_9 C20_9 C25_9 -170.2(11) . . . . ?
 C17_9 N4_9 C21_9 C20_9 -2.5(15) . . . . ?
 C17_9 N4_9 C21_9 C22_9 177.8(14) . . . . ?
 C18_9 C14_9 C15_9 C16_9 -177.9(14) . . . . ?
 C19_9 C11_9 C12_9 N2_9 167.8(12) . . . . ?
 C19_9 C11_9 C12_9 C13_9 -13.5(19) . . . . ?
 C20_9 N3_9 C13_9 C12_9 25.0(17) . . . . ?
 C20_9 N3_9 C13_9 C14_9 -155.4(10) . . . . ?
 C20_9 N3_9 C17_9 N4_9 -4.2(14) . . . . ?
 C20_9 N3_9 C17_9 C16_9 167.1(11) . . . . ?
 C20_9 C21_9 C22_9 C23_9 0(2) . . . . ?
 C21_9 N4_9 C17_9 N3_9 4.2(16) . . . . ?
 C21_9 N4_9 C17_9 C16_9 -166.0(14) . . . . ?
 C21_9 C20_9 C25_9 C24_9 8.0(14) . . . . ?
 C21_9 C22_9 C23_9 C24_9 5.9(19) . . . . ?
 C22_9 C23_9 C24_9 C25_9 -4.5(17) . . . . ?
 C22_9 C23_9 C24_9 C26_9 176.1(11) . . . . ?
 C23_9 C24_9 C25_9 C20_9 -2.5(14) . . . . ?
 C23_9 C24_9 C26_9 F4_9 177.2(9) . . . . ?
 C23_9 C24_9 C26_9 F5_9 59.2(12) . . . . ?
 C23_9 C24_9 C26_9 F6_9 -61.6(12) . . . . ?
 C25_9 C20_9 C21_9 N4_9 173.5(10) . . . . ?
 C25_9 C20_9 C21_9 C22_9 -6.7(17) . . . . ?
 C25_9 C24_9 C26_9 F4_9 -2.2(13) . . . . ?
 C25_9 C24_9 C26_9 F5_9 -120.2(10) . . . . ?
 C25_9 C24_9 C26_9 F6_9 118.9(10) . . . . ?
 C26_9 C24_9 C25_9 C20_9 176.9(8) . . . . ?

_olex2_submission_special_instructions  'No special instructions were received'
_site                              XU
_vrf_PLAT340_cu_ch_szw_1_1230_0m
;
PROBLEM: Low Bond Precision on  C-C Bonds ...............    0.01534 Ang.
RESPONSE: Due to weak diffraction of the sample.
;
