data_a1
_audit_creation_date               2026-01-08
_audit_creation_method
;
Olex2 1.5
(compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817)
;
_shelx_SHELXL_version_number       '2025/1'
_audit_contact_author_address      ?
_audit_contact_author_email        ?
_audit_contact_author_name         ''
_audit_contact_author_phone        ?
_publ_contact_author_id_orcid      ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_chemical_name_common              ?
_chemical_name_systematic          ?
_chemical_formula_moiety           'C26 H12 F6 N4'
_chemical_formula_sum              'C26 H12 F6 N4'
_chemical_formula_weight           494.40
_chemical_absolute_configuration   ?
_chemical_melting_point            ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'F' 'F' 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N' 'N' 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system        'trigonal'
_space_group_IT_number             145
_space_group_name_H-M_alt          'P 32'
_space_group_name_Hall             'P 32'
loop_
  _space_group_symop_operation_xyz
 'x, y, z'
 '-y, x-y, z+2/3'
 '-x+y, -x, z+1/3'

_cell_length_a                     32.2229(6)
_cell_length_b                     32.2229(6)
_cell_length_c                     15.7246(4)
_cell_angle_alpha                  90
_cell_angle_beta                   90
_cell_angle_gamma                  120
_cell_volume                       14139.7(6)
_cell_formula_units_Z              27
_cell_measurement_reflns_used      9983
_cell_measurement_temperature      193.00
_cell_measurement_theta_max        60.36
_cell_measurement_theta_min        3.23
_shelx_estimated_absorpt_T_max     0.904
_shelx_estimated_absorpt_T_min     0.865
_exptl_absorpt_coefficient_mu      1.151
_exptl_absorpt_correction_T_max    0.7479
_exptl_absorpt_correction_T_min    0.6863
_exptl_absorpt_correction_type     none
_exptl_absorpt_process_details
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1442 before and 0.0884 after correction.
The Ratio of minimum to maximum transmission is 0.9176.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details     ?
_exptl_crystal_colour              ?
_exptl_crystal_density_diffrn      1.568
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      ?
_exptl_crystal_description         block
_exptl_crystal_F_000               6750
_exptl_crystal_size_max            0.13
_exptl_crystal_size_mid            0.11
_exptl_crystal_size_min            0.09
_exptl_transmission_factor_max     ?
_exptl_transmission_factor_min     ?
_diffrn_reflns_av_R_equivalents    0.1648
_diffrn_reflns_av_unetI/netI       0.0653
_diffrn_reflns_Laue_measured_fraction_full  1.000
_diffrn_reflns_Laue_measured_fraction_max  1.000
_diffrn_reflns_limit_h_max         38
_diffrn_reflns_limit_h_min         -38
_diffrn_reflns_limit_k_max         38
_diffrn_reflns_limit_k_min         -38
_diffrn_reflns_limit_l_max         18
_diffrn_reflns_limit_l_min         -15
_diffrn_reflns_number              313697
_diffrn_reflns_point_group_measured_fraction_full  0.945
_diffrn_reflns_point_group_measured_fraction_max  0.945
_diffrn_reflns_theta_full          66.580
_diffrn_reflns_theta_max           66.580
_diffrn_reflns_theta_min           2.742
_diffrn_ambient_temperature        193.00
_diffrn_detector_area_resol_mean   7.41
_diffrn_detector_type              'Bruker PHOTON III-M14'
_diffrn_measured_fraction_theta_full  1.000
_diffrn_measured_fraction_theta_max  1.000
_diffrn_measurement_device         'three circle diffractometer'
_diffrn_measurement_device_type    'Bruker APEX-II CCD'
_diffrn_measurement_method         'φ and ω scans'
_diffrn_measurement_specimen_support  'nylon loop'
_diffrn_radiation_type             CuK\a
_diffrn_radiation_wavelength       1.54178
_diffrn_source                     ?
_diffrn_source_current             1.1
_diffrn_source_power               0.05500000000000001
_diffrn_source_voltage             50.0
_diffrn_standards_number           0
_reflns_Friedel_coverage           0.891
_reflns_Friedel_fraction_full      0.890
_reflns_Friedel_fraction_max       0.890
_reflns_number_gt                  24024
_reflns_number_total               31464
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression       'I > 2σ(I)'
_computing_cell_refinement         'SAINT V8.41 (?, 2016)'
_computing_data_collection         'APEX6 V2024.9-1 (Bruker, 2025)'
_computing_data_reduction          'SAINT V8.41 (?, 2016)'
_computing_molecular_graphics      'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement    'SHELXL 2025/1 (Sheldrick, 2015)'
_computing_structure_solution      'SHELXD  (Sheldrick, 2008)'
_refine_diff_density_max           0.883
_refine_diff_density_min           -0.699
_refine_diff_density_rms           0.201
_refine_ls_abs_structure_details
;
 Flack x determined using 7533 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack     0.09(6)
_refine_ls_extinction_coef         0.00098(10)
_refine_ls_extinction_expression  
 'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^'
_refine_ls_extinction_method       'SHELXL-2025/1 (Sheldrick 2025)'
_refine_ls_goodness_of_fit_ref     1.073
_refine_ls_hydrogen_treatment      constr
_refine_ls_matrix_type             full
_refine_ls_number_parameters       2918
_refine_ls_number_reflns           31464
_refine_ls_number_restraints       6229
_refine_ls_R_factor_all            0.1591
_refine_ls_R_factor_gt             0.1364
_refine_ls_restrained_S_all        1.078
_refine_ls_shift/su_max            0.005
_refine_ls_shift/su_mean           0.001
_refine_ls_structure_factor_coef   Fsqd
_refine_ls_weighting_details      
 'w=1/[σ²(Fo²)+(0.1263P)²+72.6649P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme        calc
_refine_ls_wR_factor_gt            0.3320
_refine_ls_wR_factor_ref           0.3490
_refine_special_details            ?
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2. Uiso/Uaniso restraints and constraints
F1_1 \\sim F2_1 \\sim F3_1 \\sim F4_1 \\sim F5_1 \\sim F6_1 \\sim N1_1 \\sim
N2_1 \\sim N3_1 \\sim N4_1 \\sim C1_1 \\sim C2_1 \\sim C3_1 \\sim C4_1 \\sim
C5_1 \\sim C6_1 \\sim C7_1 \\sim C8_1 \\sim C9_1 \\sim C10_1 \\sim C11_1 \\sim
C12_1 \\sim C13_1 \\sim C14_1 \\sim C15_1 \\sim C16_1 \\sim C17_1 \\sim C18_1
\\sim C19_1 \\sim C20_1 \\sim C21_1 \\sim C22_1 \\sim C23_1 \\sim C24_1 \\sim
C25_1 \\sim C26_1 \\sim F1_2 \\sim F2_2 \\sim F3_2 \\sim F4_2 \\sim F5_2 \\sim
F6_2 \\sim N1_2 \\sim N2_2 \\sim N3_2 \\sim N4_2 \\sim C1_2 \\sim C2_2 \\sim
C3_2 \\sim C4_2 \\sim C5_2 \\sim C6_2 \\sim C7_2 \\sim C8_2 \\sim C9_2 \\sim
C10_2 \\sim C11_2 \\sim C12_2 \\sim C13_2 \\sim C14_2 \\sim C15_2 \\sim C16_2
\\sim C17_2 \\sim C18_2 \\sim C19_2 \\sim C20_2 \\sim C21_2 \\sim C22_2 \\sim
C23_2 \\sim C24_2 \\sim C25_2 \\sim C26_2 \\sim F1_3 \\sim F2_3 \\sim F3_3
\\sim F4_3 \\sim F5_3 \\sim F6_3 \\sim N1_3 \\sim N2_3 \\sim N3_3 \\sim N4_3
\\sim C1_3 \\sim C2_3 \\sim C3_3 \\sim C4_3 \\sim C5_3 \\sim C6_3 \\sim C7_3
\\sim C8_3 \\sim C9_3 \\sim C10_3 \\sim C11_3 \\sim C12_3 \\sim C13_3 \\sim
C14_3 \\sim C15_3 \\sim C16_3 \\sim C17_3 \\sim C18_3 \\sim C19_3 \\sim C20_3
\\sim C21_3 \\sim C22_3 \\sim C23_3 \\sim C24_3 \\sim C25_3 \\sim C26_3 \\sim
F1_4 \\sim F2_4 \\sim F3_4 \\sim F4_4 \\sim F5_4 \\sim F6_4 \\sim N1_4 \\sim
N2_4 \\sim N3_4 \\sim N4_4 \\sim C1_4 \\sim C2_4 \\sim C3_4 \\sim C4_4 \\sim
C5_4 \\sim C6_4 \\sim C7_4 \\sim C8_4 \\sim C9_4 \\sim C10_4 \\sim C11_4 \\sim
C12_4 \\sim C13_4 \\sim C14_4 \\sim C15_4 \\sim C16_4 \\sim C17_4 \\sim C18_4
\\sim C19_4 \\sim C20_4 \\sim C21_4 \\sim C22_4 \\sim C23_4 \\sim C24_4 \\sim
C25_4 \\sim C26_4 \\sim F1_5 \\sim F2_5 \\sim F3_5 \\sim F4_5 \\sim F5_5 \\sim
F6_5 \\sim N1_5 \\sim N2_5 \\sim N3_5 \\sim N4_5 \\sim C1_5 \\sim C2_5 \\sim
C3_5 \\sim C4_5 \\sim C5_5 \\sim C6_5 \\sim C7_5 \\sim C8_5 \\sim C9_5 \\sim
C10_5 \\sim C11_5 \\sim C12_5 \\sim C13_5 \\sim C14_5 \\sim C15_5 \\sim C16_5
\\sim C17_5 \\sim C18_5 \\sim C19_5 \\sim C20_5 \\sim C21_5 \\sim C22_5 \\sim
C23_5 \\sim C24_5 \\sim C25_5 \\sim C26_5 \\sim F1_6 \\sim F2_6 \\sim F3_6
\\sim F4_6 \\sim F5_6 \\sim F6_6 \\sim N1_6 \\sim N2_6 \\sim N3_6 \\sim N4_6
\\sim C1_6 \\sim C2_6 \\sim C3_6 \\sim C4_6 \\sim C5_6 \\sim C6_6 \\sim C7_6
\\sim C8_6 \\sim C9_6 \\sim C10_6 \\sim C11_6 \\sim C12_6 \\sim C13_6 \\sim
C14_6 \\sim C15_6 \\sim C16_6 \\sim C17_6 \\sim C18_6 \\sim C19_6 \\sim C20_6
\\sim C21_6 \\sim C22_6 \\sim C23_6 \\sim C24_6 \\sim C25_6 \\sim C26_6 \\sim
F1_7 \\sim F2_7 \\sim F3_7 \\sim F4_7 \\sim F5_7 \\sim F6_7 \\sim N1_7 \\sim
N2_7 \\sim N3_7 \\sim N4_7 \\sim C1_7 \\sim C2_7 \\sim C3_7 \\sim C4_7 \\sim
C5_7 \\sim C6_7 \\sim C7_7 \\sim C8_7 \\sim C9_7 \\sim C10_7 \\sim C11_7 \\sim
C12_7 \\sim C13_7 \\sim C14_7 \\sim C15_7 \\sim C16_7 \\sim C17_7 \\sim C18_7
\\sim C19_7 \\sim C20_7 \\sim C21_7 \\sim C22_7 \\sim C23_7 \\sim C24_7 \\sim
C25_7 \\sim C26_7 \\sim F1_8 \\sim F2_8 \\sim F3_8 \\sim F4_8 \\sim F5_8 \\sim
F6_8 \\sim N1_8 \\sim N2_8 \\sim N3_8 \\sim N4_8 \\sim C1_8 \\sim C2_8 \\sim
C3_8 \\sim C4_8 \\sim C5_8 \\sim C6_8 \\sim C7_8 \\sim C8_8 \\sim C9_8 \\sim
C10_8 \\sim C11_8 \\sim C12_8 \\sim C13_8 \\sim C14_8 \\sim C15_8 \\sim C16_8
\\sim C17_8 \\sim C18_8 \\sim C19_8 \\sim C20_8 \\sim C21_8 \\sim C22_8 \\sim
C23_8 \\sim C24_8 \\sim C25_8 \\sim C26_8 \\sim F1_9 \\sim F2_9 \\sim F3_9
\\sim F4_9 \\sim F5_9 \\sim F6_9 \\sim N1_9 \\sim N2_9 \\sim N3_9 \\sim N4_9
\\sim C1_9 \\sim C2_9 \\sim C3_9 \\sim C4_9 \\sim C5_9 \\sim C6_9 \\sim C7_9
\\sim C8_9 \\sim C9_9 \\sim C10_9 \\sim C11_9 \\sim C12_9 \\sim C13_9 \\sim
C14_9 \\sim C15_9 \\sim C16_9 \\sim C17_9 \\sim C18_9 \\sim C19_9 \\sim C20_9
\\sim C21_9 \\sim C22_9 \\sim C23_9 \\sim C24_9 \\sim C25_9 \\sim C26_9: within
2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
3. Same fragment restrains
{F1_2, F2_2, F3_2, F4_2, F5_2, F6_2, N1_2, N2_2, N3_2, N4_2, C1_2, C2_2, C3_2,
C4_2, C5_2, C6_2, C7_2, C8_2, C9_2, C10_2, C11_2, C12_2, C13_2, C14_2, C15_2,
C16_2, C17_2, C18_2, C19_2, C20_2, C21_2, C22_2, C23_2, C24_2, C25_2, C26_2}
{F1_3, F2_3, F3_3, F4_3, F5_3, F6_3, N1_3, N2_3, N3_3, N4_3, C1_3, C2_3, C3_3,
C4_3, C5_3, C6_3, C7_3, C8_3, C9_3, C10_3, C11_3, C12_3, C13_3, C14_3, C15_3,
C16_3, C17_3, C18_3, C19_3, C20_3, C21_3, C22_3, C23_3, C24_3, C25_3, C26_3}
{F1_4, F2_4, F3_4, F4_4, F5_4, F6_4, N1_4, N2_4, N3_4, N4_4, C1_4, C2_4, C3_4,
C4_4, C5_4, C6_4, C7_4, C8_4, C9_4, C10_4, C11_4, C12_4, C13_4, C14_4, C15_4,
C16_4, C17_4, C18_4, C19_4, C20_4, C21_4, C22_4, C23_4, C24_4, C25_4, C26_4}
{F1_5, F2_5, F3_5, F4_5, F5_5, F6_5, N1_5, N2_5, N3_5, N4_5, C1_5, C2_5, C3_5,
C4_5, C5_5, C6_5, C7_5, C8_5, C9_5, C10_5, C11_5, C12_5, C13_5, C14_5, C15_5,
C16_5, C17_5, C18_5, C19_5, C20_5, C21_5, C22_5, C23_5, C24_5, C25_5, C26_5}
{F1_6, F2_6, F3_6, F4_6, F5_6, F6_6, N1_6, N2_6, N3_6, N4_6, C1_6, C2_6, C3_6,
C4_6, C5_6, C6_6, C7_6, C8_6, C9_6, C10_6, C11_6, C12_6, C13_6, C14_6, C15_6,
C16_6, C17_6, C18_6, C19_6, C20_6, C21_6, C22_6, C23_6, C24_6, C25_6, C26_6}
{F1_7, F2_7, F3_7, F4_7, F5_7, F6_7, N1_7, N2_7, N3_7, N4_7, C1_7, C2_7, C3_7,
C4_7, C5_7, C6_7, C7_7, C8_7, C9_7, C10_7, C11_7, C12_7, C13_7, C14_7, C15_7,
C16_7, C17_7, C18_7, C19_7, C20_7, C21_7, C22_7, C23_7, C24_7, C25_7, C26_7}
{F1_8, F2_8, F3_8, F4_8, F5_8, F6_8, N1_8, N2_8, N3_8, N4_8, C1_8, C2_8, C3_8,
C4_8, C5_8, C6_8, C7_8, C8_8, C9_8, C10_8, C11_8, C12_8, C13_8, C14_8, C15_8,
C16_8, C17_8, C18_8, C19_8, C20_8, C21_8, C22_8, C23_8, C24_8, C25_8, C26_8}
{F1_9, F2_9, F3_9, F4_9, F5_9, F6_9, N1_9, N2_9, N3_9, N4_9, C1_9, C2_9, C3_9,
C4_9, C5_9, C6_9, C7_9, C8_9, C9_9, C10_9, C11_9, C12_9, C13_9, C14_9, C15_9,
C16_9, C17_9, C18_9, C19_9, C20_9, C21_9, C22_9, C23_9, C24_9, C25_9, C26_9}
as
{F1_1, F2_1, F3_1, F4_1, F5_1, F6_1, N1_1, N2_1, N3_1, N4_1, C1_1, C2_1, C3_1,
C4_1, C5_1, C6_1, C7_1, C8_1, C9_1, C10_1, C11_1, C12_1, C13_1, C14_1, C15_1,
C16_1, C17_1, C18_1, C19_1, C20_1, C21_1, C22_1, C23_1, C24_1, C25_1, C26_1}
sigma for 1-2: 0.01 1-3: 0.02
4.a Aromatic/amide H refined with riding coordinates:
 C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C12(H12), C13(H13), C15(H15),
 C16(H16), C21(H21), C22(H22), C24(H24), C3(H3), C6(H6), C7(H7), C9(H9),
 C10(H10), C12(H12), C13(H13), C15(H15), C16(H16), C21(H21), C22(H22), C24(H24),
  C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C12(H12), C13(H13), C15(H15),
 C16(H16), C21(H21), C22(H22), C24(H24), C3(H3), C6(H6), C7(H7), C9(H9),
 C10(H10), C12(H12), C13(H13), C15(H15), C16(H16), C21(H21), C22(H22), C24(H24),
  C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C12(H12), C13(H13), C15(H15),
 C16(H16), C21(H21), C22(H22), C24(H24), C3(H3), C6(H6), C7(H7), C9(H9),
 C10(H10), C12(H12), C13(H13), C15(H15), C16(H16), C21(H21), C22(H22), C24(H24),
  C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C12(H12), C13(H13), C15(H15),
 C16(H16), C21(H21), C22(H22), C24(H24), C3(H3), C6(H6), C7(H7), C9(H9),
 C10(H10), C12(H12), C13(H13), C15(H15), C16(H16), C21(H21), C22(H22), C24(H24),
  C3(H3), C6(H6), C7(H7), C9(H9), C10(H10), C12(H12), C13(H13), C15(H15),
 C16(H16), C21(H21), C22(H22), C24(H24)
;
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary       ?
_atom_sites_solution_secondary     ?
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 F1_1 F 1.1804(6) 0.7941(6) 0.4108(7) 0.148(6) Uani 1 1 d D U . . .
 F2_1 F 1.2139(4) 0.8448(3) 0.5107(10) 0.125(5) Uani 1 1 d D U . . .
 F3_1 F 1.1739(4) 0.7716(3) 0.5403(6) 0.078(3) Uani 1 1 d D U . . .
 F4_1 F 1.0249(3) 0.7026(3) 0.7069(6) 0.063(2) Uani 1 1 d D U . . .
 F5_1 F 1.0143(3) 0.7294(3) 0.8224(5) 0.071(3) Uani 1 1 d D U . . .
 F6_1 F 1.0028(2) 0.7545(3) 0.7063(6) 0.059(2) Uani 1 1 d D U . . .
 N1_1 N 1.0118(3) 0.8240(4) 0.5304(8) 0.063(3) Uani 1 1 d D U . . .
 N2_1 N 1.0814(3) 0.8839(3) 0.5844(6) 0.036(2) Uani 1 1 d D U . . .
 N3_1 N 1.2250(3) 0.8876(3) 0.7288(9) 0.069(3) Uani 1 1 d D U . . .
 N4_1 N 1.1694(3) 0.9086(3) 0.6929(7) 0.041(2) Uani 1 1 d D U . . .
 C1_1 C 1.1738(4) 0.8049(4) 0.4878(7) 0.076(4) Uani 1 1 d D U . . .
 C2_1 C 1.1299(4) 0.8087(4) 0.4972(8) 0.059(3) Uani 1 1 d D U . . .
 C3_1 C 1.1342(4) 0.8502(4) 0.5333(8) 0.040(3) Uani 1 1 d D U . . .
 H3_1 H 1.164574 0.876477 0.548611 0.048 Uiso 1 1 calc R U . . .
 C4_1 C 1.0926(3) 0.8513(3) 0.5457(7) 0.038(2) Uani 1 1 d D U . . .
 C5_1 C 1.0479(4) 0.8137(4) 0.5173(9) 0.053(3) Uani 1 1 d D U . . .
 C6_1 C 1.0442(5) 0.7728(4) 0.4813(9) 0.063(4) Uani 1 1 d D U . . .
 H6_1 H 1.014208 0.747244 0.462605 0.076 Uiso 1 1 calc R U . . .
 C7_1 C 1.0854(4) 0.7702(4) 0.4735(10) 0.067(4) Uani 1 1 d D U . . .
 H7_1 H 1.083544 0.741880 0.451623 0.080 Uiso 1 1 calc R U . . .
 C8_1 C 1.0325(3) 0.8658(4) 0.5657(8) 0.047(3) Uani 1 1 d D U . . .
 C9_1 C 1.0127(4) 0.8954(4) 0.5863(9) 0.056(3) Uani 1 1 d D U . . .
 H9_1 H 0.978983 0.882923 0.586041 0.067 Uiso 1 1 calc R U . . .
 C10_1 C 1.0429(4) 0.9413(4) 0.6062(9) 0.055(3) Uani 1 1 d D U . . .
 H10_1 H 1.030979 0.963018 0.606088 0.066 Uiso 1 1 calc R U . . .
 C11_1 C 1.0920(4) 0.9594(3) 0.6274(9) 0.048(3) Uani 1 1 d D U . . .
 C12_1 C 1.1235(4) 1.0065(4) 0.6510(10) 0.058(3) Uani 1 1 d D U . . .
 H12_1 H 1.111893 1.028312 0.655032 0.069 Uiso 1 1 calc R U . . .
 C13_1 C 1.1700(5) 1.0222(4) 0.6685(10) 0.060(3) Uani 1 1 d D U . . .
 H13_1 H 1.191691 1.055644 0.673990 0.072 Uiso 1 1 calc R U . . .
 C14_1 C 1.1869(4) 0.9898(3) 0.6786(11) 0.061(3) Uani 1 1 d D U . . .
 C15_1 C 1.2355(4) 1.0047(4) 0.6968(13) 0.083(5) Uani 1 1 d D U . . .
 H15_1 H 1.257331 1.038006 0.703990 0.099 Uiso 1 1 calc R U . . .
 C16_1 C 1.2524(4) 0.9735(4) 0.7047(13) 0.082(5) Uani 1 1 d D U . . .
 H16_1 H 1.285734 0.984776 0.710687 0.099 Uiso 1 1 calc R U . . .
 C17_1 C 1.2181(4) 0.9232(3) 0.7034(11) 0.068(4) Uani 1 1 d D U . . .
 C18_1 C 1.1542(3) 0.9404(3) 0.6667(8) 0.041(3) Uani 1 1 d D U . . .
 C19_1 C 1.1106(3) 0.9273(3) 0.6254(8) 0.041(2) Uani 1 1 d D U . . .
 C20_1 C 1.1798(3) 0.8485(3) 0.7367(9) 0.047(3) Uani 1 1 d D U . . .
 C21_1 C 1.1662(3) 0.8015(3) 0.7616(8) 0.040(3) Uani 1 1 d D U . . .
 H21_1 H 1.189578 0.793067 0.776910 0.048 Uiso 1 1 calc R U . . .
 C22_1 C 1.1184(3) 0.7683(3) 0.7633(7) 0.035(2) Uani 1 1 d D U . . .
 H22_1 H 1.108513 0.736128 0.778546 0.042 Uiso 1 1 calc R U . . .
 C23_1 C 1.0835(3) 0.7809(3) 0.7429(6) 0.030(2) Uani 1 1 d D U . . .
 C24_1 C 1.0955(3) 0.8271(3) 0.7210(8) 0.038(3) Uani 1 1 d D U . . .
 H24_1 H 1.071929 0.835931 0.710258 0.046 Uiso 1 1 calc R U . . .
 C25_1 C 1.1443(3) 0.8600(3) 0.7157(7) 0.036(2) Uani 1 1 d D U . . .
 C26_1 C 1.0331(3) 0.7429(3) 0.7450(6) 0.040(3) Uani 1 1 d D U . . .
 F1_2 F 0.8823(5) 1.0602(4) 0.0786(6) 0.126(5) Uani 1 1 d D U . . .
 F2_2 F 0.8221(3) 1.0369(4) 0.1646(8) 0.097(4) Uani 1 1 d D U . . .
 F3_2 F 0.8923(4) 1.0767(3) 0.2111(6) 0.093(3) Uani 1 1 d D U . . .
 F4_2 F 0.9605(2) 0.9956(3) 0.3952(5) 0.059(2) Uani 1 1 d D U . . .
 F5_2 F 0.9356(4) 0.9674(4) 0.5164(5) 0.080(3) Uani 1 1 d D U . . .
 F6_2 F 0.9107(3) 0.9203(3) 0.4125(7) 0.074(3) Uani 1 1 d D U . . .
 N1_2 N 0.8645(5) 0.8696(4) 0.2136(10) 0.085(4) Uani 1 1 d D U . . .
 N2_2 N 0.7969(3) 0.8704(3) 0.2456(8) 0.057(3) Uani 1 1 d D U . . .
 N3_2 N 0.7677(3) 0.9968(4) 0.3803(7) 0.049(2) Uani 1 1 d D U . . .
 N4_2 N 0.7562(3) 0.9229(3) 0.3425(6) 0.042(2) Uani 1 1 d D U . . .
 C1_2 C 0.8660(4) 1.0419(4) 0.1536(7) 0.069(4) Uani 1 1 d D U . . .
 C2_2 C 0.8674(4) 0.9968(4) 0.1681(9) 0.058(3) Uani 1 1 d D U . . .
 C3_2 C 0.8262(4) 0.9562(3) 0.1957(8) 0.046(3) Uani 1 1 d D U . . .
 H3_2 H 0.796942 0.956277 0.202508 0.056 Uiso 1 1 calc R U . . .
 C4_2 C 0.8290(4) 0.9159(3) 0.2130(8) 0.049(3) Uani 1 1 d D U . . .
 C5_2 C 0.8724(4) 0.9153(4) 0.2036(10) 0.068(3) Uani 1 1 d D U . . .
 C6_2 C 0.9126(4) 0.9557(5) 0.1724(10) 0.072(4) Uani 1 1 d D U . . .
 H6_2 H 0.940892 0.954635 0.159595 0.087 Uiso 1 1 calc R U . . .
 C7_2 C 0.9113(4) 0.9969(5) 0.1602(10) 0.075(4) Uani 1 1 d D U . . .
 H7_2 H 0.939834 1.025718 0.146487 0.089 Uiso 1 1 calc R U . . .
 C8_2 C 0.8218(5) 0.8444(4) 0.2452(11) 0.075(4) Uani 1 1 d D U . . .
 C9_2 C 0.7942(6) 0.7936(4) 0.2576(16) 0.105(5) Uani 1 1 d D U . . .
 H9_2 H 0.809474 0.774925 0.260335 0.126 Uiso 1 1 calc R U . . .
 C10_2 C 0.7466(6) 0.7730(5) 0.2652(16) 0.111(6) Uani 1 1 d D U . . .
 H10_2 H 0.728182 0.738972 0.265548 0.134 Uiso 1 1 calc R U . . .
 C11_2 C 0.7222(5) 0.7994(4) 0.2729(14) 0.098(5) Uani 1 1 d D U . . .
 C12_2 C 0.6728(5) 0.7789(5) 0.2781(14) 0.113(7) Uani 1 1 d D U . . .
 H12_2 H 0.653174 0.745469 0.267949 0.136 Uiso 1 1 calc R U . . .
 C13_2 C 0.6518(5) 0.8048(5) 0.2973(12) 0.113(7) Uani 1 1 d D U . . .
 H13_2 H 0.617868 0.789352 0.301250 0.135 Uiso 1 1 calc R U . . .
 C14_2 C 0.6793(4) 0.8546(4) 0.3115(10) 0.082(5) Uani 1 1 d D U . . .
 C15_2 C 0.6596(4) 0.8850(5) 0.3234(10) 0.076(5) Uani 1 1 d D U . . .
 H15_2 H 0.625799 0.871015 0.320144 0.091 Uiso 1 1 calc R U . . .
 C16_2 C 0.6861(4) 0.9330(5) 0.3393(10) 0.066(4) Uani 1 1 d D U . . .
 H16_2 H 0.671509 0.952284 0.342306 0.079 Uiso 1 1 calc R U . . .
 C17_2 C 0.7366(3) 0.9532(4) 0.3511(8) 0.048(3) Uani 1 1 d D U . . .
 C18_2 C 0.7297(3) 0.8764(4) 0.3094(9) 0.057(3) Uani 1 1 d D U . . .
 C19_2 C 0.7500(4) 0.8507(3) 0.2743(10) 0.067(4) Uani 1 1 d D U . . .
 C20_2 C 0.8085(3) 0.9950(4) 0.3952(8) 0.045(3) Uani 1 1 d D U . . .
 C21_2 C 0.8522(3) 1.0303(4) 0.4307(8) 0.046(3) Uani 1 1 d D U . . .
 H21_2 H 0.856850 1.060985 0.445407 0.056 Uiso 1 1 calc R U . . .
 C22_2 C 0.8875(4) 1.0194(4) 0.4436(8) 0.044(3) Uani 1 1 d D U . . .
 H22_2 H 0.917809 1.043423 0.464376 0.053 Uiso 1 1 calc R U . . .
 C23_2 C 0.8800(3) 0.9733(3) 0.4267(7) 0.043(3) Uani 1 1 d D U . . .
 C24_2 C 0.8368(3) 0.9371(4) 0.3945(7) 0.038(2) Uani 1 1 d D U . . .
 H24_2 H 0.831223 0.905649 0.384763 0.045 Uiso 1 1 calc R U . . .
 C25_2 C 0.8023(3) 0.9496(3) 0.3774(7) 0.037(2) Uani 1 1 d D U . . .
 C26_2 C 0.9205(3) 0.9649(3) 0.4366(7) 0.051(3) Uani 1 1 d D U . . .
 F1_3 F 0.9455(5) 0.6376(5) 0.5148(7) 0.142(6) Uani 1 1 d D U . . .
 F2_3 F 0.9275(4) 0.5937(3) 0.4052(8) 0.089(3) Uani 1 1 d D U . . .
 F3_3 F 0.9621(4) 0.6692(4) 0.3904(8) 0.110(4) Uani 1 1 d D U . . .
 F4_3 F 0.8792(3) 0.7458(2) 0.2286(6) 0.061(2) Uani 1 1 d D U . . .
 F5_3 F 0.8396(4) 0.7184(4) 0.1170(5) 0.077(3) Uani 1 1 d D U . . .
 F6_3 F 0.8046(3) 0.6933(3) 0.2374(6) 0.065(2) Uani 1 1 d D U . . .
 N1_3 N 0.7509(4) 0.6251(4) 0.4182(9) 0.081(4) Uani 1 1 d D U . . .
 N2_3 N 0.7560(3) 0.5637(3) 0.3585(7) 0.048(2) Uani 1 1 d D U . . .
 N3_3 N 0.8857(4) 0.5551(3) 0.1899(8) 0.058(3) Uani 1 1 d D U . . .
 N4_3 N 0.8119(3) 0.5370(3) 0.2371(7) 0.040(2) Uani 1 1 d D U . . .
 C1_3 C 0.9284(4) 0.6329(4) 0.4378(8) 0.071(4) Uani 1 1 d D U . . .
 C2_3 C 0.8815(4) 0.6320(4) 0.4347(9) 0.060(3) Uani 1 1 d D U . . .
 C3_3 C 0.8426(3) 0.5926(4) 0.3990(8) 0.048(3) Uani 1 1 d D U . . .
 H3_3 H 0.844366 0.565707 0.378974 0.058 Uiso 1 1 calc R U . . .
 C4_3 C 0.8008(3) 0.5947(4) 0.3944(8) 0.045(3) Uani 1 1 d D U . . .
 C5_3 C 0.7970(4) 0.6339(4) 0.4255(9) 0.061(3) Uani 1 1 d D U . . .
 C6_3 C 0.8362(4) 0.6721(4) 0.4645(10) 0.067(4) Uani 1 1 d D U . . .
 H6_3 H 0.833811 0.697884 0.488501 0.081 Uiso 1 1 calc R U . . .
 C7_3 C 0.8784(5) 0.6714(5) 0.4673(11) 0.074(4) Uani 1 1 d D U . . .
 H7_3 H 0.906072 0.697773 0.491389 0.089 Uiso 1 1 calc R U . . .
 C8_3 C 0.7270(4) 0.5837(5) 0.3812(10) 0.067(3) Uani 1 1 d D U . . .
 C9_3 C 0.6767(4) 0.5538(5) 0.3698(12) 0.083(4) Uani 1 1 d D U . . .
 H9_3 H 0.655954 0.565597 0.384502 0.100 Uiso 1 1 calc R U . . .
 C10_3 C 0.6581(5) 0.5093(5) 0.3389(12) 0.089(5) Uani 1 1 d D U . . .
 H10_3 H 0.624391 0.490360 0.331789 0.107 Uiso 1 1 calc R U . . .
 C11_3 C 0.6876(4) 0.4895(4) 0.3163(11) 0.079(4) Uani 1 1 d D U . . .
 C12_3 C 0.6683(5) 0.4426(5) 0.2860(12) 0.096(6) Uani 1 1 d D U . . .
 H12_3 H 0.634624 0.423107 0.278654 0.115 Uiso 1 1 calc R U . . .
 C13_3 C 0.6975(4) 0.4253(5) 0.2674(12) 0.085(5) Uani 1 1 d D U . . .
 H13_3 H 0.684903 0.391605 0.264049 0.102 Uiso 1 1 calc R U . . .
 C14_3 C 0.7467(4) 0.4566(3) 0.2527(10) 0.067(4) Uani 1 1 d D U . . .
 C15_3 C 0.7785(5) 0.4392(4) 0.2359(11) 0.073(4) Uani 1 1 d D U . . .
 H15_3 H 0.766662 0.405610 0.236356 0.087 Uiso 1 1 calc R U . . .
 C16_3 C 0.8260(5) 0.4700(4) 0.2188(11) 0.067(4) Uani 1 1 d D U . . .
 H16_3 H 0.847098 0.457970 0.208093 0.081 Uiso 1 1 calc R U . . .
 C17_3 C 0.8431(4) 0.5199(3) 0.2174(10) 0.056(3) Uani 1 1 d D U . . .
 C18_3 C 0.7663(4) 0.5057(3) 0.2701(9) 0.054(3) Uani 1 1 d D U . . .
 C19_3 C 0.7384(3) 0.5207(4) 0.3151(9) 0.059(3) Uani 1 1 d D U . . .
 C20_3 C 0.8813(3) 0.5953(3) 0.1885(8) 0.041(3) Uani 1 1 d D U . . .
 C21_3 C 0.9164(4) 0.6432(3) 0.1696(9) 0.043(3) Uani 1 1 d D U . . .
 H21_3 H 0.948414 0.651421 0.156562 0.051 Uiso 1 1 calc R U . . .
 C22_3 C 0.9031(3) 0.6773(3) 0.1707(8) 0.036(2) Uani 1 1 d D U . . .
 H22_3 H 0.925992 0.709311 0.155738 0.044 Uiso 1 1 calc R U . . .
 C23_3 C 0.8565(3) 0.6663(3) 0.1935(7) 0.034(2) Uani 1 1 d D U . . .
 C24_3 C 0.8220(3) 0.6202(3) 0.2154(7) 0.036(2) Uani 1 1 d D U . . .
 H24_3 H 0.790478 0.612465 0.230980 0.043 Uiso 1 1 calc R U . . .
 C25_3 C 0.8357(3) 0.5856(3) 0.2137(8) 0.042(3) Uani 1 1 d D U . . .
 C26_3 C 0.8450(3) 0.7048(3) 0.1935(6) 0.038(3) Uani 1 1 d D U . . .
 F1_4 F 0.3731(5) 0.3909(4) 0.8648(5) 0.118(5) Uani 1 1 d D U . . .
 F2_4 F 0.3402(3) 0.4126(3) 0.7693(8) 0.093(4) Uani 1 1 d D U . . .
 F3_4 F 0.3692(3) 0.3702(3) 0.7340(6) 0.065(2) Uani 1 1 d D U . . .
 F4_4 F 0.5218(4) 0.4484(4) 0.5424(6) 0.078(3) Uani 1 1 d D U . . .
 F5_4 F 0.5159(4) 0.4628(5) 0.4143(7) 0.123(5) Uani 1 1 d D U . . .
 F6_4 F 0.5445(4) 0.5196(3) 0.5049(10) 0.119(5) Uani 1 1 d D U . . .
 N1_4 N 0.5530(4) 0.5709(4) 0.7118(10) 0.095(5) Uani 1 1 d D U . . .
 N2_4 N 0.4855(3) 0.5729(3) 0.6811(8) 0.064(3) Uani 1 1 d D U . . .
 N3_4 N 0.3269(3) 0.4454(3) 0.5570(9) 0.059(3) Uani 1 1 d D U . . .
 N4_4 N 0.3905(3) 0.5191(3) 0.5895(8) 0.053(3) Uani 1 1 d D U . . .
 C1_4 C 0.3774(3) 0.4062(3) 0.7867(6) 0.047(3) Uani 1 1 d D U . . .
 C2_4 C 0.4254(3) 0.4490(3) 0.7679(8) 0.042(3) Uani 1 1 d D U . . .
 C3_4 C 0.4267(4) 0.4899(3) 0.7379(8) 0.043(3) Uani 1 1 d D U . . .
 H3_4 H 0.398343 0.491914 0.732620 0.052 Uiso 1 1 calc R U . . .
 C4_4 C 0.4708(3) 0.5277(3) 0.7161(8) 0.051(3) Uani 1 1 d D U . . .
 C5_4 C 0.5136(4) 0.5273(4) 0.7341(10) 0.072(4) Uani 1 1 d D U . . .
 C6_4 C 0.5115(4) 0.4857(4) 0.7638(10) 0.073(5) Uani 1 1 d D U . . .
 H6_4 H 0.540084 0.484504 0.772987 0.088 Uiso 1 1 calc R U . . .
 C7_4 C 0.4672(4) 0.4460(4) 0.7798(10) 0.061(4) Uani 1 1 d D U . . .
 H7_4 H 0.464959 0.416883 0.798560 0.073 Uiso 1 1 calc R U . . .
 C8_4 C 0.5358(4) 0.5984(4) 0.6908(12) 0.088(5) Uani 1 1 d D U . . .
 C9_4 C 0.5588(5) 0.6490(4) 0.6769(13) 0.098(6) Uani 1 1 d D U . . .
 H9_4 H 0.592730 0.668118 0.679328 0.118 Uiso 1 1 calc R U . . .
 C10_4 C 0.5321(5) 0.6692(5) 0.6604(12) 0.095(6) Uani 1 1 d D U . . .
 H10_4 H 0.547877 0.703232 0.658030 0.114 Uiso 1 1 calc R U . . .
 C11_4 C 0.4817(5) 0.6434(4) 0.6462(11) 0.077(4) Uani 1 1 d D U . . .
 C12_4 C 0.4535(5) 0.6647(5) 0.6358(12) 0.082(5) Uani 1 1 d D U . . .
 H12_4 H 0.468508 0.698612 0.634829 0.099 Uiso 1 1 calc R U . . .
 C13_4 C 0.4055(5) 0.6383(4) 0.6269(13) 0.089(5) Uani 1 1 d D U . . .
 H13_4 H 0.386639 0.653287 0.630349 0.107 Uiso 1 1 calc R U . . .
 C14_4 C 0.3833(5) 0.5886(4) 0.6126(13) 0.080(4) Uani 1 1 d D U . . .
 C15_4 C 0.3326(5) 0.5588(5) 0.6117(13) 0.084(4) Uani 1 1 d D U . . .
 H15_4 H 0.313254 0.572914 0.621600 0.101 Uiso 1 1 calc R U . . .
 C16_4 C 0.3107(5) 0.5106(5) 0.5971(12) 0.077(4) Uani 1 1 d D U . . .
 H16_4 H 0.276813 0.491285 0.597464 0.092 Uiso 1 1 calc R U . . .
 C17_4 C 0.3404(4) 0.4900(4) 0.5811(11) 0.063(3) Uani 1 1 d D U . . .
 C18_4 C 0.4121(4) 0.5670(3) 0.6149(10) 0.062(3) Uani 1 1 d D U . . .
 C19_4 C 0.4590(4) 0.5923(3) 0.6465(9) 0.064(4) Uani 1 1 d D U . . .
 C20_4 C 0.3696(3) 0.4471(4) 0.5390(9) 0.055(3) Uani 1 1 d D U . . .
 C21_4 C 0.3771(4) 0.4094(4) 0.5154(10) 0.063(4) Uani 1 1 d D U . . .
 H21_4 H 0.350934 0.377555 0.511713 0.076 Uiso 1 1 calc R U . . .
 C22_4 C 0.4225(4) 0.4192(4) 0.4979(9) 0.058(3) Uani 1 1 d D U . . .
 H22_4 H 0.428100 0.394395 0.479250 0.069 Uiso 1 1 calc R U . . .
 C23_4 C 0.4611(3) 0.4661(4) 0.5073(9) 0.054(3) Uani 1 1 d D U . . .
 C24_4 C 0.4565(3) 0.5037(4) 0.5376(8) 0.045(3) Uani 1 1 d D U . . .
 H24_4 H 0.483099 0.535001 0.545437 0.054 Uiso 1 1 calc R U . . .
 C25_4 C 0.4096(3) 0.4921(4) 0.5556(9) 0.050(3) Uani 1 1 d D U . . .
 C26_4 C 0.5096(4) 0.4741(4) 0.4923(8) 0.071(4) Uani 1 1 d D U . . .
 F1_5 F 0.6246(4) 0.4760(4) 0.7565(6) 0.112(5) Uani 1 1 d D U . . .
 F2_5 F 0.6470(3) 0.4552(3) 0.8671(9) 0.109(4) Uani 1 1 d D U . . .
 F3_5 F 0.5976(3) 0.4808(3) 0.8778(6) 0.071(3) Uani 1 1 d D U . . .
 F4_5 F 0.6643(4) 0.6214(4) 1.0630(7) 0.091(3) Uani 1 1 d D U . . .
 F5_5 F 0.6705(5) 0.6145(5) 1.1927(7) 0.125(5) Uani 1 1 d D U . . .
 F6_5 F 0.7324(3) 0.6532(3) 1.1125(10) 0.115(5) Uani 1 1 d D U . . .
 N1_5 N 0.7848(4) 0.6750(3) 0.8920(7) 0.061(3) Uani 1 1 d D U . . .
 N2_5 N 0.8009(3) 0.6162(3) 0.9250(7) 0.052(3) Uani 1 1 d D U . . .
 N3_5 N 0.7040(5) 0.4491(4) 1.0471(11) 0.100(4) Uani 1 1 d D U . . .
 N4_5 N 0.7681(4) 0.5222(3) 1.0148(9) 0.071(3) Uani 1 1 d D U . . .
 C1_5 C 0.6371(4) 0.4885(4) 0.8352(8) 0.078(5) Uani 1 1 d D U . . .
 C2_5 C 0.6765(3) 0.5387(3) 0.8485(9) 0.049(3) Uani 1 1 d D U . . .
 C3_5 C 0.7203(3) 0.5460(3) 0.8770(8) 0.037(2) Uani 1 1 d D U . . .
 H3_5 H 0.726884 0.520537 0.883144 0.044 Uiso 1 1 calc R U . . .
 C4_5 C 0.7536(3) 0.5929(3) 0.8957(8) 0.039(2) Uani 1 1 d D U . . .
 C5_5 C 0.7448(4) 0.6310(3) 0.8787(8) 0.048(3) Uani 1 1 d D U . . .
 C6_5 C 0.7012(4) 0.6227(4) 0.8481(9) 0.054(3) Uani 1 1 d D U . . .
 H6_5 H 0.695252 0.648351 0.838125 0.065 Uiso 1 1 calc R U . . .
 C7_5 C 0.6668(4) 0.5763(4) 0.8327(10) 0.059(3) Uani 1 1 d D U . . .
 H7_5 H 0.636412 0.569245 0.811359 0.071 Uiso 1 1 calc R U . . .
 C8_5 C 0.8172(4) 0.6656(4) 0.9173(9) 0.057(3) Uani 1 1 d D U . . .
 C9_5 C 0.8669(4) 0.6984(5) 0.9315(11) 0.075(4) Uani 1 1 d D U . . .
 H9_5 H 0.878556 0.731875 0.933697 0.090 Uiso 1 1 calc R U . . .
 C10_5 C 0.8967(5) 0.6813(5) 0.9417(11) 0.078(4) Uani 1 1 d D U . . .
 H10_5 H 0.930146 0.703312 0.942826 0.094 Uiso 1 1 calc R U . . .
 C11_5 C 0.8806(4) 0.6317(4) 0.9510(11) 0.075(4) Uani 1 1 d D U . . .
 C12_5 C 0.9119(5) 0.6137(5) 0.9546(13) 0.091(5) Uani 1 1 d D U . . .
 H12_5 H 0.945281 0.634693 0.946738 0.109 Uiso 1 1 calc R U . . .
 C13_5 C 0.8952(5) 0.5668(5) 0.9691(13) 0.085(4) Uani 1 1 d D U . . .
 H13_5 H 0.917087 0.555238 0.971009 0.102 Uiso 1 1 calc R U . . .
 C14_5 C 0.8464(4) 0.5346(5) 0.9815(12) 0.081(4) Uani 1 1 d D U . . .
 C15_5 C 0.8278(6) 0.4847(5) 0.9886(13) 0.093(5) Uani 1 1 d D U . . .
 H15_5 H 0.849134 0.472521 0.982438 0.112 Uiso 1 1 calc R U . . .
 C16_5 C 0.7804(6) 0.4531(5) 1.0040(13) 0.088(4) Uani 1 1 d D U . . .
 H16_5 H 0.768015 0.419427 1.001959 0.106 Uiso 1 1 calc R U . . .
 C17_5 C 0.7500(5) 0.4726(4) 1.0234(13) 0.086(4) Uani 1 1 d D U . . .
 C18_5 C 0.8140(4) 0.5523(4) 0.9824(10) 0.069(3) Uani 1 1 d D U . . .
 C19_5 C 0.8301(3) 0.5987(4) 0.9529(9) 0.059(3) Uani 1 1 d D U . . .
 C20_5 C 0.6932(5) 0.4842(4) 1.0668(13) 0.090(4) Uani 1 1 d D U . . .
 C21_5 C 0.6504(5) 0.4817(5) 1.0954(15) 0.111(6) Uani 1 1 d D U . . .
 H21_5 H 0.622012 0.451415 1.100573 0.133 Uiso 1 1 calc R U . . .
 C22_5 C 0.6499(5) 0.5230(4) 1.1157(13) 0.090(5) Uani 1 1 d D U . . .
 H22_5 H 0.621595 0.520911 1.138405 0.109 Uiso 1 1 calc R U . . .
 C23_5 C 0.6909(4) 0.5682(4) 1.1032(9) 0.059(3) Uani 1 1 d D U . . .
 C24_5 C 0.7330(4) 0.5720(4) 1.0734(9) 0.056(3) Uani 1 1 d D U . . .
 H24_5 H 0.761330 0.602336 1.068147 0.067 Uiso 1 1 calc R U . . .
 C25_5 C 0.7327(5) 0.5298(4) 1.0511(10) 0.070(3) Uani 1 1 d D U . . .
 C26_5 C 0.6897(4) 0.6123(4) 1.1199(8) 0.076(4) Uani 1 1 d D U . . .
 F1_6 F 0.8729(4) 0.8044(4) 0.4341(6) 0.098(4) Uani 1 1 d D U . . .
 F2_6 F 0.8933(3) 0.8508(3) 0.5432(6) 0.067(3) Uani 1 1 d D U . . .
 F3_6 F 0.8601(4) 0.7755(3) 0.5626(7) 0.089(3) Uani 1 1 d D U . . .
 F4_6 F 0.6918(3) 0.7005(3) 0.7162(8) 0.099(4) Uani 1 1 d D U . . .
 F5_6 F 0.6782(4) 0.7250(4) 0.8305(7) 0.101(4) Uani 1 1 d D U . . .
 F6_6 F 0.6646(3) 0.7484(3) 0.7101(8) 0.095(4) Uani 1 1 d D U . . .
 N1_6 N 0.6801(4) 0.7950(5) 0.5086(11) 0.097(4) Uani 1 1 d D U . . .
 N2_6 N 0.7415(3) 0.8649(4) 0.5586(7) 0.064(3) Uani 1 1 d D U . . .
 N3_6 N 0.8817(3) 0.8992(4) 0.7508(7) 0.063(3) Uani 1 1 d D U . . .
 N4_6 N 0.8229(3) 0.9077(3) 0.6855(6) 0.046(2) Uani 1 1 d D U . . .
 C1_6 C 0.8592(3) 0.8084(4) 0.5113(7) 0.055(3) Uani 1 1 d D U . . .
 C2_6 C 0.8114(3) 0.8049(4) 0.5118(9) 0.056(3) Uani 1 1 d D U . . .
 C3_6 C 0.8076(3) 0.8443(4) 0.5355(8) 0.046(3) Uani 1 1 d D U . . .
 H3_6 H 0.834715 0.874419 0.548760 0.055 Uiso 1 1 calc R U . . .
 C4_6 C 0.7614(3) 0.8362(4) 0.5383(9) 0.059(3) Uani 1 1 d D U . . .
 C5_6 C 0.7222(4) 0.7940(5) 0.5052(12) 0.082(4) Uani 1 1 d D U . . .
 C6_6 C 0.7266(4) 0.7545(5) 0.4866(13) 0.093(5) Uani 1 1 d D U . . .
 H6_6 H 0.699395 0.724197 0.474378 0.111 Uiso 1 1 calc R U . . .
 C7_6 C 0.7718(4) 0.7607(5) 0.4865(12) 0.082(5) Uani 1 1 d D U . . .
 H7_6 H 0.776657 0.735139 0.469314 0.098 Uiso 1 1 calc R U . . .
 C8_6 C 0.6926(4) 0.8378(5) 0.5343(11) 0.081(4) Uani 1 1 d D U . . .
 C9_6 C 0.6645(5) 0.8606(6) 0.5357(12) 0.092(5) Uani 1 1 d D U . . .
 H9_6 H 0.631328 0.843212 0.522383 0.110 Uiso 1 1 calc R U . . .
 C10_6 C 0.6857(5) 0.9068(6) 0.5561(11) 0.085(4) Uani 1 1 d D U . . .
 H10_6 H 0.667314 0.922380 0.553314 0.102 Uiso 1 1 calc R U . . .
 C11_6 C 0.7346(5) 0.9342(5) 0.5819(10) 0.083(4) Uani 1 1 d D U . . .
 C12_6 C 0.7578(6) 0.9826(5) 0.6010(11) 0.096(5) Uani 1 1 d D U . . .
 H12_6 H 0.740991 0.999627 0.593545 0.115 Uiso 1 1 calc R U . . .
 C13_6 C 0.8032(6) 1.0065(5) 0.6298(12) 0.099(5) Uani 1 1 d D U . . .
 H13_6 H 0.818497 1.040250 0.636228 0.119 Uiso 1 1 calc R U . . .
 C14_6 C 0.8287(5) 0.9829(4) 0.6506(10) 0.083(4) Uani 1 1 d D U . . .
 C15_6 C 0.8766(5) 1.0054(5) 0.6810(11) 0.098(6) Uani 1 1 d D U . . .
 H15_6 H 0.894161 1.039457 0.682852 0.117 Uiso 1 1 calc R U . . .
 C16_6 C 0.8990(5) 0.9811(4) 0.7080(11) 0.096(6) Uani 1 1 d D U . . .
 H16_6 H 0.931839 0.997674 0.724104 0.116 Uiso 1 1 calc R U . . .
 C17_6 C 0.8712(4) 0.9296(4) 0.7110(9) 0.073(4) Uani 1 1 d D U . . .
 C18_6 C 0.8035(4) 0.9322(3) 0.6435(8) 0.063(3) Uani 1 1 d D U . . .
 C19_6 C 0.7611(4) 0.9100(4) 0.5954(7) 0.060(3) Uani 1 1 d D U . . .
 C20_6 C 0.8397(3) 0.8561(4) 0.7511(9) 0.050(3) Uani 1 1 d D U . . .
 C21_6 C 0.8289(4) 0.8119(4) 0.7878(10) 0.058(3) Uani 1 1 d D U . . .
 H21_6 H 0.853359 0.807787 0.813327 0.070 Uiso 1 1 calc R U . . .
 C22_6 C 0.7824(4) 0.7749(4) 0.7857(11) 0.058(3) Uani 1 1 d D U . . .
 H22_6 H 0.775015 0.744446 0.807424 0.070 Uiso 1 1 calc R U . . .
 C23_6 C 0.7452(3) 0.7811(3) 0.7522(9) 0.048(3) Uani 1 1 d D U . . .
 C24_6 C 0.7544(3) 0.8240(3) 0.7174(8) 0.037(2) Uani 1 1 d D U . . .
 H24_6 H 0.729451 0.828287 0.694622 0.044 Uiso 1 1 calc R U . . .
 C25_6 C 0.8018(3) 0.8609(3) 0.7173(7) 0.037(2) Uani 1 1 d D U . . .
 C26_6 C 0.6959(3) 0.7400(3) 0.7528(7) 0.061(3) Uani 1 1 d D U . . .
 F1_7 F 0.3555(4) 0.7228(4) 0.8478(6) 0.097(4) Uani 1 1 d D U . . .
 F2_7 F 0.3340(3) 0.7408(4) 0.7328(9) 0.103(4) Uani 1 1 d D U . . .
 F3_7 F 0.3726(4) 0.7026(3) 0.7302(7) 0.094(3) Uani 1 1 d D U . . .
 F4_7 F 0.5568(3) 0.8579(3) 0.5665(7) 0.080(3) Uani 1 1 d D U . . .
 F5_7 F 0.5450(4) 0.8202(4) 0.4521(6) 0.084(3) Uani 1 1 d D U . . .
 F6_7 F 0.5313(3) 0.7829(3) 0.5700(6) 0.067(2) Uani 1 1 d D U . . .
 N1_7 N 0.5430(4) 0.9152(4) 0.7475(8) 0.069(4) Uani 1 1 d D U . . .
 N2_7 N 0.4771(3) 0.9106(3) 0.6871(7) 0.063(3) Uani 1 1 d D U . . .
 N3_7 N 0.3369(4) 0.7791(4) 0.5244(9) 0.067(3) Uani 1 1 d D U . . .
 N4_7 N 0.3938(3) 0.8541(3) 0.5677(7) 0.057(3) Uani 1 1 d D U . . .
 C1_7 C 0.3706(4) 0.7387(4) 0.7706(8) 0.073(4) Uani 1 1 d D U . . .
 C2_7 C 0.4173(3) 0.7844(3) 0.7673(8) 0.051(3) Uani 1 1 d D U . . .
 C3_7 C 0.4189(4) 0.8243(3) 0.7298(8) 0.041(3) Uani 1 1 d D U . . .
 H3_7 H 0.390643 0.823038 0.709130 0.050 Uiso 1 1 calc R U . . .
 C4_7 C 0.4626(3) 0.8654(3) 0.7235(8) 0.048(3) Uani 1 1 d D U . . .
 C5_7 C 0.5045(4) 0.8694(4) 0.7595(9) 0.062(4) Uani 1 1 d D U . . .
 C6_7 C 0.5027(4) 0.8294(4) 0.7968(10) 0.064(3) Uani 1 1 d D U . . .
 H6_7 H 0.530772 0.831119 0.819692 0.077 Uiso 1 1 calc R U . . .
 C7_7 C 0.4595(4) 0.7872(5) 0.8001(9) 0.061(3) Uani 1 1 d D U . . .
 H7_7 H 0.458071 0.759580 0.824633 0.073 Uiso 1 1 calc R U . . .
 C8_7 C 0.5254(4) 0.9392(4) 0.7116(10) 0.073(4) Uani 1 1 d D U . . .
 C9_7 C 0.5472(5) 0.9896(4) 0.6966(12) 0.090(5) Uani 1 1 d D U . . .
 H9_7 H 0.580621 1.009955 0.705586 0.108 Uiso 1 1 calc R U . . .
 C10_7 C 0.5202(5) 1.0077(5) 0.6697(13) 0.102(6) Uani 1 1 d D U . . .
 H10_7 H 0.534045 1.041546 0.668280 0.122 Uiso 1 1 calc R U . . .
 C11_7 C 0.4715(5) 0.9788(4) 0.6429(11) 0.083(4) Uani 1 1 d D U . . .
 C12_7 C 0.4429(6) 0.9977(5) 0.6164(12) 0.085(4) Uani 1 1 d D U . . .
 H12_7 H 0.455803 1.031457 0.615630 0.102 Uiso 1 1 calc R U . . .
 C13_7 C 0.3972(6) 0.9684(5) 0.5919(12) 0.088(4) Uani 1 1 d D U . . .
 H13_7 H 0.376920 0.981514 0.582744 0.106 Uiso 1 1 calc R U . . .
 C14_7 C 0.3787(5) 0.9193(4) 0.5797(11) 0.072(4) Uani 1 1 d D U . . .
 C15_7 C 0.3300(5) 0.8867(5) 0.5615(12) 0.080(4) Uani 1 1 d D U . . .
 H15_7 H 0.309145 0.899288 0.554140 0.096 Uiso 1 1 calc R U . . .
 C16_7 C 0.3111(5) 0.8382(5) 0.5537(13) 0.087(4) Uani 1 1 d D U . . .
 H16_7 H 0.277549 0.816590 0.552537 0.104 Uiso 1 1 calc R U . . .
 C17_7 C 0.3455(4) 0.8223(4) 0.5475(10) 0.066(3) Uani 1 1 d D U . . .
 C18_7 C 0.4088(4) 0.8999(4) 0.5980(9) 0.066(3) Uani 1 1 d D U . . .
 C19_7 C 0.4515(4) 0.9280(3) 0.6423(8) 0.056(3) Uani 1 1 d D U . . .
 C20_7 C 0.3816(4) 0.7832(4) 0.5248(9) 0.051(3) Uani 1 1 d D U . . .
 C21_7 C 0.3929(4) 0.7471(4) 0.5058(11) 0.061(3) Uani 1 1 d D U . . .
 H21_7 H 0.368691 0.715589 0.491259 0.073 Uiso 1 1 calc R U . . .
 C22_7 C 0.4404(4) 0.7594(4) 0.5091(10) 0.056(3) Uani 1 1 d D U . . .
 H22_7 H 0.448992 0.735539 0.500212 0.067 Uiso 1 1 calc R U . . .
 C23_7 C 0.4765(3) 0.8072(4) 0.5255(8) 0.048(3) Uani 1 1 d D U . . .
 C24_7 C 0.4664(4) 0.8429(4) 0.5472(8) 0.045(3) Uani 1 1 d D U . . .
 H24_7 H 0.490771 0.874310 0.562335 0.054 Uiso 1 1 calc R U . . .
 C25_7 C 0.4180(3) 0.8297(4) 0.5452(8) 0.049(3) Uani 1 1 d D U . . .
 C26_7 C 0.5261(3) 0.8168(3) 0.5285(7) 0.050(3) Uani 1 1 d D U . . .
 F1_8 F 0.8661(5) 0.4822(5) 0.4290(7) 0.116(4) Uani 1 1 d D U . . .
 F2_8 F 0.8870(3) 0.5243(3) 0.5406(8) 0.089(3) Uani 1 1 d D U . . .
 F3_8 F 0.8570(4) 0.4494(4) 0.5505(7) 0.087(3) Uani 1 1 d D U . . .
 F4_8 F 0.6938(4) 0.3615(3) 0.7114(6) 0.079(3) Uani 1 1 d D U . . .
 F5_8 F 0.6826(4) 0.3771(4) 0.8356(7) 0.117(5) Uani 1 1 d D U . . .
 F6_8 F 0.6620(3) 0.4051(4) 0.7300(9) 0.114(5) Uani 1 1 d D U . . .
 N1_8 N 0.6725(4) 0.4680(5) 0.5295(10) 0.083(4) Uani 1 1 d D U . . .
 N2_8 N 0.7347(4) 0.5338(4) 0.5892(7) 0.061(3) Uani 1 1 d D U . . .
 N3_8 N 0.8797(4) 0.5581(4) 0.7530(9) 0.086(5) Uani 1 1 d D U . . .
 N4_8 N 0.8185(3) 0.5705(3) 0.7122(7) 0.057(3) Uani 1 1 d D U . . .
 C1_8 C 0.8526(4) 0.4830(4) 0.5072(8) 0.065(4) Uani 1 1 d D U . . .
 C2_8 C 0.8038(3) 0.4773(4) 0.5143(9) 0.050(3) Uani 1 1 d D U . . .
 C3_8 C 0.7991(4) 0.5142(4) 0.5511(8) 0.043(3) Uani 1 1 d D U . . .
 H3_8 H 0.825927 0.542937 0.570947 0.051 Uiso 1 1 calc R U . . .
 C4_8 C 0.7531(4) 0.5059(4) 0.5565(8) 0.050(3) Uani 1 1 d D U . . .
 C5_8 C 0.7129(4) 0.4638(5) 0.5256(11) 0.074(4) Uani 1 1 d D U . . .
 C6_8 C 0.7189(4) 0.4282(5) 0.4877(11) 0.071(4) Uani 1 1 d D U . . .
 H6_8 H 0.692446 0.400527 0.464002 0.086 Uiso 1 1 calc R U . . .
 C7_8 C 0.7642(4) 0.4342(4) 0.4853(11) 0.064(4) Uani 1 1 d D U . . .
 H7_8 H 0.768945 0.409299 0.464007 0.077 Uiso 1 1 calc R U . . .
 C8_8 C 0.6856(4) 0.5082(5) 0.5682(11) 0.074(3) Uani 1 1 d D U . . .
 C9_8 C 0.6585(5) 0.5322(6) 0.5788(13) 0.090(4) Uani 1 1 d D U . . .
 H9_8 H 0.624914 0.515749 0.569408 0.108 Uiso 1 1 calc R U . . .
 C10_8 C 0.6819(5) 0.5783(5) 0.6024(13) 0.093(4) Uani 1 1 d D U . . .
 H10_8 H 0.664803 0.595263 0.601691 0.112 Uiso 1 1 calc R U . . .
 C11_8 C 0.7307(5) 0.6034(5) 0.6283(11) 0.086(4) Uani 1 1 d D U . . .
 C12_8 C 0.7559(6) 0.6520(5) 0.6492(11) 0.090(4) Uani 1 1 d D U . . .
 H12_8 H 0.740612 0.670629 0.644251 0.108 Uiso 1 1 calc R U . . .
 C13_8 C 0.8018(6) 0.6730(5) 0.6763(11) 0.099(5) Uani 1 1 d D U . . .
 H13_8 H 0.818458 0.706514 0.686967 0.119 Uiso 1 1 calc R U . . .
 C14_8 C 0.8259(5) 0.6475(4) 0.6894(10) 0.083(4) Uani 1 1 d D U . . .
 C15_8 C 0.8742(5) 0.6675(5) 0.7152(12) 0.099(6) Uani 1 1 d D U . . .
 H15_8 H 0.892166 0.701175 0.723793 0.119 Uiso 1 1 calc R U . . .
 C16_8 C 0.8970(5) 0.6417(4) 0.7286(12) 0.107(6) Uani 1 1 d D U . . .
 H16_8 H 0.930669 0.657110 0.736474 0.128 Uiso 1 1 calc R U . . .
 C17_8 C 0.8676(4) 0.5905(4) 0.7302(10) 0.079(5) Uani 1 1 d D U . . .
 C18_8 C 0.7985(4) 0.5969(4) 0.6793(9) 0.069(3) Uani 1 1 d D U . . .
 C19_8 C 0.7555(4) 0.5772(4) 0.6334(9) 0.069(3) Uani 1 1 d D U . . .
 C20_8 C 0.8367(4) 0.5158(3) 0.7554(10) 0.060(3) Uani 1 1 d D U . . .
 C21_8 C 0.8289(4) 0.4701(4) 0.7775(10) 0.066(4) Uani 1 1 d D U . . .
 H21_8 H 0.855023 0.465354 0.790477 0.079 Uiso 1 1 calc R U . . .
 C22_8 C 0.7829(4) 0.4329(4) 0.7799(10) 0.060(3) Uani 1 1 d D U . . .
 H22_8 H 0.776767 0.402009 0.796643 0.071 Uiso 1 1 calc R U . . .
 C23_8 C 0.7444(3) 0.4398(3) 0.7577(9) 0.051(3) Uani 1 1 d D U . . .
 C24_8 C 0.7510(4) 0.4842(3) 0.7345(8) 0.043(3) Uani 1 1 d D U . . .
 H24_8 H 0.724843 0.488539 0.719459 0.051 Uiso 1 1 calc R U . . .
 C25_8 C 0.7981(3) 0.5221(3) 0.7342(8) 0.046(3) Uani 1 1 d D U . . .
 C26_8 C 0.6965(4) 0.3971(3) 0.7589(8) 0.065(4) Uani 1 1 d D U . . .
 F1_9 F 0.3660(6) 0.9891(4) 1.1564(7) 0.129(5) Uani 1 1 d D U . . .
 F2_9 F 0.4086(3) 1.0026(3) 1.0448(9) 0.102(4) Uani 1 1 d D U . . .
 F3_9 F 0.3348(3) 0.9760(3) 1.0335(7) 0.079(3) Uani 1 1 d D U . . .
 F4_9 F 0.2584(3) 0.8127(4) 0.8662(6) 0.077(3) Uani 1 1 d D U . . .
 F5_9 F 0.2818(4) 0.8003(4) 0.7476(5) 0.093(4) Uani 1 1 d D U . . .
 F6_9 F 0.2996(3) 0.7779(3) 0.8642(7) 0.081(3) Uani 1 1 d D U . . .
 N1_9 N 0.3388(4) 0.7856(4) 1.0832(9) 0.066(3) Uani 1 1 d D U . . .
 N2_9 N 0.4114(3) 0.8440(3) 1.0393(8) 0.049(2) Uani 1 1 d D U . . .
 N3_9 N 0.4619(4) 0.9906(3) 0.8602(9) 0.067(3) Uani 1 1 d D U . . .
 N4_9 N 0.4632(3) 0.9267(3) 0.9205(7) 0.043(2) Uani 1 1 d D U . . .
 C1_9 C 0.3666(4) 0.9713(4) 1.0817(8) 0.071(4) Uani 1 1 d D U . . .
 C2_9 C 0.3581(4) 0.9215(3) 1.0838(9) 0.055(3) Uani 1 1 d D U . . .
 C3_9 C 0.3954(4) 0.9132(4) 1.0639(9) 0.048(3) Uani 1 1 d D U . . .
 H3_9 H 0.426630 0.938826 1.051278 0.058 Uiso 1 1 calc R U . . .
 C4_9 C 0.3850(3) 0.8661(3) 1.0634(9) 0.048(3) Uani 1 1 d D U . . .
 C5_9 C 0.3382(4) 0.8278(4) 1.0798(10) 0.059(3) Uani 1 1 d D U . . .
 C6_9 C 0.3020(4) 0.8368(4) 1.1036(11) 0.061(3) Uani 1 1 d D U . . .
 H6_9 H 0.271569 0.811567 1.121155 0.073 Uiso 1 1 calc R U . . .
 C7_9 C 0.3116(4) 0.8833(4) 1.1011(11) 0.066(4) Uani 1 1 d D U . . .
 H7_9 H 0.286386 0.889873 1.111082 0.079 Uiso 1 1 calc R U . . .
 C8_9 C 0.3809(4) 0.7949(4) 1.0578(12) 0.072(4) Uani 1 1 d D U . . .
 C9_9 C 0.4028(5) 0.7659(5) 1.0615(13) 0.077(4) Uani 1 1 d D U . . .
 H9_9 H 0.383834 0.732957 1.075869 0.093 Uiso 1 1 calc R U . . .
 C10_9 C 0.4496(5) 0.7841(5) 1.0450(13) 0.080(4) Uani 1 1 d D U . . .
 H10_9 H 0.462887 0.763676 1.047438 0.096 Uiso 1 1 calc R U . . .
 C11_9 C 0.4800(4) 0.8336(4) 1.0239(11) 0.066(3) Uani 1 1 d D U . . .
 C12_9 C 0.5292(4) 0.8543(5) 1.0097(12) 0.072(4) Uani 1 1 d D U . . .
 H12_9 H 0.543934 0.835222 1.015739 0.087 Uiso 1 1 calc R U . . .
 C13_9 C 0.5563(4) 0.9008(5) 0.9876(10) 0.066(4) Uani 1 1 d D U . . .
 H13_9 H 0.590239 0.915506 0.988385 0.079 Uiso 1 1 calc R U . . .
 C14_9 C 0.5349(3) 0.9278(4) 0.9633(10) 0.059(3) Uani 1 1 d D U . . .
 C15_9 C 0.5616(4) 0.9762(4) 0.9362(11) 0.072(4) Uani 1 1 d D U . . .
 H15_9 H 0.595562 0.991845 0.936553 0.086 Uiso 1 1 calc R U . . .
 C16_9 C 0.5398(4) 1.0012(5) 0.9095(12) 0.078(5) Uani 1 1 d D U . . .
 H16_9 H 0.558161 1.034543 0.897882 0.094 Uiso 1 1 calc R U . . .
 C17_9 C 0.4887(4) 0.9758(4) 0.8995(11) 0.065(4) Uani 1 1 d D U . . .
 C18_9 C 0.4844(3) 0.9050(4) 0.9648(8) 0.043(3) Uani 1 1 d D U . . .
 C19_9 C 0.4579(3) 0.8614(4) 1.0083(9) 0.048(3) Uani 1 1 d D U . . .
 C20_9 C 0.4179(4) 0.9501(3) 0.8507(10) 0.054(3) Uani 1 1 d D U . . .
 C21_9 C 0.3771(4) 0.9452(4) 0.8100(10) 0.060(3) Uani 1 1 d D U . . .
 H21_9 H 0.377223 0.972153 0.785112 0.073 Uiso 1 1 calc R U . . .
 C22_9 C 0.3371(4) 0.9010(4) 0.8067(9) 0.055(3) Uani 1 1 d D U . . .
 H22_9 H 0.307974 0.897324 0.785004 0.065 Uiso 1 1 calc R U . . .
 C23_9 C 0.3393(3) 0.8605(3) 0.8357(8) 0.044(3) Uani 1 1 d D U . . .
 C24_9 C 0.3785(3) 0.8641(3) 0.8774(8) 0.040(3) Uani 1 1 d D U . . .
 H24_9 H 0.378995 0.836679 0.898022 0.048 Uiso 1 1 calc R U . . .
 C25_9 C 0.4174(3) 0.9101(3) 0.8877(8) 0.040(3) Uani 1 1 d D U . . .
 C26_9 C 0.2958(4) 0.8139(4) 0.8275(7) 0.062(4) Uani 1 1 d D U . . .


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 F1_1 C1_1 1.306(11) . ?
 F2_1 C1_1 1.340(11) . ?
 F3_1 C1_1 1.354(10) . ?
 F4_1 C26_1 1.334(9) . ?
 F5_1 C26_1 1.331(10) . ?
 F6_1 C26_1 1.352(9) . ?
 N1_1 C5_1 1.375(10) . ?
 N1_1 C8_1 1.292(11) . ?
 N2_1 C4_1 1.406(9) . ?
 N2_1 C8_1 1.409(10) . ?
 N2_1 C19_1 1.394(9) . ?
 N3_1 C17_1 1.334(11) . ?
 N3_1 C20_1 1.376(10) . ?
 N4_1 C17_1 1.403(10) . ?
 N4_1 C18_1 1.403(9) . ?
 N4_1 C25_1 1.403(9) . ?
 C1_1 C2_1 1.486(11) . ?
 C2_1 C3_1 1.394(10) . ?
 C2_1 C7_1 1.398(11) . ?
 C3_1 H3_1 0.9500 . ?
 C3_1 C4_1 1.375(10) . ?
 C4_1 C5_1 1.413(10) . ?
 C5_1 C6_1 1.384(11) . ?
 C6_1 H6_1 0.9500 . ?
 C6_1 C7_1 1.374(12) . ?
 C7_1 H7_1 0.9500 . ?
 C8_1 C9_1 1.427(11) . ?
 C9_1 H9_1 0.9500 . ?
 C9_1 C10_1 1.340(12) . ?
 C10_1 H10_1 0.9500 . ?
 C10_1 C11_1 1.428(12) . ?
 C11_1 C12_1 1.388(12) . ?
 C11_1 C19_1 1.432(10) . ?
 C12_1 H12_1 0.9500 . ?
 C12_1 C13_1 1.349(12) . ?
 C13_1 H13_1 0.9500 . ?
 C13_1 C14_1 1.408(11) . ?
 C14_1 C15_1 1.418(12) . ?
 C14_1 C18_1 1.415(10) . ?
 C15_1 H15_1 0.9500 . ?
 C15_1 C16_1 1.369(12) . ?
 C16_1 H16_1 0.9500 . ?
 C16_1 C17_1 1.435(11) . ?
 C18_1 C19_1 1.406(10) . ?
 C20_1 C21_1 1.405(10) . ?
 C20_1 C25_1 1.406(10) . ?
 C21_1 H21_1 0.9500 . ?
 C21_1 C22_1 1.368(10) . ?
 C22_1 H22_1 0.9500 . ?
 C22_1 C23_1 1.411(10) . ?
 C23_1 C24_1 1.382(9) . ?
 C23_1 C26_1 1.468(10) . ?
 C24_1 H24_1 0.9500 . ?
 C24_1 C25_1 1.391(10) . ?
 F1_2 C1_2 1.305(11) . ?
 F2_2 C1_2 1.355(11) . ?
 F3_2 C1_2 1.357(10) . ?
 F4_2 C26_2 1.338(10) . ?
 F5_2 C26_2 1.332(10) . ?
 F6_2 C26_2 1.362(10) . ?
 N1_2 C5_2 1.374(11) . ?
 N1_2 C8_2 1.298(11) . ?
 N2_2 C4_2 1.403(10) . ?
 N2_2 C8_2 1.421(10) . ?
 N2_2 C19_2 1.388(10) . ?
 N3_2 C17_2 1.333(10) . ?
 N3_2 C20_2 1.367(10) . ?
 N4_2 C17_2 1.410(10) . ?
 N4_2 C18_2 1.401(9) . ?
 N4_2 C25_2 1.405(9) . ?
 C1_2 C2_2 1.493(11) . ?
 C2_2 C3_2 1.388(10) . ?
 C2_2 C7_2 1.419(11) . ?
 C3_2 H3_2 0.9500 . ?
 C3_2 C4_2 1.373(10) . ?
 C4_2 C5_2 1.414(11) . ?
 C5_2 C6_2 1.389(11) . ?
 C6_2 H6_2 0.9500 . ?
 C6_2 C7_2 1.361(12) . ?
 C7_2 H7_2 0.9500 . ?
 C8_2 C9_2 1.432(12) . ?
 C9_2 H9_2 0.9500 . ?
 C9_2 C10_2 1.337(13) . ?
 C10_2 H10_2 0.9500 . ?
 C10_2 C11_2 1.425(13) . ?
 C11_2 C12_2 1.389(12) . ?
 C11_2 C19_2 1.432(11) . ?
 C12_2 H12_2 0.9500 . ?
 C12_2 C13_2 1.348(13) . ?
 C13_2 H13_2 0.9500 . ?
 C13_2 C14_2 1.408(12) . ?
 C14_2 C15_2 1.421(12) . ?
 C14_2 C18_2 1.413(11) . ?
 C15_2 H15_2 0.9500 . ?
 C15_2 C16_2 1.364(12) . ?
 C16_2 H16_2 0.9500 . ?
 C16_2 C17_2 1.431(11) . ?
 C18_2 C19_2 1.400(11) . ?
 C20_2 C21_2 1.408(10) . ?
 C20_2 C25_2 1.400(10) . ?
 C21_2 H21_2 0.9500 . ?
 C21_2 C22_2 1.366(10) . ?
 C22_2 H22_2 0.9500 . ?
 C22_2 C23_2 1.407(10) . ?
 C23_2 C24_2 1.389(10) . ?
 C23_2 C26_2 1.466(10) . ?
 C24_2 H24_2 0.9500 . ?
 C24_2 C25_2 1.386(10) . ?
 F1_3 C1_3 1.307(11) . ?
 F2_3 C1_3 1.352(11) . ?
 F3_3 C1_3 1.354(11) . ?
 F4_3 C26_3 1.344(9) . ?
 F5_3 C26_3 1.321(10) . ?
 F6_3 C26_3 1.352(9) . ?
 N1_3 C5_3 1.371(11) . ?
 N1_3 C8_3 1.297(11) . ?
 N2_3 C4_3 1.400(10) . ?
 N2_3 C8_3 1.421(10) . ?
 N2_3 C19_3 1.385(10) . ?
 N3_3 C17_3 1.342(10) . ?
 N3_3 C20_3 1.373(10) . ?
 N4_3 C17_3 1.403(10) . ?
 N4_3 C18_3 1.402(9) . ?
 N4_3 C25_3 1.406(9) . ?
 C1_3 C2_3 1.498(11) . ?
 C2_3 C3_3 1.381(10) . ?
 C2_3 C7_3 1.417(11) . ?
 C3_3 H3_3 0.9500 . ?
 C3_3 C4_3 1.382(10) . ?
 C4_3 C5_3 1.415(10) . ?
 C5_3 C6_3 1.390(11) . ?
 C6_3 H6_3 0.9500 . ?
 C6_3 C7_3 1.373(12) . ?
 C7_3 H7_3 0.9500 . ?
 C8_3 C9_3 1.423(11) . ?
 C9_3 H9_3 0.9500 . ?
 C9_3 C10_3 1.338(13) . ?
 C10_3 H10_3 0.9500 . ?
 C10_3 C11_3 1.431(12) . ?
 C11_3 C12_3 1.397(12) . ?
 C11_3 C19_3 1.428(11) . ?
 C12_3 H12_3 0.9500 . ?
 C12_3 C13_3 1.348(13) . ?
 C13_3 H13_3 0.9500 . ?
 C13_3 C14_3 1.407(12) . ?
 C14_3 C15_3 1.418(12) . ?
 C14_3 C18_3 1.407(11) . ?
 C15_3 H15_3 0.9500 . ?
 C15_3 C16_3 1.372(12) . ?
 C16_3 H16_3 0.9500 . ?
 C16_3 C17_3 1.418(11) . ?
 C18_3 C19_3 1.406(11) . ?
 C20_3 C21_3 1.416(10) . ?
 C20_3 C25_3 1.398(10) . ?
 C21_3 H21_3 0.9500 . ?
 C21_3 C22_3 1.363(10) . ?
 C22_3 H22_3 0.9500 . ?
 C22_3 C23_3 1.408(9) . ?
 C23_3 C24_3 1.382(10) . ?
 C23_3 C26_3 1.463(9) . ?
 C24_3 H24_3 0.9500 . ?
 C24_3 C25_3 1.387(10) . ?
 F1_4 C1_4 1.304(10) . ?
 F2_4 C1_4 1.343(10) . ?
 F3_4 C1_4 1.340(10) . ?
 F4_4 C26_4 1.336(10) . ?
 F5_4 C26_4 1.323(11) . ?
 F6_4 C26_4 1.344(10) . ?
 N1_4 C5_4 1.387(10) . ?
 N1_4 C8_4 1.302(12) . ?
 N2_4 C4_4 1.401(9) . ?
 N2_4 C8_4 1.412(11) . ?
 N2_4 C19_4 1.397(10) . ?
 N3_4 C17_4 1.333(11) . ?
 N3_4 C20_4 1.379(10) . ?
 N4_4 C17_4 1.410(10) . ?
 N4_4 C18_4 1.395(10) . ?
 N4_4 C25_4 1.397(9) . ?
 C1_4 C2_4 1.500(10) . ?
 C2_4 C3_4 1.382(10) . ?
 C2_4 C7_4 1.411(11) . ?
 C3_4 H3_4 0.9500 . ?
 C3_4 C4_4 1.374(10) . ?
 C4_4 C5_4 1.414(11) . ?
 C5_4 C6_4 1.391(11) . ?
 C6_4 H6_4 0.9500 . ?
 C6_4 C7_4 1.382(11) . ?
 C7_4 H7_4 0.9500 . ?
 C8_4 C9_4 1.430(11) . ?
 C9_4 H9_4 0.9500 . ?
 C9_4 C10_4 1.339(13) . ?
 C10_4 H10_4 0.9500 . ?
 C10_4 C11_4 1.423(12) . ?
 C11_4 C12_4 1.394(12) . ?
 C11_4 C19_4 1.429(11) . ?
 C12_4 H12_4 0.9500 . ?
 C12_4 C13_4 1.349(13) . ?
 C13_4 H13_4 0.9500 . ?
 C13_4 C14_4 1.408(12) . ?
 C14_4 C15_4 1.422(12) . ?
 C14_4 C18_4 1.412(11) . ?
 C15_4 H15_4 0.9500 . ?
 C15_4 C16_4 1.367(12) . ?
 C16_4 H16_4 0.9500 . ?
 C16_4 C17_4 1.433(11) . ?
 C18_4 C19_4 1.401(11) . ?
 C20_4 C21_4 1.402(11) . ?
 C20_4 C25_4 1.401(10) . ?
 C21_4 H21_4 0.9500 . ?
 C21_4 C22_4 1.363(11) . ?
 C22_4 H22_4 0.9500 . ?
 C22_4 C23_4 1.404(10) . ?
 C23_4 C24_4 1.378(10) . ?
 C23_4 C26_4 1.470(10) . ?
 C24_4 H24_4 0.9500 . ?
 C24_4 C25_4 1.393(10) . ?
 F1_5 C1_5 1.301(11) . ?
 F2_5 C1_5 1.358(11) . ?
 F3_5 C1_5 1.345(10) . ?
 F4_5 C26_5 1.341(11) . ?
 F5_5 C26_5 1.320(11) . ?
 F6_5 C26_5 1.353(10) . ?
 N1_5 C5_5 1.375(10) . ?
 N1_5 C8_5 1.289(11) . ?
 N2_5 C4_5 1.396(9) . ?
 N2_5 C8_5 1.410(10) . ?
 N2_5 C19_5 1.388(10) . ?
 N3_5 C17_5 1.336(11) . ?
 N3_5 C20_5 1.378(11) . ?
 N4_5 C17_5 1.406(10) . ?
 N4_5 C18_5 1.398(10) . ?
 N4_5 C25_5 1.403(10) . ?
 C1_5 C2_5 1.490(11) . ?
 C2_5 C3_5 1.385(10) . ?
 C2_5 C7_5 1.415(11) . ?
 C3_5 H3_5 0.9500 . ?
 C3_5 C4_5 1.379(10) . ?
 C4_5 C5_5 1.418(10) . ?
 C5_5 C6_5 1.378(11) . ?
 C6_5 H6_5 0.9500 . ?
 C6_5 C7_5 1.366(11) . ?
 C7_5 H7_5 0.9500 . ?
 C8_5 C9_5 1.426(11) . ?
 C9_5 H9_5 0.9500 . ?
 C9_5 C10_5 1.333(13) . ?
 C10_5 H10_5 0.9500 . ?
 C10_5 C11_5 1.420(12) . ?
 C11_5 C12_5 1.393(12) . ?
 C11_5 C19_5 1.432(11) . ?
 C12_5 H12_5 0.9500 . ?
 C12_5 C13_5 1.346(13) . ?
 C13_5 H13_5 0.9500 . ?
 C13_5 C14_5 1.398(12) . ?
 C14_5 C15_5 1.415(12) . ?
 C14_5 C18_5 1.415(11) . ?
 C15_5 H15_5 0.9500 . ?
 C15_5 C16_5 1.369(13) . ?
 C16_5 H16_5 0.9500 . ?
 C16_5 C17_5 1.439(11) . ?
 C18_5 C19_5 1.396(11) . ?
 C20_5 C21_5 1.411(11) . ?
 C20_5 C25_5 1.403(11) . ?
 C21_5 H21_5 0.9500 . ?
 C21_5 C22_5 1.377(11) . ?
 C22_5 H22_5 0.9500 . ?
 C22_5 C23_5 1.408(11) . ?
 C23_5 C24_5 1.383(10) . ?
 C23_5 C26_5 1.464(10) . ?
 C24_5 H24_5 0.9500 . ?
 C24_5 C25_5 1.399(10) . ?
 F1_6 C1_6 1.319(11) . ?
 F2_6 C1_6 1.351(10) . ?
 F3_6 C1_6 1.344(10) . ?
 F4_6 C26_6 1.341(10) . ?
 F5_6 C26_6 1.332(11) . ?
 F6_6 C26_6 1.347(10) . ?
 N1_6 C5_6 1.375(11) . ?
 N1_6 C8_6 1.294(12) . ?
 N2_6 C4_6 1.399(10) . ?
 N2_6 C8_6 1.420(11) . ?
 N2_6 C19_6 1.387(10) . ?
 N3_6 C17_6 1.340(11) . ?
 N3_6 C20_6 1.372(10) . ?
 N4_6 C17_6 1.409(10) . ?
 N4_6 C18_6 1.396(10) . ?
 N4_6 C25_6 1.399(9) . ?
 C1_6 C2_6 1.488(10) . ?
 C2_6 C3_6 1.383(10) . ?
 C2_6 C7_6 1.414(11) . ?
 C3_6 H3_6 0.9500 . ?
 C3_6 C4_6 1.379(10) . ?
 C4_6 C5_6 1.413(11) . ?
 C5_6 C6_6 1.383(12) . ?
 C6_6 H6_6 0.9500 . ?
 C6_6 C7_6 1.366(12) . ?
 C7_6 H7_6 0.9500 . ?
 C8_6 C9_6 1.423(11) . ?
 C9_6 H9_6 0.9500 . ?
 C9_6 C10_6 1.329(13) . ?
 C10_6 H10_6 0.9500 . ?
 C10_6 C11_6 1.427(12) . ?
 C11_6 C12_6 1.384(12) . ?
 C11_6 C19_6 1.433(11) . ?
 C12_6 H12_6 0.9500 . ?
 C12_6 C13_6 1.346(13) . ?
 C13_6 H13_6 0.9500 . ?
 C13_6 C14_6 1.407(12) . ?
 C14_6 C15_6 1.421(12) . ?
 C14_6 C18_6 1.419(11) . ?
 C15_6 H15_6 0.9500 . ?
 C15_6 C16_6 1.374(13) . ?
 C16_6 H16_6 0.9500 . ?
 C16_6 C17_6 1.438(11) . ?
 C18_6 C19_6 1.404(11) . ?
 C20_6 C21_6 1.411(10) . ?
 C20_6 C25_6 1.408(10) . ?
 C21_6 H21_6 0.9500 . ?
 C21_6 C22_6 1.372(11) . ?
 C22_6 H22_6 0.9500 . ?
 C22_6 C23_6 1.411(10) . ?
 C23_6 C24_6 1.376(10) . ?
 C23_6 C26_6 1.475(10) . ?
 C24_6 H24_6 0.9500 . ?
 C24_6 C25_6 1.391(10) . ?
 F1_7 C1_7 1.314(11) . ?
 F2_7 C1_7 1.352(11) . ?
 F3_7 C1_7 1.353(10) . ?
 F4_7 C26_7 1.333(10) . ?
 F5_7 C26_7 1.326(10) . ?
 F6_7 C26_7 1.353(10) . ?
 N1_7 C5_7 1.386(10) . ?
 N1_7 C8_7 1.293(11) . ?
 N2_7 C4_7 1.411(10) . ?
 N2_7 C8_7 1.409(11) . ?
 N2_7 C19_7 1.398(10) . ?
 N3_7 C17_7 1.327(11) . ?
 N3_7 C20_7 1.380(10) . ?
 N4_7 C17_7 1.407(10) . ?
 N4_7 C18_7 1.387(10) . ?
 N4_7 C25_7 1.403(9) . ?
 C1_7 C2_7 1.490(11) . ?
 C2_7 C3_7 1.390(10) . ?
 C2_7 C7_7 1.415(11) . ?
 C3_7 H3_7 0.9500 . ?
 C3_7 C4_7 1.372(10) . ?
 C4_7 C5_7 1.410(11) . ?
 C5_7 C6_7 1.391(11) . ?
 C6_7 H6_7 0.9500 . ?
 C6_7 C7_7 1.375(12) . ?
 C7_7 H7_7 0.9500 . ?
 C8_7 C9_7 1.430(11) . ?
 C9_7 H9_7 0.9500 . ?
 C9_7 C10_7 1.338(13) . ?
 C10_7 H10_7 0.9500 . ?
 C10_7 C11_7 1.429(13) . ?
 C11_7 C12_7 1.398(12) . ?
 C11_7 C19_7 1.428(11) . ?
 C12_7 H12_7 0.9500 . ?
 C12_7 C13_7 1.349(13) . ?
 C13_7 H13_7 0.9500 . ?
 C13_7 C14_7 1.399(12) . ?
 C14_7 C15_7 1.414(12) . ?
 C14_7 C18_7 1.418(11) . ?
 C15_7 H15_7 0.9500 . ?
 C15_7 C16_7 1.369(13) . ?
 C16_7 H16_7 0.9500 . ?
 C16_7 C17_7 1.437(11) . ?
 C18_7 C19_7 1.397(11) . ?
 C20_7 C21_7 1.412(10) . ?
 C20_7 C25_7 1.402(11) . ?
 C21_7 H21_7 0.9500 . ?
 C21_7 C22_7 1.375(11) . ?
 C22_7 H22_7 0.9500 . ?
 C22_7 C23_7 1.414(10) . ?
 C23_7 C24_7 1.386(10) . ?
 C23_7 C26_7 1.471(10) . ?
 C24_7 H24_7 0.9500 . ?
 C24_7 C25_7 1.397(10) . ?
 F1_8 C1_8 1.309(11) . ?
 F2_8 C1_8 1.342(11) . ?
 F3_8 C1_8 1.345(10) . ?
 F4_8 C26_8 1.334(10) . ?
 F5_8 C26_8 1.334(11) . ?
 F6_8 C26_8 1.343(10) . ?
 N1_8 C5_8 1.376(11) . ?
 N1_8 C8_8 1.299(11) . ?
 N2_8 C4_8 1.399(9) . ?
 N2_8 C8_8 1.409(11) . ?
 N2_8 C19_8 1.397(10) . ?
 N3_8 C17_8 1.335(11) . ?
 N3_8 C20_8 1.375(10) . ?
 N4_8 C17_8 1.407(11) . ?
 N4_8 C18_8 1.396(10) . ?
 N4_8 C25_8 1.400(9) . ?
 C1_8 C2_8 1.492(11) . ?
 C2_8 C3_8 1.396(10) . ?
 C2_8 C7_8 1.409(11) . ?
 C3_8 H3_8 0.9500 . ?
 C3_8 C4_8 1.372(10) . ?
 C4_8 C5_8 1.412(11) . ?
 C5_8 C6_8 1.388(11) . ?
 C6_8 H6_8 0.9500 . ?
 C6_8 C7_8 1.374(12) . ?
 C7_8 H7_8 0.9500 . ?
 C8_8 C9_8 1.433(11) . ?
 C9_8 H9_8 0.9500 . ?
 C9_8 C10_8 1.340(13) . ?
 C10_8 H10_8 0.9500 . ?
 C10_8 C11_8 1.421(13) . ?
 C11_8 C12_8 1.396(12) . ?
 C11_8 C19_8 1.430(11) . ?
 C12_8 H12_8 0.9500 . ?
 C12_8 C13_8 1.352(13) . ?
 C13_8 H13_8 0.9500 . ?
 C13_8 C14_8 1.399(12) . ?
 C14_8 C15_8 1.415(12) . ?
 C14_8 C18_8 1.422(11) . ?
 C15_8 H15_8 0.9500 . ?
 C15_8 C16_8 1.371(13) . ?
 C16_8 H16_8 0.9500 . ?
 C16_8 C17_8 1.434(11) . ?
 C18_8 C19_8 1.400(11) . ?
 C20_8 C21_8 1.406(11) . ?
 C20_8 C25_8 1.400(10) . ?
 C21_8 H21_8 0.9500 . ?
 C21_8 C22_8 1.364(11) . ?
 C22_8 H22_8 0.9500 . ?
 C22_8 C23_8 1.410(10) . ?
 C23_8 C24_8 1.387(10) . ?
 C23_8 C26_8 1.468(10) . ?
 C24_8 H24_8 0.9500 . ?
 C24_8 C25_8 1.393(10) . ?
 F1_9 C1_9 1.312(11) . ?
 F2_9 C1_9 1.349(11) . ?
 F3_9 C1_9 1.343(10) . ?
 F4_9 C26_9 1.332(10) . ?
 F5_9 C26_9 1.332(10) . ?
 F6_9 C26_9 1.356(10) . ?
 N1_9 C5_9 1.370(10) . ?
 N1_9 C8_9 1.297(11) . ?
 N2_9 C4_9 1.408(9) . ?
 N2_9 C8_9 1.413(10) . ?
 N2_9 C19_9 1.397(9) . ?
 N3_9 C17_9 1.332(11) . ?
 N3_9 C20_9 1.373(10) . ?
 N4_9 C17_9 1.411(10) . ?
 N4_9 C18_9 1.386(9) . ?
 N4_9 C25_9 1.395(9) . ?
 C1_9 C2_9 1.488(11) . ?
 C2_9 C3_9 1.392(10) . ?
 C2_9 C7_9 1.410(11) . ?
 C3_9 H3_9 0.9500 . ?
 C3_9 C4_9 1.382(10) . ?
 C4_9 C5_9 1.414(10) . ?
 C5_9 C6_9 1.388(11) . ?
 C6_9 H6_9 0.9500 . ?
 C6_9 C7_9 1.370(11) . ?
 C7_9 H7_9 0.9500 . ?
 C8_9 C9_9 1.425(11) . ?
 C9_9 H9_9 0.9500 . ?
 C9_9 C10_9 1.342(12) . ?
 C10_9 H10_9 0.9500 . ?
 C10_9 C11_9 1.431(12) . ?
 C11_9 C12_9 1.396(12) . ?
 C11_9 C19_9 1.419(10) . ?
 C12_9 H12_9 0.9500 . ?
 C12_9 C13_9 1.350(13) . ?
 C13_9 H13_9 0.9500 . ?
 C13_9 C14_9 1.407(12) . ?
 C14_9 C15_9 1.420(12) . ?
 C14_9 C18_9 1.410(10) . ?
 C15_9 H15_9 0.9500 . ?
 C15_9 C16_9 1.370(12) . ?
 C16_9 H16_9 0.9500 . ?
 C16_9 C17_9 1.435(11) . ?
 C18_9 C19_9 1.404(10) . ?
 C20_9 C21_9 1.400(11) . ?
 C20_9 C25_9 1.404(10) . ?
 C21_9 H21_9 0.9500 . ?
 C21_9 C22_9 1.362(11) . ?
 C22_9 H22_9 0.9500 . ?
 C22_9 C23_9 1.416(10) . ?
 C23_9 C24_9 1.375(10) . ?
 C23_9 C26_9 1.461(10) . ?
 C24_9 H24_9 0.9500 . ?
 C24_9 C25_9 1.391(10) . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 C8_1 N1_1 C5_1 105.0(8) . . ?
 C4_1 N2_1 C8_1 104.6(7) . . ?
 C19_1 N2_1 C4_1 130.7(7) . . ?
 C19_1 N2_1 C8_1 124.4(7) . . ?
 C17_1 N3_1 C20_1 105.0(8) . . ?
 C18_1 N4_1 C17_1 122.0(8) . . ?
 C25_1 N4_1 C17_1 105.7(7) . . ?
 C25_1 N4_1 C18_1 132.3(8) . . ?
 F1_1 C1_1 F2_1 107.2(12) . . ?
 F1_1 C1_1 F3_1 106.8(10) . . ?
 F1_1 C1_1 C2_1 113.7(11) . . ?
 F2_1 C1_1 F3_1 102.2(10) . . ?
 F2_1 C1_1 C2_1 113.4(9) . . ?
 F3_1 C1_1 C2_1 112.7(10) . . ?
 C3_1 C2_1 C1_1 118.5(9) . . ?
 C3_1 C2_1 C7_1 121.7(9) . . ?
 C7_1 C2_1 C1_1 119.8(9) . . ?
 C2_1 C3_1 H3_1 121.6 . . ?
 C4_1 C3_1 C2_1 116.9(9) . . ?
 C4_1 C3_1 H3_1 121.6 . . ?
 N2_1 C4_1 C5_1 104.2(7) . . ?
 C3_1 C4_1 N2_1 134.3(8) . . ?
 C3_1 C4_1 C5_1 121.4(8) . . ?
 N1_1 C5_1 C4_1 111.5(8) . . ?
 N1_1 C5_1 C6_1 127.7(9) . . ?
 C6_1 C5_1 C4_1 120.8(9) . . ?
 C5_1 C6_1 H6_1 121.1 . . ?
 C7_1 C6_1 C5_1 117.9(10) . . ?
 C7_1 C6_1 H6_1 121.1 . . ?
 C2_1 C7_1 H7_1 119.5 . . ?
 C6_1 C7_1 C2_1 121.1(10) . . ?
 C6_1 C7_1 H7_1 119.5 . . ?
 N1_1 C8_1 N2_1 114.1(8) . . ?
 N1_1 C8_1 C9_1 128.6(9) . . ?
 N2_1 C8_1 C9_1 117.3(8) . . ?
 C8_1 C9_1 H9_1 121.0 . . ?
 C10_1 C9_1 C8_1 118.0(9) . . ?
 C10_1 C9_1 H9_1 121.0 . . ?
 C9_1 C10_1 H10_1 118.3 . . ?
 C9_1 C10_1 C11_1 123.4(9) . . ?
 C11_1 C10_1 H10_1 118.3 . . ?
 C10_1 C11_1 C19_1 118.6(8) . . ?
 C12_1 C11_1 C10_1 124.3(9) . . ?
 C12_1 C11_1 C19_1 117.1(9) . . ?
 C11_1 C12_1 H12_1 118.9 . . ?
 C13_1 C12_1 C11_1 122.2(10) . . ?
 C13_1 C12_1 H12_1 118.9 . . ?
 C12_1 C13_1 H13_1 119.6 . . ?
 C12_1 C13_1 C14_1 120.9(10) . . ?
 C14_1 C13_1 H13_1 119.6 . . ?
 C13_1 C14_1 C15_1 122.8(9) . . ?
 C13_1 C14_1 C18_1 118.2(9) . . ?
 C18_1 C14_1 C15_1 119.0(9) . . ?
 C14_1 C15_1 H15_1 118.4 . . ?
 C16_1 C15_1 C14_1 123.1(10) . . ?
 C16_1 C15_1 H15_1 118.4 . . ?
 C15_1 C16_1 H16_1 121.2 . . ?
 C15_1 C16_1 C17_1 117.6(10) . . ?
 C17_1 C16_1 H16_1 121.2 . . ?
 N3_1 C17_1 N4_1 112.6(8) . . ?
 N3_1 C17_1 C16_1 126.9(9) . . ?
 N4_1 C17_1 C16_1 118.8(9) . . ?
 N4_1 C18_1 C14_1 116.5(8) . . ?
 N4_1 C18_1 C19_1 125.4(7) . . ?
 C19_1 C18_1 C14_1 118.0(8) . . ?
 N2_1 C19_1 C11_1 114.8(8) . . ?
 N2_1 C19_1 C18_1 125.9(7) . . ?
 C18_1 C19_1 C11_1 119.2(8) . . ?
 N3_1 C20_1 C21_1 129.0(8) . . ?
 N3_1 C20_1 C25_1 111.4(8) . . ?
 C21_1 C20_1 C25_1 119.5(8) . . ?
 C20_1 C21_1 H21_1 121.0 . . ?
 C22_1 C21_1 C20_1 118.1(8) . . ?
 C22_1 C21_1 H21_1 121.0 . . ?
 C21_1 C22_1 H22_1 119.4 . . ?
 C21_1 C22_1 C23_1 121.2(8) . . ?
 C23_1 C22_1 H22_1 119.4 . . ?
 C22_1 C23_1 C26_1 117.7(7) . . ?
 C24_1 C23_1 C22_1 122.3(8) . . ?
 C24_1 C23_1 C26_1 120.0(7) . . ?
 C23_1 C24_1 H24_1 122.1 . . ?
 C23_1 C24_1 C25_1 115.8(8) . . ?
 C25_1 C24_1 H24_1 122.1 . . ?
 N4_1 C25_1 C20_1 105.2(7) . . ?
 C24_1 C25_1 N4_1 131.8(8) . . ?
 C24_1 C25_1 C20_1 123.0(7) . . ?
 F4_1 C26_1 F6_1 104.5(8) . . ?
 F4_1 C26_1 C23_1 113.5(8) . . ?
 F5_1 C26_1 F4_1 104.9(8) . . ?
 F5_1 C26_1 F6_1 103.3(8) . . ?
 F5_1 C26_1 C23_1 115.2(9) . . ?
 F6_1 C26_1 C23_1 114.3(7) . . ?
 C8_2 N1_2 C5_2 106.5(9) . . ?
 C4_2 N2_2 C8_2 106.0(8) . . ?
 C19_2 N2_2 C4_2 131.4(8) . . ?
 C19_2 N2_2 C8_2 122.6(8) . . ?
 C17_2 N3_2 C20_2 104.2(8) . . ?
 C18_2 N4_2 C17_2 122.3(8) . . ?
 C18_2 N4_2 C25_2 133.9(8) . . ?
 C25_2 N4_2 C17_2 103.8(7) . . ?
 F1_2 C1_2 F2_2 109.2(11) . . ?
 F1_2 C1_2 F3_2 106.6(10) . . ?
 F1_2 C1_2 C2_2 112.2(10) . . ?
 F2_2 C1_2 F3_2 101.3(10) . . ?
 F2_2 C1_2 C2_2 113.8(9) . . ?
 F3_2 C1_2 C2_2 113.1(10) . . ?
 C3_2 C2_2 C1_2 119.0(9) . . ?
 C3_2 C2_2 C7_2 120.8(9) . . ?
 C7_2 C2_2 C1_2 120.0(9) . . ?
 C2_2 C3_2 H3_2 121.0 . . ?
 C4_2 C3_2 C2_2 118.0(9) . . ?
 C4_2 C3_2 H3_2 121.0 . . ?
 N2_2 C4_2 C5_2 104.0(8) . . ?
 C3_2 C4_2 N2_2 134.3(9) . . ?
 C3_2 C4_2 C5_2 121.6(9) . . ?
 N1_2 C5_2 C4_2 110.4(9) . . ?
 N1_2 C5_2 C6_2 129.0(10) . . ?
 C6_2 C5_2 C4_2 119.4(9) . . ?
 C5_2 C6_2 H6_2 120.3 . . ?
 C7_2 C6_2 C5_2 119.5(10) . . ?
 C7_2 C6_2 H6_2 120.3 . . ?
 C2_2 C7_2 H7_2 119.9 . . ?
 C6_2 C7_2 C2_2 120.2(11) . . ?
 C6_2 C7_2 H7_2 119.9 . . ?
 N1_2 C8_2 N2_2 111.6(9) . . ?
 N1_2 C8_2 C9_2 128.7(11) . . ?
 N2_2 C8_2 C9_2 117.5(10) . . ?
 C8_2 C9_2 H9_2 120.6 . . ?
 C10_2 C9_2 C8_2 118.9(12) . . ?
 C10_2 C9_2 H9_2 120.6 . . ?
 C9_2 C10_2 H10_2 118.4 . . ?
 C9_2 C10_2 C11_2 123.3(12) . . ?
 C11_2 C10_2 H10_2 118.4 . . ?
 C10_2 C11_2 C19_2 118.6(10) . . ?
 C12_2 C11_2 C10_2 124.3(11) . . ?
 C12_2 C11_2 C19_2 117.1(10) . . ?
 C11_2 C12_2 H12_2 119.0 . . ?
 C13_2 C12_2 C11_2 122.0(12) . . ?
 C13_2 C12_2 H12_2 119.0 . . ?
 C12_2 C13_2 H13_2 119.4 . . ?
 C12_2 C13_2 C14_2 121.1(12) . . ?
 C14_2 C13_2 H13_2 119.4 . . ?
 C13_2 C14_2 C15_2 124.3(11) . . ?
 C13_2 C14_2 C18_2 118.4(11) . . ?
 C18_2 C14_2 C15_2 117.3(9) . . ?
 C14_2 C15_2 H15_2 117.8 . . ?
 C16_2 C15_2 C14_2 124.4(10) . . ?
 C16_2 C15_2 H15_2 117.8 . . ?
 C15_2 C16_2 H16_2 121.2 . . ?
 C15_2 C16_2 C17_2 117.7(10) . . ?
 C17_2 C16_2 H16_2 121.2 . . ?
 N3_2 C17_2 N4_2 113.8(7) . . ?
 N3_2 C17_2 C16_2 127.5(9) . . ?
 N4_2 C17_2 C16_2 118.1(9) . . ?
 N4_2 C18_2 C14_2 117.2(9) . . ?
 C19_2 C18_2 N4_2 124.4(9) . . ?
 C19_2 C18_2 C14_2 118.5(9) . . ?
 N2_2 C19_2 C11_2 115.6(9) . . ?
 N2_2 C19_2 C18_2 125.5(9) . . ?
 C18_2 C19_2 C11_2 118.7(10) . . ?
 N3_2 C20_2 C21_2 128.8(9) . . ?
 N3_2 C20_2 C25_2 111.8(8) . . ?
 C25_2 C20_2 C21_2 119.2(8) . . ?
 C20_2 C21_2 H21_2 120.8 . . ?
 C22_2 C21_2 C20_2 118.3(9) . . ?
 C22_2 C21_2 H21_2 120.8 . . ?
 C21_2 C22_2 H22_2 119.4 . . ?
 C21_2 C22_2 C23_2 121.3(9) . . ?
 C23_2 C22_2 H22_2 119.4 . . ?
 C22_2 C23_2 C26_2 118.3(8) . . ?
 C24_2 C23_2 C22_2 121.7(8) . . ?
 C24_2 C23_2 C26_2 119.7(8) . . ?
 C23_2 C24_2 H24_2 121.9 . . ?
 C25_2 C24_2 C23_2 116.1(8) . . ?
 C25_2 C24_2 H24_2 121.9 . . ?
 C20_2 C25_2 N4_2 106.0(7) . . ?
 C24_2 C25_2 N4_2 130.8(8) . . ?
 C24_2 C25_2 C20_2 123.2(8) . . ?
 F4_2 C26_2 F6_2 105.9(8) . . ?
 F4_2 C26_2 C23_2 115.4(8) . . ?
 F5_2 C26_2 F4_2 103.1(9) . . ?
 F5_2 C26_2 F6_2 102.2(9) . . ?
 F5_2 C26_2 C23_2 114.9(9) . . ?
 F6_2 C26_2 C23_2 113.9(8) . . ?
 C8_3 N1_3 C5_3 105.9(9) . . ?
 C4_3 N2_3 C8_3 104.6(7) . . ?
 C19_3 N2_3 C4_3 132.4(8) . . ?
 C19_3 N2_3 C8_3 122.8(8) . . ?
 C17_3 N3_3 C20_3 104.9(8) . . ?
 C17_3 N4_3 C25_3 106.2(7) . . ?
 C18_3 N4_3 C17_3 120.0(7) . . ?
 C18_3 N4_3 C25_3 133.7(8) . . ?
 F1_3 C1_3 F2_3 105.7(11) . . ?
 F1_3 C1_3 F3_3 107.5(11) . . ?
 F1_3 C1_3 C2_3 113.3(11) . . ?
 F2_3 C1_3 F3_3 103.3(10) . . ?
 F2_3 C1_3 C2_3 114.8(9) . . ?
 F3_3 C1_3 C2_3 111.5(10) . . ?
 C3_3 C2_3 C1_3 118.3(8) . . ?
 C3_3 C2_3 C7_3 122.3(9) . . ?
 C7_3 C2_3 C1_3 119.4(9) . . ?
 C2_3 C3_3 H3_3 122.2 . . ?
 C2_3 C3_3 C4_3 115.7(9) . . ?
 C4_3 C3_3 H3_3 122.2 . . ?
 N2_3 C4_3 C5_3 104.9(7) . . ?
 C3_3 C4_3 N2_3 131.8(8) . . ?
 C3_3 C4_3 C5_3 123.2(8) . . ?
 N1_3 C5_3 C4_3 110.8(9) . . ?
 N1_3 C5_3 C6_3 129.1(9) . . ?
 C6_3 C5_3 C4_3 119.8(9) . . ?
 C5_3 C6_3 H6_3 121.0 . . ?
 C7_3 C6_3 C5_3 117.9(10) . . ?
 C7_3 C6_3 H6_3 121.0 . . ?
 C2_3 C7_3 H7_3 119.5 . . ?
 C6_3 C7_3 C2_3 121.1(10) . . ?
 C6_3 C7_3 H7_3 119.5 . . ?
 N1_3 C8_3 N2_3 113.1(9) . . ?
 N1_3 C8_3 C9_3 129.9(10) . . ?
 C9_3 C8_3 N2_3 116.5(9) . . ?
 C8_3 C9_3 H9_3 119.3 . . ?
 C10_3 C9_3 C8_3 121.3(11) . . ?
 C10_3 C9_3 H9_3 119.3 . . ?
 C9_3 C10_3 H10_3 119.1 . . ?
 C9_3 C10_3 C11_3 121.8(11) . . ?
 C11_3 C10_3 H10_3 119.1 . . ?
 C12_3 C11_3 C10_3 122.0(10) . . ?
 C12_3 C11_3 C19_3 119.5(10) . . ?
 C19_3 C11_3 C10_3 118.0(10) . . ?
 C11_3 C12_3 H12_3 120.2 . . ?
 C13_3 C12_3 C11_3 119.7(12) . . ?
 C13_3 C12_3 H12_3 120.1 . . ?
 C12_3 C13_3 H13_3 119.8 . . ?
 C12_3 C13_3 C14_3 120.5(11) . . ?
 C14_3 C13_3 H13_3 119.8 . . ?
 C13_3 C14_3 C15_3 121.5(10) . . ?
 C13_3 C14_3 C18_3 119.1(10) . . ?
 C18_3 C14_3 C15_3 118.4(9) . . ?
 C14_3 C15_3 H15_3 119.4 . . ?
 C16_3 C15_3 C14_3 121.1(10) . . ?
 C16_3 C15_3 H15_3 119.4 . . ?
 C15_3 C16_3 H16_3 120.5 . . ?
 C15_3 C16_3 C17_3 119.0(10) . . ?
 C17_3 C16_3 H16_3 120.5 . . ?
 N3_3 C17_3 N4_3 111.9(7) . . ?
 N3_3 C17_3 C16_3 128.1(9) . . ?
 N4_3 C17_3 C16_3 119.6(9) . . ?
 N4_3 C18_3 C14_3 117.2(8) . . ?
 N4_3 C18_3 C19_3 124.0(8) . . ?
 C19_3 C18_3 C14_3 118.7(8) . . ?
 N2_3 C19_3 C11_3 116.9(9) . . ?
 N2_3 C19_3 C18_3 125.3(8) . . ?
 C18_3 C19_3 C11_3 117.9(9) . . ?
 N3_3 C20_3 C21_3 129.0(8) . . ?
 N3_3 C20_3 C25_3 112.3(7) . . ?
 C25_3 C20_3 C21_3 118.6(7) . . ?
 C20_3 C21_3 H21_3 120.8 . . ?
 C22_3 C21_3 C20_3 118.4(8) . . ?
 C22_3 C21_3 H21_3 120.8 . . ?
 C21_3 C22_3 H22_3 119.1 . . ?
 C21_3 C22_3 C23_3 121.7(8) . . ?
 C23_3 C22_3 H22_3 119.1 . . ?
 C22_3 C23_3 C26_3 118.5(7) . . ?
 C24_3 C23_3 C22_3 121.2(7) . . ?
 C24_3 C23_3 C26_3 120.4(7) . . ?
 C23_3 C24_3 H24_3 121.6 . . ?
 C23_3 C24_3 C25_3 116.8(8) . . ?
 C25_3 C24_3 H24_3 121.6 . . ?
 C20_3 C25_3 N4_3 104.5(7) . . ?
 C24_3 C25_3 N4_3 132.2(8) . . ?
 C24_3 C25_3 C20_3 123.2(7) . . ?
 F4_3 C26_3 F6_3 105.2(8) . . ?
 F4_3 C26_3 C23_3 113.9(7) . . ?
 F5_3 C26_3 F4_3 103.2(8) . . ?
 F5_3 C26_3 F6_3 106.7(8) . . ?
 F5_3 C26_3 C23_3 114.4(8) . . ?
 F6_3 C26_3 C23_3 112.6(8) . . ?
 C8_4 N1_4 C5_4 105.6(10) . . ?
 C4_4 N2_4 C8_4 104.9(8) . . ?
 C19_4 N2_4 C4_4 130.8(9) . . ?
 C19_4 N2_4 C8_4 124.2(8) . . ?
 C17_4 N3_4 C20_4 103.4(8) . . ?
 C18_4 N4_4 C17_4 122.3(8) . . ?
 C18_4 N4_4 C25_4 131.7(9) . . ?
 C25_4 N4_4 C17_4 105.2(7) . . ?
 F1_4 C1_4 F2_4 108.4(10) . . ?
 F1_4 C1_4 F3_4 108.5(9) . . ?
 F1_4 C1_4 C2_4 113.5(9) . . ?
 F2_4 C1_4 C2_4 114.2(8) . . ?
 F3_4 C1_4 F2_4 101.5(8) . . ?
 F3_4 C1_4 C2_4 109.9(9) . . ?
 C3_4 C2_4 C1_4 118.0(8) . . ?
 C3_4 C2_4 C7_4 122.6(8) . . ?
 C7_4 C2_4 C1_4 119.5(8) . . ?
 C2_4 C3_4 H3_4 121.5 . . ?
 C4_4 C3_4 C2_4 116.9(9) . . ?
 C4_4 C3_4 H3_4 121.5 . . ?
 N2_4 C4_4 C5_4 105.3(7) . . ?
 C3_4 C4_4 N2_4 132.9(9) . . ?
 C3_4 C4_4 C5_4 121.7(8) . . ?
 N1_4 C5_4 C4_4 110.1(8) . . ?
 N1_4 C5_4 C6_4 129.8(10) . . ?
 C6_4 C5_4 C4_4 119.9(8) . . ?
 C5_4 C6_4 H6_4 120.6 . . ?
 C7_4 C6_4 C5_4 118.9(10) . . ?
 C7_4 C6_4 H6_4 120.6 . . ?
 C2_4 C7_4 H7_4 120.3 . . ?
 C6_4 C7_4 C2_4 119.5(10) . . ?
 C6_4 C7_4 H7_4 120.3 . . ?
 N1_4 C8_4 N2_4 112.7(9) . . ?
 N1_4 C8_4 C9_4 131.4(11) . . ?
 N2_4 C8_4 C9_4 115.9(10) . . ?
 C8_4 C9_4 H9_4 120.3 . . ?
 C10_4 C9_4 C8_4 119.5(12) . . ?
 C10_4 C9_4 H9_4 120.3 . . ?
 C9_4 C10_4 H10_4 117.7 . . ?
 C9_4 C10_4 C11_4 124.6(11) . . ?
 C11_4 C10_4 H10_4 117.7 . . ?
 C10_4 C11_4 C19_4 116.8(10) . . ?
 C12_4 C11_4 C10_4 124.3(10) . . ?
 C12_4 C11_4 C19_4 118.8(10) . . ?
 C11_4 C12_4 H12_4 119.1 . . ?
 C13_4 C12_4 C11_4 121.7(11) . . ?
 C13_4 C12_4 H12_4 119.1 . . ?
 C12_4 C13_4 H13_4 119.8 . . ?
 C12_4 C13_4 C14_4 120.3(12) . . ?
 C14_4 C13_4 H13_4 119.8 . . ?
 C13_4 C14_4 C15_4 121.9(11) . . ?
 C13_4 C14_4 C18_4 118.0(10) . . ?
 C18_4 C14_4 C15_4 119.0(10) . . ?
 C14_4 C15_4 H15_4 118.9 . . ?
 C16_4 C15_4 C14_4 122.2(11) . . ?
 C16_4 C15_4 H15_4 118.9 . . ?
 C15_4 C16_4 H16_4 120.9 . . ?
 C15_4 C16_4 C17_4 118.2(11) . . ?
 C17_4 C16_4 H16_4 120.9 . . ?
 N3_4 C17_4 N4_4 113.2(8) . . ?
 N3_4 C17_4 C16_4 128.0(9) . . ?
 N4_4 C17_4 C16_4 118.8(9) . . ?
 N4_4 C18_4 C14_4 116.7(9) . . ?
 N4_4 C18_4 C19_4 122.8(8) . . ?
 C19_4 C18_4 C14_4 120.4(9) . . ?
 N2_4 C19_4 C11_4 116.2(9) . . ?
 N2_4 C19_4 C18_4 126.9(8) . . ?
 C18_4 C19_4 C11_4 116.9(9) . . ?
 N3_4 C20_4 C21_4 128.3(9) . . ?
 N3_4 C20_4 C25_4 112.7(8) . . ?
 C25_4 C20_4 C21_4 118.7(8) . . ?
 C20_4 C21_4 H21_4 120.6 . . ?
 C22_4 C21_4 C20_4 118.9(10) . . ?
 C22_4 C21_4 H21_4 120.6 . . ?
 C21_4 C22_4 H22_4 120.0 . . ?
 C21_4 C22_4 C23_4 120.0(10) . . ?
 C23_4 C22_4 H22_4 120.0 . . ?
 C22_4 C23_4 C26_4 117.6(9) . . ?
 C24_4 C23_4 C22_4 123.7(9) . . ?
 C24_4 C23_4 C26_4 118.4(8) . . ?
 C23_4 C24_4 H24_4 122.7 . . ?
 C23_4 C24_4 C25_4 114.6(8) . . ?
 C25_4 C24_4 H24_4 122.7 . . ?
 N4_4 C25_4 C20_4 104.7(7) . . ?
 C24_4 C25_4 N4_4 131.8(8) . . ?
 C24_4 C25_4 C20_4 123.5(8) . . ?
 F4_4 C26_4 F6_4 104.1(10) . . ?
 F4_4 C26_4 C23_4 114.4(10) . . ?
 F5_4 C26_4 F4_4 104.1(10) . . ?
 F5_4 C26_4 F6_4 106.1(11) . . ?
 F5_4 C26_4 C23_4 113.4(10) . . ?
 F6_4 C26_4 C23_4 113.8(9) . . ?
 C8_5 N1_5 C5_5 104.8(9) . . ?
 C4_5 N2_5 C8_5 105.7(7) . . ?
 C19_5 N2_5 C4_5 131.6(8) . . ?
 C19_5 N2_5 C8_5 122.6(8) . . ?
 C17_5 N3_5 C20_5 105.1(9) . . ?
 C18_5 N4_5 C17_5 121.2(8) . . ?
 C18_5 N4_5 C25_5 134.3(9) . . ?
 C25_5 N4_5 C17_5 104.3(8) . . ?
 F1_5 C1_5 F2_5 105.5(11) . . ?
 F1_5 C1_5 F3_5 107.4(10) . . ?
 F1_5 C1_5 C2_5 115.6(10) . . ?
 F2_5 C1_5 C2_5 113.3(9) . . ?
 F3_5 C1_5 F2_5 104.2(10) . . ?
 F3_5 C1_5 C2_5 110.1(9) . . ?
 C3_5 C2_5 C1_5 118.2(8) . . ?
 C3_5 C2_5 C7_5 123.5(8) . . ?
 C7_5 C2_5 C1_5 118.3(9) . . ?
 C2_5 C3_5 H3_5 122.4 . . ?
 C4_5 C3_5 C2_5 115.2(8) . . ?
 C4_5 C3_5 H3_5 122.4 . . ?
 N2_5 C4_5 C5_5 103.5(7) . . ?
 C3_5 C4_5 N2_5 134.7(8) . . ?
 C3_5 C4_5 C5_5 121.6(8) . . ?
 N1_5 C5_5 C4_5 112.0(8) . . ?
 N1_5 C5_5 C6_5 126.2(9) . . ?
 C6_5 C5_5 C4_5 121.7(8) . . ?
 C5_5 C6_5 H6_5 121.2 . . ?
 C7_5 C6_5 C5_5 117.6(9) . . ?
 C7_5 C6_5 H6_5 121.2 . . ?
 C2_5 C7_5 H7_5 119.9 . . ?
 C6_5 C7_5 C2_5 120.1(9) . . ?
 C6_5 C7_5 H7_5 119.9 . . ?
 N1_5 C8_5 N2_5 113.8(8) . . ?
 N1_5 C8_5 C9_5 128.1(10) . . ?
 N2_5 C8_5 C9_5 118.0(9) . . ?
 C8_5 C9_5 H9_5 120.4 . . ?
 C10_5 C9_5 C8_5 119.1(11) . . ?
 C10_5 C9_5 H9_5 120.4 . . ?
 C9_5 C10_5 H10_5 118.5 . . ?
 C9_5 C10_5 C11_5 123.0(11) . . ?
 C11_5 C10_5 H10_5 118.5 . . ?
 C10_5 C11_5 C19_5 118.4(10) . . ?
 C12_5 C11_5 C10_5 122.7(10) . . ?
 C12_5 C11_5 C19_5 118.8(10) . . ?
 C11_5 C12_5 H12_5 119.8 . . ?
 C13_5 C12_5 C11_5 120.4(12) . . ?
 C13_5 C12_5 H12_5 119.8 . . ?
 C12_5 C13_5 H13_5 119.1 . . ?
 C12_5 C13_5 C14_5 121.8(11) . . ?
 C14_5 C13_5 H13_5 119.1 . . ?
 C13_5 C14_5 C15_5 122.2(11) . . ?
 C13_5 C14_5 C18_5 119.0(10) . . ?
 C15_5 C14_5 C18_5 118.7(10) . . ?
 C14_5 C15_5 H15_5 118.7 . . ?
 C16_5 C15_5 C14_5 122.6(12) . . ?
 C16_5 C15_5 H15_5 118.7 . . ?
 C15_5 C16_5 H16_5 121.2 . . ?
 C15_5 C16_5 C17_5 117.6(12) . . ?
 C17_5 C16_5 H16_5 121.2 . . ?
 N3_5 C17_5 N4_5 112.7(9) . . ?
 N3_5 C17_5 C16_5 127.9(10) . . ?
 N4_5 C17_5 C16_5 119.4(10) . . ?
 N4_5 C18_5 C14_5 117.5(9) . . ?
 C19_5 C18_5 N4_5 124.1(9) . . ?
 C19_5 C18_5 C14_5 118.4(9) . . ?
 N2_5 C19_5 C11_5 116.3(9) . . ?
 N2_5 C19_5 C18_5 125.3(9) . . ?
 C18_5 C19_5 C11_5 118.4(9) . . ?
 N3_5 C20_5 C21_5 131.7(11) . . ?
 N3_5 C20_5 C25_5 110.5(9) . . ?
 C25_5 C20_5 C21_5 117.8(9) . . ?
 C20_5 C21_5 H21_5 120.0 . . ?
 C22_5 C21_5 C20_5 120.0(11) . . ?
 C22_5 C21_5 H21_5 120.0 . . ?
 C21_5 C22_5 H22_5 119.7 . . ?
 C21_5 C22_5 C23_5 120.6(11) . . ?
 C23_5 C22_5 H22_5 119.7 . . ?
 C22_5 C23_5 C26_5 120.9(9) . . ?
 C24_5 C23_5 C22_5 120.7(9) . . ?
 C24_5 C23_5 C26_5 118.4(9) . . ?
 C23_5 C24_5 H24_5 121.0 . . ?
 C23_5 C24_5 C25_5 117.9(10) . . ?
 C25_5 C24_5 H24_5 121.0 . . ?
 N4_5 C25_5 C20_5 106.3(8) . . ?
 C24_5 C25_5 N4_5 131.3(10) . . ?
 C24_5 C25_5 C20_5 122.3(9) . . ?
 F4_5 C26_5 F6_5 99.4(10) . . ?
 F4_5 C26_5 C23_5 114.1(10) . . ?
 F5_5 C26_5 F4_5 102.2(10) . . ?
 F5_5 C26_5 F6_5 107.3(11) . . ?
 F5_5 C26_5 C23_5 116.7(11) . . ?
 F6_5 C26_5 C23_5 115.0(9) . . ?
 C8_6 N1_6 C5_6 104.5(9) . . ?
 C4_6 N2_6 C8_6 105.4(8) . . ?
 C19_6 N2_6 C4_6 131.9(8) . . ?
 C19_6 N2_6 C8_6 122.7(8) . . ?
 C17_6 N3_6 C20_6 105.1(8) . . ?
 C18_6 N4_6 C17_6 123.1(8) . . ?
 C18_6 N4_6 C25_6 131.8(8) . . ?
 C25_6 N4_6 C17_6 105.0(7) . . ?
 F1_6 C1_6 F2_6 107.4(9) . . ?
 F1_6 C1_6 F3_6 109.6(10) . . ?
 F1_6 C1_6 C2_6 112.4(10) . . ?
 F2_6 C1_6 C2_6 111.2(8) . . ?
 F3_6 C1_6 F2_6 104.3(9) . . ?
 F3_6 C1_6 C2_6 111.5(9) . . ?
 C3_6 C2_6 C1_6 119.6(8) . . ?
 C3_6 C2_6 C7_6 123.5(9) . . ?
 C7_6 C2_6 C1_6 116.9(9) . . ?
 C2_6 C3_6 H3_6 122.6 . . ?
 C4_6 C3_6 C2_6 114.7(9) . . ?
 C4_6 C3_6 H3_6 122.6 . . ?
 N2_6 C4_6 C5_6 103.7(8) . . ?
 C3_6 C4_6 N2_6 133.7(9) . . ?
 C3_6 C4_6 C5_6 122.0(9) . . ?
 N1_6 C5_6 C4_6 112.4(9) . . ?
 N1_6 C5_6 C6_6 126.0(10) . . ?
 C6_6 C5_6 C4_6 120.7(9) . . ?
 C5_6 C6_6 H6_6 121.3 . . ?
 C7_6 C6_6 C5_6 117.3(11) . . ?
 C7_6 C6_6 H6_6 121.4 . . ?
 C2_6 C7_6 H7_6 119.9 . . ?
 C6_6 C7_6 C2_6 120.3(10) . . ?
 C6_6 C7_6 H7_6 119.9 . . ?
 N1_6 C8_6 N2_6 113.5(9) . . ?
 N1_6 C8_6 C9_6 128.0(11) . . ?
 N2_6 C8_6 C9_6 118.3(10) . . ?
 C8_6 C9_6 H9_6 120.7 . . ?
 C10_6 C9_6 C8_6 118.6(12) . . ?
 C10_6 C9_6 H9_6 120.7 . . ?
 C9_6 C10_6 H10_6 118.3 . . ?
 C9_6 C10_6 C11_6 123.5(11) . . ?
 C11_6 C10_6 H10_6 118.3 . . ?
 C10_6 C11_6 C19_6 118.7(10) . . ?
 C12_6 C11_6 C10_6 124.4(11) . . ?
 C12_6 C11_6 C19_6 116.7(11) . . ?
 C11_6 C12_6 H12_6 118.8 . . ?
 C13_6 C12_6 C11_6 122.4(12) . . ?
 C13_6 C12_6 H12_6 118.8 . . ?
 C12_6 C13_6 H13_6 118.9 . . ?
 C12_6 C13_6 C14_6 122.1(12) . . ?
 C14_6 C13_6 H13_6 118.9 . . ?
 C13_6 C14_6 C15_6 125.5(11) . . ?
 C13_6 C14_6 C18_6 116.8(10) . . ?
 C15_6 C14_6 C18_6 117.7(10) . . ?
 C14_6 C15_6 H15_6 118.0 . . ?
 C16_6 C15_6 C14_6 124.1(11) . . ?
 C16_6 C15_6 H15_6 118.0 . . ?
 C15_6 C16_6 H16_6 121.1 . . ?
 C15_6 C16_6 C17_6 117.8(11) . . ?
 C17_6 C16_6 H16_6 121.1 . . ?
 N3_6 C17_6 N4_6 112.6(8) . . ?
 N3_6 C17_6 C16_6 128.2(11) . . ?
 N4_6 C17_6 C16_6 117.7(10) . . ?
 N4_6 C18_6 C14_6 117.1(9) . . ?
 N4_6 C18_6 C19_6 124.2(8) . . ?
 C19_6 C18_6 C14_6 118.7(9) . . ?
 N2_6 C19_6 C11_6 115.1(9) . . ?
 N2_6 C19_6 C18_6 125.2(8) . . ?
 C18_6 C19_6 C11_6 119.6(9) . . ?
 N3_6 C20_6 C21_6 130.1(9) . . ?
 N3_6 C20_6 C25_6 111.0(8) . . ?
 C25_6 C20_6 C21_6 118.4(8) . . ?
 C20_6 C21_6 H21_6 120.7 . . ?
 C22_6 C21_6 C20_6 118.5(9) . . ?
 C22_6 C21_6 H21_6 120.7 . . ?
 C21_6 C22_6 H22_6 119.2 . . ?
 C21_6 C22_6 C23_6 121.5(9) . . ?
 C23_6 C22_6 H22_6 119.2 . . ?
 C22_6 C23_6 C26_6 118.7(8) . . ?
 C24_6 C23_6 C22_6 121.4(8) . . ?
 C24_6 C23_6 C26_6 119.9(8) . . ?
 C23_6 C24_6 H24_6 121.6 . . ?
 C23_6 C24_6 C25_6 116.8(8) . . ?
 C25_6 C24_6 H24_6 121.6 . . ?
 N4_6 C25_6 C20_6 105.8(7) . . ?
 C24_6 C25_6 N4_6 130.9(8) . . ?
 C24_6 C25_6 C20_6 123.3(8) . . ?
 F4_6 C26_6 F6_6 104.5(9) . . ?
 F4_6 C26_6 C23_6 113.5(9) . . ?
 F5_6 C26_6 F4_6 103.2(9) . . ?
 F5_6 C26_6 F6_6 107.5(10) . . ?
 F5_6 C26_6 C23_6 113.9(10) . . ?
 F6_6 C26_6 C23_6 113.3(8) . . ?
 C8_7 N1_7 C5_7 105.7(9) . . ?
 C8_7 N2_7 C4_7 104.5(8) . . ?
 C19_7 N2_7 C4_7 131.4(9) . . ?
 C19_7 N2_7 C8_7 123.9(8) . . ?
 C17_7 N3_7 C20_7 104.0(8) . . ?
 C18_7 N4_7 C17_7 121.5(8) . . ?
 C18_7 N4_7 C25_7 133.5(9) . . ?
 C25_7 N4_7 C17_7 104.9(7) . . ?
 F1_7 C1_7 F2_7 105.2(10) . . ?
 F1_7 C1_7 F3_7 105.5(10) . . ?
 F1_7 C1_7 C2_7 114.3(10) . . ?
 F2_7 C1_7 C2_7 114.1(9) . . ?
 F3_7 C1_7 F2_7 104.8(10) . . ?
 F3_7 C1_7 C2_7 112.1(9) . . ?
 C3_7 C2_7 C1_7 118.8(8) . . ?
 C3_7 C2_7 C7_7 120.2(9) . . ?
 C7_7 C2_7 C1_7 120.9(9) . . ?
 C2_7 C3_7 H3_7 121.0 . . ?
 C4_7 C3_7 C2_7 118.1(9) . . ?
 C4_7 C3_7 H3_7 121.0 . . ?
 C3_7 C4_7 N2_7 132.7(9) . . ?
 C3_7 C4_7 C5_7 122.1(8) . . ?
 C5_7 C4_7 N2_7 105.2(8) . . ?
 N1_7 C5_7 C4_7 110.4(9) . . ?
 N1_7 C5_7 C6_7 130.3(10) . . ?
 C6_7 C5_7 C4_7 119.3(9) . . ?
 C5_7 C6_7 H6_7 120.5 . . ?
 C7_7 C6_7 C5_7 119.0(10) . . ?
 C7_7 C6_7 H6_7 120.5 . . ?
 C2_7 C7_7 H7_7 119.5 . . ?
 C6_7 C7_7 C2_7 121.0(10) . . ?
 C6_7 C7_7 H7_7 119.5 . . ?
 N1_7 C8_7 N2_7 113.6(9) . . ?
 N1_7 C8_7 C9_7 129.5(11) . . ?
 N2_7 C8_7 C9_7 116.9(10) . . ?
 C8_7 C9_7 H9_7 120.3 . . ?
 C10_7 C9_7 C8_7 119.3(12) . . ?
 C10_7 C9_7 H9_7 120.3 . . ?
 C9_7 C10_7 H10_7 118.3 . . ?
 C9_7 C10_7 C11_7 123.4(12) . . ?
 C11_7 C10_7 H10_7 118.3 . . ?
 C12_7 C11_7 C10_7 123.5(11) . . ?
 C12_7 C11_7 C19_7 118.6(10) . . ?
 C19_7 C11_7 C10_7 117.9(10) . . ?
 C11_7 C12_7 H12_7 119.8 . . ?
 C13_7 C12_7 C11_7 120.4(11) . . ?
 C13_7 C12_7 H12_7 119.8 . . ?
 C12_7 C13_7 H13_7 119.0 . . ?
 C12_7 C13_7 C14_7 122.0(12) . . ?
 C14_7 C13_7 H13_7 119.0 . . ?
 C13_7 C14_7 C15_7 123.6(10) . . ?
 C13_7 C14_7 C18_7 118.2(10) . . ?
 C15_7 C14_7 C18_7 117.7(9) . . ?
 C14_7 C15_7 H15_7 118.0 . . ?
 C16_7 C15_7 C14_7 124.0(11) . . ?
 C16_7 C15_7 H15_7 118.0 . . ?
 C15_7 C16_7 H16_7 122.2 . . ?
 C15_7 C16_7 C17_7 115.5(11) . . ?
 C17_7 C16_7 H16_7 122.2 . . ?
 N3_7 C17_7 N4_7 113.5(8) . . ?
 N3_7 C17_7 C16_7 126.9(10) . . ?
 N4_7 C17_7 C16_7 119.6(9) . . ?
 N4_7 C18_7 C14_7 116.5(9) . . ?
 N4_7 C18_7 C19_7 124.6(9) . . ?
 C19_7 C18_7 C14_7 118.9(9) . . ?
 N2_7 C19_7 C11_7 115.9(9) . . ?
 C18_7 C19_7 N2_7 125.4(8) . . ?
 C18_7 C19_7 C11_7 118.7(9) . . ?
 N3_7 C20_7 C21_7 127.5(9) . . ?
 N3_7 C20_7 C25_7 112.1(8) . . ?
 C25_7 C20_7 C21_7 120.4(8) . . ?
 C20_7 C21_7 H21_7 121.2 . . ?
 C22_7 C21_7 C20_7 117.6(10) . . ?
 C22_7 C21_7 H21_7 121.2 . . ?
 C21_7 C22_7 H22_7 119.6 . . ?
 C21_7 C22_7 C23_7 120.7(9) . . ?
 C23_7 C22_7 H22_7 119.6 . . ?
 C22_7 C23_7 C26_7 116.8(8) . . ?
 C24_7 C23_7 C22_7 122.9(8) . . ?
 C24_7 C23_7 C26_7 120.0(8) . . ?
 C23_7 C24_7 H24_7 122.2 . . ?
 C23_7 C24_7 C25_7 115.5(9) . . ?
 C25_7 C24_7 H24_7 122.2 . . ?
 C20_7 C25_7 N4_7 104.9(7) . . ?
 C24_7 C25_7 N4_7 132.2(9) . . ?
 C24_7 C25_7 C20_7 122.7(8) . . ?
 F4_7 C26_7 F6_7 104.8(9) . . ?
 F4_7 C26_7 C23_7 114.3(8) . . ?
 F5_7 C26_7 F4_7 104.0(9) . . ?
 F5_7 C26_7 F6_7 105.5(8) . . ?
 F5_7 C26_7 C23_7 113.3(9) . . ?
 F6_7 C26_7 C23_7 114.0(8) . . ?
 C8_8 N1_8 C5_8 105.6(9) . . ?
 C4_8 N2_8 C8_8 104.6(7) . . ?
 C19_8 N2_8 C4_8 132.8(9) . . ?
 C19_8 N2_8 C8_8 122.6(8) . . ?
 C17_8 N3_8 C20_8 103.9(9) . . ?
 C18_8 N4_8 C17_8 123.4(8) . . ?
 C18_8 N4_8 C25_8 131.9(9) . . ?
 C25_8 N4_8 C17_8 104.8(7) . . ?
 F1_8 C1_8 F2_8 105.6(11) . . ?
 F1_8 C1_8 F3_8 106.8(10) . . ?
 F1_8 C1_8 C2_8 114.0(10) . . ?
 F2_8 C1_8 F3_8 103.4(10) . . ?
 F2_8 C1_8 C2_8 113.0(9) . . ?
 F3_8 C1_8 C2_8 113.1(9) . . ?
 C3_8 C2_8 C1_8 118.7(8) . . ?
 C3_8 C2_8 C7_8 122.9(9) . . ?
 C7_8 C2_8 C1_8 118.4(8) . . ?
 C2_8 C3_8 H3_8 122.4 . . ?
 C4_8 C3_8 C2_8 115.2(9) . . ?
 C4_8 C3_8 H3_8 122.4 . . ?
 N2_8 C4_8 C5_8 105.3(8) . . ?
 C3_8 C4_8 N2_8 131.5(9) . . ?
 C3_8 C4_8 C5_8 123.2(8) . . ?
 N1_8 C5_8 C4_8 110.4(9) . . ?
 N1_8 C5_8 C6_8 128.9(10) . . ?
 C6_8 C5_8 C4_8 120.1(9) . . ?
 C5_8 C6_8 H6_8 120.9 . . ?
 C7_8 C6_8 C5_8 118.2(10) . . ?
 C7_8 C6_8 H6_8 120.9 . . ?
 C2_8 C7_8 H7_8 119.9 . . ?
 C6_8 C7_8 C2_8 120.3(10) . . ?
 C6_8 C7_8 H7_8 119.9 . . ?
 N1_8 C8_8 N2_8 113.6(8) . . ?
 N1_8 C8_8 C9_8 127.8(11) . . ?
 N2_8 C8_8 C9_8 117.8(10) . . ?
 C8_8 C9_8 H9_8 120.8 . . ?
 C10_8 C9_8 C8_8 118.3(12) . . ?
 C10_8 C9_8 H9_8 120.8 . . ?
 C9_8 C10_8 H10_8 118.0 . . ?
 C9_8 C10_8 C11_8 124.0(11) . . ?
 C11_8 C10_8 H10_8 118.0 . . ?
 C10_8 C11_8 C19_8 117.8(10) . . ?
 C12_8 C11_8 C10_8 124.4(11) . . ?
 C12_8 C11_8 C19_8 117.8(10) . . ?
 C11_8 C12_8 H12_8 119.6 . . ?
 C13_8 C12_8 C11_8 120.9(11) . . ?
 C13_8 C12_8 H12_8 119.6 . . ?
 C12_8 C13_8 H13_8 118.6 . . ?
 C12_8 C13_8 C14_8 122.8(12) . . ?
 C14_8 C13_8 H13_8 118.6 . . ?
 C13_8 C14_8 C15_8 125.5(11) . . ?
 C13_8 C14_8 C18_8 116.7(11) . . ?
 C15_8 C14_8 C18_8 117.7(10) . . ?
 C14_8 C15_8 H15_8 117.7 . . ?
 C16_8 C15_8 C14_8 124.6(11) . . ?
 C16_8 C15_8 H15_8 117.7 . . ?
 C15_8 C16_8 H16_8 121.5 . . ?
 C15_8 C16_8 C17_8 117.0(12) . . ?
 C17_8 C16_8 H16_8 121.5 . . ?
 N3_8 C17_8 N4_8 113.4(8) . . ?
 N3_8 C17_8 C16_8 128.5(10) . . ?
 N4_8 C17_8 C16_8 117.9(10) . . ?
 N4_8 C18_8 C14_8 116.5(9) . . ?
 N4_8 C18_8 C19_8 124.5(9) . . ?
 C19_8 C18_8 C14_8 118.9(9) . . ?
 N2_8 C19_8 C11_8 115.7(9) . . ?
 N2_8 C19_8 C18_8 125.6(9) . . ?
 C18_8 C19_8 C11_8 118.7(9) . . ?
 N3_8 C20_8 C21_8 127.6(10) . . ?
 N3_8 C20_8 C25_8 112.1(8) . . ?
 C25_8 C20_8 C21_8 120.3(9) . . ?
 C20_8 C21_8 H21_8 120.8 . . ?
 C22_8 C21_8 C20_8 118.3(10) . . ?
 C22_8 C21_8 H21_8 120.8 . . ?
 C21_8 C22_8 H22_8 119.7 . . ?
 C21_8 C22_8 C23_8 120.7(10) . . ?
 C23_8 C22_8 H22_8 119.7 . . ?
 C22_8 C23_8 C26_8 116.4(8) . . ?
 C24_8 C23_8 C22_8 122.4(8) . . ?
 C24_8 C23_8 C26_8 121.2(8) . . ?
 C23_8 C24_8 H24_8 121.8 . . ?
 C23_8 C24_8 C25_8 116.3(8) . . ?
 C25_8 C24_8 H24_8 121.8 . . ?
 C20_8 C25_8 N4_8 105.4(7) . . ?
 C24_8 C25_8 N4_8 132.6(9) . . ?
 C24_8 C25_8 C20_8 122.0(8) . . ?
 F4_8 C26_8 F6_8 105.8(10) . . ?
 F4_8 C26_8 C23_8 112.7(9) . . ?
 F5_8 C26_8 F4_8 103.3(9) . . ?
 F5_8 C26_8 F6_8 106.8(10) . . ?
 F5_8 C26_8 C23_8 113.9(10) . . ?
 F6_8 C26_8 C23_8 113.5(9) . . ?
 C8_9 N1_9 C5_9 106.8(8) . . ?
 C4_9 N2_9 C8_9 104.7(7) . . ?
 C19_9 N2_9 C4_9 133.5(8) . . ?
 C19_9 N2_9 C8_9 121.7(8) . . ?
 C17_9 N3_9 C20_9 104.7(8) . . ?
 C18_9 N4_9 C17_9 121.7(8) . . ?
 C18_9 N4_9 C25_9 133.5(8) . . ?
 C25_9 N4_9 C17_9 104.8(7) . . ?
 F1_9 C1_9 F2_9 106.7(11) . . ?
 F1_9 C1_9 F3_9 106.0(10) . . ?
 F1_9 C1_9 C2_9 114.6(11) . . ?
 F2_9 C1_9 C2_9 113.2(9) . . ?
 F3_9 C1_9 F2_9 102.1(10) . . ?
 F3_9 C1_9 C2_9 113.2(10) . . ?
 C3_9 C2_9 C1_9 119.3(9) . . ?
 C3_9 C2_9 C7_9 121.2(9) . . ?
 C7_9 C2_9 C1_9 119.3(9) . . ?
 C2_9 C3_9 H3_9 121.5 . . ?
 C4_9 C3_9 C2_9 116.9(9) . . ?
 C4_9 C3_9 H3_9 121.5 . . ?
 N2_9 C4_9 C5_9 104.9(7) . . ?
 C3_9 C4_9 N2_9 133.0(8) . . ?
 C3_9 C4_9 C5_9 121.8(8) . . ?
 N1_9 C5_9 C4_9 109.7(8) . . ?
 N1_9 C5_9 C6_9 128.9(9) . . ?
 C6_9 C5_9 C4_9 120.4(9) . . ?
 C5_9 C6_9 H6_9 121.0 . . ?
 C7_9 C6_9 C5_9 117.9(10) . . ?
 C7_9 C6_9 H6_9 121.0 . . ?
 C2_9 C7_9 H7_9 119.3 . . ?
 C6_9 C7_9 C2_9 121.4(10) . . ?
 C6_9 C7_9 H7_9 119.3 . . ?
 N1_9 C8_9 N2_9 112.6(8) . . ?
 N1_9 C8_9 C9_9 129.6(10) . . ?
 N2_9 C8_9 C9_9 116.6(9) . . ?
 C8_9 C9_9 H9_9 119.3 . . ?
 C10_9 C9_9 C8_9 121.4(11) . . ?
 C10_9 C9_9 H9_9 119.3 . . ?
 C9_9 C10_9 H10_9 119.1 . . ?
 C9_9 C10_9 C11_9 121.9(11) . . ?
 C11_9 C10_9 H10_9 119.1 . . ?
 C12_9 C11_9 C10_9 123.5(10) . . ?
 C12_9 C11_9 C19_9 118.7(10) . . ?
 C19_9 C11_9 C10_9 117.5(9) . . ?
 C11_9 C12_9 H12_9 119.3 . . ?
 C13_9 C12_9 C11_9 121.4(11) . . ?
 C13_9 C12_9 H12_9 119.3 . . ?
 C12_9 C13_9 H13_9 119.6 . . ?
 C12_9 C13_9 C14_9 120.8(10) . . ?
 C14_9 C13_9 H13_9 119.6 . . ?
 C13_9 C14_9 C15_9 123.1(10) . . ?
 C13_9 C14_9 C18_9 117.9(9) . . ?
 C18_9 C14_9 C15_9 119.0(9) . . ?
 C14_9 C15_9 H15_9 119.0 . . ?
 C16_9 C15_9 C14_9 122.1(10) . . ?
 C16_9 C15_9 H15_9 119.0 . . ?
 C15_9 C16_9 H16_9 120.8 . . ?
 C15_9 C16_9 C17_9 118.5(10) . . ?
 C17_9 C16_9 H16_9 120.8 . . ?
 N3_9 C17_9 N4_9 113.1(8) . . ?
 N3_9 C17_9 C16_9 127.8(10) . . ?
 N4_9 C17_9 C16_9 118.3(9) . . ?
 N4_9 C18_9 C14_9 117.4(8) . . ?
 N4_9 C18_9 C19_9 122.8(8) . . ?
 C19_9 C18_9 C14_9 119.8(8) . . ?
 N2_9 C19_9 C11_9 117.6(8) . . ?
 N2_9 C19_9 C18_9 124.4(8) . . ?
 C18_9 C19_9 C11_9 117.9(8) . . ?
 N3_9 C20_9 C21_9 128.4(9) . . ?
 N3_9 C20_9 C25_9 111.3(8) . . ?
 C21_9 C20_9 C25_9 120.4(8) . . ?
 C20_9 C21_9 H21_9 120.7 . . ?
 C22_9 C21_9 C20_9 118.6(9) . . ?
 C22_9 C21_9 H21_9 120.7 . . ?
 C21_9 C22_9 H22_9 120.2 . . ?
 C21_9 C22_9 C23_9 119.7(9) . . ?
 C23_9 C22_9 H22_9 120.2 . . ?
 C22_9 C23_9 C26_9 117.0(8) . . ?
 C24_9 C23_9 C22_9 122.8(8) . . ?
 C24_9 C23_9 C26_9 119.8(8) . . ?
 C23_9 C24_9 H24_9 121.8 . . ?
 C23_9 C24_9 C25_9 116.4(8) . . ?
 C25_9 C24_9 H24_9 121.8 . . ?
 N4_9 C25_9 C20_9 106.1(7) . . ?
 C24_9 C25_9 N4_9 131.9(8) . . ?
 C24_9 C25_9 C20_9 121.4(8) . . ?
 F4_9 C26_9 F5_9 105.6(9) . . ?
 F4_9 C26_9 F6_9 104.3(9) . . ?
 F4_9 C26_9 C23_9 112.2(9) . . ?
 F5_9 C26_9 F6_9 106.3(9) . . ?
 F5_9 C26_9 C23_9 114.5(10) . . ?
 F6_9 C26_9 C23_9 113.1(8) . . ?

loop_
  _geom_torsion_atom_site_label_1
  _geom_torsion_atom_site_label_2
  _geom_torsion_atom_site_label_3
  _geom_torsion_atom_site_label_4
  _geom_torsion
  _geom_torsion_site_symmetry_1
  _geom_torsion_site_symmetry_2
  _geom_torsion_site_symmetry_3
  _geom_torsion_site_symmetry_4
  _geom_torsion_publ_flag
 F1_1 C1_1 C2_1 C3_1 -127.4(14) . . . . ?
 F1_1 C1_1 C2_1 C7_1 55.5(17) . . . . ?
 F2_1 C1_1 C2_1 C3_1 -4.7(17) . . . . ?
 F2_1 C1_1 C2_1 C7_1 178.3(13) . . . . ?
 F3_1 C1_1 C2_1 C3_1 110.9(13) . . . . ?
 F3_1 C1_1 C2_1 C7_1 -66.2(16) . . . . ?
 N1_1 C5_1 C6_1 C7_1 179.2(14) . . . . ?
 N1_1 C8_1 C9_1 C10_1 -166.3(15) . . . . ?
 N2_1 C4_1 C5_1 N1_1 5.3(15) . . . . ?
 N2_1 C4_1 C5_1 C6_1 -174.9(12) . . . . ?
 N2_1 C8_1 C9_1 C10_1 13(2) . . . . ?
 N3_1 C20_1 C21_1 C22_1 -179.0(14) . . . . ?
 N3_1 C20_1 C25_1 N4_1 0.7(16) . . . . ?
 N3_1 C20_1 C25_1 C24_1 -177.9(13) . . . . ?
 N4_1 C18_1 C19_1 N2_1 -18(2) . . . . ?
 N4_1 C18_1 C19_1 C11_1 159.2(13) . . . . ?
 C1_1 C2_1 C3_1 C4_1 -176.2(11) . . . . ?
 C1_1 C2_1 C7_1 C6_1 -179.9(13) . . . . ?
 C2_1 C3_1 C4_1 N2_1 174.7(13) . . . . ?
 C2_1 C3_1 C4_1 C5_1 -4.5(18) . . . . ?
 C3_1 C2_1 C7_1 C6_1 3(2) . . . . ?
 C3_1 C4_1 C5_1 N1_1 -175.3(12) . . . . ?
 C3_1 C4_1 C5_1 C6_1 5(2) . . . . ?
 C4_1 N2_1 C8_1 N1_1 8.3(15) . . . . ?
 C4_1 N2_1 C8_1 C9_1 -171.0(12) . . . . ?
 C4_1 N2_1 C19_1 C11_1 156.4(12) . . . . ?
 C4_1 N2_1 C19_1 C18_1 -27(2) . . . . ?
 C4_1 C5_1 C6_1 C7_1 -1(2) . . . . ?
 C5_1 N1_1 C8_1 N2_1 -5.0(16) . . . . ?
 C5_1 N1_1 C8_1 C9_1 174.2(14) . . . . ?
 C5_1 C6_1 C7_1 C2_1 -3(2) . . . . ?
 C7_1 C2_1 C3_1 C4_1 0.9(19) . . . . ?
 C8_1 N1_1 C5_1 C4_1 -0.4(16) . . . . ?
 C8_1 N1_1 C5_1 C6_1 179.9(15) . . . . ?
 C8_1 N2_1 C4_1 C3_1 173.1(14) . . . . ?
 C8_1 N2_1 C4_1 C5_1 -7.6(13) . . . . ?
 C8_1 N2_1 C19_1 C11_1 -16.4(18) . . . . ?
 C8_1 N2_1 C19_1 C18_1 160.5(13) . . . . ?
 C8_1 C9_1 C10_1 C11_1 -15(2) . . . . ?
 C9_1 C10_1 C11_1 C12_1 -177.7(15) . . . . ?
 C9_1 C10_1 C11_1 C19_1 2(2) . . . . ?
 C10_1 C11_1 C12_1 C13_1 -178.2(15) . . . . ?
 C10_1 C11_1 C19_1 N2_1 13.7(18) . . . . ?
 C10_1 C11_1 C19_1 C18_1 -163.4(13) . . . . ?
 C11_1 C12_1 C13_1 C14_1 -12(3) . . . . ?
 C12_1 C11_1 C19_1 N2_1 -166.9(12) . . . . ?
 C12_1 C11_1 C19_1 C18_1 16.0(19) . . . . ?
 C12_1 C13_1 C14_1 C15_1 179.9(18) . . . . ?
 C12_1 C13_1 C14_1 C18_1 2(3) . . . . ?
 C13_1 C14_1 C15_1 C16_1 -178.3(19) . . . . ?
 C13_1 C14_1 C18_1 N4_1 -168.1(14) . . . . ?
 C13_1 C14_1 C18_1 C19_1 16(2) . . . . ?
 C14_1 C15_1 C16_1 C17_1 -7(3) . . . . ?
 C14_1 C18_1 C19_1 N2_1 158.4(13) . . . . ?
 C14_1 C18_1 C19_1 C11_1 -24.8(19) . . . . ?
 C15_1 C14_1 C18_1 N4_1 14(2) . . . . ?
 C15_1 C14_1 C18_1 C19_1 -162.0(16) . . . . ?
 C15_1 C16_1 C17_1 N3_1 -163.6(19) . . . . ?
 C15_1 C16_1 C17_1 N4_1 1(3) . . . . ?
 C17_1 N3_1 C20_1 C21_1 -180.0(16) . . . . ?
 C17_1 N3_1 C20_1 C25_1 0.1(18) . . . . ?
 C17_1 N4_1 C18_1 C14_1 -21(2) . . . . ?
 C17_1 N4_1 C18_1 C19_1 155.3(14) . . . . ?
 C17_1 N4_1 C25_1 C20_1 -1.2(15) . . . . ?
 C17_1 N4_1 C25_1 C24_1 177.2(14) . . . . ?
 C18_1 N4_1 C17_1 N3_1 179.9(13) . . . . ?
 C18_1 N4_1 C17_1 C16_1 13(2) . . . . ?
 C18_1 N4_1 C25_1 C20_1 -179.5(13) . . . . ?
 C18_1 N4_1 C25_1 C24_1 -1(2) . . . . ?
 C18_1 C14_1 C15_1 C16_1 -1(3) . . . . ?
 C19_1 N2_1 C4_1 C3_1 -1(2) . . . . ?
 C19_1 N2_1 C4_1 C5_1 178.6(12) . . . . ?
 C19_1 N2_1 C8_1 N1_1 -177.4(12) . . . . ?
 C19_1 N2_1 C8_1 C9_1 3.3(19) . . . . ?
 C19_1 C11_1 C12_1 C13_1 2(2) . . . . ?
 C20_1 N3_1 C17_1 N4_1 -0.9(19) . . . . ?
 C20_1 N3_1 C17_1 C16_1 164.5(18) . . . . ?
 C20_1 C21_1 C22_1 C23_1 -1.7(18) . . . . ?
 C21_1 C20_1 C25_1 N4_1 -179.3(12) . . . . ?
 C21_1 C20_1 C25_1 C24_1 2(2) . . . . ?
 C21_1 C22_1 C23_1 C24_1 -0.6(18) . . . . ?
 C21_1 C22_1 C23_1 C26_1 179.1(11) . . . . ?
 C22_1 C23_1 C24_1 C25_1 3.5(17) . . . . ?
 C22_1 C23_1 C26_1 F4_1 -45.6(13) . . . . ?
 C22_1 C23_1 C26_1 F5_1 75.3(12) . . . . ?
 C22_1 C23_1 C26_1 F6_1 -165.3(10) . . . . ?
 C23_1 C24_1 C25_1 N4_1 177.6(12) . . . . ?
 C23_1 C24_1 C25_1 C20_1 -4.3(18) . . . . ?
 C24_1 C23_1 C26_1 F4_1 134.0(10) . . . . ?
 C24_1 C23_1 C26_1 F5_1 -105.1(11) . . . . ?
 C24_1 C23_1 C26_1 F6_1 14.4(14) . . . . ?
 C25_1 N4_1 C17_1 N3_1 1.3(18) . . . . ?
 C25_1 N4_1 C17_1 C16_1 -165.4(15) . . . . ?
 C25_1 N4_1 C18_1 C14_1 157.4(14) . . . . ?
 C25_1 N4_1 C18_1 C19_1 -27(2) . . . . ?
 C25_1 C20_1 C21_1 C22_1 1(2) . . . . ?
 C26_1 C23_1 C24_1 C25_1 -176.2(10) . . . . ?
 F1_2 C1_2 C2_2 C3_2 -128.5(13) . . . . ?
 F1_2 C1_2 C2_2 C7_2 56.6(17) . . . . ?
 F2_2 C1_2 C2_2 C3_2 -3.9(17) . . . . ?
 F2_2 C1_2 C2_2 C7_2 -178.9(13) . . . . ?
 F3_2 C1_2 C2_2 C3_2 110.9(13) . . . . ?
 F3_2 C1_2 C2_2 C7_2 -64.0(16) . . . . ?
 N1_2 C5_2 C6_2 C7_2 173.9(17) . . . . ?
 N1_2 C8_2 C9_2 C10_2 -159(2) . . . . ?
 N2_2 C4_2 C5_2 N1_2 11.2(17) . . . . ?
 N2_2 C4_2 C5_2 C6_2 -179.8(14) . . . . ?
 N2_2 C8_2 C9_2 C10_2 3(3) . . . . ?
 N3_2 C20_2 C21_2 C22_2 176.6(14) . . . . ?
 N3_2 C20_2 C25_2 N4_2 5.3(15) . . . . ?
 N3_2 C20_2 C25_2 C24_2 -174.0(12) . . . . ?
 N4_2 C18_2 C19_2 N2_2 -19(2) . . . . ?
 N4_2 C18_2 C19_2 C11_2 156.2(15) . . . . ?
 C1_2 C2_2 C3_2 C4_2 -176.6(11) . . . . ?
 C1_2 C2_2 C7_2 C6_2 -179.2(14) . . . . ?
 C2_2 C3_2 C4_2 N2_2 175.9(14) . . . . ?
 C2_2 C3_2 C4_2 C5_2 0(2) . . . . ?
 C3_2 C2_2 C7_2 C6_2 6(2) . . . . ?
 C3_2 C4_2 C5_2 N1_2 -172.0(13) . . . . ?
 C3_2 C4_2 C5_2 C6_2 -3(2) . . . . ?
 C4_2 N2_2 C8_2 N1_2 -1.8(19) . . . . ?
 C4_2 N2_2 C8_2 C9_2 -166.6(16) . . . . ?
 C4_2 N2_2 C19_2 C11_2 157.3(16) . . . . ?
 C4_2 N2_2 C19_2 C18_2 -28(3) . . . . ?
 C4_2 C5_2 C6_2 C7_2 7(2) . . . . ?
 C5_2 N1_2 C8_2 N2_2 9(2) . . . . ?
 C5_2 N1_2 C8_2 C9_2 171.3(19) . . . . ?
 C5_2 C6_2 C7_2 C2_2 -9(2) . . . . ?
 C7_2 C2_2 C3_2 C4_2 -2(2) . . . . ?
 C8_2 N1_2 C5_2 C4_2 -13(2) . . . . ?
 C8_2 N1_2 C5_2 C6_2 179.8(18) . . . . ?
 C8_2 N2_2 C4_2 C3_2 178.2(15) . . . . ?
 C8_2 N2_2 C4_2 C5_2 -5.7(15) . . . . ?
 C8_2 N2_2 C19_2 C11_2 -23(2) . . . . ?
 C8_2 N2_2 C19_2 C18_2 152.1(15) . . . . ?
 C8_2 C9_2 C10_2 C11_2 -9(4) . . . . ?
 C9_2 C10_2 C11_2 C12_2 178(2) . . . . ?
 C9_2 C10_2 C11_2 C19_2 -1(4) . . . . ?
 C10_2 C11_2 C12_2 C13_2 170(2) . . . . ?
 C10_2 C11_2 C19_2 N2_2 17(3) . . . . ?
 C10_2 C11_2 C19_2 C18_2 -158.8(19) . . . . ?
 C11_2 C12_2 C13_2 C14_2 1(4) . . . . ?
 C12_2 C11_2 C19_2 N2_2 -162.7(18) . . . . ?
 C12_2 C11_2 C19_2 C18_2 22(3) . . . . ?
 C12_2 C13_2 C14_2 C15_2 173.4(19) . . . . ?
 C12_2 C13_2 C14_2 C18_2 -3(3) . . . . ?
 C13_2 C14_2 C15_2 C16_2 178.3(17) . . . . ?
 C13_2 C14_2 C18_2 N4_2 -165.7(14) . . . . ?
 C13_2 C14_2 C18_2 C19_2 15(2) . . . . ?
 C14_2 C15_2 C16_2 C17_2 -5(2) . . . . ?
 C14_2 C18_2 C19_2 N2_2 160.8(14) . . . . ?
 C14_2 C18_2 C19_2 C11_2 -24(2) . . . . ?
 C15_2 C14_2 C18_2 N4_2 18(2) . . . . ?
 C15_2 C14_2 C18_2 C19_2 -162.0(14) . . . . ?
 C15_2 C16_2 C17_2 N3_2 -168.4(14) . . . . ?
 C15_2 C16_2 C17_2 N4_2 2(2) . . . . ?
 C17_2 N3_2 C20_2 C21_2 -176.2(14) . . . . ?
 C17_2 N3_2 C20_2 C25_2 -1.7(15) . . . . ?
 C17_2 N4_2 C18_2 C14_2 -20.9(19) . . . . ?
 C17_2 N4_2 C18_2 C19_2 158.6(14) . . . . ?
 C17_2 N4_2 C25_2 C20_2 -6.3(13) . . . . ?
 C17_2 N4_2 C25_2 C24_2 172.9(13) . . . . ?
 C18_2 N4_2 C17_2 N3_2 -177.2(12) . . . . ?
 C18_2 N4_2 C17_2 C16_2 10.7(19) . . . . ?
 C18_2 N4_2 C25_2 C20_2 177.3(13) . . . . ?
 C18_2 N4_2 C25_2 C24_2 -4(2) . . . . ?
 C18_2 C14_2 C15_2 C16_2 -5(2) . . . . ?
 C19_2 N2_2 C4_2 C3_2 -2(3) . . . . ?
 C19_2 N2_2 C4_2 C5_2 174.2(15) . . . . ?
 C19_2 N2_2 C8_2 N1_2 178.3(15) . . . . ?
 C19_2 N2_2 C8_2 C9_2 14(2) . . . . ?
 C19_2 C11_2 C12_2 C13_2 -10(3) . . . . ?
 C20_2 N3_2 C17_2 N4_2 -2.6(15) . . . . ?
 C20_2 N3_2 C17_2 C16_2 168.5(14) . . . . ?
 C20_2 C21_2 C22_2 C23_2 -4(2) . . . . ?
 C21_2 C20_2 C25_2 N4_2 -179.6(12) . . . . ?
 C21_2 C20_2 C25_2 C24_2 1(2) . . . . ?
 C21_2 C22_2 C23_2 C24_2 1(2) . . . . ?
 C21_2 C22_2 C23_2 C26_2 176.0(12) . . . . ?
 C22_2 C23_2 C24_2 C25_2 2.1(18) . . . . ?
 C22_2 C23_2 C26_2 F4_2 -52.3(14) . . . . ?
 C22_2 C23_2 C26_2 F5_2 67.5(14) . . . . ?
 C22_2 C23_2 C26_2 F6_2 -175.1(11) . . . . ?
 C23_2 C24_2 C25_2 N4_2 177.6(12) . . . . ?
 C23_2 C24_2 C25_2 C20_2 -3.3(18) . . . . ?
 C24_2 C23_2 C26_2 F4_2 122.5(12) . . . . ?
 C24_2 C23_2 C26_2 F5_2 -117.8(12) . . . . ?
 C24_2 C23_2 C26_2 F6_2 -0.4(15) . . . . ?
 C25_2 N4_2 C17_2 N3_2 5.8(15) . . . . ?
 C25_2 N4_2 C17_2 C16_2 -166.2(12) . . . . ?
 C25_2 N4_2 C18_2 C14_2 155.0(13) . . . . ?
 C25_2 N4_2 C18_2 C19_2 -26(2) . . . . ?
 C25_2 C20_2 C21_2 C22_2 2(2) . . . . ?
 C26_2 C23_2 C24_2 C25_2 -172.5(10) . . . . ?
 F1_3 C1_3 C2_3 C3_3 -122.2(15) . . . . ?
 F1_3 C1_3 C2_3 C7_3 58.4(18) . . . . ?
 F2_3 C1_3 C2_3 C3_3 -0.6(18) . . . . ?
 F2_3 C1_3 C2_3 C7_3 180.0(14) . . . . ?
 F3_3 C1_3 C2_3 C3_3 116.4(14) . . . . ?
 F3_3 C1_3 C2_3 C7_3 -63.0(17) . . . . ?
 N1_3 C5_3 C6_3 C7_3 176.5(17) . . . . ?
 N1_3 C8_3 C9_3 C10_3 -172(2) . . . . ?
 N2_3 C4_3 C5_3 N1_3 6.7(17) . . . . ?
 N2_3 C4_3 C5_3 C6_3 -179.1(14) . . . . ?
 N2_3 C8_3 C9_3 C10_3 0(3) . . . . ?
 N3_3 C20_3 C21_3 C22_3 178.7(14) . . . . ?
 N3_3 C20_3 C25_3 N4_3 3.9(16) . . . . ?
 N3_3 C20_3 C25_3 C24_3 -178.3(13) . . . . ?
 N4_3 C18_3 C19_3 N2_3 -24(2) . . . . ?
 N4_3 C18_3 C19_3 C11_3 156.0(15) . . . . ?
 C1_3 C2_3 C3_3 C4_3 -177.2(12) . . . . ?
 C1_3 C2_3 C7_3 C6_3 179.2(15) . . . . ?
 C2_3 C3_3 C4_3 N2_3 175.6(14) . . . . ?
 C2_3 C3_3 C4_3 C5_3 -1(2) . . . . ?
 C3_3 C2_3 C7_3 C6_3 0(3) . . . . ?
 C3_3 C4_3 C5_3 N1_3 -175.7(13) . . . . ?
 C3_3 C4_3 C5_3 C6_3 -1(2) . . . . ?
 C4_3 N2_3 C8_3 N1_3 6.8(18) . . . . ?
 C4_3 N2_3 C8_3 C9_3 -166.1(14) . . . . ?
 C4_3 N2_3 C19_3 C11_3 156.0(15) . . . . ?
 C4_3 N2_3 C19_3 C18_3 -24(2) . . . . ?
 C4_3 C5_3 C6_3 C7_3 3(2) . . . . ?
 C5_3 N1_3 C8_3 N2_3 -2.7(19) . . . . ?
 C5_3 N1_3 C8_3 C9_3 169.0(18) . . . . ?
 C5_3 C6_3 C7_3 C2_3 -3(3) . . . . ?
 C7_3 C2_3 C3_3 C4_3 2(2) . . . . ?
 C8_3 N1_3 C5_3 C4_3 -2.6(19) . . . . ?
 C8_3 N1_3 C5_3 C6_3 -176.1(17) . . . . ?
 C8_3 N2_3 C4_3 C3_3 175.0(15) . . . . ?
 C8_3 N2_3 C4_3 C5_3 -7.6(15) . . . . ?
 C8_3 N2_3 C19_3 C11_3 -19(2) . . . . ?
 C8_3 N2_3 C19_3 C18_3 160.9(15) . . . . ?
 C8_3 C9_3 C10_3 C11_3 0(3) . . . . ?
 C9_3 C10_3 C11_3 C12_3 178(2) . . . . ?
 C9_3 C10_3 C11_3 C19_3 -9(3) . . . . ?
 C10_3 C11_3 C12_3 C13_3 -178.5(19) . . . . ?
 C10_3 C11_3 C19_3 N2_3 18(2) . . . . ?
 C10_3 C11_3 C19_3 C18_3 -161.8(16) . . . . ?
 C11_3 C12_3 C13_3 C14_3 -20(3) . . . . ?
 C12_3 C11_3 C19_3 N2_3 -169.5(16) . . . . ?
 C12_3 C11_3 C19_3 C18_3 11(3) . . . . ?
 C12_3 C13_3 C14_3 C15_3 177.8(18) . . . . ?
 C12_3 C13_3 C14_3 C18_3 9(3) . . . . ?
 C13_3 C14_3 C15_3 C16_3 177.7(18) . . . . ?
 C13_3 C14_3 C18_3 N4_3 -165.8(15) . . . . ?
 C13_3 C14_3 C18_3 C19_3 11(2) . . . . ?
 C14_3 C15_3 C16_3 C17_3 -1(3) . . . . ?
 C14_3 C18_3 C19_3 N2_3 159.7(15) . . . . ?
 C14_3 C18_3 C19_3 C11_3 -20(2) . . . . ?
 C15_3 C14_3 C18_3 N4_3 25(2) . . . . ?
 C15_3 C14_3 C18_3 C19_3 -157.9(15) . . . . ?
 C15_3 C16_3 C17_3 N3_3 -169.0(17) . . . . ?
 C15_3 C16_3 C17_3 N4_3 3(2) . . . . ?
 C17_3 N3_3 C20_3 C21_3 175.6(15) . . . . ?
 C17_3 N3_3 C20_3 C25_3 -1.0(18) . . . . ?
 C17_3 N4_3 C18_3 C14_3 -23(2) . . . . ?
 C17_3 N4_3 C18_3 C19_3 160.0(15) . . . . ?
 C17_3 N4_3 C25_3 C20_3 -5.1(15) . . . . ?
 C17_3 N4_3 C25_3 C24_3 177.4(15) . . . . ?
 C18_3 N4_3 C17_3 N3_3 -177.5(13) . . . . ?
 C18_3 N4_3 C17_3 C16_3 9(2) . . . . ?
 C18_3 N4_3 C25_3 C20_3 177.8(14) . . . . ?
 C18_3 N4_3 C25_3 C24_3 0(3) . . . . ?
 C18_3 C14_3 C15_3 C16_3 -14(3) . . . . ?
 C19_3 N2_3 C4_3 C3_3 -1(3) . . . . ?
 C19_3 N2_3 C4_3 C5_3 176.7(14) . . . . ?
 C19_3 N2_3 C8_3 N1_3 -177.1(14) . . . . ?
 C19_3 N2_3 C8_3 C9_3 10(2) . . . . ?
 C19_3 C11_3 C12_3 C13_3 9(3) . . . . ?
 C20_3 N3_3 C17_3 N4_3 -2.4(18) . . . . ?
 C20_3 N3_3 C17_3 C16_3 170.0(17) . . . . ?
 C20_3 C21_3 C22_3 C23_3 3(2) . . . . ?
 C21_3 C20_3 C25_3 N4_3 -173.1(12) . . . . ?
 C21_3 C20_3 C25_3 C24_3 5(2) . . . . ?
 C21_3 C22_3 C23_3 C24_3 0(2) . . . . ?
 C21_3 C22_3 C23_3 C26_3 179.7(12) . . . . ?
 C22_3 C23_3 C24_3 C25_3 -0.2(18) . . . . ?
 C22_3 C23_3 C26_3 F4_3 -43.5(14) . . . . ?
 C22_3 C23_3 C26_3 F5_3 74.8(13) . . . . ?
 C22_3 C23_3 C26_3 F6_3 -163.2(10) . . . . ?
 C23_3 C24_3 C25_3 N4_3 175.0(13) . . . . ?
 C23_3 C24_3 C25_3 C20_3 -2.1(19) . . . . ?
 C24_3 C23_3 C26_3 F4_3 136.4(11) . . . . ?
 C24_3 C23_3 C26_3 F5_3 -105.2(12) . . . . ?
 C24_3 C23_3 C26_3 F6_3 16.7(15) . . . . ?
 C25_3 N4_3 C17_3 N3_3 4.9(17) . . . . ?
 C25_3 N4_3 C17_3 C16_3 -168.2(14) . . . . ?
 C25_3 N4_3 C18_3 C14_3 153.3(15) . . . . ?
 C25_3 N4_3 C18_3 C19_3 -23(2) . . . . ?
 C25_3 C20_3 C21_3 C22_3 -5(2) . . . . ?
 C26_3 C23_3 C24_3 C25_3 179.9(11) . . . . ?
 F1_4 C1_4 C2_4 C3_4 -123.0(13) . . . . ?
 F1_4 C1_4 C2_4 C7_4 58.1(16) . . . . ?
 F2_4 C1_4 C2_4 C3_4 1.9(16) . . . . ?
 F2_4 C1_4 C2_4 C7_4 -177.0(12) . . . . ?
 F3_4 C1_4 C2_4 C3_4 115.2(12) . . . . ?
 F3_4 C1_4 C2_4 C7_4 -63.7(15) . . . . ?
 N1_4 C5_4 C6_4 C7_4 -178.4(17) . . . . ?
 N1_4 C8_4 C9_4 C10_4 -176(2) . . . . ?
 N2_4 C4_4 C5_4 N1_4 0.7(18) . . . . ?
 N2_4 C4_4 C5_4 C6_4 -175.0(15) . . . . ?
 N2_4 C8_4 C9_4 C10_4 3(3) . . . . ?
 N3_4 C20_4 C21_4 C22_4 178.0(15) . . . . ?
 N3_4 C20_4 C25_4 N4_4 2.8(17) . . . . ?
 N3_4 C20_4 C25_4 C24_4 -175.8(13) . . . . ?
 N4_4 C18_4 C19_4 N2_4 -20(3) . . . . ?
 N4_4 C18_4 C19_4 C11_4 161.8(15) . . . . ?
 C1_4 C2_4 C3_4 C4_4 -176.1(11) . . . . ?
 C1_4 C2_4 C7_4 C6_4 -178.9(14) . . . . ?
 C2_4 C3_4 C4_4 N2_4 177.0(14) . . . . ?
 C2_4 C3_4 C4_4 C5_4 -8(2) . . . . ?
 C3_4 C2_4 C7_4 C6_4 2(2) . . . . ?
 C3_4 C4_4 C5_4 N1_4 -175.3(14) . . . . ?
 C3_4 C4_4 C5_4 C6_4 9(2) . . . . ?
 C4_4 N2_4 C8_4 N1_4 13(2) . . . . ?
 C4_4 N2_4 C8_4 C9_4 -166.9(16) . . . . ?
 C4_4 N2_4 C19_4 C11_4 156.8(15) . . . . ?
 C4_4 N2_4 C19_4 C18_4 -21(3) . . . . ?
 C4_4 C5_4 C6_4 C7_4 -4(3) . . . . ?
 C5_4 N1_4 C8_4 N2_4 -12(2) . . . . ?
 C5_4 N1_4 C8_4 C9_4 167(2) . . . . ?
 C5_4 C6_4 C7_4 C2_4 -2(3) . . . . ?
 C7_4 C2_4 C3_4 C4_4 3(2) . . . . ?
 C8_4 N1_4 C5_4 C4_4 7(2) . . . . ?
 C8_4 N1_4 C5_4 C6_4 -178.0(19) . . . . ?
 C8_4 N2_4 C4_4 C3_4 168.0(16) . . . . ?
 C8_4 N2_4 C4_4 C5_4 -7.4(16) . . . . ?
 C8_4 N2_4 C19_4 C11_4 -20(2) . . . . ?
 C8_4 N2_4 C19_4 C18_4 162.1(16) . . . . ?
 C8_4 C9_4 C10_4 C11_4 -7(3) . . . . ?
 C9_4 C10_4 C11_4 C12_4 175(2) . . . . ?
 C9_4 C10_4 C11_4 C19_4 -3(3) . . . . ?
 C10_4 C11_4 C12_4 C13_4 -176.5(19) . . . . ?
 C10_4 C11_4 C19_4 N2_4 15(2) . . . . ?
 C10_4 C11_4 C19_4 C18_4 -166.7(16) . . . . ?
 C11_4 C12_4 C13_4 C14_4 -12(3) . . . . ?
 C12_4 C11_4 C19_4 N2_4 -162.1(16) . . . . ?
 C12_4 C11_4 C19_4 C18_4 16(2) . . . . ?
 C12_4 C13_4 C14_4 C15_4 173(2) . . . . ?
 C12_4 C13_4 C14_4 C18_4 5(3) . . . . ?
 C13_4 C14_4 C15_4 C16_4 179.4(19) . . . . ?
 C13_4 C14_4 C18_4 N4_4 -171.8(16) . . . . ?
 C13_4 C14_4 C18_4 C19_4 12(3) . . . . ?
 C14_4 C15_4 C16_4 C17_4 -1(3) . . . . ?
 C14_4 C18_4 C19_4 N2_4 155.4(17) . . . . ?
 C14_4 C18_4 C19_4 C11_4 -22(2) . . . . ?
 C15_4 C14_4 C18_4 N4_4 20(3) . . . . ?
 C15_4 C14_4 C18_4 C19_4 -156.5(17) . . . . ?
 C15_4 C16_4 C17_4 N3_4 -172.5(18) . . . . ?
 C15_4 C16_4 C17_4 N4_4 6(3) . . . . ?
 C17_4 N3_4 C20_4 C21_4 175.9(16) . . . . ?
 C17_4 N3_4 C20_4 C25_4 2.7(18) . . . . ?
 C17_4 N4_4 C18_4 C14_4 -15(2) . . . . ?
 C17_4 N4_4 C18_4 C19_4 161.4(15) . . . . ?
 C17_4 N4_4 C25_4 C20_4 -6.8(15) . . . . ?
 C17_4 N4_4 C25_4 C24_4 171.6(16) . . . . ?
 C18_4 N4_4 C17_4 N3_4 -179.4(14) . . . . ?
 C18_4 N4_4 C17_4 C16_4 2(2) . . . . ?
 C18_4 N4_4 C25_4 C20_4 -176.9(14) . . . . ?
 C18_4 N4_4 C25_4 C24_4 2(3) . . . . ?
 C18_4 C14_4 C15_4 C16_4 -12(3) . . . . ?
 C19_4 N2_4 C4_4 C3_4 -9(3) . . . . ?
 C19_4 N2_4 C4_4 C5_4 175.3(15) . . . . ?
 C19_4 N2_4 C8_4 N1_4 -169.9(16) . . . . ?
 C19_4 N2_4 C8_4 C9_4 11(3) . . . . ?
 C19_4 C11_4 C12_4 C13_4 1(3) . . . . ?
 C20_4 N3_4 C17_4 N4_4 -7.4(18) . . . . ?
 C20_4 N3_4 C17_4 C16_4 171.4(17) . . . . ?
 C20_4 C21_4 C22_4 C23_4 3(2) . . . . ?
 C21_4 C20_4 C25_4 N4_4 -171.1(14) . . . . ?
 C21_4 C20_4 C25_4 C24_4 10(2) . . . . ?
 C21_4 C22_4 C23_4 C24_4 3(2) . . . . ?
 C21_4 C22_4 C23_4 C26_4 176.5(14) . . . . ?
 C22_4 C23_4 C24_4 C25_4 -2(2) . . . . ?
 C22_4 C23_4 C26_4 F4_4 -58.7(16) . . . . ?
 C22_4 C23_4 C26_4 F5_4 60.4(17) . . . . ?
 C22_4 C23_4 C26_4 F6_4 -178.3(13) . . . . ?
 C23_4 C24_4 C25_4 N4_4 177.3(14) . . . . ?
 C23_4 C24_4 C25_4 C20_4 -4(2) . . . . ?
 C24_4 C23_4 C26_4 F4_4 115.1(14) . . . . ?
 C24_4 C23_4 C26_4 F5_4 -125.7(14) . . . . ?
 C24_4 C23_4 C26_4 F6_4 -4.4(18) . . . . ?
 C25_4 N4_4 C17_4 N3_4 9.3(18) . . . . ?
 C25_4 N4_4 C17_4 C16_4 -169.6(15) . . . . ?
 C25_4 N4_4 C18_4 C14_4 154.1(16) . . . . ?
 C25_4 N4_4 C18_4 C19_4 -30(2) . . . . ?
 C25_4 C20_4 C21_4 C22_4 -9(2) . . . . ?
 C26_4 C23_4 C24_4 C25_4 -175.7(12) . . . . ?
 F1_5 C1_5 C2_5 C3_5 -111.2(14) . . . . ?
 F1_5 C1_5 C2_5 C7_5 69.9(17) . . . . ?
 F2_5 C1_5 C2_5 C3_5 10.7(17) . . . . ?
 F2_5 C1_5 C2_5 C7_5 -168.2(13) . . . . ?
 F3_5 C1_5 C2_5 C3_5 126.9(13) . . . . ?
 F3_5 C1_5 C2_5 C7_5 -52.0(16) . . . . ?
 N1_5 C5_5 C6_5 C7_5 174.8(14) . . . . ?
 N1_5 C8_5 C9_5 C10_5 -167.2(16) . . . . ?
 N2_5 C4_5 C5_5 N1_5 3.3(15) . . . . ?
 N2_5 C4_5 C5_5 C6_5 -180.0(13) . . . . ?
 N2_5 C8_5 C9_5 C10_5 8(2) . . . . ?
 N3_5 C20_5 C21_5 C22_5 176(2) . . . . ?
 N3_5 C20_5 C25_5 N4_5 4(2) . . . . ?
 N3_5 C20_5 C25_5 C24_5 -173.6(17) . . . . ?
 N4_5 C18_5 C19_5 N2_5 -23(3) . . . . ?
 N4_5 C18_5 C19_5 C11_5 157.3(16) . . . . ?
 C1_5 C2_5 C3_5 C4_5 -174.0(11) . . . . ?
 C1_5 C2_5 C7_5 C6_5 176.7(13) . . . . ?
 C2_5 C3_5 C4_5 N2_5 -179.7(14) . . . . ?
 C2_5 C3_5 C4_5 C5_5 -6.0(19) . . . . ?
 C3_5 C2_5 C7_5 C6_5 -2(2) . . . . ?
 C3_5 C4_5 C5_5 N1_5 -172.2(12) . . . . ?
 C3_5 C4_5 C5_5 C6_5 5(2) . . . . ?
 C4_5 N2_5 C8_5 N1_5 4.2(16) . . . . ?
 C4_5 N2_5 C8_5 C9_5 -171.4(13) . . . . ?
 C4_5 N2_5 C19_5 C11_5 159.3(14) . . . . ?
 C4_5 N2_5 C19_5 C18_5 -21(2) . . . . ?
 C4_5 C5_5 C6_5 C7_5 -1(2) . . . . ?
 C5_5 N1_5 C8_5 N2_5 -2.1(17) . . . . ?
 C5_5 N1_5 C8_5 C9_5 172.9(15) . . . . ?
 C5_5 C6_5 C7_5 C2_5 0(2) . . . . ?
 C7_5 C2_5 C3_5 C4_5 5(2) . . . . ?
 C8_5 N1_5 C5_5 C4_5 -0.8(16) . . . . ?
 C8_5 N1_5 C5_5 C6_5 -177.4(15) . . . . ?
 C8_5 N2_5 C4_5 C3_5 170.4(15) . . . . ?
 C8_5 N2_5 C4_5 C5_5 -4.2(14) . . . . ?
 C8_5 N2_5 C19_5 C11_5 -17(2) . . . . ?
 C8_5 N2_5 C19_5 C18_5 162.9(14) . . . . ?
 C8_5 C9_5 C10_5 C11_5 -9(3) . . . . ?
 C9_5 C10_5 C11_5 C12_5 174.5(18) . . . . ?
 C9_5 C10_5 C11_5 C19_5 -3(3) . . . . ?
 C10_5 C11_5 C12_5 C13_5 175.6(19) . . . . ?
 C10_5 C11_5 C19_5 N2_5 15(2) . . . . ?
 C10_5 C11_5 C19_5 C18_5 -164.6(15) . . . . ?
 C11_5 C12_5 C13_5 C14_5 0(3) . . . . ?
 C12_5 C11_5 C19_5 N2_5 -162.0(15) . . . . ?
 C12_5 C11_5 C19_5 C18_5 18(2) . . . . ?
 C12_5 C13_5 C14_5 C15_5 174(2) . . . . ?
 C12_5 C13_5 C14_5 C18_5 -3(3) . . . . ?
 C13_5 C14_5 C15_5 C16_5 177(2) . . . . ?
 C13_5 C14_5 C18_5 N4_5 -164.9(17) . . . . ?
 C13_5 C14_5 C18_5 C19_5 14(3) . . . . ?
 C14_5 C15_5 C16_5 C17_5 -7(3) . . . . ?
 C14_5 C18_5 C19_5 N2_5 159.0(15) . . . . ?
 C14_5 C18_5 C19_5 C11_5 -21(2) . . . . ?
 C15_5 C14_5 C18_5 N4_5 19(3) . . . . ?
 C15_5 C14_5 C18_5 C19_5 -163.0(17) . . . . ?
 C15_5 C16_5 C17_5 N3_5 -174(2) . . . . ?
 C15_5 C16_5 C17_5 N4_5 8(3) . . . . ?
 C17_5 N3_5 C20_5 C21_5 180(2) . . . . ?
 C17_5 N3_5 C20_5 C25_5 3(2) . . . . ?
 C17_5 N4_5 C18_5 C14_5 -18(2) . . . . ?
 C17_5 N4_5 C18_5 C19_5 163.8(17) . . . . ?
 C17_5 N4_5 C25_5 C20_5 -9(2) . . . . ?
 C17_5 N4_5 C25_5 C24_5 168.7(19) . . . . ?
 C18_5 N4_5 C17_5 N3_5 -173.6(17) . . . . ?
 C18_5 N4_5 C17_5 C16_5 4(3) . . . . ?
 C18_5 N4_5 C25_5 C20_5 176.9(18) . . . . ?
 C18_5 N4_5 C25_5 C24_5 -6(3) . . . . ?
 C18_5 C14_5 C15_5 C16_5 -6(3) . . . . ?
 C19_5 N2_5 C4_5 C3_5 -6(3) . . . . ?
 C19_5 N2_5 C4_5 C5_5 179.1(14) . . . . ?
 C19_5 N2_5 C8_5 N1_5 -178.7(13) . . . . ?
 C19_5 N2_5 C8_5 C9_5 6(2) . . . . ?
 C19_5 C11_5 C12_5 C13_5 -7(3) . . . . ?
 C20_5 N3_5 C17_5 N4_5 -9(2) . . . . ?
 C20_5 N3_5 C17_5 C16_5 174(2) . . . . ?
 C20_5 C21_5 C22_5 C23_5 4(3) . . . . ?
 C21_5 C20_5 C25_5 N4_5 -173.6(19) . . . . ?
 C21_5 C20_5 C25_5 C24_5 9(3) . . . . ?
 C21_5 C22_5 C23_5 C24_5 -2(3) . . . . ?
 C21_5 C22_5 C23_5 C26_5 176.3(18) . . . . ?
 C22_5 C23_5 C24_5 C25_5 4(2) . . . . ?
 C22_5 C23_5 C26_5 F4_5 -71.5(19) . . . . ?
 C22_5 C23_5 C26_5 F5_5 48(2) . . . . ?
 C22_5 C23_5 C26_5 F6_5 174.6(16) . . . . ?
 C23_5 C24_5 C25_5 N4_5 175.7(17) . . . . ?
 C23_5 C24_5 C25_5 C20_5 -7(3) . . . . ?
 C24_5 C23_5 C26_5 F4_5 107.3(15) . . . . ?
 C24_5 C23_5 C26_5 F5_5 -133.7(15) . . . . ?
 C24_5 C23_5 C26_5 F6_5 -6.6(19) . . . . ?
 C25_5 N4_5 C17_5 N3_5 11(2) . . . . ?
 C25_5 N4_5 C17_5 C16_5 -170.9(18) . . . . ?
 C25_5 N4_5 C18_5 C14_5 155.8(18) . . . . ?
 C25_5 N4_5 C18_5 C19_5 -23(3) . . . . ?
 C25_5 C20_5 C21_5 C22_5 -7(3) . . . . ?
 C26_5 C23_5 C24_5 C25_5 -174.9(14) . . . . ?
 F1_6 C1_6 C2_6 C3_6 -114.7(14) . . . . ?
 F1_6 C1_6 C2_6 C7_6 64.6(17) . . . . ?
 F2_6 C1_6 C2_6 C3_6 5.8(17) . . . . ?
 F2_6 C1_6 C2_6 C7_6 -174.9(14) . . . . ?
 F3_6 C1_6 C2_6 C3_6 121.8(14) . . . . ?
 F3_6 C1_6 C2_6 C7_6 -58.9(17) . . . . ?
 N1_6 C5_6 C6_6 C7_6 -179.9(19) . . . . ?
 N1_6 C8_6 C9_6 C10_6 -173(2) . . . . ?
 N2_6 C4_6 C5_6 N1_6 -3(2) . . . . ?
 N2_6 C4_6 C5_6 C6_6 -172.8(17) . . . . ?
 N2_6 C8_6 C9_6 C10_6 3(3) . . . . ?
 N3_6 C20_6 C21_6 C22_6 173.9(15) . . . . ?
 N3_6 C20_6 C25_6 N4_6 7.4(15) . . . . ?
 N3_6 C20_6 C25_6 C24_6 -173.6(12) . . . . ?
 N4_6 C18_6 C19_6 N2_6 -23(2) . . . . ?
 N4_6 C18_6 C19_6 C11_6 156.5(12) . . . . ?
 C1_6 C2_6 C3_6 C4_6 -176.5(12) . . . . ?
 C1_6 C2_6 C7_6 C6_6 179.0(17) . . . . ?
 C2_6 C3_6 C4_6 N2_6 179.9(15) . . . . ?
 C2_6 C3_6 C4_6 C5_6 -11(2) . . . . ?
 C3_6 C2_6 C7_6 C6_6 -2(3) . . . . ?
 C3_6 C4_6 C5_6 N1_6 -175.3(16) . . . . ?
 C3_6 C4_6 C5_6 C6_6 15(3) . . . . ?
 C4_6 N2_6 C8_6 N1_6 5(2) . . . . ?
 C4_6 N2_6 C8_6 C9_6 -170.9(16) . . . . ?
 C4_6 N2_6 C19_6 C11_6 161.0(14) . . . . ?
 C4_6 N2_6 C19_6 C18_6 -19(2) . . . . ?
 C4_6 C5_6 C6_6 C7_6 -12(3) . . . . ?
 C5_6 N1_6 C8_6 N2_6 -7(2) . . . . ?
 C5_6 N1_6 C8_6 C9_6 168.8(19) . . . . ?
 C5_6 C6_6 C7_6 C2_6 5(3) . . . . ?
 C7_6 C2_6 C3_6 C4_6 4(2) . . . . ?
 C8_6 N1_6 C5_6 C4_6 6(2) . . . . ?
 C8_6 N1_6 C5_6 C6_6 175(2) . . . . ?
 C8_6 N2_6 C4_6 C3_6 169.7(17) . . . . ?
 C8_6 N2_6 C4_6 C5_6 -1.1(17) . . . . ?
 C8_6 N2_6 C19_6 C11_6 -20.0(19) . . . . ?
 C8_6 N2_6 C19_6 C18_6 159.6(14) . . . . ?
 C8_6 C9_6 C10_6 C11_6 -4(3) . . . . ?
 C9_6 C10_6 C11_6 C12_6 178.1(18) . . . . ?
 C9_6 C10_6 C11_6 C19_6 -7(3) . . . . ?
 C10_6 C11_6 C12_6 C13_6 176.1(17) . . . . ?
 C10_6 C11_6 C19_6 N2_6 18.2(19) . . . . ?
 C10_6 C11_6 C19_6 C18_6 -161.5(14) . . . . ?
 C11_6 C12_6 C13_6 C14_6 -7(3) . . . . ?
 C12_6 C11_6 C19_6 N2_6 -166.3(13) . . . . ?
 C12_6 C11_6 C19_6 C18_6 14(2) . . . . ?
 C12_6 C13_6 C14_6 C15_6 179.8(17) . . . . ?
 C12_6 C13_6 C14_6 C18_6 -3(3) . . . . ?
 C13_6 C14_6 C15_6 C16_6 173.9(17) . . . . ?
 C13_6 C14_6 C18_6 N4_6 -162.5(14) . . . . ?
 C13_6 C14_6 C18_6 C19_6 17(2) . . . . ?
 C14_6 C15_6 C16_6 C17_6 -4(3) . . . . ?
 C14_6 C18_6 C19_6 N2_6 157.0(13) . . . . ?
 C14_6 C18_6 C19_6 C11_6 -23.4(19) . . . . ?
 C15_6 C14_6 C18_6 N4_6 15(2) . . . . ?
 C15_6 C14_6 C18_6 C19_6 -164.9(14) . . . . ?
 C15_6 C16_6 C17_6 N3_6 -164.7(15) . . . . ?
 C15_6 C16_6 C17_6 N4_6 0(2) . . . . ?
 C17_6 N3_6 C20_6 C21_6 -176.7(16) . . . . ?
 C17_6 N3_6 C20_6 C25_6 -5.0(16) . . . . ?
 C17_6 N4_6 C18_6 C14_6 -20.1(18) . . . . ?
 C17_6 N4_6 C18_6 C19_6 160.1(12) . . . . ?
 C17_6 N4_6 C25_6 C20_6 -6.6(13) . . . . ?
 C17_6 N4_6 C25_6 C24_6 174.5(13) . . . . ?
 C18_6 N4_6 C17_6 N3_6 179.5(12) . . . . ?
 C18_6 N4_6 C17_6 C16_6 12.2(19) . . . . ?
 C18_6 N4_6 C25_6 C20_6 178.3(13) . . . . ?
 C18_6 N4_6 C25_6 C24_6 -1(2) . . . . ?
 C18_6 C14_6 C15_6 C16_6 -4(3) . . . . ?
 C19_6 N2_6 C4_6 C3_6 -11(3) . . . . ?
 C19_6 N2_6 C4_6 C5_6 178.0(15) . . . . ?
 C19_6 N2_6 C8_6 N1_6 -173.8(15) . . . . ?
 C19_6 N2_6 C8_6 C9_6 10(2) . . . . ?
 C19_6 C11_6 C12_6 C13_6 1(2) . . . . ?
 C20_6 N3_6 C17_6 N4_6 0.6(16) . . . . ?
 C20_6 N3_6 C17_6 C16_6 166.4(14) . . . . ?
 C20_6 C21_6 C22_6 C23_6 -3(3) . . . . ?
 C21_6 C20_6 C25_6 N4_6 -179.8(13) . . . . ?
 C21_6 C20_6 C25_6 C24_6 -1(2) . . . . ?
 C21_6 C22_6 C23_6 C24_6 2(2) . . . . ?
 C21_6 C22_6 C23_6 C26_6 -179.3(14) . . . . ?
 C22_6 C23_6 C24_6 C25_6 0(2) . . . . ?
 C22_6 C23_6 C26_6 F4_6 -53.6(17) . . . . ?
 C22_6 C23_6 C26_6 F5_6 64.2(16) . . . . ?
 C22_6 C23_6 C26_6 F6_6 -172.5(13) . . . . ?
 C23_6 C24_6 C25_6 N4_6 178.2(13) . . . . ?
 C23_6 C24_6 C25_6 C20_6 -0.5(19) . . . . ?
 C24_6 C23_6 C26_6 F4_6 124.9(13) . . . . ?
 C24_6 C23_6 C26_6 F5_6 -117.3(13) . . . . ?
 C24_6 C23_6 C26_6 F6_6 6.0(17) . . . . ?
 C25_6 N4_6 C17_6 N3_6 3.9(15) . . . . ?
 C25_6 N4_6 C17_6 C16_6 -163.5(12) . . . . ?
 C25_6 N4_6 C18_6 C14_6 154.3(13) . . . . ?
 C25_6 N4_6 C18_6 C19_6 -26(2) . . . . ?
 C25_6 C20_6 C21_6 C22_6 3(2) . . . . ?
 C26_6 C23_6 C24_6 C25_6 -178.6(11) . . . . ?
 F1_7 C1_7 C2_7 C3_7 -119.2(13) . . . . ?
 F1_7 C1_7 C2_7 C7_7 62.2(16) . . . . ?
 F2_7 C1_7 C2_7 C3_7 2.0(17) . . . . ?
 F2_7 C1_7 C2_7 C7_7 -176.7(13) . . . . ?
 F3_7 C1_7 C2_7 C3_7 120.9(13) . . . . ?
 F3_7 C1_7 C2_7 C7_7 -57.8(16) . . . . ?
 N1_7 C5_7 C6_7 C7_7 -179.2(16) . . . . ?
 N1_7 C8_7 C9_7 C10_7 -170(2) . . . . ?
 N2_7 C4_7 C5_7 N1_7 1.2(16) . . . . ?
 N2_7 C4_7 C5_7 C6_7 -176.5(14) . . . . ?
 N2_7 C8_7 C9_7 C10_7 7(3) . . . . ?
 N3_7 C20_7 C21_7 C22_7 179.0(15) . . . . ?
 N3_7 C20_7 C25_7 N4_7 6.8(16) . . . . ?
 N3_7 C20_7 C25_7 C24_7 -178.0(12) . . . . ?
 N4_7 C18_7 C19_7 N2_7 -22(3) . . . . ?
 N4_7 C18_7 C19_7 C11_7 157.3(15) . . . . ?
 C1_7 C2_7 C3_7 C4_7 -176.8(11) . . . . ?
 C1_7 C2_7 C7_7 C6_7 179.7(13) . . . . ?
 C2_7 C3_7 C4_7 N2_7 177.2(13) . . . . ?
 C2_7 C3_7 C4_7 C5_7 -5(2) . . . . ?
 C3_7 C2_7 C7_7 C6_7 1(2) . . . . ?
 C3_7 C4_7 C5_7 N1_7 -177.1(12) . . . . ?
 C3_7 C4_7 C5_7 C6_7 5(2) . . . . ?
 C4_7 N2_7 C8_7 N1_7 8.9(18) . . . . ?
 C4_7 N2_7 C8_7 C9_7 -169.0(14) . . . . ?
 C4_7 N2_7 C19_7 C11_7 156.6(15) . . . . ?
 C4_7 N2_7 C19_7 C18_7 -24(3) . . . . ?
 C4_7 C5_7 C6_7 C7_7 -2(2) . . . . ?
 C5_7 N1_7 C8_7 N2_7 -8.1(19) . . . . ?
 C5_7 N1_7 C8_7 C9_7 169.5(17) . . . . ?
 C5_7 C6_7 C7_7 C2_7 -1(2) . . . . ?
 C7_7 C2_7 C3_7 C4_7 1.8(19) . . . . ?
 C8_7 N1_7 C5_7 C4_7 4.1(18) . . . . ?
 C8_7 N1_7 C5_7 C6_7 -178.6(17) . . . . ?
 C8_7 N2_7 C4_7 C3_7 172.5(15) . . . . ?
 C8_7 N2_7 C4_7 C5_7 -5.5(15) . . . . ?
 C8_7 N2_7 C19_7 C11_7 -18(2) . . . . ?
 C8_7 N2_7 C19_7 C18_7 162.3(15) . . . . ?
 C8_7 C9_7 C10_7 C11_7 -9(3) . . . . ?
 C9_7 C10_7 C11_7 C12_7 179(2) . . . . ?
 C9_7 C10_7 C11_7 C19_7 -2(3) . . . . ?
 C10_7 C11_7 C12_7 C13_7 -180(2) . . . . ?
 C10_7 C11_7 C19_7 N2_7 15(2) . . . . ?
 C10_7 C11_7 C19_7 C18_7 -164.8(17) . . . . ?
 C11_7 C12_7 C13_7 C14_7 -10(3) . . . . ?
 C12_7 C11_7 C19_7 N2_7 -165.8(16) . . . . ?
 C12_7 C11_7 C19_7 C18_7 14(2) . . . . ?
 C12_7 C13_7 C14_7 C15_7 174.2(19) . . . . ?
 C12_7 C13_7 C14_7 C18_7 3(3) . . . . ?
 C13_7 C14_7 C15_7 C16_7 -176.5(19) . . . . ?
 C13_7 C14_7 C18_7 N4_7 -166.1(16) . . . . ?
 C13_7 C14_7 C18_7 C19_7 12(2) . . . . ?
 C14_7 C15_7 C16_7 C17_7 -13(3) . . . . ?
 C14_7 C18_7 C19_7 N2_7 159.4(15) . . . . ?
 C14_7 C18_7 C19_7 C11_7 -21(2) . . . . ?
 C15_7 C14_7 C18_7 N4_7 22(2) . . . . ?
 C15_7 C14_7 C18_7 C19_7 -159.3(16) . . . . ?
 C15_7 C16_7 C17_7 N3_7 -166.8(17) . . . . ?
 C15_7 C16_7 C17_7 N4_7 14(2) . . . . ?
 C17_7 N3_7 C20_7 C21_7 179.2(16) . . . . ?
 C17_7 N3_7 C20_7 C25_7 -2.4(17) . . . . ?
 C17_7 N4_7 C18_7 C14_7 -22(2) . . . . ?
 C17_7 N4_7 C18_7 C19_7 160.1(15) . . . . ?
 C17_7 N4_7 C25_7 C20_7 -8.0(14) . . . . ?
 C17_7 N4_7 C25_7 C24_7 177.4(14) . . . . ?
 C18_7 N4_7 C17_7 N3_7 -176.2(14) . . . . ?
 C18_7 N4_7 C17_7 C16_7 3(2) . . . . ?
 C18_7 N4_7 C25_7 C20_7 176.2(14) . . . . ?
 C18_7 N4_7 C25_7 C24_7 2(3) . . . . ?
 C18_7 C14_7 C15_7 C16_7 -5(3) . . . . ?
 C19_7 N2_7 C4_7 C3_7 -2(3) . . . . ?
 C19_7 N2_7 C4_7 C5_7 179.5(14) . . . . ?
 C19_7 N2_7 C8_7 N1_7 -175.6(14) . . . . ?
 C19_7 N2_7 C8_7 C9_7 6(2) . . . . ?
 C19_7 C11_7 C12_7 C13_7 1(3) . . . . ?
 C20_7 N3_7 C17_7 N4_7 -3.2(18) . . . . ?
 C20_7 N3_7 C17_7 C16_7 177.2(17) . . . . ?
 C20_7 C21_7 C22_7 C23_7 -4(2) . . . . ?
 C21_7 C20_7 C25_7 N4_7 -174.7(13) . . . . ?
 C21_7 C20_7 C25_7 C24_7 1(2) . . . . ?
 C21_7 C22_7 C23_7 C24_7 6(2) . . . . ?
 C21_7 C22_7 C23_7 C26_7 179.5(14) . . . . ?
 C22_7 C23_7 C24_7 C25_7 -5(2) . . . . ?
 C22_7 C23_7 C26_7 F4_7 -162.3(12) . . . . ?
 C22_7 C23_7 C26_7 F5_7 78.8(14) . . . . ?
 C22_7 C23_7 C26_7 F6_7 -41.8(16) . . . . ?
 C23_7 C24_7 C25_7 N4_7 175.3(13) . . . . ?
 C23_7 C24_7 C25_7 C20_7 1.6(19) . . . . ?
 C24_7 C23_7 C26_7 F4_7 10.9(17) . . . . ?
 C24_7 C23_7 C26_7 F5_7 -108.0(13) . . . . ?
 C24_7 C23_7 C26_7 F6_7 131.4(12) . . . . ?
 C25_7 N4_7 C17_7 N3_7 7.4(17) . . . . ?
 C25_7 N4_7 C17_7 C16_7 -172.9(15) . . . . ?
 C25_7 N4_7 C18_7 C14_7 153.6(15) . . . . ?
 C25_7 N4_7 C18_7 C19_7 -25(3) . . . . ?
 C25_7 C20_7 C21_7 C22_7 1(2) . . . . ?
 C26_7 C23_7 C24_7 C25_7 -177.8(11) . . . . ?
 F1_8 C1_8 C2_8 C3_8 -119.0(14) . . . . ?
 F1_8 C1_8 C2_8 C7_8 62.5(17) . . . . ?
 F2_8 C1_8 C2_8 C3_8 1.6(17) . . . . ?
 F2_8 C1_8 C2_8 C7_8 -176.9(13) . . . . ?
 F3_8 C1_8 C2_8 C3_8 118.6(13) . . . . ?
 F3_8 C1_8 C2_8 C7_8 -59.8(17) . . . . ?
 N1_8 C5_8 C6_8 C7_8 174.0(19) . . . . ?
 N1_8 C8_8 C9_8 C10_8 -164(2) . . . . ?
 N2_8 C4_8 C5_8 N1_8 7.0(19) . . . . ?
 N2_8 C4_8 C5_8 C6_8 179.3(16) . . . . ?
 N2_8 C8_8 C9_8 C10_8 5(3) . . . . ?
 N3_8 C20_8 C21_8 C22_8 176.9(16) . . . . ?
 N3_8 C20_8 C25_8 N4_8 3.9(17) . . . . ?
 N3_8 C20_8 C25_8 C24_8 -178.6(13) . . . . ?
 N4_8 C18_8 C19_8 N2_8 -23(2) . . . . ?
 N4_8 C18_8 C19_8 C11_8 158.9(15) . . . . ?
 C1_8 C2_8 C3_8 C4_8 -179.0(12) . . . . ?
 C1_8 C2_8 C7_8 C6_8 -177.6(15) . . . . ?
 C2_8 C3_8 C4_8 N2_8 179.6(14) . . . . ?
 C2_8 C3_8 C4_8 C5_8 -1(2) . . . . ?
 C3_8 C2_8 C7_8 C6_8 4(3) . . . . ?
 C3_8 C4_8 C5_8 N1_8 -172.1(15) . . . . ?
 C3_8 C4_8 C5_8 C6_8 0(3) . . . . ?
 C4_8 N2_8 C8_8 N1_8 2(2) . . . . ?
 C4_8 N2_8 C8_8 C9_8 -168.3(16) . . . . ?
 C4_8 N2_8 C19_8 C11_8 157.0(16) . . . . ?
 C4_8 N2_8 C19_8 C18_8 -21(3) . . . . ?
 C4_8 C5_8 C6_8 C7_8 3(3) . . . . ?
 C5_8 N1_8 C8_8 N2_8 2(2) . . . . ?
 C5_8 N1_8 C8_8 C9_8 171(2) . . . . ?
 C5_8 C6_8 C7_8 C2_8 -5(3) . . . . ?
 C7_8 C2_8 C3_8 C4_8 -1(2) . . . . ?
 C8_8 N1_8 C5_8 C4_8 -6(2) . . . . ?
 C8_8 N1_8 C5_8 C6_8 -177(2) . . . . ?
 C8_8 N2_8 C4_8 C3_8 173.8(16) . . . . ?
 C8_8 N2_8 C4_8 C5_8 -5.3(17) . . . . ?
 C8_8 N2_8 C19_8 C11_8 -23(2) . . . . ?
 C8_8 N2_8 C19_8 C18_8 158.7(16) . . . . ?
 C8_8 C9_8 C10_8 C11_8 -9(3) . . . . ?
 C9_8 C10_8 C11_8 C12_8 177(2) . . . . ?
 C9_8 C10_8 C11_8 C19_8 -3(3) . . . . ?
 C10_8 C11_8 C12_8 C13_8 177.5(19) . . . . ?
 C10_8 C11_8 C19_8 N2_8 18(2) . . . . ?
 C10_8 C11_8 C19_8 C18_8 -163.3(17) . . . . ?
 C11_8 C12_8 C13_8 C14_8 -3(3) . . . . ?
 C12_8 C11_8 C19_8 N2_8 -161.8(15) . . . . ?
 C12_8 C11_8 C19_8 C18_8 17(2) . . . . ?
 C12_8 C13_8 C14_8 C15_8 178.0(19) . . . . ?
 C12_8 C13_8 C14_8 C18_8 -5(3) . . . . ?
 C13_8 C14_8 C15_8 C16_8 179.2(19) . . . . ?
 C13_8 C14_8 C18_8 N4_8 -164.6(14) . . . . ?
 C13_8 C14_8 C18_8 C19_8 19(2) . . . . ?
 C14_8 C15_8 C16_8 C17_8 -11(3) . . . . ?
 C14_8 C18_8 C19_8 N2_8 153.0(15) . . . . ?
 C14_8 C18_8 C19_8 C11_8 -25(2) . . . . ?
 C15_8 C14_8 C18_8 N4_8 13(2) . . . . ?
 C15_8 C14_8 C18_8 C19_8 -163.4(16) . . . . ?
 C15_8 C16_8 C17_8 N3_8 -170.2(18) . . . . ?
 C15_8 C16_8 C17_8 N4_8 4(3) . . . . ?
 C17_8 N3_8 C20_8 C21_8 -178.8(17) . . . . ?
 C17_8 N3_8 C20_8 C25_8 -0.1(19) . . . . ?
 C17_8 N4_8 C18_8 C14_8 -20(2) . . . . ?
 C17_8 N4_8 C18_8 C19_8 156.3(15) . . . . ?
 C17_8 N4_8 C25_8 C20_8 -5.8(15) . . . . ?
 C17_8 N4_8 C25_8 C24_8 177.0(15) . . . . ?
 C18_8 N4_8 C17_8 N3_8 -173.6(14) . . . . ?
 C18_8 N4_8 C17_8 C16_8 11(2) . . . . ?
 C18_8 N4_8 C25_8 C20_8 174.1(14) . . . . ?
 C18_8 N4_8 C25_8 C24_8 -3(3) . . . . ?
 C18_8 C14_8 C15_8 C16_8 2(3) . . . . ?
 C19_8 N2_8 C4_8 C3_8 -6(3) . . . . ?
 C19_8 N2_8 C4_8 C5_8 174.7(16) . . . . ?
 C19_8 N2_8 C8_8 N1_8 -177.9(15) . . . . ?
 C19_8 N2_8 C8_8 C9_8 12(2) . . . . ?
 C19_8 C11_8 C12_8 C13_8 -2(3) . . . . ?
 C20_8 N3_8 C17_8 N4_8 -3.9(19) . . . . ?
 C20_8 N3_8 C17_8 C16_8 170.8(18) . . . . ?
 C20_8 C21_8 C22_8 C23_8 2(2) . . . . ?
 C21_8 C20_8 C25_8 N4_8 -177.3(14) . . . . ?
 C21_8 C20_8 C25_8 C24_8 0(2) . . . . ?
 C21_8 C22_8 C23_8 C24_8 -1(2) . . . . ?
 C21_8 C22_8 C23_8 C26_8 177.5(14) . . . . ?
 C22_8 C23_8 C24_8 C25_8 0(2) . . . . ?
 C22_8 C23_8 C26_8 F4_8 -54.1(16) . . . . ?
 C22_8 C23_8 C26_8 F5_8 63.1(16) . . . . ?
 C22_8 C23_8 C26_8 F6_8 -174.4(13) . . . . ?
 C23_8 C24_8 C25_8 N4_8 177.5(14) . . . . ?
 C23_8 C24_8 C25_8 C20_8 1(2) . . . . ?
 C24_8 C23_8 C26_8 F4_8 124.7(13) . . . . ?
 C24_8 C23_8 C26_8 F5_8 -118.0(14) . . . . ?
 C24_8 C23_8 C26_8 F6_8 4.5(18) . . . . ?
 C25_8 N4_8 C17_8 N3_8 6.3(18) . . . . ?
 C25_8 N4_8 C17_8 C16_8 -169.0(15) . . . . ?
 C25_8 N4_8 C18_8 C14_8 160.5(14) . . . . ?
 C25_8 N4_8 C18_8 C19_8 -24(2) . . . . ?
 C25_8 C20_8 C21_8 C22_8 -2(2) . . . . ?
 C26_8 C23_8 C24_8 C25_8 -178.9(12) . . . . ?
 F1_9 C1_9 C2_9 C3_9 -111.1(15) . . . . ?
 F1_9 C1_9 C2_9 C7_9 72.6(18) . . . . ?
 F2_9 C1_9 C2_9 C3_9 11.6(18) . . . . ?
 F2_9 C1_9 C2_9 C7_9 -164.7(14) . . . . ?
 F3_9 C1_9 C2_9 C3_9 127.1(14) . . . . ?
 F3_9 C1_9 C2_9 C7_9 -49.2(18) . . . . ?
 N1_9 C5_9 C6_9 C7_9 174.4(17) . . . . ?
 N1_9 C8_9 C9_9 C10_9 -169(2) . . . . ?
 N2_9 C4_9 C5_9 N1_9 12.2(18) . . . . ?
 N2_9 C4_9 C5_9 C6_9 -178.5(15) . . . . ?
 N2_9 C8_9 C9_9 C10_9 -2(3) . . . . ?
 N3_9 C20_9 C21_9 C22_9 178.8(16) . . . . ?
 N3_9 C20_9 C25_9 N4_9 -0.7(18) . . . . ?
 N3_9 C20_9 C25_9 C24_9 -172.5(13) . . . . ?
 N4_9 C18_9 C19_9 N2_9 -25(2) . . . . ?
 N4_9 C18_9 C19_9 C11_9 156.9(14) . . . . ?
 C1_9 C2_9 C3_9 C4_9 -177.4(12) . . . . ?
 C1_9 C2_9 C7_9 C6_9 180.0(15) . . . . ?
 C2_9 C3_9 C4_9 N2_9 173.1(15) . . . . ?
 C2_9 C3_9 C4_9 C5_9 2(2) . . . . ?
 C3_9 C2_9 C7_9 C6_9 4(3) . . . . ?
 C3_9 C4_9 C5_9 N1_9 -174.4(14) . . . . ?
 C3_9 C4_9 C5_9 C6_9 -5(2) . . . . ?
 C4_9 N2_9 C8_9 N1_9 5(2) . . . . ?
 C4_9 N2_9 C8_9 C9_9 -163.5(16) . . . . ?
 C4_9 N2_9 C19_9 C11_9 153.8(16) . . . . ?
 C4_9 N2_9 C19_9 C18_9 -25(2) . . . . ?
 C4_9 C5_9 C6_9 C7_9 7(3) . . . . ?
 C5_9 N1_9 C8_9 N2_9 2(2) . . . . ?
 C5_9 N1_9 C8_9 C9_9 169(2) . . . . ?
 C5_9 C6_9 C7_9 C2_9 -7(3) . . . . ?
 C7_9 C2_9 C3_9 C4_9 -1(2) . . . . ?
 C8_9 N1_9 C5_9 C4_9 -9(2) . . . . ?
 C8_9 N1_9 C5_9 C6_9 -177.2(19) . . . . ?
 C8_9 N2_9 C4_9 C3_9 177.5(17) . . . . ?
 C8_9 N2_9 C4_9 C5_9 -10.2(16) . . . . ?
 C8_9 N2_9 C19_9 C11_9 -22(2) . . . . ?
 C8_9 N2_9 C19_9 C18_9 159.6(15) . . . . ?
 C8_9 C9_9 C10_9 C11_9 1(3) . . . . ?
 C9_9 C10_9 C11_9 C12_9 177(2) . . . . ?
 C9_9 C10_9 C11_9 C19_9 -9(3) . . . . ?
 C10_9 C11_9 C12_9 C13_9 178.1(19) . . . . ?
 C10_9 C11_9 C19_9 N2_9 19(2) . . . . ?
 C10_9 C11_9 C19_9 C18_9 -162.2(16) . . . . ?
 C11_9 C12_9 C13_9 C14_9 -11(3) . . . . ?
 C12_9 C11_9 C19_9 N2_9 -166.9(15) . . . . ?
 C12_9 C11_9 C19_9 C18_9 12(2) . . . . ?
 C12_9 C13_9 C14_9 C15_9 -177.4(17) . . . . ?
 C12_9 C13_9 C14_9 C18_9 1(2) . . . . ?
 C13_9 C14_9 C15_9 C16_9 177.2(17) . . . . ?
 C13_9 C14_9 C18_9 N4_9 -163.4(14) . . . . ?
 C13_9 C14_9 C18_9 C19_9 15(2) . . . . ?
 C14_9 C15_9 C16_9 C17_9 -7(3) . . . . ?
 C14_9 C18_9 C19_9 N2_9 156.9(14) . . . . ?
 C14_9 C18_9 C19_9 C11_9 -22(2) . . . . ?
 C15_9 C14_9 C18_9 N4_9 15(2) . . . . ?
 C15_9 C14_9 C18_9 C19_9 -166.0(15) . . . . ?
 C15_9 C16_9 C17_9 N3_9 -166.5(19) . . . . ?
 C15_9 C16_9 C17_9 N4_9 2(3) . . . . ?
 C17_9 N3_9 C20_9 C21_9 -176.9(18) . . . . ?
 C17_9 N3_9 C20_9 C25_9 2.2(19) . . . . ?
 C17_9 N4_9 C18_9 C14_9 -21(2) . . . . ?
 C17_9 N4_9 C18_9 C19_9 160.4(14) . . . . ?
 C17_9 N4_9 C25_9 C20_9 -1.1(15) . . . . ?
 C17_9 N4_9 C25_9 C24_9 169.5(15) . . . . ?
 C18_9 N4_9 C17_9 N3_9 -177.4(14) . . . . ?
 C18_9 N4_9 C17_9 C16_9 12(2) . . . . ?
 C18_9 N4_9 C25_9 C20_9 178.9(14) . . . . ?
 C18_9 N4_9 C25_9 C24_9 -11(3) . . . . ?
 C18_9 C14_9 C15_9 C16_9 -2(3) . . . . ?
 C19_9 N2_9 C4_9 C3_9 1(3) . . . . ?
 C19_9 N2_9 C4_9 C5_9 173.5(15) . . . . ?
 C19_9 N2_9 C8_9 N1_9 -177.9(15) . . . . ?
 C19_9 N2_9 C8_9 C9_9 13(2) . . . . ?
 C19_9 C11_9 C12_9 C13_9 5(3) . . . . ?
 C20_9 N3_9 C17_9 N4_9 -3(2) . . . . ?
 C20_9 N3_9 C17_9 C16_9 166.2(18) . . . . ?
 C20_9 C21_9 C22_9 C23_9 -7(2) . . . . ?
 C21_9 C20_9 C25_9 N4_9 178.6(14) . . . . ?
 C21_9 C20_9 C25_9 C24_9 7(2) . . . . ?
 C21_9 C22_9 C23_9 C24_9 8(2) . . . . ?
 C21_9 C22_9 C23_9 C26_9 -177.7(13) . . . . ?
 C22_9 C23_9 C24_9 C25_9 -2(2) . . . . ?
 C22_9 C23_9 C26_9 F4_9 -56.3(15) . . . . ?
 C22_9 C23_9 C26_9 F5_9 64.1(15) . . . . ?
 C22_9 C23_9 C26_9 F6_9 -174.0(12) . . . . ?
 C23_9 C24_9 C25_9 N4_9 -174.8(13) . . . . ?
 C23_9 C24_9 C25_9 C20_9 -5(2) . . . . ?
 C24_9 C23_9 C26_9 F4_9 117.8(13) . . . . ?
 C24_9 C23_9 C26_9 F5_9 -121.8(13) . . . . ?
 C24_9 C23_9 C26_9 F6_9 0.2(16) . . . . ?
 C25_9 N4_9 C17_9 N3_9 2.6(19) . . . . ?
 C25_9 N4_9 C17_9 C16_9 -167.7(15) . . . . ?
 C25_9 N4_9 C18_9 C14_9 158.9(14) . . . . ?
 C25_9 N4_9 C18_9 C19_9 -20(2) . . . . ?
 C25_9 C20_9 C21_9 C22_9 0(2) . . . . ?
 C26_9 C23_9 C24_9 C25_9 -175.8(11) . . . . ?

_olex2_submission_special_instructions  'No special instructions were received'

# start Validation Reply Form
_vrf_PLAT340_a1
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PROBLEM: Low Bond Precision on  C-C Bonds ...............    0.01807 Ang.  
RESPONSE:  Due to weak diffraction of the sample.
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# end Validation Reply Form
