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2.20 -4 4 0 2.30 0.40 -4 4 0 0.50 1.00 -4 4 0 1.30 0.40 -5 -4 0 155.38 10.30 -5 -4 0 168.68 20.60 -5 -4 0 168.68 15.60 5 4 0 134.59 16.50 -5 4 0 124.29 14.40 -5 4 0 141.59 12.20 5 4 0 150.98 10.20 -5 4 0 156.18 10.10 -5 4 0 146.89 10.10 -6 -4 0 47.50 7.30 -6 -4 0 35.00 10.80 6 -4 0 41.80 2.90 6 4 0 27.70 10.60 -6 4 0 29.20 6.20 6 4 0 35.70 2.80 -6 4 0 35.60 2.70 7 -4 0 1.90 0.60 -7 -4 0 2.00 2.60 -7 -4 0 0.80 6.50 7 4 0 2.50 0.60 8 -4 0 18.30 1.90 -8 -4 0 20.10 4.60 -8 -4 0 14.00 8.60 -8 4 0 21.40 9.90 8 4 0 17.60 1.70 -9 -4 0 1.20 5.50 -9 4 0 -0.60 6.40 9 4 0 0.90 0.60 0 -5 0 0.70 0.40 0 -5 0 2.40 1.20 0 -5 0 0.30 3.00 0 -5 0 1.10 1.60 0 5 0 0.70 1.30 0 5 0 6.80 3.50 0 5 0 1.30 0.40 -1 -5 0 227.08 17.70 -1 -5 0 219.28 17.00 1 -5 0 193.78 13.40 -1 -5 0 199.08 13.50 -1 5 0 194.68 13.40 1 5 0 181.18 17.00 -1 5 0 188.28 16.70 1 5 0 173.68 17.80 1 5 0 203.48 13.40 -1 5 0 208.98 14.60 2 -5 0 1014.70 64.69 2 -5 0 880.31 62.39 -2 5 0 887.71 62.29 3 -5 0 1.10 0.30 3 -5 0 6.50 3.50 -3 -5 0 2.00 0.60 3 5 0 1.20 4.00 3 5 0 4.00 3.90 3 5 0 1.30 3.30 -3 5 0 1.70 0.30 -3 5 0 1.00 1.50 -3 5 0 4.80 1.40 -3 5 0 1.50 0.40 -3 5 0 1.70 2.90 4 -5 0 8.10 0.80 -4 -5 0 7.30 4.80 -4 -5 0 10.90 4.50 -4 -5 0 9.90 1.20 -4 5 0 9.70 2.90 -4 5 0 7.80 0.80 4 5 0 11.10 6.40 4 5 0 7.70 5.50 -4 5 0 8.40 0.90 -4 5 0 8.60 4.60 -5 -5 0 2.70 3.20 -5 -5 0 -1.30 3.60 5 5 0 -7.70 4.00 5 5 0 5.50 5.00 5 5 0 4.60 5.40 -5 5 0 3.30 2.30 5 5 0 1.00 0.40 -5 5 0 1.10 0.50 -5 5 0 2.10 2.00 -6 -5 0 2.50 7.00 -6 -5 0 0.10 0.60 -6 -5 0 1.10 2.60 6 5 0 -0.10 0.30 -6 5 0 -2.00 2.40 -6 5 0 -1.60 4.30 -7 -5 0 0.60 2.80 -7 -5 0 2.10 5.20 7 5 0 1.50 0.50 -8 -5 0 6.10 3.60 -8 -5 0 -0.90 4.90 -8 5 0 7.70 8.20 8 5 0 5.80 1.00 -9 -5 0 1.60 5.70 -9 5 0 -8.30 6.90 9 5 0 1.60 0.70 0 -6 0 321.97 20.90 0 6 0 295.87 25.80 0 6 0 280.27 24.50 0 6 0 330.67 20.90 -1 -6 0 135.39 11.60 -1 -6 0 120.09 8.10 1 -6 0 114.99 8.00 1 -6 0 134.49 11.20 -1 -6 0 128.39 12.40 1 6 0 102.79 12.70 1 6 0 115.29 8.00 -1 6 0 107.49 13.20 1 6 0 97.69 11.60 -1 6 0 115.39 8.00 -1 6 0 105.69 9.40 -2 6 0 649.83 44.00 -2 6 0 567.34 41.30 3 -6 0 318.47 22.20 -3 -6 0 335.47 22.40 -3 -6 0 339.97 29.60 -3 -6 0 362.06 28.40 -3 6 0 335.27 22.10 -3 6 0 319.77 25.90 -3 6 0 325.77 22.20 4 -6 0 206.08 14.20 -4 -6 0 226.78 20.40 -4 -6 0 229.38 23.40 4 6 0 187.78 22.50 -4 6 0 203.68 17.90 -4 6 0 248.38 18.90 -4 6 0 208.78 14.20 -4 6 0 203.18 14.10 4 6 0 194.38 20.90 -5 -6 0 -0.20 0.70 -5 -6 0 -1.30 2.40 -5 -6 0 3.30 4.50 -5 6 0 0.20 0.50 -5 6 0 1.70 1.70 5 6 0 2.70 5.10 -5 6 0 -1.30 5.30 5 6 0 0.80 0.40 -5 6 0 0.30 0.30 -6 -6 0 23.40 9.00 -6 -6 0 26.50 6.60 -6 6 0 20.90 7.10 6 6 0 27.50 2.20 -7 -6 0 0.50 2.90 -7 -6 0 -2.00 4.30 7 6 0 2.70 0.60 -8 -6 0 8.00 3.90 -8 -6 0 2.60 6.20 -8 6 0 -5.60 8.30 8 6 0 7.40 1.10 -9 -6 0 21.70 10.90 -9 6 0 14.90 10.00 9 6 0 32.90 2.70 0 -7 0 2.10 1.50 0 -7 0 2.80 2.30 0 -7 0 -0.50 3.90 0 7 0 2.50 0.60 0 7 0 5.00 5.00 0 7 0 1.40 1.70 0 7 0 0.80 2.40 1 -7 0 532.05 34.70 -1 -7 0 606.94 38.90 -1 7 0 488.55 40.00 1 7 0 471.45 39.40 1 7 0 477.95 41.20 -2 -7 0 52.49 8.00 2 -7 0 41.80 3.20 2 7 0 45.90 10.40 2 7 0 42.10 3.10 -2 7 0 44.30 4.40 -2 7 0 33.90 7.10 -2 7 0 39.30 3.10 2 7 0 32.60 7.80 3 -7 0 150.08 10.20 -3 -7 0 152.88 10.50 -3 -7 0 152.38 17.00 -3 -7 0 148.89 15.90 -3 7 0 147.39 10.20 -3 7 0 145.69 14.70 -3 7 0 150.98 10.10 4 -7 0 3.30 4.40 -4 -7 0 0.40 2.90 4 -7 0 0.40 0.30 -4 -7 0 0.40 0.80 -4 -7 0 -1.90 3.10 4 7 0 9.40 6.00 -4 7 0 0.00 0.60 -4 7 0 2.70 2.80 -4 7 0 -1.80 4.40 -4 7 0 0.90 1.10 -4 7 0 0.50 0.30 4 7 0 -2.80 3.50 4 7 0 -2.60 5.10 -5 -7 0 121.29 17.20 -5 -7 0 120.59 13.70 -5 7 0 94.29 7.10 -5 7 0 109.39 13.30 -6 -7 0 17.90 8.90 -6 -7 0 35.20 7.80 -6 7 0 20.00 7.60 6 7 0 19.20 1.80 -7 -7 0 11.10 4.70 -7 -7 0 5.80 6.30 7 7 0 7.70 1.40 -8 -7 0 13.00 4.70 -8 -7 0 9.50 7.80 -9 7 0 -4.20 8.30 0 -8 0 168.78 14.40 0 8 0 182.08 17.60 -1 -8 0 11.80 3.60 -1 -8 0 6.50 3.30 1 -8 0 11.70 3.70 -1 -8 0 6.90 1.80 -1 -8 0 25.40 7.30 1 8 0 6.40 3.90 -1 8 0 4.90 2.20 1 8 0 24.40 7.10 1 8 0 7.70 1.10 -1 8 0 4.20 3.70 -1 8 0 19.10 6.30 1 8 0 6.30 4.90 -1 8 0 8.40 1.10 -2 -8 0 15.70 5.00 2 -8 0 16.60 1.70 -2 -8 0 18.00 5.70 -2 -8 0 13.20 1.60 2 8 0 11.30 6.10 2 8 0 16.40 7.60 -2 8 0 14.50 5.40 -2 8 0 14.00 2.80 2 8 0 15.30 1.50 -3 -8 0 2.50 0.90 -3 -8 0 -0.80 2.60 3 -8 0 7.90 5.30 -3 -8 0 1.10 2.70 3 -8 0 0.80 0.60 -3 8 0 1.80 2.90 -3 8 0 1.70 0.70 -3 8 0 3.80 1.50 3 8 0 3.20 5.50 3 8 0 1.40 4.40 -3 8 0 6.50 4.80 -4 -8 0 41.50 8.60 -4 -8 0 41.90 10.20 4 -8 0 28.50 2.50 -4 8 0 31.70 2.40 -4 8 0 30.90 2.60 -4 8 0 47.60 8.30 -5 -8 0 66.89 14.40 -5 -8 0 80.79 11.70 -5 8 0 85.39 12.30 -6 -8 0 22.10 9.30 -6 -8 0 41.60 9.00 6 8 0 34.10 2.70 -6 8 0 34.60 9.10 -7 -8 0 34.50 8.10 -7 -8 0 33.20 11.90 7 8 0 34.40 2.80 -8 -8 0 0.60 5.20 -8 -8 0 3.50 3.60 8 8 0 4.10 0.90 0 -9 0 -0.70 2.20 0 -9 0 4.60 5.60 0 -9 0 0.80 1.70 0 -9 0 0.30 0.70 0 9 0 0.30 2.00 0 9 0 0.30 3.30 0 9 0 -4.90 4.50 0 9 0 0.00 0.50 1 -9 0 24.60 7.50 1 -9 0 9.80 3.70 -1 -9 0 11.40 4.70 -1 -9 0 10.00 3.50 -1 -9 0 7.60 1.30 1 9 0 6.00 1.00 1 9 0 8.70 4.50 1 9 0 5.60 4.80 -1 9 0 23.20 7.30 1 9 0 23.10 7.70 -1 9 0 6.60 4.60 -1 9 0 6.40 2.80 -1 9 0 8.40 1.10 2 -9 0 7.90 1.20 2 -9 0 16.80 7.60 -2 -9 0 25.00 7.10 -2 -9 0 7.20 3.70 -2 -9 0 8.80 4.50 2 9 0 7.00 1.10 2 9 0 8.40 5.90 2 9 0 21.80 7.80 -2 9 0 7.40 1.00 -2 9 0 5.20 3.80 -2 9 0 7.30 6.00 -2 9 0 5.70 2.30 -3 -9 0 183.38 19.30 -3 -9 0 199.08 19.50 -3 9 0 174.48 12.30 -4 -9 0 3.00 4.00 -4 -9 0 1.20 3.40 -4 9 0 2.50 0.70 4 9 0 8.60 6.50 -4 9 0 0.50 4.50 -5 -9 0 2.20 3.50 -5 9 0 -1.70 5.20 5 9 0 14.90 7.20 -6 -9 0 18.90 6.30 -6 -9 0 12.40 7.30 -7 -9 0 24.50 10.40 -7 -9 0 37.30 9.00 7 9 0 29.50 2.60 -8 -9 0 19.40 10.30 -8 -9 0 21.90 6.80 8 9 0 23.10 2.20 0 -10 0 1.30 1.40 0 -10 0 1.30 2.60 0 -10 0 -0.70 1.70 0 10 0 0.20 0.50 0 10 0 0.30 2.40 0 10 0 -2.40 2.80 0 10 0 -1.40 5.10 -1 -10 0 4.40 3.70 -1 -10 0 4.60 2.70 1 -10 0 1.00 0.80 1 -10 0 3.90 3.10 1 10 0 1.70 0.60 -1 10 0 1.40 0.60 1 10 0 1.60 6.00 1 10 0 3.50 4.30 -1 10 0 0.70 1.90 -1 10 0 2.90 4.00 -1 10 0 4.40 5.90 1 10 0 1.20 3.10 2 -10 0 1.20 0.90 -2 -10 0 3.00 3.10 -2 -10 0 2.30 3.50 2 10 0 15.30 7.20 -2 10 0 7.00 5.60 2 10 0 5.70 1.00 -2 10 0 3.40 4.00 -2 10 0 3.90 0.80 3 -10 0 5.90 1.10 -3 -10 0 8.80 5.10 -3 -10 0 5.20 3.80 -3 10 0 13.40 6.20 3 10 0 21.60 7.90 -3 10 0 8.20 1.10 -4 -10 0 58.29 11.60 -4 -10 0 70.59 13.50 -4 10 0 86.89 11.70 -4 10 0 57.99 4.50 -5 -10 0 -3.00 2.40 -5 -10 0 -0.50 3.40 5 10 0 2.70 6.30 -5 10 0 1.50 5.50 -6 -10 0 5.20 4.50 -6 -10 0 7.40 5.70 -6 10 0 1.90 7.80 -7 -10 0 1.80 4.90 -7 -10 0 5.50 4.40 7 10 0 2.40 0.70 0 -11 0 -0.20 1.80 0 -11 0 -0.80 2.50 0 11 0 -1.10 7.70 0 11 0 -0.10 0.40 1 -11 0 2.60 3.10 -1 -11 0 3.10 3.50 1 -11 0 3.90 3.90 -1 -11 0 4.20 2.80 1 11 0 0.70 5.20 -1 11 0 2.00 0.60 -1 11 0 4.40 4.50 -1 11 0 1.40 5.50 1 11 0 2.20 3.30 -2 -11 0 76.39 11.30 2 11 0 62.89 4.80 -2 11 0 63.39 4.80 -3 -11 0 4.30 3.60 -3 -11 0 1.70 3.40 3 11 0 13.50 8.20 -3 11 0 3.70 0.70 -4 -11 0 3.80 4.00 -4 -11 0 2.10 4.00 4 11 0 4.00 6.90 -4 11 0 10.00 5.90 -5 -11 0 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10.10 1.40 4 -9 -3 22.90 2.10 -4 9 3 27.70 2.40 4 9 -3 26.30 2.10 -3 -9 3 18.00 11.60 3 -9 -3 4.60 2.80 -3 -9 3 4.40 3.40 3 -9 -3 2.90 0.70 3 9 -3 11.90 6.20 -3 9 3 13.70 5.80 -3 9 3 3.00 1.00 -2 -9 3 5.90 3.30 2 -9 -3 4.60 0.90 -2 -9 3 12.30 6.50 2 -9 -3 8.10 4.00 2 9 -3 3.10 3.30 -2 9 3 15.30 6.50 -2 9 3 4.10 1.10 2 9 -3 1.80 5.30 -2 9 3 1.90 5.50 1 -9 -3 39.90 8.60 -1 -9 3 37.70 3.10 1 -9 -3 33.40 3.10 1 9 -3 31.10 6.90 1 9 -3 31.80 7.70 -1 9 3 32.40 10.20 -1 9 3 40.90 3.20 0 -9 3 46.20 3.60 0 -9 -3 56.99 10.80 0 -9 -3 45.30 3.60 0 9 3 45.30 3.60 0 9 -3 35.70 7.50 0 9 3 35.10 11.20 0 9 -3 38.00 6.50 1 -9 3 117.99 8.20 -1 -9 -3 139.59 13.00 1 9 3 127.79 8.30 -1 9 -3 101.59 12.30 -1 9 -3 104.39 10.80 1 9 3 81.39 17.20 -2 -9 -3 71.69 10.50 -2 -9 -3 70.19 13.70 -2 9 -3 67.89 7.00 2 9 3 64.49 4.80 -2 9 -3 48.20 8.00 -3 -9 -3 168.38 19.20 -3 -9 -3 155.58 19.80 3 9 3 142.19 10.50 -3 9 -3 157.48 17.10 -4 -9 -3 356.26 34.20 -4 -9 -3 327.47 33.50 -5 -9 -3 203.68 24.30 -5 -9 -3 209.98 27.10 -5 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10.80 1.70 -1 5 18 7.60 2.00 0 -5 18 -8.40 6.10 0 5 18 -1.60 1.60 0 5 -18 3.20 13.60 -1 0 19 29.80 3.30 -1 -1 19 -1.10 0.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)'