data_9-Eu
_audit_creation_date               2025-06-08
_audit_creation_method
;
Olex2 1.5
(compiled 2025.05.31 svn.r86d253d1 for OlexSys, GUI svn.r7254)
;
_shelx_SHELXL_version_number       '2019/3'
loop_
  _audit_author_name
  _audit_author_email
  _audit_author_address
 'Lu, Z.' ? ?

_audit_contact_author_address      ?
_audit_contact_author_email        ?
_audit_contact_author_name         ''
_audit_contact_author_phone        ?
_publ_contact_author_id_orcid      ?
_publ_section_references
;
D. Kratzert, I. Krossing, (2018), J. Appl. Cryst. 51, 928-934.

Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Kratzert, D., Holstein, J.J. & Krossing, I. (2015). J. Appl. Cryst. 48, 933-938.

Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_chemical_name_common              ?
_chemical_name_systematic          ?
_chemical_formula_moiety          
 'C30 H37 Eu2 Mo12 N6 O55 P9, 3(H3 O), 10(H2 O), 3(C5 H6 N)'
_chemical_formula_sum              'C45 H84 Eu2 Mo12 N9 O68 P9'
_chemical_formula_weight           3573.14
_chemical_melting_point            ?
_chemical_oxdiff_formula           Eu2Mo12P9O85H85C50H50N10
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Eu' 'Eu' -0.1578 3.6682
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Mo' 'Mo' -1.6832 0.6857
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system        'tetragonal'
_space_group_IT_number             84
_space_group_name_H-M_alt          'P 42/m'
_space_group_name_Hall             '-P 4c'
loop_
  _space_group_symop_operation_xyz
 'x, y, z'
 '-x, -y, z'
 '-y, x, z+1/2'
 'y, -x, z+1/2'
 '-x, -y, -z'
 'x, y, -z'
 'y, -x, -z-1/2'
 '-y, x, -z-1/2'

_cell_length_a                     20.2729(3)
_cell_length_b                     20.2729(3)
_cell_length_c                     31.3042(5)
_cell_angle_alpha                  90
_cell_angle_beta                   90
_cell_angle_gamma                  90
_cell_volume                       12865.7(4)
_cell_formula_units_Z              4
_cell_measurement_reflns_used      31398
_cell_measurement_temperature      100(3)
_cell_measurement_theta_max        30.6960
_cell_measurement_theta_min        2.0300
_shelx_estimated_absorpt_T_max     0.894
_shelx_estimated_absorpt_T_min     0.658
_exptl_absorpt_coefficient_mu      2.283
_exptl_absorpt_correction_T_max    1.00000
_exptl_absorpt_correction_T_min    0.70205
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details     ?
_exptl_crystal_colour              'brownish red'
_exptl_crystal_colour_modifier     brownish
_exptl_crystal_colour_primary      red
_exptl_crystal_density_diffrn      1.845
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      ?
_exptl_crystal_description         block
_exptl_crystal_F_000               6904
_exptl_crystal_size_max            0.2
_exptl_crystal_size_mid            0.05
_exptl_crystal_size_min            0.05
_exptl_transmission_factor_max     ?
_exptl_transmission_factor_min     ?
_diffrn_reflns_av_R_equivalents    0.0548
_diffrn_reflns_av_unetI/netI       0.0294
_diffrn_reflns_Laue_measured_fraction_full  0.999
_diffrn_reflns_Laue_measured_fraction_max  0.999
_diffrn_reflns_limit_h_max         24
_diffrn_reflns_limit_h_min         -24
_diffrn_reflns_limit_k_max         24
_diffrn_reflns_limit_k_min         -24
_diffrn_reflns_limit_l_max         35
_diffrn_reflns_limit_l_min         -37
_diffrn_reflns_number              92251
_diffrn_reflns_point_group_measured_fraction_full  0.999
_diffrn_reflns_point_group_measured_fraction_max  0.999
_diffrn_reflns_theta_full          25.027
_diffrn_reflns_theta_max           25.027
_diffrn_reflns_theta_min           1.644
_diffrn_ambient_environment        N~2~
_diffrn_ambient_temperature        100(3)
_diffrn_detector                   'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean   10.0000
_diffrn_detector_type              HyPix
_diffrn_measured_fraction_theta_full  0.999
_diffrn_measured_fraction_theta_max  0.999
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
--------------------------------------------------------------------------
  1  ω    -62.00  24.00   0.50   17.50    --   10.16 -43.00 -79.00  172
  2  ω    -37.00  16.00   0.50   17.50    --   -9.38 -82.00 141.00  106
  3  ω    -18.00  44.00   0.50   17.50    --   10.16 -99.00   0.00  124
  4  ω    -24.00  52.00   0.50   17.50    --   -9.38  38.00 120.00  152
;
_diffrn_measurement_device         'four-circle diffractometer'
_diffrn_measurement_device_type    'XtaLAB Synergy R, HyPix'
_diffrn_measurement_method         'ω scans'
_diffrn_orient_matrix_type        
 'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11        -0.0187689000
_diffrn_orient_matrix_UB_12        -0.0094360000
_diffrn_orient_matrix_UB_13        -0.0181274000
_diffrn_orient_matrix_UB_21        0.0009666000
_diffrn_orient_matrix_UB_22        0.0329458000
_diffrn_orient_matrix_UB_23        -0.0076006000
_diffrn_orient_matrix_UB_31        0.0295127000
_diffrn_orient_matrix_UB_32        -0.0070801000
_diffrn_orient_matrix_UB_33        -0.0112623000
_diffrn_radiation_monochromator    mirror
_diffrn_radiation_probe            x-ray
_diffrn_radiation_type             'Mo K\a'
_diffrn_radiation_wavelength       0.71073
_diffrn_source                     'micro-focus sealed X-ray tube'
_diffrn_source_type                'Mova (Mo) X-ray Source'
_reflns_Friedel_coverage           0.000
_reflns_Friedel_fraction_full      .
_reflns_Friedel_fraction_max       .
_reflns_number_gt                  9071
_reflns_number_total               11598
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences. Completness statistics refer to single and
 composite reflections containing twin component 1 only.
;
_reflns_threshold_expression       'I > 2σ(I)'
_computing_cell_refinement         'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)'
_computing_data_collection         'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)'
_computing_data_reduction          'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)'
_computing_molecular_graphics      'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement    'SHELXL 2019/3 (Sheldrick, 2015)'
_computing_structure_solution      'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max           2.433
_refine_diff_density_min           -1.254
_refine_diff_density_rms           0.189
_refine_ls_extinction_coef         .
_refine_ls_extinction_method       none
_refine_ls_goodness_of_fit_ref     1.159
_refine_ls_hydrogen_treatment      mixed
_refine_ls_matrix_type             full
_refine_ls_number_parameters       1267
_refine_ls_number_reflns           11598
_refine_ls_number_restraints       1636
_refine_ls_R_factor_all            0.1141
_refine_ls_R_factor_gt             0.0900
_refine_ls_restrained_S_all        1.092
_refine_ls_shift/su_max            0.001
_refine_ls_shift/su_mean           0.000
_refine_ls_structure_factor_coef   Fsqd
_refine_ls_weighting_details      
 'w=1/[σ²(Fo²)+(0.0507P)²+326.0091P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme        calc
_refine_ls_wR_factor_gt            0.2046
_refine_ls_wR_factor_ref           0.2205
_refine_special_details
;
 Refined as a 2-component twin.
;
_olex2_refinement_description
;
1. Twinned data refinement
 Scales: 0.9611(10)
 0.0389(10)
2. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All N(H) groups, All P(H) groups
 At 1.5 times of:
  All O(H,H) groups, All O(H,H,H) groups
3. Restrained distances
 N10-C51 = N10-C55
 1.33 with sigma of 0.02
 N8-C40 = N8-C36
 1.33 with sigma of 0.02
 N7-C31 = N7-C35
 1.33 with sigma of 0.02
 N12-C56 = N12-C60
 1.33 with sigma of 0.02
 N11-C50 = N11-C46
 1.33 with sigma of 0.02
 C31-C32 = C34-C35
 1.38 with sigma of 0.02
 C32-C33 = C33-C34
 1.37 with sigma of 0.02
 C40-C39 = C37-C36
 1.38 with sigma of 0.02
 O6-N2
 1.904 with sigma of 0.02
 C39-C38 = C38-C37
 1.37 with sigma of 0.02
 N4-C20 = N4-C16
 1.33 with sigma of 0.02
 C56-C57 = C59-C60
 1.38 with sigma of 0.02
 C50-C49 = C47-C46
 1.38 with sigma of 0.02
 N6-C30 = N6-C26
 1.33 with sigma of 0.02
 C57-C58 = C58-C59
 1.37 with sigma of 0.02
 C49-C48 = C48-C47
 1.37 with sigma of 0.02
 N3-C11 = N3-C15
 1.33 with sigma of 0.02
 Mo5-O4
 1.92 with sigma of 0.02
 N2-C10 = N2-C6
 1.33 with sigma of 0.02
 C11-C12 = C14-C15
 1.38 with sigma of 0.02
 C30-C29 = C27-C26
 1.38 with sigma of 0.02
 C20-C19 = C17-C16
 1.38 with sigma of 0.02
 O5-Mo5
 1.877 with sigma of 0.02
 C10-C9 = C7-C6
 1.38 with sigma of 0.02
 C12-C13 = C13-C14
 1.37 with sigma of 0.02
 C29-C28 = C28-C27
 1.37 with sigma of 0.02
 C19-C18 = C18-C17
 1.37 with sigma of 0.02
 N9-C41 = N9-C45
 1.33 with sigma of 0.02
 C9-C8 = C8-C7
 1.37 with sigma of 0.02
 C21-C22 = C24-C25
 1.38 with sigma of 0.02
 C22-C23 = C23-C24
 1.37 with sigma of 0.02
 C51-C52 = C54-C55
 1.38 with sigma of 0.02
 C41-C42 = C44-C45
 1.38 with sigma of 0.02
 C52-C53 = C53-C54
 1.37 with sigma of 0.02
 C42-C43 = C43-C44
 1.37 with sigma of 0.02
 Mo1-O4
 1.333 with sigma of 0.02
 Mo4-O4
 1.92 with sigma of 0.02
 N1-C1 = N1-C5
 1.33 with sigma of 0.02
 C1-C2 = C4-C5
 1.38 with sigma of 0.02
 C2-C3 = C3-C4
 1.37 with sigma of 0.02
 O5-Mo3
 1.312 with sigma of 0.02
 Mo6-O6
 1.792 with sigma of 0.02
 Mo4-O6
 1.961 with sigma of 0.02
 O5-Mo6
 1.941 with sigma of 0.02
 N5-Mo5
 2.2 with sigma of 0.02
 N5-C21 = N5-C25
 1.33 with sigma of 0.02
 N8-C39
 2.4 with sigma of 0.04
 N7-C32
 2.4 with sigma of 0.04
 N8-C37
 2.39 with sigma of 0.04
 N7-C34
 2.39 with sigma of 0.04
 C31-C33
 2.36 with sigma of 0.04
 C32-C34
 2.35 with sigma of 0.04
 N12-C57
 2.4 with sigma of 0.04
 C33-C35
 2.37 with sigma of 0.04
 C40-C38
 2.36 with sigma of 0.04
 N11-C49
 2.4 with sigma of 0.04
 C39-C37
 2.35 with sigma of 0.04
 N12-C59
 2.39 with sigma of 0.04
 C38-C36
 2.37 with sigma of 0.04
 N11-C47
 2.39 with sigma of 0.04
 C50-C48
 2.36 with sigma of 0.04
 C56-C58
 2.36 with sigma of 0.04
 C49-C47
 2.35 with sigma of 0.04
 C57-C59
 2.35 with sigma of 0.04
 C48-C46
 2.37 with sigma of 0.04
 C58-C60
 2.37 with sigma of 0.04
 N6-C29
 2.4 with sigma of 0.04
 N4-C19
 2.4 with sigma of 0.04
 N3-C12
 2.4 with sigma of 0.04
 N6-C27
 2.39 with sigma of 0.04
 N2-C9
 2.4 with sigma of 0.04
 N3-C14
 2.39 with sigma of 0.04
 N4-C17
 2.39 with sigma of 0.04
 N2-C7
 2.39 with sigma of 0.04
 C20-C18
 2.36 with sigma of 0.04
 C11-C13
 2.36 with sigma of 0.04
 C30-C28
 2.36 with sigma of 0.04
 C10-C8
 2.36 with sigma of 0.04
 C12-C14
 2.35 with sigma of 0.04
 C29-C27
 2.35 with sigma of 0.04
 C19-C17
 2.35 with sigma of 0.04
 C9-C7
 2.35 with sigma of 0.04
 C18-C16
 2.37 with sigma of 0.04
 C13-C15
 2.37 with sigma of 0.04
 C28-C26
 2.37 with sigma of 0.04
 C8-C6
 2.37 with sigma of 0.04
 C21-C23
 2.36 with sigma of 0.04
 N9-C42
 2.4 with sigma of 0.04
 C22-C24
 2.35 with sigma of 0.04
 N10-C52
 2.4 with sigma of 0.04
 C23-C25
 2.37 with sigma of 0.04
 N10-C54
 2.39 with sigma of 0.04
 N9-C44
 2.39 with sigma of 0.04
 C41-C43
 2.36 with sigma of 0.04
 C51-C53
 2.36 with sigma of 0.04
 C42-C44
 2.35 with sigma of 0.04
 C52-C54
 2.35 with sigma of 0.04
 C53-C55
 2.37 with sigma of 0.04
 C43-C45
 2.37 with sigma of 0.04
 C1-C3
 2.36 with sigma of 0.04
 N1-C2
 2.4 with sigma of 0.04
 N1-C4
 2.39 with sigma of 0.04
 C2-C4
 2.35 with sigma of 0.04
 C3-C5
 2.37 with sigma of 0.04
 N5-C22
 2.4 with sigma of 0.04
 N5-C24
 2.39 with sigma of 0.04
 N8-C37 \\sim N8-C39
 with sigma of 0.04
 N7-C34 \\sim N7-C32
 with sigma of 0.04
 C33-C35 \\sim C33-C31 \\sim C34-C32 \\sim C35-C31
 with sigma of 0.04
 C38-C36 \\sim C38-C40 \\sim C37-C39 \\sim C36-C40
 with sigma of 0.04
 N11-C47 \\sim N11-C49
 with sigma of 0.04
 N12-C59 \\sim N12-C57
 with sigma of 0.04
 C48-C46 \\sim C48-C50 \\sim C47-C49 \\sim C46-C50
 with sigma of 0.04
 C58-C60 \\sim C58-C56 \\sim C59-C57 \\sim C60-C56
 with sigma of 0.04
 N3-C14 \\sim N3-C12
 with sigma of 0.04
 N6-C27 \\sim N6-C29
 with sigma of 0.04
 N4-C17 \\sim N4-C19
 with sigma of 0.04
 C13-C15 \\sim C13-C11 \\sim C14-C12 \\sim C15-C11
 with sigma of 0.04
 C28-C26 \\sim C28-C30 \\sim C27-C29 \\sim C26-C30
 with sigma of 0.04
 C18-C16 \\sim C18-C20 \\sim C17-C19 \\sim C16-C20
 with sigma of 0.04
 N2-C7 \\sim N2-C9
 with sigma of 0.04
 C8-C6 \\sim C8-C10 \\sim C7-C9 \\sim C6-C10
 with sigma of 0.04
 C23-C25 \\sim C23-C21 \\sim C24-C22 \\sim C25-C21
 with sigma of 0.04
 N10-C54 \\sim N10-C52
 with sigma of 0.04
 N9-C44 \\sim N9-C42
 with sigma of 0.04
 C43-C45 \\sim C43-C41 \\sim C44-C42 \\sim C45-C41
 with sigma of 0.04
 C53-C55 \\sim C53-C51 \\sim C54-C52 \\sim C55-C51
 with sigma of 0.04
 N1-C1 \\sim N1-C5
 with sigma of 0.02
 C1-C2 \\sim C2-C3 \\sim C3-C4 \\sim C4-C5
 with sigma of 0.02
 C3-C5 \\sim C3-C1 \\sim C4-C2 \\sim C5-C1
 with sigma of 0.04
 N1-C4 \\sim N1-C2
 with sigma of 0.04
 N5-C24 \\sim N5-C22
 with sigma of 0.04
4. Restrained planarity
 N8, C36, C37, C38, C39, C40
 with sigma of 0.1
 N7, C31, C32, C33, C34, C35
 with sigma of 0.1
 N12, C56, C57, C58, C59, C60
 with sigma of 0.1
 N11, C50, C49, C48, C47, C46
 with sigma of 0.04
 N3, C11, C12, C13, C14, C15
 with sigma of 0.1
 N6, C26, C27, C28, C29, C30
 with sigma of 0.1
 N4, C16, C17, C18, C19, C20
 with sigma of 0.1
 N2, C6, C7, C8, C9, C10
 with sigma of 0.1
 N10, C51, C52, C53, C54, C55
 with sigma of 0.1
 N9, C41, C42, C43, C44, C45
 with sigma of 0.02
 N1, C1, C2, C3, C4, C5
 with sigma of 0.1
 N5, C21, C22, C23, C24, C25
 with sigma of 0.1
5. Uiso/Uaniso restraints and constraints
N8 \\sim C36 \\sim C37 \\sim C38 \\sim C39 \\sim C40: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
N7 \\sim C31 \\sim C32 \\sim C33 \\sim C34 \\sim C35: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
N11 \\sim C46 \\sim C47 \\sim C48 \\sim C49 \\sim C50: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
N12 \\sim C56 \\sim C57 \\sim C58 \\sim C59 \\sim C60: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
N3 \\sim C11 \\sim C12 \\sim C13 \\sim C14 \\sim C15: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
N4 \\sim C16 \\sim C17 \\sim C18 \\sim C19 \\sim C20: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
N6 \\sim C26 \\sim C27 \\sim C28 \\sim C29 \\sim C30: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
N2 \\sim C6 \\sim C7 \\sim C8 \\sim C9 \\sim C10: within 2A with sigma of 0.04
and sigma for terminal atoms of 0.08 within 2A
N9 \\sim C41 \\sim C42 \\sim C43 \\sim C44 \\sim C45: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
N10 \\sim C51 \\sim C52 \\sim C53 \\sim C54 \\sim C55: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
N1 \\sim C1 \\sim C2 \\sim C3 \\sim C4 \\sim C5: within 2A with sigma of 0.04
and sigma for terminal atoms of 0.08 within 2A
O1 \\sim O6: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08
within 2A
O2 \\sim O5: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08
within 2A
N5 \\sim C21 \\sim C22 \\sim C23 \\sim C24 \\sim C25: within 2A with sigma of
0.04 and sigma for terminal atoms of 0.08 within 2A
Uanis(N8) \\sim Ueq, Uanis(C40) \\sim Ueq, Uanis(C39) \\sim Ueq, Uanis(C38)
\\sim Ueq, Uanis(C37) \\sim Ueq, Uanis(C36) \\sim Ueq: with sigma of 0.03 and
sigma for terminal atoms of 0.06
Uanis(N7) \\sim Ueq, Uanis(C32) \\sim Ueq, Uanis(C33) \\sim Ueq, Uanis(C35)
\\sim Ueq, Uanis(C31) \\sim Ueq, Uanis(C34) \\sim Ueq: with sigma of 0.03 and
sigma for terminal atoms of 0.06
Uanis(N11) \\sim Ueq, Uanis(C49) \\sim Ueq, Uanis(C48) \\sim Ueq, Uanis(C46)
\\sim Ueq, Uanis(C50) \\sim Ueq, Uanis(C47) \\sim Ueq: with sigma of 0.05 and
sigma for terminal atoms of 0.1
Uanis(N12) \\sim Ueq, Uanis(C57) \\sim Ueq, Uanis(C58) \\sim Ueq, Uanis(C60)
\\sim Ueq, Uanis(C56) \\sim Ueq, Uanis(C59) \\sim Ueq: with sigma of 0.07 and
sigma for terminal atoms of 0.14
Uanis(N6) \\sim Ueq, Uanis(C29) \\sim Ueq, Uanis(C28) \\sim Ueq, Uanis(C26)
\\sim Ueq, Uanis(C30) \\sim Ueq, Uanis(C27) \\sim Ueq: with sigma of 0.1 and
sigma for terminal atoms of 0.2
Uanis(N4) \\sim Ueq, Uanis(C19) \\sim Ueq, Uanis(C18) \\sim Ueq, Uanis(C16)
\\sim Ueq, Uanis(C20) \\sim Ueq, Uanis(C17) \\sim Ueq: with sigma of 0.1 and
sigma for terminal atoms of 0.2
Uanis(O26) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04
Uanis(O28) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(N9) \\sim Ueq, Uanis(C42) \\sim Ueq, Uanis(C43) \\sim Ueq, Uanis(C45)
\\sim Ueq, Uanis(C41) \\sim Ueq, Uanis(C44) \\sim Ueq: with sigma of 0.05 and
sigma for terminal atoms of 0.1
Uanis(N10) \\sim Ueq, Uanis(C55) \\sim Ueq, Uanis(C54) \\sim Ueq, Uanis(C53)
\\sim Ueq, Uanis(C52) \\sim Ueq, Uanis(C51) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(O35) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O36) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04
Uanis(O47) \\sim Ueq: with sigma of 0.03 and sigma for terminal atoms of 0.06
Uanis(Mo6) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O1) \\sim Ueq: with sigma of 0.1 and sigma for terminal atoms of 0.2
Uanis(O44) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(O42) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04
Uanis(O50) \\sim Ueq: with sigma of 0.03 and sigma for terminal atoms of 0.06
Uanis(O37) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04
Uanis(O40) \\sim Ueq: with sigma of 0.03 and sigma for terminal atoms of 0.06
Uanis(O54) \\sim Ueq: with sigma of 0.03 and sigma for terminal atoms of 0.06
Uanis(O5) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04
Uanis(O38) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04
Uanis(O43) \\sim Ueq: with sigma of 0.03 and sigma for terminal atoms of 0.06
Uanis(O6) \\sim Ueq: with sigma of 0.03 and sigma for terminal atoms of 0.06
Uanis(O52) \\sim Ueq: with sigma of 0.04 and sigma for terminal atoms of 0.08
Uanis(O45) \\sim Ueq: with sigma of 0.04 and sigma for terminal atoms of 0.08
Uanis(O48) \\sim Ueq: with sigma of 0.03 and sigma for terminal atoms of 0.06
Uanis(O51) \\sim Ueq: with sigma of 0.03 and sigma for terminal atoms of 0.06
Uanis(O46) \\sim Ueq: with sigma of 0.04 and sigma for terminal atoms of 0.08
Uanis(O53) \\sim Ueq: with sigma of 0.04 and sigma for terminal atoms of 0.08
Uanis(O25) \\sim Ueq: with sigma of 0.03 and sigma for terminal atoms of 0.06
Uanis(O41) \\sim Ueq: with sigma of 0.04 and sigma for terminal atoms of 0.08
Uanis(Mo5) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04
Uanis(O4) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04
Uanis(N5) \\sim Ueq, Uanis(C25) \\sim Ueq, Uanis(C24) \\sim Ueq, Uanis(C23)
\\sim Ueq, Uanis(C22) \\sim Ueq, Uanis(C21) \\sim Ueq: with sigma of 0.03 and
sigma for terminal atoms of 0.06
6. Rigid body (RIGU) restrains
 N8, C36, C37, C38, C39, C40
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N7, C31, C32, C33, C34, C35
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N11, C46, C47, C48, C49, C50
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N12, C56, C57, C58, C59, C60
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N6, C26, C27, C28, C29, C30
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N4, C16, C17, C18, C19, C20
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N3, C11, C12, C13, C14, C15
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N2, C6, C7, C8, C9, C10
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N9, C41, C42, C43, C44, C45
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N10, C51, C52, C53, C54, C55
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N1, C1, C2, C3, C4, C5
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 N5, C21, C22, C23, C24, C25
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
7. Others
 1*[Sof(O26)]+1*[Sof(O28)]+1*[Sof(O27)]=1 with esd of 0.001
 1*[Sof(H3)]+1*[Sof(O26)]=1 with esd of 0.001
 1*[Sof(H2)]+1*[Sof(O28)]=1 with esd of 0.001
 1*[Sof(O27)]+1*[Sof(H1)]=1 with esd of 0.001
 1*[Sof(Mo4)+Sof(Mo5)+Sof(Mo6)+Sof(O4)+Sof(O5)+Sof(O6)+Sof(N4)+Sof(N5)+Sof(N6)+
 Sof(C16)+Sof(H16)+Sof(C17)+Sof(H17)+Sof(C18)+Sof(H18)+Sof(C19)+Sof(H19)+
 Sof(C20)+Sof(H20)+Sof(C21)+Sof(H21)+Sof(C22)+Sof(H22)+Sof(C23)+Sof(H23)+
 Sof(C24)+Sof(H24)+Sof(C25)+Sof(H25)+Sof(C26)+Sof(H26)+Sof(C27)+Sof(H27)+
 Sof(C28)+Sof(H28)+Sof(C29)+Sof(H29)+Sof(C30)+Sof(H30)]+1*[Sof(Mo1)+Sof(Mo2)+
 Sof(Mo3)+Sof(O1)+Sof(O2)+Sof(O3)+Sof(N1)+Sof(N2)+Sof(N3)+Sof(C1)+Sof(H1A)+
 Sof(C2)+Sof(H2A)+Sof(C3)+Sof(H3A)+Sof(C4)+Sof(H4A)+Sof(C5)+Sof(H5A)+Sof(C6)+
 Sof(H6A)+Sof(C7)+Sof(H7A)+Sof(C8)+Sof(H8A)+Sof(C9)+Sof(H9)+Sof(C10)+Sof(H10)+
 Sof(C11)+Sof(H11)+Sof(C12)+Sof(H12)+Sof(C13)+Sof(H13)+Sof(C14)+Sof(H14)+
 Sof(C15)+Sof(H15)]=1 with esd of 0.00001
 Sof(P7)=Sof(H7)=0.5*(1-FVAR(2))
 Sof(P8)=Sof(H8)=0.5*FVAR(2)
 Sof(P5)=Sof(H5)=0.5*(1-FVAR(3))
 Sof(P6)=Sof(H6)=0.5*FVAR(3)
 Sof(Mo4)=Sof(Mo5)=Sof(Mo6)=Sof(O4)=Sof(O5)=Sof(O6)=Sof(N4)=Sof(N5)=Sof(N6)=
 Sof(C16)=Sof(H16)=Sof(C17)=Sof(H17)=Sof(C18)=Sof(H18)=Sof(C19)=Sof(H19)=
 Sof(C20)=Sof(H20)=Sof(C21)=Sof(H21)=Sof(C22)=Sof(H22)=Sof(C23)=Sof(H23)=
 Sof(C24)=Sof(H24)=Sof(C25)=Sof(H25)=Sof(C26)=Sof(H26)=Sof(C27)=Sof(H27)=
 Sof(C28)=Sof(H28)=Sof(C29)=Sof(H29)=Sof(C30)=Sof(H30)=FVAR(9)
 Sof(Mo1)=Sof(Mo2)=Sof(Mo3)=Sof(O1)=Sof(O2)=Sof(O3)=Sof(N1)=Sof(N2)=Sof(N3)=
 Sof(C1)=Sof(H1A)=Sof(C2)=Sof(H2A)=Sof(C3)=Sof(H3A)=Sof(C4)=Sof(H4A)=Sof(C5)=
 Sof(H5A)=Sof(C6)=Sof(H6A)=Sof(C7)=Sof(H7A)=Sof(C8)=Sof(H8A)=Sof(C9)=Sof(H9)=
 Sof(C10)=Sof(H10)=Sof(C11)=Sof(H11)=Sof(C12)=Sof(H12)=Sof(C13)=Sof(H13)=
 Sof(C14)=Sof(H14)=Sof(C15)=Sof(H15)=FVAR(10)
 Fixed Sof: O36(0.5) H36A(0.5) H36B(0.5) H36C(0.5) O38(0.5) H38A(0.5)
 H38B(0.5) O39(0.375) H39A(0.375) H39B(0.375) O40(0.375) H40A(0.375)
 H40B(0.375) O41(0.5) H41A(0.5) H41B(0.5) O42(0.25) H42A(0.25) H42B(0.25)
 O43(0.25) H43A(0.25) H43B(0.25) O44(0.1875) H44A(0.1875) H44B(0.1875)
 O45(0.09375) H45A(0.09375) H45B(0.09375) O46(0.125) H46A(0.125) H46B(0.125)
 O47(0.125) H47A(0.125) H47B(0.125) O48(0.25) H48A(0.25) H48B(0.25) O50(0.25)
 H50A(0.25) H50B(0.25) O51(0.25) H51A(0.25) H51B(0.25) O52(0.09375)
 H52A(0.09375) H52B(0.09375) O53(0.125) H53A(0.125) H53B(0.125) O54(0.25)
 H54A(0.25) H54B(0.25) N7(0.667) H7B(0.667) C31(0.667) H31(0.667) C32(0.667)
 H32(0.667) C33(0.667) H33(0.667) C34(0.667) H34(0.667) C35(0.667) H35(0.667)
 N8(0.16633) H8B(0.16633) C36(0.16633) H36(0.16633) C37(0.16633) H37(0.16633)
 C38(0.16633) H38(0.16633) C39(0.16633) H39(0.16633) C40(0.16633) H40(0.16633)
 N9(0.25) H9A(0.25) C41(0.25) H41(0.25) C42(0.25) H42(0.25) C43(0.25) H43(0.25)
 C44(0.25) H44(0.25) C45(0.25) H45(0.25) N10(0.166667) H10A(0.166667)
 C51(0.166667) H51(0.166667) C52(0.166667) H52(0.166667) C53(0.166667)
 H53(0.166667) C54(0.166667) H54(0.166667) C55(0.166667) H55(0.166667)
 N11(0.166667) H11A(0.166667) C46(0.166667) H46(0.166667) C47(0.166667)
 H47(0.166667) C48(0.166667) H48(0.166667) C49(0.166667) H49(0.166667)
 C50(0.166667) H50(0.166667) N12(0.083333) H12A(0.083333) C56(0.083333)
 H56(0.083333) C57(0.083333) H57(0.083333) C58(0.083333) H58(0.083333)
 C59(0.083333) H59(0.083333) C60(0.083333) H60(0.083333)
8.a Riding coordinates:
 P1(H1), P2(H2), P3(H3), P4(H4), P5(H5), P6(H6), P7(H7), P8(H8), O35(H35A,H35B,
 H35C), O36(H36A,H36B,H36C), O37(H37A,H37B), O38(H38A,H38B), O39(H39A,H39B),
 O40(H40A,H40B), O41(H41A,H41B), O42(H42A,H42B), O43(H43A,H43B), O44(H44A,H44B),
  O45(H45A,H45B), O46(H46A,H46B), O47(H47A,H47B), O48(H48A,H48B), O50(H50A,
 H50B), O51(H51A,H51B), O52(H52A,H52B), O53(H53A,H53B), O54(H54A,H54B)
8.b Aromatic/amide H refined with riding coordinates:
 C1(H1A), C2(H2A), C3(H3A), C4(H4A), C5(H5A), C6(H6A), C7(H7A), C8(H8A),
 C9(H9), C10(H10), C11(H11), C12(H12), C13(H13), C14(H14), C15(H15), C16(H16),
 C17(H17), C18(H18), C19(H19), C20(H20), C21(H21), C22(H22), C23(H23), C24(H24),
  C25(H25), C26(H26), C27(H27), C28(H28), C29(H29), C30(H30), N7(H7B), C31(H31),
  C32(H32), C33(H33), C34(H34), C35(H35), N8(H8B), C36(H36), C37(H37), C38(H38),
  C39(H39), C40(H40), N9(H9A), C41(H41), C42(H42), C43(H43), C44(H44), C45(H45),
  N10(H10A), C51(H51), C52(H52), C53(H53), C54(H54), C55(H55), N11(H11A),
 C46(H46), C47(H47), C48(H48), C49(H49), C50(H50), N12(H12A), C56(H56),
 C57(H57), C58(H58), C59(H59), C60(H60)
;
_atom_sites_solution_hydrogens     mixed
_atom_sites_solution_primary       dual
_atom_sites_solution_secondary     ?
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 Eu1 Eu 0.27181(4) 0.77330(4) 0.55949(2) 0.0482(2) Uani 1 1 d . . . . .
 Mo1 Mo 0.30645(8) 0.83716(9) 0.68830(4) 0.0456(4) Uani 0.834(2) 1 d D . P C .
 Mo2 Mo 0.19719(9) 0.77909(9) 0.68688(4) 0.0517(5) Uani 0.834(2) 1 d . . P C .
 Mo3 Mo 0.30213(9) 0.71201(8) 0.68801(4) 0.0489(4) Uani 0.834(2) 1 d D . P C .
 Mo4 Mo 0.2315(7) 0.8410(6) 0.6896(3) 0.084(4) Uani 0.166(2) 1 d D . P C .
 Mo5 Mo 0.3369(6) 0.7833(6) 0.6904(2) 0.076(3) Uani 0.166(2) 1 d D U P C .
 Mo6 Mo 0.2289(6) 0.7204(5) 0.6900(2) 0.072(3) Uani 0.166(2) 1 d D U P C .
 Mo7 Mo 0.27774(9) 0.96216(7) 0.60397(4) 0.0607(4) Uani 1 1 d . . . . .
 Mo8 Mo 0.10453(9) 0.68924(10) 0.60421(4) 0.0703(5) Uani 1 1 d . . . . .
 Mo9 Mo 0.42853(8) 0.68012(8) 0.60522(4) 0.0561(4) Uani 1 1 d . . . . .
 P1 P 0.3997(2) 0.8446(2) 0.60520(11) 0.0495(10) Uani 1 1 d . . . . .
 H1 H 0.462372 0.865599 0.593475 0.059 Uiso 0.552(17) 1 d R U P . .
 P2 P 0.2652(3) 0.6323(2) 0.60312(13) 0.0613(12) Uani 1 1 d . . . . .
 H2 H 0.259694 0.567187 0.589576 0.074 Uiso 0.652(16) 1 d R U P . .
 P3 P 0.1512(3) 0.8520(3) 0.60128(13) 0.0665(13) Uani 1 1 d . . . . .
 H3 H 0.101865 0.892626 0.585001 0.080 Uiso 0.796(16) 1 d R U P . .
 P4 P 0.2549(4) 0.9281(3) 0.500000 0.0539(15) Uani 1 2 d S T P . .
 H4 H 0.186341 0.930358 0.500000 0.065 Uiso 1 2 d R U P . .
 P5 P 0.4139(10) 0.7185(13) 0.500000 0.046(6) Uani 0.54(5) 2 d S T P A 2
 H5 H 0.448005 0.777971 0.500000 0.055 Uiso 0.54(5) 2 d R U P A 2
 P6 P 0.3925(10) 0.6806(16) 0.500000 0.048(7) Uani 0.46(5) 2 d S T P A 1
 H6 H 0.359952 0.620216 0.500000 0.057 Uiso 0.46(5) 2 d R U P A 1
 P7 P 0.145(2) 0.687(3) 0.500000 0.084(15) Uani 0.59(8) 2 d S T P B 2
 H7 H 0.178405 0.627381 0.500000 0.08(15) Uiso 0.59(8) 2 d R . P B 2
 P8 P 0.1236(11) 0.7241(18) 0.500000 0.039(7) Uani 0.41(8) 2 d S T P B 1
 H8 H 0.092047 0.784959 0.500000 0.047 Uiso 0.41(8) 2 d R U P B 1
 O1 O 0.2299(7) 0.8472(7) 0.7233(3) 0.055(3) Uani 0.834(2) 1 d . U P C .
 O2 O 0.3480(6) 0.7719(6) 0.7252(3) 0.051(3) Uani 0.834(2) 1 d . U P C .
 O3 O 0.2256(7) 0.7091(7) 0.7239(4) 0.063(4) Uani 0.834(2) 1 d . . P . .
 O4 O 0.3044(16) 0.852(2) 0.7288(8) 0.08(2) Uani 0.166(2) 1 d D U P C .
 O5 O 0.3036(15) 0.7207(18) 0.7292(6) 0.082(17) Uani 0.166(2) 1 d D U P . .
 O6 O 0.2045(12) 0.7752(12) 0.7319(8) 0.083(16) Uani 0.166(2) 1 d D U P C .
 O7 O 0.2700(5) 0.7758(5) 0.6412(3) 0.044(2) Uani 1 1 d . . . . .
 O8 O 0.2815(7) 0.9186(5) 0.6543(3) 0.065(3) Uani 1 1 d . . . . .
 O9 O 0.3958(5) 0.8457(5) 0.6539(3) 0.048(2) Uani 1 1 d . . . . .
 O10 O 0.3890(5) 0.6964(6) 0.6561(3) 0.059(3) Uani 1 1 d . . . . .
 O11 O 0.2680(6) 0.6340(6) 0.6518(3) 0.064(3) Uani 1 1 d . . . . .
 O12 O 0.1409(6) 0.7136(7) 0.6542(3) 0.071(4) Uani 1 1 d . . . . .
 O13 O 0.1462(6) 0.8506(6) 0.6498(3) 0.063(3) Uani 1 1 d . . . . .
 O14 O 0.2177(7) 0.8760(6) 0.5840(3) 0.065(3) Uani 1 1 d . . . . .
 O15 O 0.3486(8) 0.8875(7) 0.5840(3) 0.093(5) Uani 1 1 d . . . . .
 O16 O 0.3873(6) 0.7777(6) 0.5854(3) 0.058(3) Uani 1 1 d . . . . .
 O17 O 0.3256(6) 0.6631(6) 0.5823(3) 0.063(3) Uani 1 1 d . . . . .
 O18 O 0.2091(6) 0.6724(7) 0.5845(3) 0.076(4) Uani 1 1 d . . . . .
 O19 O 0.1454(7) 0.7837(8) 0.5816(4) 0.085(4) Uani 1 1 d . . . . .
 O20 O 0.2066(8) 1.0056(7) 0.6082(4) 0.088(4) Uani 1 1 d . . . . .
 O21 O 0.3389(8) 1.0204(7) 0.6087(4) 0.087(4) Uani 1 1 d . . . . .
 O22 O 0.5031(7) 0.7139(7) 0.6114(3) 0.077(4) Uani 1 1 d . . . . .
 O23 O 0.4438(8) 0.5979(7) 0.6089(4) 0.094(5) Uani 1 1 d . . . . .
 O24 O 0.0952(9) 0.6102(9) 0.6101(4) 0.102(5) Uani 1 1 d . . . . .
 O25 O 0.0266(7) 0.7199(9) 0.6075(4) 0.101(5) Uani 1 1 d . U . . .
 O26 O 0.094(3) 0.900(3) 0.5847(16) 0.065(17) Uani 0.204(16) 1 d . U P . .
 O27 O 0.4641(18) 0.873(2) 0.5928(9) 0.108(14) Uani 0.448(17) 1 d . . P . .
 O28 O 0.2642(17) 0.5606(16) 0.5887(8) 0.060(9) Uani 0.348(16) 1 d . U P . .
 O29 O 0.2783(7) 0.9681(5) 0.5384(3) 0.062(3) Uani 1 1 d . . . . .
 O30 O 0.4378(5) 0.6803(5) 0.5392(3) 0.055(3) Uani 1 1 d . . . . .
 O31 O 0.1024(6) 0.6805(7) 0.5385(3) 0.070(4) Uani 1 1 d . . . . .
 O32 O 0.2744(7) 0.8550(7) 0.500000 0.045(3) Uani 1 2 d S T P . .
 O33 O 0.3409(7) 0.7342(7) 0.500000 0.042(3) Uani 1 2 d S T P . .
 O34 O 0.2008(8) 0.7352(8) 0.500000 0.053(4) Uani 1 2 d S T P . .
 N1 N 0.3488(7) 0.9075(7) 0.7341(4) 0.054(4) Uani 0.834(2) 1 d D U P C 1
 N2 N 0.1118(7) 0.7869(8) 0.7298(4) 0.067(4) Uani 0.834(2) 1 d D U P C 1
 N3 N 0.3375(8) 0.6351(7) 0.7326(4) 0.059(4) Uani 0.834(2) 1 d D U P C 1
 N4 N 0.193(5) 0.922(4) 0.727(2) 0.11(2) Uani 0.166(2) 1 d D U P C 2
 N5 N 0.424(2) 0.790(4) 0.7332(19) 0.077(15) Uani 0.166(2) 1 d D U P C 2
 N6 N 0.190(5) 0.637(4) 0.733(3) 0.10(2) Uani 0.166(2) 1 d D U P C 3
 C1 C 0.3859(9) 0.9581(8) 0.7215(5) 0.077(6) Uani 0.834(2) 1 d D U P C 1
 H1A H 0.393630 0.964199 0.691881 0.093 Uiso 0.834(2) 1 calc R U P C 1
 C2 C 0.4133(11) 1.0019(10) 0.7501(5) 0.099(8) Uani 0.834(2) 1 d D U P C 1
 H2A H 0.440300 1.037052 0.740177 0.119 Uiso 0.834(2) 1 calc R U P C 1
 C3 C 0.4013(12) 0.9944(10) 0.7928(5) 0.084(6) Uani 0.834(2) 1 d D U P C 1
 H3A H 0.418835 1.024818 0.812858 0.101 Uiso 0.834(2) 1 calc R U P C 1
 C4 C 0.3638(11) 0.9425(10) 0.8060(4) 0.077(6) Uani 0.834(2) 1 d D U P C 1
 H4A H 0.355834 0.935627 0.835592 0.093 Uiso 0.834(2) 1 calc R U P C 1
 C5 C 0.3376(10) 0.9000(9) 0.7761(4) 0.061(5) Uani 0.834(2) 1 d D U P C 1
 H5A H 0.310925 0.864293 0.785493 0.073 Uiso 0.834(2) 1 calc R U P C 1
 C6 C 0.0496(8) 0.7890(9) 0.7149(5) 0.068(5) Uani 0.834(2) 1 d D U P C 1
 H6A H 0.042490 0.785101 0.685020 0.081 Uiso 0.834(2) 1 calc R U P C 1
 C7 C -0.0038(8) 0.7966(10) 0.7413(5) 0.076(5) Uani 0.834(2) 1 d D U P C 1
 H7A H -0.047150 0.797046 0.729706 0.091 Uiso 0.834(2) 1 calc R U P C 1
 C8 C 0.0054(9) 0.8036(12) 0.7841(5) 0.079(6) Uani 0.834(2) 1 d D U P C 1
 H8A H -0.031069 0.810733 0.802569 0.095 Uiso 0.834(2) 1 calc R U P C 1
 C9 C 0.0682(9) 0.8000(13) 0.8002(5) 0.088(6) Uani 0.834(2) 1 d D U P C 1
 H9 H 0.075678 0.802816 0.830113 0.106 Uiso 0.834(2) 1 calc R U P C 1
 C10 C 0.1200(9) 0.7924(12) 0.7724(5) 0.074(6) Uani 0.834(2) 1 d D U P C 1
 H10 H 0.163438 0.790830 0.783710 0.089 Uiso 0.834(2) 1 calc R U P C 1
 C11 C 0.3591(8) 0.5778(8) 0.7173(5) 0.062(5) Uani 0.834(2) 1 d D U P C 1
 H11 H 0.364035 0.572932 0.687305 0.075 Uiso 0.834(2) 1 calc R U P C 1
 C12 C 0.3747(11) 0.5253(9) 0.7434(5) 0.086(6) Uani 0.834(2) 1 d D U P C 1
 H12 H 0.389372 0.484571 0.731797 0.103 Uiso 0.834(2) 1 calc R U P C 1
 C13 C 0.3684(14) 0.5335(10) 0.7868(5) 0.094(7) Uani 0.834(2) 1 d D U P C 1
 H13 H 0.378897 0.498304 0.805570 0.113 Uiso 0.834(2) 1 calc R U P C 1
 C14 C 0.3475(12) 0.5915(10) 0.8025(5) 0.080(6) Uani 0.834(2) 1 d D U P C 1
 H14 H 0.344025 0.597770 0.832531 0.096 Uiso 0.834(2) 1 calc R U P C 1
 C15 C 0.3310(11) 0.6417(9) 0.7748(5) 0.071(5) Uani 0.834(2) 1 d D U P C 1
 H15 H 0.314626 0.682063 0.786007 0.086 Uiso 0.834(2) 1 calc R U P C 1
 C16 C 0.163(5) 0.976(5) 0.712(2) 0.11(2) Uani 0.166(2) 1 d D U P C 2
 H16 H 0.161425 0.982435 0.681756 0.136 Uiso 0.166(2) 1 calc R U P C 2
 C17 C 0.136(6) 1.022(4) 0.739(3) 0.12(2) Uani 0.166(2) 1 d D U P C 2
 H17 H 0.114788 1.059876 0.727791 0.139 Uiso 0.166(2) 1 calc R U P C 2
 C18 C 0.138(6) 1.011(5) 0.782(3) 0.12(2) Uani 0.166(2) 1 d D U P C 2
 H18 H 0.118955 1.042223 0.800908 0.142 Uiso 0.166(2) 1 calc R U P C 2
 C19 C 0.169(6) 0.957(5) 0.7979(19) 0.12(2) Uani 0.166(2) 1 d D U P C 2
 H19 H 0.170699 0.949088 0.827785 0.141 Uiso 0.166(2) 1 calc R U P C 2
 C20 C 0.198(6) 0.913(4) 0.770(3) 0.12(2) Uani 0.166(2) 1 d D U P C 2
 H20 H 0.220501 0.875146 0.780556 0.141 Uiso 0.166(2) 1 calc R U P C 2
 C21 C 0.487(3) 0.799(5) 0.7198(16) 0.077(16) Uani 0.166(2) 1 d D U P C 2
 H21 H 0.495804 0.797864 0.690012 0.092 Uiso 0.166(2) 1 calc R U P C 2
 C22 C 0.538(2) 0.810(5) 0.748(2) 0.069(15) Uani 0.166(2) 1 d D U P C 2
 H22 H 0.581692 0.816298 0.737496 0.083 Uiso 0.166(2) 1 calc R U P C 2
 C23 C 0.526(3) 0.811(5) 0.7904(19) 0.069(15) Uani 0.166(2) 1 d D U P C 2
 H23 H 0.560642 0.816768 0.810145 0.083 Uiso 0.166(2) 1 calc R U P C 2
 C24 C 0.463(3) 0.803(4) 0.8051(15) 0.059(14) Uani 0.166(2) 1 d D U P C 2
 H24 H 0.453011 0.805463 0.834731 0.071 Uiso 0.166(2) 1 calc R U P C 2
 C25 C 0.413(2) 0.792(4) 0.776(2) 0.075(15) Uani 0.166(2) 1 d D U P C 2
 H25 H 0.369277 0.785733 0.785804 0.090 Uiso 0.166(2) 1 calc R U P C 2
 C26 C 0.173(6) 0.576(5) 0.719(2) 0.10(2) Uani 0.166(2) 1 d D U P C 3
 H26 H 0.175870 0.566354 0.689628 0.122 Uiso 0.166(2) 1 calc R U P C 3
 C27 C 0.152(6) 0.529(4) 0.748(3) 0.11(2) Uani 0.166(2) 1 d D U P C 3
 H27 H 0.140076 0.486106 0.737593 0.127 Uiso 0.166(2) 1 calc R U P C 3
 C28 C 0.148(6) 0.544(4) 0.790(3) 0.11(2) Uani 0.166(2) 1 d D U P C 3
 H28 H 0.133810 0.511419 0.809710 0.130 Uiso 0.166(2) 1 calc R U P C 3
 C29 C 0.166(6) 0.605(5) 0.804(2) 0.11(2) Uani 0.166(2) 1 d D U P C 3
 H29 H 0.164038 0.615298 0.833479 0.136 Uiso 0.166(2) 1 calc R U P C 3
 C30 C 0.186(5) 0.652(4) 0.775(3) 0.11(2) Uani 0.166(2) 1 d D U P C 3
 H30 H 0.196889 0.694652 0.784100 0.133 Uiso 0.166(2) 1 calc R U P C 3
 O35 O 0.5392(11) 0.9470(11) 0.6445(7) 0.164(8) Uani 1 1 d . U . . .
 H35A H 0.575332 0.963319 0.634440 0.246 Uiso 1 1 d R U . . .
 H35B H 0.510000 0.938767 0.625393 0.246 Uiso 1 1 d R U . . .
 H35C H 0.552088 0.906541 0.646084 0.246 Uiso 1 1 d R U . . .
 O36 O 0.449(2) 0.4757(18) 0.6406(13) 0.146(15) Uani 0.5 1 d . U P . .
 H36A H 0.479636 0.447872 0.632285 0.218 Uiso 0.5 1 d R U P . .
 H36B H 0.487404 0.494472 0.640557 0.218 Uiso 0.5 1 d R U P . .
 H36C H 0.422515 0.505243 0.629775 0.218 Uiso 0.5 1 d R U P . .
 O37 O 0.7874(14) 0.7460(13) 0.3538(6) 0.187(11) Uani 1 1 d . U . . .
 H37A H 0.778023 0.704827 0.358295 0.281 Uiso 1 1 d R U . . .
 H37B H 0.825152 0.767897 0.354186 0.281 Uiso 1 1 d R U . . .
 O38 O 0.072(2) 0.1849(19) 0.6339(12) 0.140(14) Uani 0.5 1 d . U P . .
 H38A H 0.110126 0.204585 0.637096 0.210 Uiso 0.5 1 d R U P . .
 H38B H 0.053020 0.201354 0.611478 0.210 Uiso 0.5 1 d R U P . .
 O39 O 0.592(3) 0.811(3) 0.6460(18) 0.15(2) Uani 0.375 1 d . . P D -1
 H39A H 0.632604 0.822866 0.641412 0.225 Uiso 0.375 1 d R U P D -1
 H39B H 0.585393 0.778746 0.627972 0.225 Uiso 0.375 1 d R U P D -1
 O40 O 0.313(3) 0.160(3) 0.635(2) 0.18(3) Uani 0.375 1 d . U P . .
 H40A H 0.273342 0.163805 0.644754 0.268 Uiso 0.375 1 d R U P . .
 H40B H 0.312001 0.141393 0.609794 0.268 Uiso 0.375 1 d R U P . .
 O41 O 0.320(3) 0.457(2) 0.6294(14) 0.19(2) Uani 0.5 1 d . U P . .
 H41A H 0.342591 0.492407 0.619916 0.281 Uiso 0.5 1 d R U P . .
 H41B H 0.353967 0.435372 0.639099 0.281 Uiso 0.5 1 d R U P . .
 O42 O 0.230(4) 0.388(5) 0.635(3) 0.16(3) Uani 0.25 1 d . U P . .
 H42A H 0.262597 0.415248 0.632603 0.237 Uiso 0.25 1 d R U P . .
 H42B H 0.196287 0.408737 0.624122 0.237 Uiso 0.25 1 d R U P . .
 O43 O 0.138(5) 0.462(5) 0.600(3) 0.18(4) Uani 0.25 1 d . U P . .
 H43A H 0.155218 0.501598 0.599436 0.268 Uiso 0.25 1 d R U P . .
 H43B H 0.136648 0.450220 0.573346 0.268 Uiso 0.25 1 d R U P . .
 O44 O 0.028(6) 0.477(6) 0.617(4) 0.15(4) Uani 0.1875 1 d . U P . .
 H44A H 0.070741 0.473415 0.619464 0.227 Uiso 0.1875 1 d R U P . .
 H44B H 0.019471 0.517084 0.624992 0.227 Uiso 0.1875 1 d R U P . .
 O45 O 0.224(8) 0.461(9) 0.500000 0.16(6) Uani 0.1875 2 d S TU P . .
 H45A H 0.223803 0.494497 0.517010 0.233 Uiso 0.0938 1 d R U P . .
 H45B H 0.223803 0.426617 0.517010 0.233 Uiso 0.0938 1 d R U P . .
 O46 O 0.197(8) 0.533(8) 0.500000 0.20(6) Uani 0.25 2 d S TU P . .
 H46A H 0.214027 0.537264 0.525280 0.295 Uiso 0.125 1 d R U P . .
 H46B H 0.229067 0.541197 0.482500 0.295 Uiso 0.125 1 d R U P . .
 O47 O 0.008(6) 0.544(6) 0.520(4) 0.12(4) Uani 0.125 1 d . U P . .
 H47A H 0.050441 0.539692 0.515564 0.173 Uiso 0.125 1 d R U P . .
 H47B H -0.004010 0.535120 0.545689 0.173 Uiso 0.125 1 d R U P . .
 O48 O 0.931(4) 0.942(4) 0.388(3) 0.15(3) Uani 0.25 1 d . U P . .
 H48A H 0.892277 0.959405 0.382551 0.230 Uiso 0.25 1 d R U P . .
 H48B H 0.934309 0.944355 0.415680 0.230 Uiso 0.25 1 d R U P . .
 O50 O 0.015(5) 0.062(5) 0.663(3) 0.15(3) Uani 0.25 1 d . U P . .
 H50A H 0.039332 0.060591 0.640706 0.220 Uiso 0.25 1 d R U P . .
 H50B H 0.001813 0.021441 0.667125 0.220 Uiso 0.25 1 d R U P . .
 O51 O 0.023(3) 1.005(5) 0.639(2) 0.11(2) Uani 0.25 1 d . U P . .
 H51A H 0.016238 0.990548 0.664943 0.169 Uiso 0.25 1 d R U P . .
 H51B H 0.009978 0.975808 0.620763 0.169 Uiso 0.25 1 d R U P . .
 O52 O 0.032(9) 0.922(10) 0.500000 0.18(7) Uani 0.1875 2 d S TU P . .
 H52A H 0.065436 0.910485 0.484010 0.263 Uiso 0.0938 1 d R U P . .
 H52B H 0.046656 0.917267 0.526010 0.263 Uiso 0.0938 1 d R U P . .
 O53 O 0.042(7) 0.699(8) 0.731(5) 0.13(5) Uani 0.125 1 d . U P . .
 H53A H 0.025403 0.679497 0.708102 0.196 Uiso 0.125 1 d R U P . .
 H53B H 0.025693 0.679867 0.753452 0.196 Uiso 0.125 1 d R U P . .
 O54 O 0.033(4) 0.956(4) 0.673(3) 0.13(3) Uani 0.25 1 d . U P . .
 H54A H 0.006525 0.980227 0.688873 0.199 Uiso 0.25 1 d R U P . .
 H54B H 0.072856 0.972077 0.675213 0.199 Uiso 0.25 1 d R U P . .
 N7 N 0.4873(16) 0.7973(17) 0.7290(12) 0.140(10) Uani 0.667 1 d D U P E 1
 H7B H 0.456713 0.783192 0.711358 0.168 Uiso 0.667 1 calc R U P E 1
 C31 C 0.4727(15) 0.7961(16) 0.7703(13) 0.137(11) Uani 0.667 1 d D U P E 1
 H31 H 0.430779 0.781493 0.780019 0.164 Uiso 0.667 1 calc R U P E 1
 C32 C 0.521(2) 0.817(2) 0.7991(10) 0.144(11) Uani 0.667 1 d D U P E 1
 H32 H 0.513047 0.817260 0.829040 0.172 Uiso 0.667 1 calc R U P E 1
 C33 C 0.5804(17) 0.837(2) 0.7828(12) 0.135(11) Uani 0.667 1 d D U P E 1
 H33 H 0.613791 0.851793 0.801900 0.162 Uiso 0.667 1 calc R U P E 1
 C34 C 0.5930(15) 0.8371(19) 0.7400(13) 0.137(10) Uani 0.667 1 d D U P E 1
 H34 H 0.635084 0.850127 0.729604 0.164 Uiso 0.667 1 calc R U P E 1
 C35 C 0.5438(19) 0.818(2) 0.7116(10) 0.143(11) Uani 0.667 1 d D U P E 1
 H35 H 0.550055 0.819217 0.681534 0.172 Uiso 0.667 1 calc R U P E 1
 N8 N 0.612(3) 0.847(3) 0.4588(13) 0.044(12) Uani 0.1663 1 d D U P F -1
 H8B H 0.620381 0.851329 0.431329 0.052 Uiso 0.1663 1 calc R U P F -1
 C36 C 0.639(2) 0.888(2) 0.4869(13) 0.043(13) Uani 0.1663 1 d D U P F -1
 H36 H 0.667347 0.922548 0.476997 0.052 Uiso 0.1663 1 calc R U P F -1
 C37 C 0.628(3) 0.882(3) 0.5300(13) 0.047(13) Uani 0.1663 1 d D U P F -1
 H37 H 0.646880 0.911669 0.549758 0.057 Uiso 0.1663 1 calc R U P F -1
 C38 C 0.588(4) 0.832(3) 0.5438(14) 0.054(14) Uani 0.1663 1 d D U P F -1
 H38 H 0.580593 0.826333 0.573551 0.065 Uiso 0.1663 1 calc R U P F -1
 C39 C 0.559(3) 0.790(3) 0.5155(17) 0.052(14) Uani 0.1663 1 d D U P F -1
 H39 H 0.530861 0.756347 0.525051 0.063 Uiso 0.1663 1 calc R U P F -1
 C40 C 0.572(3) 0.799(3) 0.4725(16) 0.048(13) Uani 0.1663 1 d D U P F -1
 H40 H 0.552497 0.769544 0.452390 0.058 Uiso 0.1663 1 calc R U P F -1
 N9 N 0.508(3) 0.964(3) 0.4609(16) 0.095(15) Uani 0.25 1 d D U P G -1
 H9A H 0.505086 0.952461 0.433907 0.114 Uiso 0.25 1 calc R U P G -1
 C41 C 0.565(3) 0.990(3) 0.476(2) 0.097(15) Uani 0.25 1 d D U P G -1
 H41 H 0.601354 0.994272 0.457269 0.116 Uiso 0.25 1 calc R U P G -1
 C42 C 0.570(2) 1.008(3) 0.518(2) 0.085(15) Uani 0.25 1 d D U P G -1
 H42 H 0.609519 1.026215 0.529019 0.102 Uiso 0.25 1 calc R U P G -1
 C43 C 0.516(3) 1.001(3) 0.5440(17) 0.069(14) Uani 0.25 1 d D U P G -1
 H43 H 0.518345 1.014068 0.573146 0.083 Uiso 0.25 1 calc R U P G -1
 C44 C 0.458(2) 0.975(3) 0.5286(17) 0.064(13) Uani 0.25 1 d D U P G -1
 H44 H 0.421254 0.970070 0.546880 0.076 Uiso 0.25 1 calc R U P G -1
 C45 C 0.455(3) 0.957(2) 0.4861(17) 0.077(14) Uani 0.25 1 d D U P G -1
 H45 H 0.414828 0.939353 0.474902 0.093 Uiso 0.25 1 calc R U P G -1
 N10 N 0.172(4) 0.088(3) 0.516(3) 0.100(17) Uani 0.1667 1 d D U P H -1
 H10A H 0.153650 0.050686 0.524405 0.120 Uiso 0.1667 1 calc R U P H -1
 C51 C 0.189(6) 0.133(5) 0.545(3) 0.098(18) Uani 0.1667 1 d D U P H -1
 H51 H 0.182035 0.124877 0.574535 0.118 Uiso 0.1667 1 calc R U P H -1
 C52 C 0.217(5) 0.192(4) 0.533(3) 0.100(18) Uani 0.1667 1 d D U P H -1
 H52 H 0.229481 0.224390 0.553571 0.119 Uiso 0.1667 1 calc R U P H -1
 C53 C 0.227(4) 0.204(3) 0.490(3) 0.100(18) Uani 0.1667 1 d D U P H -1
 H53 H 0.246873 0.244507 0.481554 0.120 Uiso 0.1667 1 calc R U P H -1
 C54 C 0.210(6) 0.158(5) 0.461(2) 0.100(18) Uani 0.1667 1 d D U P H -1
 H54 H 0.216813 0.165987 0.431384 0.120 Uiso 0.1667 1 calc R U P H -1
 C55 C 0.181(5) 0.100(4) 0.474(3) 0.099(17) Uani 0.1667 1 d D U P H -1
 H55 H 0.168691 0.067802 0.453853 0.119 Uiso 0.1667 1 calc R U P H -1
 N11 N 0.379(3) 0.525(3) 0.5131(19) 0.077(16) Uani 0.1667 1 d D U P I -1
 H11A H 0.358627 0.561025 0.521042 0.092 Uiso 0.1667 1 calc R U P I -1
 C46 C 0.393(4) 0.515(3) 0.4716(18) 0.075(16) Uani 0.1667 1 d D U P I -1
 H46 H 0.379451 0.546553 0.450891 0.089 Uiso 0.1667 1 calc R U P I -1
 C47 C 0.425(4) 0.458(4) 0.4589(16) 0.072(16) Uani 0.1667 1 d D U P I -1
 H47 H 0.435056 0.451022 0.429641 0.086 Uiso 0.1667 1 calc R U P I -1
 C48 C 0.443(3) 0.413(3) 0.4890(18) 0.066(16) Uani 0.1667 1 d D U P I -1
 H48 H 0.465188 0.374010 0.480379 0.080 Uiso 0.1667 1 calc R U P I -1
 C49 C 0.430(3) 0.424(3) 0.5310(18) 0.070(16) Uani 0.1667 1 d D U P I -1
 H49 H 0.443671 0.392270 0.551937 0.084 Uiso 0.1667 1 calc R U P I -1
 C50 C 0.398(4) 0.481(3) 0.5428(16) 0.072(16) Uani 0.1667 1 d D U P I -1
 H50 H 0.388130 0.488572 0.572088 0.086 Uiso 0.1667 1 calc R U P I -1
 N12 N 0.066(7) 0.282(6) 0.460(3) 0.07(3) Uani 0.0833 1 d D U P J -1
 H12A H 0.057771 0.274188 0.432559 0.083 Uiso 0.0833 1 calc R U P J -1
 C56 C 0.094(7) 0.339(5) 0.471(3) 0.07(3) Uani 0.0833 1 d D U P J -1
 H56 H 0.104136 0.371066 0.449836 0.088 Uiso 0.0833 1 calc R U P J -1
 C57 C 0.108(6) 0.352(5) 0.513(4) 0.07(3) Uani 0.0833 1 d D U P J -1
 H57 H 0.127421 0.392815 0.521658 0.084 Uiso 0.0833 1 calc R U P J -1
 C58 C 0.093(7) 0.305(6) 0.543(3) 0.06(2) Uani 0.0833 1 d D U P J -1
 H58 H 0.103512 0.313061 0.572468 0.072 Uiso 0.0833 1 calc R U P J -1
 C59 C 0.064(6) 0.247(5) 0.532(3) 0.06(2) Uani 0.0833 1 d D U P J -1
 H59 H 0.053166 0.215360 0.552462 0.068 Uiso 0.0833 1 calc R U P J -1
 C60 C 0.052(5) 0.236(5) 0.489(3) 0.06(2) Uani 0.0833 1 d D U P J -1
 H60 H 0.032713 0.194965 0.480141 0.072 Uiso 0.0833 1 calc R U P J -1


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 Eu1 Eu1 3.7247(13) 6_556 ?
 Eu1 O7 2.560(8) . ?
 Eu1 O14 2.476(12) . ?
 Eu1 O16 2.479(12) . ?
 Eu1 O17 2.587(12) . ?
 Eu1 O18 2.533(14) . ?
 Eu1 O19 2.662(14) . ?
 Eu1 O32 2.493(9) . ?
 Eu1 O33 2.462(9) . ?
 Eu1 O34 2.477(10) . ?
 Mo1 Mo2 2.509(2) . ?
 Mo1 Mo3 2.538(2) . ?
 Mo1 Mo5 1.255(13) . ?
 Mo1 O1 1.911(12) . ?
 Mo1 O2 1.947(12) . ?
 Mo1 O7 2.064(9) . ?
 Mo1 O8 2.029(11) . ?
 Mo1 O9 2.114(10) . ?
 Mo1 N1 2.197(13) . ?
 Mo2 Mo3 2.525(3) . ?
 Mo2 O1 1.911(13) . ?
 Mo2 O3 1.921(14) . ?
 Mo2 O7 2.055(9) . ?
 Mo2 O12 2.028(12) . ?
 Mo2 O13 2.125(12) . ?
 Mo2 N2 2.197(14) . ?
 Mo3 O2 1.922(12) . ?
 Mo3 O3 1.917(13) . ?
 Mo3 O7 2.060(9) . ?
 Mo3 O10 2.050(11) . ?
 Mo3 O11 2.066(11) . ?
 Mo3 N3 2.212(14) . ?
 Mo4 Mo5 2.436(19) . ?
 Mo4 Mo6 2.447(16) . ?
 Mo4 O4 1.93(2) . ?
 Mo4 O6 1.96(2) . ?
 Mo4 O7 2.156(14) . ?
 Mo4 O8 2.173(16) . ?
 Mo4 O13 2.140(17) . ?
 Mo4 N4 2.17(7) . ?
 Mo5 Mo6 2.536(15) . ?
 Mo5 O4 1.95(2) . ?
 Mo5 O5 1.88(2) . ?
 Mo5 O7 2.058(14) . ?
 Mo5 O9 2.080(13) . ?
 Mo5 O10 2.319(17) . ?
 Mo5 N5 2.22(2) . ?
 Mo6 O5 1.95(2) . ?
 Mo6 O6 1.79(2) . ?
 Mo6 O7 2.071(12) . ?
 Mo6 O11 2.263(16) . ?
 Mo6 O12 2.110(16) . ?
 Mo6 N6 2.29(6) . ?
 Mo7 O8 1.807(10) . ?
 Mo7 O14 2.219(12) . ?
 Mo7 O15 2.179(13) . ?
 Mo7 O20 1.695(16) . ?
 Mo7 O21 1.719(14) . ?
 Mo7 O29 2.057(10) . ?
 Mo8 O12 1.799(11) . ?
 Mo8 O18 2.233(13) . ?
 Mo8 O19 2.204(14) . ?
 Mo8 O24 1.624(17) . ?
 Mo8 O25 1.700(16) . ?
 Mo8 O31 2.066(10) . ?
 Mo9 O10 1.812(10) . ?
 Mo9 O16 2.236(12) . ?
 Mo9 O17 2.232(12) . ?
 Mo9 O22 1.670(14) . ?
 Mo9 O23 1.699(14) . ?
 Mo9 O30 2.075(9) . ?
 P1 H1 1.3900 . ?
 P1 O9 1.528(9) . ?
 P1 O15 1.506(14) . ?
 P1 O16 1.513(12) . ?
 P1 O27 1.48(3) . ?
 P2 H2 1.3916 . ?
 P2 O11 1.525(11) . ?
 P2 O17 1.521(13) . ?
 P2 O18 1.515(14) . ?
 P2 O28 1.52(3) . ?
 P3 H3 1.3927 . ?
 P3 O13 1.523(10) . ?
 P3 O14 1.532(13) . ?
 P3 O19 1.519(16) . ?
 P3 O26 1.59(5) . ?
 P4 H4 1.3899 . ?
 P4 O29 1.525(11) 6_556 ?
 P4 O29 1.525(11) . ?
 P4 O32 1.535(15) . ?
 P5 H5 1.3906 . ?
 P5 O30 1.530(14) . ?
 P5 O30 1.530(14) 6_556 ?
 P5 O33 1.51(2) . ?
 P6 H6 1.3909 . ?
 P6 O30 1.532(16) 6_556 ?
 P6 O30 1.532(16) . ?
 P6 O33 1.51(2) . ?
 P7 H7 1.3875 . ?
 P7 O31 1.48(2) 6_556 ?
 P7 O31 1.48(2) . ?
 P7 O34 1.50(2) . ?
 P8 H8 1.3899 . ?
 P8 O31 1.55(2) 6_556 ?
 P8 O31 1.55(2) . ?
 P8 O34 1.58(3) . ?
 O26 H3 0.2097 . ?
 O27 H1 0.1598 . ?
 O28 H2 0.1637 . ?
 N1 C1 1.331(13) . ?
 N1 C5 1.343(12) . ?
 N2 C6 1.345(16) . ?
 N2 C10 1.349(15) . ?
 N3 C11 1.332(15) . ?
 N3 C15 1.332(15) . ?
 N4 C16 1.339(19) . ?
 N4 C20 1.345(19) . ?
 N5 C21 1.353(19) . ?
 N5 C25 1.348(19) . ?
 N6 H22 1.46(9) 8_657 ?
 N6 C26 1.344(19) . ?
 N6 C30 1.344(19) . ?
 C1 H1A 0.9500 . ?
 C1 C2 1.377(12) . ?
 C2 H2A 0.9500 . ?
 C2 C3 1.367(12) . ?
 C3 H3A 0.9500 . ?
 C3 C4 1.363(12) . ?
 C4 H4A 0.9500 . ?
 C4 C5 1.379(12) . ?
 C5 H5A 0.9500 . ?
 C6 H6A 0.9500 . ?
 C6 C7 1.371(16) . ?
 C7 H7A 0.9500 . ?
 C7 C8 1.361(16) . ?
 C8 H8A 0.9500 . ?
 C8 C9 1.370(17) . ?
 C9 H9 0.9500 . ?
 C9 C10 1.372(16) . ?
 C10 H10 0.9500 . ?
 C11 H11 0.9500 . ?
 C11 C12 1.380(16) . ?
 C12 H12 0.9500 . ?
 C12 C13 1.372(16) . ?
 C13 H13 0.9500 . ?
 C13 C14 1.343(17) . ?
 C14 H14 0.9500 . ?
 C14 C15 1.380(16) . ?
 C15 H15 0.9500 . ?
 C16 H16 0.9500 . ?
 C16 C17 1.379(19) . ?
 C17 H17 0.9500 . ?
 C17 C18 1.365(19) . ?
 C18 H18 0.9500 . ?
 C18 C19 1.363(19) . ?
 C19 H19 0.9500 . ?
 C19 C20 1.381(19) . ?
 C20 H20 0.9500 . ?
 C21 H21 0.9500 . ?
 C21 C22 1.379(19) . ?
 C22 H22 0.9500 . ?
 C22 C23 1.359(19) . ?
 C23 H23 0.9500 . ?
 C23 C24 1.365(19) . ?
 C24 H24 0.9500 . ?
 C24 C25 1.380(19) . ?
 C25 H25 0.9500 . ?
 C26 H26 0.9500 . ?
 C26 C27 1.381(19) . ?
 C27 H27 0.9500 . ?
 C27 C28 1.363(19) . ?
 C28 H28 0.9500 . ?
 C28 C29 1.361(19) . ?
 C29 H29 0.9500 . ?
 C29 C30 1.380(19) . ?
 C30 H30 0.9500 . ?
 O35 H35A 0.8626 . ?
 O35 H35B 0.8586 . ?
 O35 H35C 0.8617 . ?
 O36 H36A 0.8808 . ?
 O36 H36B 1.43(8) 2_665 ?
 O36 H36B 0.8697 . ?
 O36 H36C 0.8699 . ?
 O37 H37A 0.8668 . ?
 O37 H37B 0.8853 . ?
 O38 H38A 0.8736 . ?
 O38 H38B 0.8698 . ?
 O39 H39A 0.8698 . ?
 O39 H39B 0.8695 . ?
 O40 H40A 0.8701 . ?
 O40 H40B 0.8695 . ?
 O41 H41A 0.8992 . ?
 O41 H41B 0.8698 . ?
 O41 H42A 1.4454 . ?
 O42 H42A 0.8699 . ?
 O42 H42B 0.8697 . ?
 O43 H43A 0.8697 . ?
 O43 H43B 0.8701 . ?
 O44 H44A 0.8700 . ?
 O44 H44B 0.8707 . ?
 O44 H44B 1.0(2) 2_565 ?
 O45 O45 0.0(3) 6_556 ?
 O45 H45A 0.8696 . ?
 O45 H45A 0.8696(13) 6_556 ?
 O45 H45B 0.8705 6_556 ?
 O45 H45B 0.8705 . ?
 O46 H45A 1.0883 . ?
 O46 H46A 0.8697 . ?
 O46 H46A 0.8697 6_556 ?
 O46 H46B 0.8700 . ?
 O46 H46B 0.8700 6_556 ?
 O47 H47A 1.40(19) 6_556 ?
 O47 H47A 0.8702 . ?
 O47 H47B 0.8701 . ?
 O48 H48A 0.8696 . ?
 O48 H48B 0.8699 . ?
 O48 O51 1.66(11) 5_676 ?
 O50 H50A 0.8700 . ?
 O50 H50B 0.8697 . ?
 O50 O51 1.74(13) 2_565 ?
 O50 O51 1.39(11) 1_545 ?
 O50 O54 1.08(10) 2_565 ?
 O51 H51A 0.8703 . ?
 O51 H51A 1.13(9) 2_575 ?
 O51 H51B 0.95(13) 2_575 ?
 O51 H51B 0.8695 . ?
 O51 O54 1.74(12) 2_575 ?
 O52 H52A 0.8700 . ?
 O52 H52A 0.8700(11) 6_556 ?
 O52 H52B 0.8701 6_556 ?
 O52 H52B 0.8701 . ?
 O53 H53A 0.8703 . ?
 O53 H53B 0.8691 . ?
 O54 H51A 0.8172 . ?
 O54 H54A 0.8696 . ?
 O54 H54B 0.8700 . ?
 N7 H7B 0.8800 . ?
 N7 C31 1.327(18) . ?
 N7 C35 1.335(18) . ?
 C31 H31 0.9500 . ?
 C31 C32 1.398(18) . ?
 C32 H32 0.9500 . ?
 C32 C33 1.369(19) . ?
 C33 H33 0.9500 . ?
 C33 C34 1.366(18) . ?
 C34 H34 0.9500 . ?
 C34 C35 1.391(18) . ?
 C35 H35 0.9500 . ?
 N8 H8B 0.8800 . ?
 N8 C36 1.334(19) . ?
 N8 C40 1.342(19) . ?
 C36 H36 0.9500 . ?
 C36 C37 1.376(19) . ?
 C37 H37 0.9500 . ?
 C37 C38 1.359(19) . ?
 C38 H38 0.9500 . ?
 C38 C39 1.355(19) . ?
 C39 H39 0.9500 . ?
 C39 C40 1.380(19) . ?
 C40 H40 0.9500 . ?
 N9 H9A 0.8800 . ?
 N9 C41 1.345(19) . ?
 N9 C45 1.343(19) . ?
 C41 H41 0.9500 . ?
 C41 C42 1.384(19) . ?
 C42 H42 0.9500 . ?
 C42 C43 1.367(19) . ?
 C43 H43 0.9500 . ?
 C43 C44 1.363(19) . ?
 C44 H44 0.9500 . ?
 C44 C45 1.383(19) . ?
 C45 H45 0.9500 . ?
 N10 H10A 0.8800 . ?
 N10 C51 1.339(19) . ?
 N10 C55 1.344(19) . ?
 C51 H51 0.9500 . ?
 C51 C52 1.380(19) . ?
 C52 H52 0.9500 . ?
 C52 C53 1.361(19) . ?
 C53 H53 0.9500 . ?
 C53 C54 1.363(19) . ?
 C54 H54 0.9500 . ?
 C54 C55 1.376(19) . ?
 C55 H55 0.9500 . ?
 N11 H11A 0.8800 . ?
 N11 C46 1.345(19) . ?
 N11 C50 1.344(19) . ?
 C46 H46 0.9500 . ?
 C46 C47 1.381(19) . ?
 C47 H47 0.9500 . ?
 C47 C48 1.361(19) . ?
 C48 H48 0.9500 . ?
 C48 C49 1.359(19) . ?
 C49 H49 0.9500 . ?
 C49 C50 1.384(19) . ?
 C50 H50 0.9500 . ?
 N12 H12A 0.8800 . ?
 N12 C56 1.339(19) . ?
 N12 C60 1.340(19) . ?
 C56 H56 0.9500 . ?
 C56 C57 1.383(19) . ?
 C57 H57 0.9500 . ?
 C57 C58 1.364(19) . ?
 C58 H58 0.9500 . ?
 C58 C59 1.363(19) . ?
 C59 H59 0.9500 . ?
 C59 C60 1.382(19) . ?
 C60 H60 0.9500 . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 O7 Eu1 Eu1 178.6(2) . 6_556 ?
 O7 Eu1 O17 75.4(3) . . ?
 O7 Eu1 O19 74.0(3) . . ?
 O14 Eu1 Eu1 108.0(2) . 6_556 ?
 O14 Eu1 O7 70.6(3) . . ?
 O14 Eu1 O16 106.7(4) . . ?
 O14 Eu1 O17 145.9(3) . . ?
 O14 Eu1 O18 111.2(4) . . ?
 O14 Eu1 O19 55.0(4) . . ?
 O14 Eu1 O32 71.4(3) . . ?
 O14 Eu1 O34 103.7(5) . . ?
 O16 Eu1 Eu1 109.1(2) . 6_556 ?
 O16 Eu1 O7 71.7(3) . . ?
 O16 Eu1 O17 62.8(4) . . ?
 O16 Eu1 O18 113.7(4) . . ?
 O16 Eu1 O19 145.2(3) . . ?
 O16 Eu1 O32 101.5(4) . . ?
 O17 Eu1 Eu1 106.0(2) . 6_556 ?
 O17 Eu1 O19 113.7(4) . . ?
 O18 Eu1 Eu1 108.0(2) . 6_556 ?
 O18 Eu1 O7 72.5(3) . . ?
 O18 Eu1 O17 55.2(4) . . ?
 O18 Eu1 O19 60.0(5) . . ?
 O19 Eu1 Eu1 105.1(3) . 6_556 ?
 O32 Eu1 Eu1 41.7(2) . 6_556 ?
 O32 Eu1 O7 137.2(3) . . ?
 O32 Eu1 O17 140.5(4) . . ?
 O32 Eu1 O18 141.1(4) . . ?
 O32 Eu1 O19 99.3(4) . . ?
 O33 Eu1 Eu1 40.9(2) . 6_556 ?
 O33 Eu1 O7 140.4(3) . . ?
 O33 Eu1 O14 139.2(4) . . ?
 O33 Eu1 O16 73.8(3) . . ?
 O33 Eu1 O17 72.0(4) . . ?
 O33 Eu1 O18 105.0(4) . . ?
 O33 Eu1 O19 140.3(4) . . ?
 O33 Eu1 O32 68.7(4) . . ?
 O33 Eu1 O34 70.2(4) . . ?
 O34 Eu1 Eu1 41.2(3) . 6_556 ?
 O34 Eu1 O7 138.6(4) . . ?
 O34 Eu1 O16 143.7(4) . . ?
 O34 Eu1 O17 100.6(4) . . ?
 O34 Eu1 O18 71.9(4) . . ?
 O34 Eu1 O19 70.2(4) . . ?
 O34 Eu1 O32 70.0(4) . . ?
 Mo2 Mo1 Mo3 60.04(7) . . ?
 Mo5 Mo1 Mo2 91.6(5) . . ?
 Mo5 Mo1 Mo3 31.7(5) . . ?
 Mo5 Mo1 O1 117.5(6) . . ?
 Mo5 Mo1 O2 33.5(5) . . ?
 Mo5 Mo1 O7 72.0(5) . . ?
 Mo5 Mo1 O8 149.0(5) . . ?
 Mo5 Mo1 O9 71.1(5) . . ?
 Mo5 Mo1 N1 109.7(6) . . ?
 O1 Mo1 Mo2 49.0(4) . . ?
 O1 Mo1 Mo3 94.6(4) . . ?
 O1 Mo1 O2 94.8(5) . . ?
 O1 Mo1 O7 100.6(5) . . ?
 O1 Mo1 O8 90.7(5) . . ?
 O1 Mo1 O9 168.3(5) . . ?
 O1 Mo1 N1 82.7(5) . . ?
 O2 Mo1 Mo2 94.2(4) . . ?
 O2 Mo1 Mo3 48.6(4) . . ?
 O2 Mo1 O7 99.7(4) . . ?
 O2 Mo1 O8 166.4(5) . . ?
 O2 Mo1 O9 89.2(5) . . ?
 O2 Mo1 N1 83.4(5) . . ?
 O7 Mo1 Mo2 52.3(3) . . ?
 O7 Mo1 Mo3 51.9(3) . . ?
 O7 Mo1 O9 89.6(4) . . ?
 O7 Mo1 N1 175.2(4) . . ?
 O8 Mo1 Mo2 98.8(4) . . ?
 O8 Mo1 Mo3 143.4(3) . . ?
 O8 Mo1 O7 91.5(4) . . ?
 O8 Mo1 O9 83.1(5) . . ?
 O8 Mo1 N1 84.9(5) . . ?
 O9 Mo1 Mo2 141.8(3) . . ?
 O9 Mo1 Mo3 96.3(3) . . ?
 O9 Mo1 N1 86.8(4) . . ?
 N1 Mo1 Mo2 131.4(4) . . ?
 N1 Mo1 Mo3 131.7(4) . . ?
 Mo1 Mo2 Mo3 60.57(7) . . ?
 O1 Mo2 Mo1 49.0(4) . . ?
 O1 Mo2 Mo3 95.1(4) . . ?
 O1 Mo2 O3 94.0(5) . . ?
 O1 Mo2 O7 100.9(5) . . ?
 O1 Mo2 O12 166.0(5) . . ?
 O1 Mo2 O13 90.1(5) . . ?
 O1 Mo2 N2 81.7(6) . . ?
 O3 Mo2 Mo1 94.1(4) . . ?
 O3 Mo2 Mo3 48.8(4) . . ?
 O3 Mo2 O7 100.4(5) . . ?
 O3 Mo2 O12 89.4(5) . . ?
 O3 Mo2 O13 168.3(5) . . ?
 O3 Mo2 N2 85.4(6) . . ?
 O7 Mo2 Mo1 52.6(3) . . ?
 O7 Mo2 Mo3 52.2(3) . . ?
 O7 Mo2 O13 89.5(4) . . ?
 O7 Mo2 N2 173.4(5) . . ?
 O12 Mo2 Mo1 144.4(3) . . ?
 O12 Mo2 Mo3 97.4(4) . . ?
 O12 Mo2 O7 91.9(4) . . ?
 O12 Mo2 O13 84.1(5) . . ?
 O12 Mo2 N2 85.0(5) . . ?
 O13 Mo2 Mo1 96.8(3) . . ?
 O13 Mo2 Mo3 141.7(3) . . ?
 O13 Mo2 N2 84.3(5) . . ?
 N2 Mo2 Mo1 130.6(4) . . ?
 N2 Mo2 Mo3 133.9(4) . . ?
 Mo2 Mo3 Mo1 59.40(7) . . ?
 O2 Mo3 Mo1 49.4(4) . . ?
 O2 Mo3 Mo2 94.3(4) . . ?
 O2 Mo3 O7 100.7(5) . . ?
 O2 Mo3 O10 88.7(5) . . ?
 O2 Mo3 O11 168.1(5) . . ?
 O2 Mo3 N3 84.6(5) . . ?
 O3 Mo3 Mo1 93.3(4) . . ?
 O3 Mo3 Mo2 48.9(4) . . ?
 O3 Mo3 O2 93.2(5) . . ?
 O3 Mo3 O7 100.4(5) . . ?
 O3 Mo3 O10 167.6(5) . . ?
 O3 Mo3 O11 91.5(5) . . ?
 O3 Mo3 N3 82.5(6) . . ?
 O7 Mo3 Mo1 52.1(3) . . ?
 O7 Mo3 Mo2 52.1(3) . . ?
 O7 Mo3 O11 89.1(4) . . ?
 O7 Mo3 N3 173.7(5) . . ?
 O10 Mo3 Mo1 97.3(3) . . ?
 O10 Mo3 Mo2 143.1(3) . . ?
 O10 Mo3 O7 91.3(4) . . ?
 O10 Mo3 O11 84.4(5) . . ?
 O10 Mo3 N3 85.5(5) . . ?
 O11 Mo3 Mo1 141.2(3) . . ?
 O11 Mo3 Mo2 97.0(4) . . ?
 O11 Mo3 N3 85.2(5) . . ?
 N3 Mo3 Mo1 133.7(4) . . ?
 N3 Mo3 Mo2 131.4(4) . . ?
 Mo5 Mo4 Mo6 62.6(5) . . ?
 O4 Mo4 Mo5 51.4(7) . . ?
 O4 Mo4 Mo6 97.2(15) . . ?
 O4 Mo4 O6 82.0(19) . . ?
 O4 Mo4 O7 103.8(9) . . ?
 O4 Mo4 O8 83.4(16) . . ?
 O4 Mo4 O13 167.7(13) . . ?
 O4 Mo4 N4 81(3) . . ?
 O6 Mo4 Mo5 84.9(8) . . ?
 O6 Mo4 Mo6 46.3(7) . . ?
 O6 Mo4 O7 99.1(8) . . ?
 O6 Mo4 O8 165.4(11) . . ?
 O6 Mo4 O13 103.3(11) . . ?
 O6 Mo4 N4 93(3) . . ?
 O7 Mo4 Mo5 52.8(4) . . ?
 O7 Mo4 Mo6 53.0(4) . . ?
 O7 Mo4 O8 85.2(5) . . ?
 O7 Mo4 N4 168(3) . . ?
 O8 Mo4 Mo5 86.7(6) . . ?
 O8 Mo4 Mo6 137.4(6) . . ?
 O13 Mo4 Mo5 139.3(6) . . ?
 O13 Mo4 Mo6 94.4(6) . . ?
 O13 Mo4 O7 86.5(5) . . ?
 O13 Mo4 O8 90.9(6) . . ?
 O13 Mo4 N4 88(3) . . ?
 N4 Mo4 Mo5 132(3) . . ?
 N4 Mo4 Mo6 138(3) . . ?
 N4 Mo4 O8 84(3) . . ?
 Mo1 Mo5 Mo4 31.9(5) . . ?
 Mo1 Mo5 Mo6 90.7(7) . . ?
 Mo1 Mo5 O4 41.3(10) . . ?
 Mo1 Mo5 O5 116.3(15) . . ?
 Mo1 Mo5 O7 72.6(6) . . ?
 Mo1 Mo5 O9 74.1(5) . . ?
 Mo1 Mo5 O10 149.3(6) . . ?
 Mo1 Mo5 N5 112(2) . . ?
 Mo4 Mo5 Mo6 58.9(5) . . ?
 O4 Mo5 Mo4 50.8(7) . . ?
 O4 Mo5 Mo6 94.0(14) . . ?
 O4 Mo5 O7 106.9(9) . . ?
 O4 Mo5 O9 95.8(16) . . ?
 O4 Mo5 O10 168.6(10) . . ?
 O4 Mo5 N5 82(2) . . ?
 O5 Mo5 Mo4 90.9(13) . . ?
 O5 Mo5 Mo6 49.7(7) . . ?
 O5 Mo5 O4 88(2) . . ?
 O5 Mo5 O7 101.3(8) . . ?
 O5 Mo5 O9 165.9(12) . . ?
 O5 Mo5 O10 87.1(13) . . ?
 O5 Mo5 N5 86(2) . . ?
 O7 Mo5 Mo4 56.6(5) . . ?
 O7 Mo5 Mo6 52.3(4) . . ?
 O7 Mo5 O9 90.7(5) . . ?
 O7 Mo5 O10 84.1(5) . . ?
 O7 Mo5 N5 169(2) . . ?
 O9 Mo5 Mo4 101.9(6) . . ?
 O9 Mo5 Mo6 143.0(6) . . ?
 O9 Mo5 O10 86.9(6) . . ?
 O9 Mo5 N5 81(2) . . ?
 O10 Mo5 Mo4 139.4(6) . . ?
 O10 Mo5 Mo6 90.5(5) . . ?
 N5 Mo5 Mo4 132(2) . . ?
 N5 Mo5 Mo6 136(2) . . ?
 N5 Mo5 O10 88(2) . . ?
 Mo4 Mo6 Mo5 58.5(5) . . ?
 O5 Mo6 Mo4 89.0(12) . . ?
 O5 Mo6 Mo5 47.4(7) . . ?
 O5 Mo6 O7 98.6(8) . . ?
 O5 Mo6 O11 93.6(12) . . ?
 O5 Mo6 O12 172.3(8) . . ?
 O5 Mo6 N6 84(3) . . ?
 O6 Mo6 Mo4 52.3(8) . . ?
 O6 Mo6 Mo5 85.5(9) . . ?
 O6 Mo6 O5 75.6(15) . . ?
 O6 Mo6 O7 108.3(9) . . ?
 O6 Mo6 O11 164.7(10) . . ?
 O6 Mo6 O12 101.3(12) . . ?
 O6 Mo6 N6 86(2) . . ?
 O7 Mo6 Mo4 56.3(4) . . ?
 O7 Mo6 Mo5 51.9(4) . . ?
 O7 Mo6 O11 83.7(5) . . ?
 O7 Mo6 O12 89.1(5) . . ?
 O7 Mo6 N6 165(2) . . ?
 O11 Mo6 Mo4 139.7(5) . . ?
 O11 Mo6 Mo5 95.2(6) . . ?
 O11 Mo6 N6 82(2) . . ?
 O12 Mo6 Mo4 94.7(7) . . ?
 O12 Mo6 Mo5 140.0(6) . . ?
 O12 Mo6 O11 88.0(6) . . ?
 O12 Mo6 N6 89(3) . . ?
 N6 Mo6 Mo4 138(2) . . ?
 N6 Mo6 Mo5 131(3) . . ?
 O8 Mo7 O14 83.4(5) . . ?
 O8 Mo7 O15 83.3(5) . . ?
 O8 Mo7 O29 153.9(4) . . ?
 O15 Mo7 O14 74.6(6) . . ?
 O20 Mo7 O8 102.8(6) . . ?
 O20 Mo7 O14 87.9(6) . . ?
 O20 Mo7 O15 160.8(6) . . ?
 O20 Mo7 O21 104.5(7) . . ?
 O20 Mo7 O29 93.0(5) . . ?
 O21 Mo7 O8 103.4(6) . . ?
 O21 Mo7 O14 163.9(5) . . ?
 O21 Mo7 O15 91.5(7) . . ?
 O21 Mo7 O29 92.3(5) . . ?
 O29 Mo7 O14 76.6(4) . . ?
 O29 Mo7 O15 75.5(4) . . ?
 O12 Mo8 O18 83.9(5) . . ?
 O12 Mo8 O19 83.5(5) . . ?
 O12 Mo8 O31 154.0(5) . . ?
 O19 Mo8 O18 71.8(5) . . ?
 O24 Mo8 O12 102.7(6) . . ?
 O24 Mo8 O18 89.5(7) . . ?
 O24 Mo8 O19 159.7(7) . . ?
 O24 Mo8 O25 104.2(9) . . ?
 O24 Mo8 O31 91.5(6) . . ?
 O25 Mo8 O12 103.2(6) . . ?
 O25 Mo8 O18 162.6(6) . . ?
 O25 Mo8 O19 93.0(7) . . ?
 O25 Mo8 O31 94.1(6) . . ?
 O31 Mo8 O18 74.5(4) . . ?
 O31 Mo8 O19 76.3(5) . . ?
 O10 Mo9 O16 85.3(4) . . ?
 O10 Mo9 O17 84.1(4) . . ?
 O10 Mo9 O30 156.1(4) . . ?
 O17 Mo9 O16 72.4(4) . . ?
 O22 Mo9 O10 102.9(5) . . ?
 O22 Mo9 O16 90.4(6) . . ?
 O22 Mo9 O17 161.0(5) . . ?
 O22 Mo9 O23 103.3(8) . . ?
 O22 Mo9 O30 91.9(5) . . ?
 O23 Mo9 O10 101.6(6) . . ?
 O23 Mo9 O16 162.7(6) . . ?
 O23 Mo9 O17 92.3(7) . . ?
 O23 Mo9 O30 93.0(5) . . ?
 O30 Mo9 O16 75.9(4) . . ?
 O30 Mo9 O17 76.4(4) . . ?
 O9 P1 H1 107.8 . . ?
 O15 P1 H1 109.6 . . ?
 O15 P1 O9 113.5(6) . . ?
 O15 P1 O16 102.9(8) . . ?
 O16 P1 H1 108.5 . . ?
 O16 P1 O9 114.4(6) . . ?
 O27 P1 H1 5.3 . . ?
 O27 P1 O9 107.6(11) . . ?
 O27 P1 O15 105.3(18) . . ?
 O27 P1 O16 112.9(16) . . ?
 O11 P2 H2 109.2 . . ?
 O17 P2 H2 108.9 . . ?
 O17 P2 O11 112.9(7) . . ?
 O17 P2 O28 106.0(13) . . ?
 O18 P2 H2 109.4 . . ?
 O18 P2 O11 113.6(7) . . ?
 O18 P2 O17 102.8(7) . . ?
 O18 P2 O28 112.8(14) . . ?
 O28 P2 H2 3.8 . . ?
 O28 P2 O11 108.5(11) . . ?
 O13 P3 H3 109.1 . . ?
 O13 P3 O14 114.7(7) . . ?
 O13 P3 O26 107(2) . . ?
 O14 P3 H3 108.3 . . ?
 O14 P3 O26 109(2) . . ?
 O19 P3 H3 109.6 . . ?
 O19 P3 O13 112.6(7) . . ?
 O19 P3 O14 102.4(7) . . ?
 O19 P3 O26 111(2) . . ?
 O26 P3 H3 2.5 . . ?
 O29 P4 H4 107.1 . . ?
 O29 P4 H4 107.1 6_556 . ?
 O29 P4 O29 103.9(9) . 6_556 ?
 O29 P4 O32 115.7(5) . . ?
 O29 P4 O32 115.7(5) 6_556 . ?
 O32 P4 H4 106.8 . . ?
 O30 P5 H5 106.3 6_556 . ?
 O30 P5 H5 106.3 . . ?
 O30 P5 O30 106.7(13) . 6_556 ?
 O33 P5 H5 107.7 . . ?
 O33 P5 O30 114.6(12) . . ?
 O33 P5 O30 114.6(12) . 6_556 ?
 O30 P6 H6 106.3 . . ?
 O30 P6 H6 106.3 6_556 . ?
 O30 P6 O30 106.4(15) . 6_556 ?
 O33 P6 H6 107.7 . . ?
 O33 P6 O30 114.7(14) . 6_556 ?
 O33 P6 O30 114.7(14) . . ?
 O31 P7 H7 102.0 6_556 . ?
 O31 P7 H7 102.0 . . ?
 O31 P7 O31 109(2) 6_556 . ?
 O31 P7 O34 120(2) . . ?
 O31 P7 O34 120(2) 6_556 . ?
 O34 P7 H7 101.1 . . ?
 O31 P8 H8 112.2 . . ?
 O31 P8 H8 112.2 6_556 . ?
 O31 P8 O31 101.6(18) . 6_556 ?
 O31 P8 O34 110.8(16) 6_556 . ?
 O31 P8 O34 110.8(16) . . ?
 O34 P8 H8 109.2 . . ?
 Mo2 O1 Mo1 82.1(5) . . ?
 Mo3 O2 Mo1 82.0(5) . . ?
 Mo3 O3 Mo2 82.3(4) . . ?
 Mo4 O4 Mo5 77.7(9) . . ?
 Mo5 O5 Mo6 82.8(9) . . ?
 Mo6 O6 Mo4 81.3(10) . . ?
 Mo1 O7 Eu1 136.1(4) . . ?
 Mo1 O7 Mo4 42.2(4) . . ?
 Mo1 O7 Mo6 86.9(4) . . ?
 Mo2 O7 Eu1 134.9(5) . . ?
 Mo2 O7 Mo1 75.0(3) . . ?
 Mo2 O7 Mo3 75.7(3) . . ?
 Mo2 O7 Mo4 39.8(4) . . ?
 Mo2 O7 Mo5 87.2(4) . . ?
 Mo2 O7 Mo6 38.4(4) . . ?
 Mo3 O7 Eu1 133.9(4) . . ?
 Mo3 O7 Mo1 76.0(3) . . ?
 Mo3 O7 Mo4 90.0(4) . . ?
 Mo3 O7 Mo6 42.5(4) . . ?
 Mo4 O7 Eu1 136.0(5) . . ?
 Mo5 O7 Eu1 137.7(5) . . ?
 Mo5 O7 Mo1 35.5(4) . . ?
 Mo5 O7 Mo3 46.1(4) . . ?
 Mo5 O7 Mo4 70.6(6) . . ?
 Mo5 O7 Mo6 75.8(5) . . ?
 Mo6 O7 Eu1 137.0(5) . . ?
 Mo6 O7 Mo4 70.7(5) . . ?
 Mo1 O8 Mo4 42.3(4) . . ?
 Mo7 O8 Mo1 150.0(6) . . ?
 Mo7 O8 Mo4 141.0(8) . . ?
 Mo5 O9 Mo1 34.8(4) . . ?
 P1 O9 Mo1 123.4(6) . . ?
 P1 O9 Mo5 124.7(6) . . ?
 Mo3 O10 Mo5 42.7(3) . . ?
 Mo9 O10 Mo3 146.8(6) . . ?
 Mo9 O10 Mo5 138.3(6) . . ?
 Mo3 O11 Mo6 40.1(4) . . ?
 P2 O11 Mo3 125.3(6) . . ?
 P2 O11 Mo6 122.1(7) . . ?
 Mo2 O12 Mo6 38.2(4) . . ?
 Mo8 O12 Mo2 148.1(7) . . ?
 Mo8 O12 Mo6 145.7(7) . . ?
 Mo2 O13 Mo4 39.4(4) . . ?
 P3 O13 Mo2 121.6(7) . . ?
 P3 O13 Mo4 121.9(7) . . ?
 Mo7 O14 Eu1 120.4(6) . . ?
 P3 O14 Eu1 103.4(6) . . ?
 P3 O14 Mo7 129.3(6) . . ?
 P1 O15 Mo7 136.6(7) . . ?
 Mo9 O16 Eu1 114.3(5) . . ?
 P1 O16 Eu1 108.8(6) . . ?
 P1 O16 Mo9 128.1(6) . . ?
 Mo9 O17 Eu1 110.5(5) . . ?
 P2 O17 Eu1 97.6(6) . . ?
 P2 O17 Mo9 132.7(6) . . ?
 Mo8 O18 Eu1 116.0(6) . . ?
 P2 O18 Eu1 100.1(6) . . ?
 P2 O18 Mo8 133.5(7) . . ?
 Mo8 O19 Eu1 112.1(7) . . ?
 P3 O19 Eu1 96.0(6) . . ?
 P3 O19 Mo8 133.6(7) . . ?
 P3 O26 H3 16.7 . . ?
 P1 O27 H1 52.9 . . ?
 P2 O28 H2 34.8 . . ?
 P4 O29 Mo7 138.9(7) . . ?
 P5 O30 Mo9 140.4(8) . . ?
 P6 O30 Mo9 138.0(9) . . ?
 P7 O31 Mo8 142.1(9) . . ?
 P8 O31 Mo8 135.8(11) . . ?
 Eu1 O32 Eu1 96.7(5) . 6_556 ?
 P4 O32 Eu1 129.5(3) . 6_556 ?
 P4 O32 Eu1 129.5(3) . . ?
 Eu1 O33 Eu1 98.3(5) . 6_556 ?
 P5 O33 Eu1 128.6(4) . . ?
 P6 O33 Eu1 128.8(4) . 6_556 ?
 P6 O33 Eu1 128.8(4) . . ?
 Eu1 O34 Eu1 97.5(5) . 6_556 ?
 P7 O34 Eu1 130.1(6) . . ?
 P8 O34 Eu1 128.3(5) . 6_556 ?
 P8 O34 Eu1 128.3(5) . . ?
 C1 N1 Mo1 121.9(9) . . ?
 C1 N1 C5 118.2(14) . . ?
 C5 N1 Mo1 119.9(10) . . ?
 C6 N2 Mo2 121.9(10) . . ?
 C6 N2 C10 117.1(14) . . ?
 C10 N2 Mo2 121.0(12) . . ?
 C11 N3 Mo3 119.6(10) . . ?
 C11 N3 C15 118.5(15) . . ?
 C15 N3 Mo3 121.5(12) . . ?
 C16 N4 Mo4 125(5) . . ?
 C16 N4 C20 120(3) . . ?
 C20 N4 Mo4 114(5) . . ?
 C21 N5 Mo5 125(4) . . ?
 C25 N5 Mo5 118(4) . . ?
 C25 N5 C21 117(3) . . ?
 Mo6 N6 H22 165(7) . 8_657 ?
 C26 N6 Mo6 125(5) . . ?
 C26 N6 H22 58(4) . 8_657 ?
 C30 N6 Mo6 116(5) . . ?
 C30 N6 H22 63(4) . 8_657 ?
 C30 N6 C26 119(3) . . ?
 N1 C1 H1A 118.9 . . ?
 N1 C1 C2 122.3(13) . . ?
 C2 C1 H1A 118.9 . . ?
 C1 C2 H2A 120.3 . . ?
 C3 C2 C1 119.3(13) . . ?
 C3 C2 H2A 120.3 . . ?
 C2 C3 H3A 120.6 . . ?
 C4 C3 C2 118.9(12) . . ?
 C4 C3 H3A 120.6 . . ?
 C3 C4 H4A 120.3 . . ?
 C3 C4 C5 119.4(12) . . ?
 C5 C4 H4A 120.3 . . ?
 N1 C5 C4 121.9(13) . . ?
 N1 C5 H5A 119.0 . . ?
 C4 C5 H5A 119.0 . . ?
 N2 C6 H6A 118.8 . . ?
 N2 C6 C7 122.4(14) . . ?
 C7 C6 H6A 118.8 . . ?
 C6 C7 H7A 120.1 . . ?
 C8 C7 C6 119.7(14) . . ?
 C8 C7 H7A 120.1 . . ?
 C7 C8 H8A 120.5 . . ?
 C7 C8 C9 119.0(13) . . ?
 C9 C8 H8A 120.5 . . ?
 C8 C9 H9 120.6 . . ?
 C8 C9 C10 118.9(13) . . ?
 C10 C9 H9 120.6 . . ?
 N2 C10 C9 122.9(15) . . ?
 N2 C10 H10 118.6 . . ?
 C9 C10 H10 118.6 . . ?
 N3 C11 H11 118.8 . . ?
 N3 C11 C12 122.4(14) . . ?
 C12 C11 H11 118.8 . . ?
 C11 C12 H12 121.0 . . ?
 C13 C12 C11 118.1(14) . . ?
 C13 C12 H12 121.0 . . ?
 C12 C13 H13 120.0 . . ?
 C14 C13 C12 120.0(14) . . ?
 C14 C13 H13 120.0 . . ?
 C13 C14 H14 120.3 . . ?
 C13 C14 C15 119.4(14) . . ?
 C15 C14 H14 120.3 . . ?
 N3 C15 C14 121.7(15) . . ?
 N3 C15 H15 119.1 . . ?
 C14 C15 H15 119.1 . . ?
 N4 C16 H16 119.7 . . ?
 N4 C16 C17 121(2) . . ?
 C17 C16 H16 119.7 . . ?
 C16 C17 H17 120.4 . . ?
 C18 C17 C16 119.2(18) . . ?
 C18 C17 H17 120.4 . . ?
 C17 C18 H18 119.9 . . ?
 C19 C18 C17 120.3(18) . . ?
 C19 C18 H18 119.9 . . ?
 C18 C19 H19 120.5 . . ?
 C18 C19 C20 119.0(18) . . ?
 C20 C19 H19 120.5 . . ?
 N4 C20 C19 121(2) . . ?
 N4 C20 H20 119.7 . . ?
 C19 C20 H20 119.7 . . ?
 N5 C21 H21 118.9 . . ?
 N5 C21 C22 122(2) . . ?
 C22 C21 H21 118.9 . . ?
 C21 C22 H22 120.5 . . ?
 C23 C22 C21 119.0(18) . . ?
 C23 C22 H22 120.5 . . ?
 C22 C23 H23 119.9 . . ?
 C22 C23 C24 120.2(17) . . ?
 C24 C23 H23 119.9 . . ?
 C23 C24 H24 120.8 . . ?
 C23 C24 C25 118.4(17) . . ?
 C25 C24 H24 120.8 . . ?
 N5 C25 C24 123(2) . . ?
 N5 C25 H25 118.6 . . ?
 C24 C25 H25 118.6 . . ?
 N6 C26 H22 65(4) . 8_657 ?
 N6 C26 H26 119.4 . . ?
 N6 C26 C27 121(2) . . ?
 H26 C26 H22 165.5 . 8_657 ?
 C27 C26 H22 58(4) . 8_657 ?
 C27 C26 H26 119.4 . . ?
 C26 C27 H22 61(4) . 8_657 ?
 C26 C27 H27 120.5 . . ?
 H27 C27 H22 165.6 . 8_657 ?
 C28 C27 H22 60(4) . 8_657 ?
 C28 C27 C26 119.0(18) . . ?
 C28 C27 H27 120.5 . . ?
 C27 C28 H22 59(4) . 8_657 ?
 C27 C28 H28 119.9 . . ?
 H28 C28 H22 165.7 . 8_657 ?
 C29 C28 H22 63(4) . 8_657 ?
 C29 C28 C27 120.2(18) . . ?
 C29 C28 H28 119.9 . . ?
 C28 C29 H22 58(4) . 8_657 ?
 C28 C29 H29 120.5 . . ?
 C28 C29 C30 119.1(18) . . ?
 H29 C29 H22 165.6 . 8_657 ?
 C30 C29 H22 63(4) . 8_657 ?
 C30 C29 H29 120.5 . . ?
 N6 C30 H22 63(4) . 8_657 ?
 N6 C30 C29 121(2) . . ?
 N6 C30 H30 119.4 . . ?
 C29 C30 H22 60(4) . 8_657 ?
 C29 C30 H30 119.4 . . ?
 H30 C30 H22 167.6 . 8_657 ?
 H35A O35 H35B 113.9 . . ?
 H35A O35 H35C 97.5 . . ?
 H35B O35 H35C 93.7 . . ?
 H36A O36 H36B 68.2 . 2_665 ?
 H36A O36 H36B 69.0 . . ?
 H36A O36 H36C 139.6 . . ?
 H36B O36 H36B 0.9 . 2_665 ?
 H36B O36 H36C 104.5 . . ?
 H36C O36 H36B 105.3 . 2_665 ?
 H37A O37 H37B 132.1 . . ?
 H38A O38 H19 106.7 . 8_657 ?
 H38A O38 H38B 107.9 . . ?
 H38B O38 H19 132.9 . 8_657 ?
 H39A O39 H39B 104.6 . . ?
 H40A O40 H40B 109.5 . . ?
 H41A O41 H41B 96.8 . . ?
 H41A O41 H42A 154.0 . . ?
 H41B O41 H42A 108.4 . . ?
 H42A O42 H42B 104.6 . . ?
 H43A O43 H43B 104.5 . . ?
 H44A O44 H44B 104.5 . . ?
 H44A O44 H44B 158.7 . 2_565 ?
 H44B O44 H44B 67.5 . 2_565 ?
 O45 O45 H45A 0(10) 6_556 6_556 ?
 O45 O45 H45A 0.0 6_556 . ?
 O45 O45 H45B 0.0 6_556 . ?
 O45 O45 H45B 0(10) 6_556 6_556 ?
 H45A O45 H45A 75.5 . 6_556 ?
 H45A O45 H45B 180.0 . 6_556 ?
 H45A O45 H45B 104.5 . . ?
 H45B O45 H45A 180.0 . 6_556 ?
 H45B O45 H45A 104.5 6_556 6_556 ?
 H45B O45 H45B 75.4 . 6_556 ?
 H45A O46 H45A 58.6 . 6_556 ?
 H45A O46 H46A 108.6 . 6_556 ?
 H45A O46 H46A 55.1 6_556 6_556 ?
 H45A O46 H46A 55.1 . . ?
 H45A O46 H46B 94.0 6_556 6_556 ?
 H45A O46 H46B 94.0 . . ?
 H45A O46 H46B 56.9 . 6_556 ?
 H46A O46 H45A 108.6 . 6_556 ?
 H46A O46 H46A 131.0 . 6_556 ?
 H46A O46 H46B 26.5 . 6_556 ?
 H46A O46 H46B 104.5 6_556 6_556 ?
 H46A O46 H46B 104.5 . . ?
 H46B O46 H45A 56.9 . 6_556 ?
 H46B O46 H46A 26.5 . 6_556 ?
 H46B O46 H46B 78.1 . 6_556 ?
 H47A O47 H47A 43.6 . 6_556 ?
 H47A O47 H47B 113.4 . . ?
 H47B O47 H47A 154.2 . 6_556 ?
 H48A O48 H48B 104.6 . . ?
 O51 O48 H48A 98.5 5_676 . ?
 O51 O48 H48B 115.1 5_676 . ?
 H50A O50 H50B 104.5 . . ?
 O51 O50 H50A 57.2 1_545 . ?
 O51 O50 H50A 82.3 2_565 . ?
 O51 O50 H50B 47.5 1_545 . ?
 O51 O50 H50B 35.3 2_565 . ?
 O51 O50 O51 33(5) 1_545 2_565 ?
 O54 O50 H50A 137.5 2_565 . ?
 O54 O50 H50B 50.9 2_565 . ?
 O54 O50 O51 58(7) 2_565 2_565 ?
 O54 O50 O51 89(9) 2_565 1_545 ?
 O48 O51 H50B 161(9) 5_676 2_565 ?
 O48 O51 H51A 136(10) 5_676 2_575 ?
 O48 O51 H51A 141.2 5_676 . ?
 O48 O51 H51B 105.7 5_676 . ?
 O48 O51 H51B 80(9) 5_676 2_575 ?
 O48 O51 O54 114(7) 5_676 2_575 ?
 O50 O51 O48 79(7) 1_565 5_676 ?
 O50 O51 H50B 86(10) 1_565 2_565 ?
 O50 O51 H51A 58(8) 1_565 2_575 ?
 O50 O51 H51A 76.1 1_565 . ?
 O50 O51 H51B 154.4 1_565 . ?
 O50 O51 H51B 86(10) 1_565 2_575 ?
 O50 O51 O54 39(5) 1_565 2_575 ?
 H51A O51 H50B 35.6 2_575 2_565 ?
 H51A O51 H50B 20.3 . 2_565 ?
 H51A O51 H51A 42.4 . 2_575 ?
 H51A O51 H51B 109.5 . . ?
 H51A O51 H51B 126.6 . 2_575 ?
 H51A O51 H51B 85.5 2_575 2_575 ?
 H51B O51 H50B 110.8 2_575 2_565 ?
 H51B O51 H50B 93.0 . 2_565 ?
 H51B O51 H51A 108.7 . 2_575 ?
 H51B O51 H51B 71.0 . 2_575 ?
 O54 O51 H50B 57(6) 2_575 2_565 ?
 O54 O51 H51A 59.2 2_575 . ?
 O54 O51 H51A 22(7) 2_575 2_575 ?
 O54 O51 H51B 121.8 2_575 . ?
 O54 O51 H51B 75(8) 2_575 2_575 ?
 H52A O52 H52A 70.2 . 6_556 ?
 H52A O52 H52B 34.2 . 6_556 ?
 H52A O52 H52B 104.5 . . ?
 H52B O52 H52A 104.5 6_556 6_556 ?
 H52B O52 H52A 34.2 . 6_556 ?
 H52B O52 H52B 138.7 . 6_556 ?
 H53A O53 H53B 109.4 . . ?
 O50 O54 H50B 52(6) 2_565 2_565 ?
 O50 O54 H51A 79.9 2_565 . ?
 O50 O54 H54A 78.4 2_565 . ?
 O50 O54 H54B 166.9 2_565 . ?
 H51A O54 H50B 30.6 . 2_565 ?
 H51A O54 H54A 56.7 . . ?
 H51A O54 H54B 95.5 . . ?
 H54A O54 H50B 47.9 . 2_565 ?
 H54A O54 H54B 109.5 . . ?
 H54B O54 H50B 125.7 . 2_565 ?
 C31 N7 H7B 116.7 . . ?
 C31 N7 C35 127(3) . . ?
 C35 N7 H7B 116.7 . . ?
 N7 C31 H31 121.1 . . ?
 N7 C31 C32 118(2) . . ?
 C32 C31 H31 121.1 . . ?
 C31 C32 H32 121.1 . . ?
 C33 C32 C31 117.8(17) . . ?
 C33 C32 H32 121.1 . . ?
 C32 C33 H33 119.0 . . ?
 C34 C33 C32 122.1(17) . . ?
 C34 C33 H33 119.0 . . ?
 C33 C34 H34 120.2 . . ?
 C33 C34 C35 119.5(17) . . ?
 C35 C34 H34 120.2 . . ?
 N7 C35 C34 116(2) . . ?
 N7 C35 H35 121.9 . . ?
 C34 C35 H35 121.9 . . ?
 C36 N8 H8B 120.1 . . ?
 C36 N8 C40 120(3) . . ?
 C40 N8 H8B 120.1 . . ?
 N8 C36 H36 119.5 . . ?
 N8 C36 C37 121(2) . . ?
 C37 C36 H36 119.5 . . ?
 C36 C37 H37 120.5 . . ?
 C38 C37 C36 119.0(17) . . ?
 C38 C37 H37 120.5 . . ?
 C37 C38 H38 119.8 . . ?
 C39 C38 C37 120.4(17) . . ?
 C39 C38 H38 119.8 . . ?
 C38 C39 H39 120.5 . . ?
 C38 C39 C40 118.9(18) . . ?
 C40 C39 H39 120.5 . . ?
 N8 C40 C39 121(2) . . ?
 N8 C40 H40 119.6 . . ?
 C39 C40 H40 119.6 . . ?
 C41 N9 H9A 119.2 . . ?
 C45 N9 H9A 119.2 . . ?
 C45 N9 C41 122(3) . . ?
 N9 C41 H41 120.0 . . ?
 N9 C41 C42 120(2) . . ?
 C42 C41 H41 120.0 . . ?
 C41 C42 H42 120.7 . . ?
 C43 C42 C41 118.6(17) . . ?
 C43 C42 H42 120.7 . . ?
 C42 C43 H43 119.6 . . ?
 C44 C43 C42 120.9(17) . . ?
 C44 C43 H43 119.6 . . ?
 C43 C44 H44 120.3 . . ?
 C43 C44 C45 119.3(17) . . ?
 C45 C44 H44 120.3 . . ?
 N9 C45 C44 120(2) . . ?
 N9 C45 H45 120.2 . . ?
 C44 C45 H45 120.2 . . ?
 C51 N10 H10A 120.1 . . ?
 C51 N10 C55 120(3) . . ?
 C55 N10 H10A 120.1 . . ?
 N10 C51 H51 119.4 . . ?
 N10 C51 C52 121(2) . . ?
 C52 C51 H51 119.4 . . ?
 C51 C52 H52 120.5 . . ?
 C53 C52 C51 118.9(18) . . ?
 C53 C52 H52 120.5 . . ?
 C52 C53 H53 120.0 . . ?
 C52 C53 C54 120.1(18) . . ?
 C54 C53 H53 120.0 . . ?
 C53 C54 H54 120.3 . . ?
 C53 C54 C55 119.3(18) . . ?
 C55 C54 H54 120.3 . . ?
 N10 C55 C54 121(2) . . ?
 N10 C55 H55 119.6 . . ?
 C54 C55 H55 119.6 . . ?
 C46 N11 H11A 119.6 . . ?
 C50 N11 H11A 119.6 . . ?
 C50 N11 C46 121(3) . . ?
 N11 C46 H46 120.1 . . ?
 N11 C46 C47 120(2) . . ?
 C47 C46 H46 120.1 . . ?
 C46 C47 H47 120.4 . . ?
 C48 C47 C46 119.2(17) . . ?
 C48 C47 H47 120.4 . . ?
 C47 C48 H48 119.5 . . ?
 C49 C48 C47 121.0(18) . . ?
 C49 C48 H48 119.5 . . ?
 C48 C49 H49 120.7 . . ?
 C48 C49 C50 118.6(17) . . ?
 C50 C49 H49 120.7 . . ?
 N11 C50 C49 120(2) . . ?
 N11 C50 H50 119.8 . . ?
 C49 C50 H50 119.8 . . ?
 C56 N12 H12A 119.4 . . ?
 C56 N12 C60 121(3) . . ?
 C60 N12 H12A 119.4 . . ?
 N12 C56 H56 119.8 . . ?
 N12 C56 C57 120(2) . . ?
 C57 C56 H56 119.8 . . ?
 C56 C57 H57 120.7 . . ?
 C58 C57 C56 118.7(18) . . ?
 C58 C57 H57 120.7 . . ?
 C57 C58 H58 119.7 . . ?
 C59 C58 C57 120.6(18) . . ?
 C59 C58 H58 119.7 . . ?
 C58 C59 H59 120.4 . . ?
 C58 C59 C60 119.3(18) . . ?
 C60 C59 H59 120.4 . . ?
 N12 C60 C59 120(2) . . ?
 N12 C60 H60 120.1 . . ?
 C59 C60 H60 120.1 . . ?

loop_
  _geom_torsion_atom_site_label_1
  _geom_torsion_atom_site_label_2
  _geom_torsion_atom_site_label_3
  _geom_torsion_atom_site_label_4
  _geom_torsion
  _geom_torsion_site_symmetry_1
  _geom_torsion_site_symmetry_2
  _geom_torsion_site_symmetry_3
  _geom_torsion_site_symmetry_4
  _geom_torsion_publ_flag
 Mo1 Mo5 O5 Mo6 66.3(13) . . . . ?
 Mo1 N1 C1 C2 -179.1(13) . . . . ?
 Mo1 N1 C5 C4 179.2(17) . . . . ?
 Mo2 Mo1 Mo5 Mo4 -4.7(4) . . . . ?
 Mo2 Mo1 Mo5 Mo6 -0.6(3) . . . . ?
 Mo2 Mo1 Mo5 O4 -96(2) . . . . ?
 Mo2 Mo1 Mo5 O5 -44.9(9) . . . . ?
 Mo2 Mo1 Mo5 O7 49.3(3) . . . . ?
 Mo2 Mo1 Mo5 O9 145.2(3) . . . . ?
 Mo2 Mo1 Mo5 O10 91.5(15) . . . . ?
 Mo2 Mo1 Mo5 N5 -142(2) . . . . ?
 Mo2 N2 C6 C7 -177.3(13) . . . . ?
 Mo2 N2 C10 C9 177.3(19) . . . . ?
 Mo3 Mo1 Mo5 Mo4 -9.1(9) . . . . ?
 Mo3 Mo1 Mo5 Mo6 -5.0(4) . . . . ?
 Mo3 Mo1 Mo5 O4 -100(2) . . . . ?
 Mo3 Mo1 Mo5 O5 -49.3(9) . . . . ?
 Mo3 Mo1 Mo5 O7 44.9(6) . . . . ?
 Mo3 Mo1 Mo5 O9 140.8(7) . . . . ?
 Mo3 Mo1 Mo5 O10 87.1(16) . . . . ?
 Mo3 Mo1 Mo5 N5 -146(2) . . . . ?
 Mo3 N3 C11 C12 -172.5(13) . . . . ?
 Mo3 N3 C15 C14 174.1(17) . . . . ?
 Mo4 Mo5 O5 Mo6 46.4(11) . . . . ?
 Mo4 N4 C16 C17 174(8) . . . . ?
 Mo4 N4 C20 C19 -173(8) . . . . ?
 Mo5 Mo6 O6 Mo4 53.0(8) . . . . ?
 Mo5 N5 C21 C22 173(6) . . . . ?
 Mo5 N5 C25 C24 -173(6) . . . . ?
 Mo6 N6 C26 C27 178(7) . . . . ?
 Mo6 N6 C30 C29 -178(7) . . . . ?
 O1 Mo1 Mo5 Mo4 38.7(6) . . . . ?
 O1 Mo1 Mo5 Mo6 42.8(6) . . . . ?
 O1 Mo1 Mo5 O4 -52(2) . . . . ?
 O1 Mo1 Mo5 O5 -1.5(11) . . . . ?
 O1 Mo1 Mo5 O7 92.7(5) . . . . ?
 O1 Mo1 Mo5 O9 -171.3(5) . . . . ?
 O1 Mo1 Mo5 O10 134.9(14) . . . . ?
 O1 Mo1 Mo5 N5 -99(2) . . . . ?
 O2 Mo1 Mo5 Mo4 90.6(11) . . . . ?
 O2 Mo1 Mo5 Mo6 94.7(11) . . . . ?
 O2 Mo1 Mo5 O4 -1(2) . . . . ?
 O2 Mo1 Mo5 O5 50.4(11) . . . . ?
 O2 Mo1 Mo5 O7 144.6(12) . . . . ?
 O2 Mo1 Mo5 O9 -119.5(11) . . . . ?
 O2 Mo1 Mo5 O10 -173(2) . . . . ?
 O2 Mo1 Mo5 N5 -47(2) . . . . ?
 O4 Mo5 O5 Mo6 97.1(13) . . . . ?
 O5 Mo6 O6 Mo4 100.1(11) . . . . ?
 O7 Mo1 Mo5 Mo4 -54.0(6) . . . . ?
 O7 Mo1 Mo5 Mo6 -49.9(4) . . . . ?
 O7 Mo1 Mo5 O4 -145(2) . . . . ?
 O7 Mo1 Mo5 O5 -94.2(9) . . . . ?
 O7 Mo1 Mo5 O9 95.9(4) . . . . ?
 O7 Mo1 Mo5 O10 42.2(14) . . . . ?
 O7 Mo1 Mo5 N5 169(2) . . . . ?
 O7 Mo5 O5 Mo6 -9.7(14) . . . . ?
 O7 Mo6 O6 Mo4 5.7(12) . . . . ?
 O8 Mo1 Mo5 Mo4 -114.7(13) . . . . ?
 O8 Mo1 Mo5 Mo6 -110.6(11) . . . . ?
 O8 Mo1 Mo5 O4 154(2) . . . . ?
 O8 Mo1 Mo5 O5 -154.9(11) . . . . ?
 O8 Mo1 Mo5 O7 -60.7(12) . . . . ?
 O8 Mo1 Mo5 O9 35.2(12) . . . . ?
 O8 Mo1 Mo5 O10 -19(2) . . . . ?
 O8 Mo1 Mo5 N5 108(2) . . . . ?
 O9 Mo1 Mo5 Mo4 -149.9(5) . . . . ?
 O9 Mo1 Mo5 Mo6 -145.8(4) . . . . ?
 O9 Mo1 Mo5 O4 119(2) . . . . ?
 O9 Mo1 Mo5 O5 169.9(10) . . . . ?
 O9 Mo1 Mo5 O7 -95.9(4) . . . . ?
 O9 Mo1 Mo5 O10 -53.7(14) . . . . ?
 O9 Mo1 Mo5 N5 73(2) . . . . ?
 O9 Mo5 O5 Mo6 -158(4) . . . . ?
 O9 P1 O15 Mo7 10.3(18) . . . . ?
 O9 P1 O16 Eu1 99.7(6) . . . . ?
 O9 P1 O16 Mo9 -45.5(11) . . . . ?
 O10 Mo5 O5 Mo6 -93.1(11) . . . . ?
 O11 Mo6 O6 Mo4 146(4) . . . . ?
 O11 P2 O17 Eu1 -104.0(7) . . . . ?
 O11 P2 O17 Mo9 23.1(13) . . . . ?
 O11 P2 O18 Eu1 103.0(6) . . . . ?
 O11 P2 O18 Mo8 -38.5(13) . . . . ?
 O12 Mo6 O6 Mo4 -87.1(9) . . . . ?
 O13 P3 O14 Eu1 104.8(7) . . . . ?
 O13 P3 O14 Mo7 -45.2(12) . . . . ?
 O13 P3 O19 Eu1 -107.9(6) . . . . ?
 O13 P3 O19 Mo8 20.6(15) . . . . ?
 O14 Mo7 O8 Mo1 59.1(15) . . . . ?
 O14 Mo7 O8 Mo4 -18.7(11) . . . . ?
 O14 P3 O13 Mo2 -72.3(10) . . . . ?
 O14 P3 O13 Mo4 -25.5(12) . . . . ?
 O14 P3 O19 Eu1 15.7(7) . . . . ?
 O14 P3 O19 Mo8 144.2(11) . . . . ?
 O15 Mo7 O8 Mo1 -16.1(15) . . . . ?
 O15 Mo7 O8 Mo4 -93.9(12) . . . . ?
 O15 P1 O9 Mo1 45.6(11) . . . . ?
 O15 P1 O9 Mo5 87.9(11) . . . . ?
 O15 P1 O16 Eu1 -23.9(7) . . . . ?
 O15 P1 O16 Mo9 -169.0(8) . . . . ?
 O16 Mo9 O10 Mo3 62.4(12) . . . . ?
 O16 Mo9 O10 Mo5 -10.1(9) . . . . ?
 O16 P1 O9 Mo1 -72.1(9) . . . . ?
 O16 P1 O9 Mo5 -29.8(11) . . . . ?
 O16 P1 O15 Mo7 134.5(14) . . . . ?
 O17 Mo9 O10 Mo3 -10.4(12) . . . . ?
 O17 Mo9 O10 Mo5 -82.8(10) . . . . ?
 O17 P2 O11 Mo3 40.3(12) . . . . ?
 O17 P2 O11 Mo6 88.8(10) . . . . ?
 O17 P2 O18 Eu1 -19.3(6) . . . . ?
 O17 P2 O18 Mo8 -160.8(10) . . . . ?
 O18 Mo8 O12 Mo2 67.2(15) . . . . ?
 O18 Mo8 O12 Mo6 -6.4(13) . . . . ?
 O18 P2 O11 Mo3 -76.2(11) . . . . ?
 O18 P2 O11 Mo6 -27.6(11) . . . . ?
 O18 P2 O17 Eu1 18.7(6) . . . . ?
 O18 P2 O17 Mo9 145.9(9) . . . . ?
 O19 Mo8 O12 Mo2 -5.1(14) . . . . ?
 O19 Mo8 O12 Mo6 -78.6(13) . . . . ?
 O19 P3 O13 Mo2 44.2(11) . . . . ?
 O19 P3 O13 Mo4 90.9(11) . . . . ?
 O19 P3 O14 Eu1 -17.3(7) . . . . ?
 O19 P3 O14 Mo7 -167.4(8) . . . . ?
 O20 Mo7 O8 Mo1 145.4(15) . . . . ?
 O20 Mo7 O8 Mo4 67.6(12) . . . . ?
 O21 Mo7 O8 Mo1 -106.1(15) . . . . ?
 O21 Mo7 O8 Mo4 176.1(11) . . . . ?
 O22 Mo9 O10 Mo3 151.7(12) . . . . ?
 O22 Mo9 O10 Mo5 79.3(10) . . . . ?
 O23 Mo9 O10 Mo3 -101.6(13) . . . . ?
 O23 Mo9 O10 Mo5 -174.0(10) . . . . ?
 O24 Mo8 O12 Mo2 155.2(15) . . . . ?
 O24 Mo8 O12 Mo6 81.7(14) . . . . ?
 O25 Mo8 O12 Mo2 -96.6(15) . . . . ?
 O25 Mo8 O12 Mo6 -170.2(13) . . . . ?
 O26 P3 O13 Mo2 167(2) . . . . ?
 O26 P3 O13 Mo4 -147(3) . . . . ?
 O26 P3 O14 Eu1 -135(2) . . . . ?
 O26 P3 O14 Mo7 74(2) . . . . ?
 O26 P3 O19 Eu1 132(2) . . . . ?
 O26 P3 O19 Mo8 -99(2) . . . . ?
 O27 P1 O9 Mo1 161.6(19) . . . . ?
 O27 P1 O9 Mo5 -156(2) . . . . ?
 O27 P1 O15 Mo7 -107.0(19) . . . . ?
 O27 P1 O16 Eu1 -136.8(15) . . . . ?
 O27 P1 O16 Mo9 78.0(17) . . . . ?
 O28 P2 O11 Mo3 157.5(16) . . . . ?
 O28 P2 O11 Mo6 -154.0(15) . . . . ?
 O28 P2 O17 Eu1 137.3(12) . . . . ?
 O28 P2 O17 Mo9 -95.5(15) . . . . ?
 O28 P2 O18 Eu1 -133.0(12) . . . . ?
 O28 P2 O18 Mo8 85.5(15) . . . . ?
 O29 Mo7 O8 Mo1 19(3) . . . . ?
 O29 Mo7 O8 Mo4 -58(2) . . . . ?
 O29 P4 O29 Mo7 -177.8(5) 6_556 . . . ?
 O29 P4 O32 Eu1 -165.3(8) . . . 6_556 ?
 O29 P4 O32 Eu1 -43.5(13) 6_556 . . 6_556 ?
 O29 P4 O32 Eu1 43.5(13) . . . . ?
 O29 P4 O32 Eu1 165.3(8) 6_556 . . . ?
 O30 Mo9 O10 Mo3 25(2) . . . . ?
 O30 Mo9 O10 Mo5 -47.7(18) . . . . ?
 O30 P5 O30 Mo9 -173.0(5) 6_556 . . . ?
 O30 P5 O33 Eu1 -166.4(10) . . . 6_556 ?
 O30 P5 O33 Eu1 166.4(10) 6_556 . . . ?
 O30 P5 O33 Eu1 43(3) . . . . ?
 O30 P5 O33 Eu1 -43(3) 6_556 . . 6_556 ?
 O30 P6 O30 Mo9 -179.8(5) 6_556 . . . ?
 O30 P6 O33 Eu1 42(3) 6_556 . . 6_556 ?
 O30 P6 O33 Eu1 -165.7(11) 6_556 . . . ?
 O30 P6 O33 Eu1 -42(3) . . . . ?
 O30 P6 O33 Eu1 165.7(11) . . . 6_556 ?
 O31 Mo8 O12 Mo2 34(3) . . . . ?
 O31 Mo8 O12 Mo6 -40(2) . . . . ?
 O31 P7 O31 Mo8 -172.3(6) 6_556 . . . ?
 O31 P7 O34 Eu1 -32(7) 6_556 . . 6_556 ?
 O31 P7 O34 Eu1 170(2) 6_556 . . . ?
 O31 P7 O34 Eu1 -170(2) . . . 6_556 ?
 O31 P7 O34 Eu1 32(7) . . . . ?
 O31 P8 O31 Mo8 -178.5(5) 6_556 . . . ?
 O31 P8 O34 Eu1 51(3) 6_556 . . 6_556 ?
 O31 P8 O34 Eu1 162.7(11) . . . 6_556 ?
 O31 P8 O34 Eu1 -51(3) . . . . ?
 O31 P8 O34 Eu1 -162.7(11) 6_556 . . . ?
 O32 P4 O29 Mo7 -49.9(15) . . . . ?
 O33 P5 O30 Mo9 -45(3) . . . . ?
 O33 P6 O30 Mo9 52(3) . . . . ?
 O34 P7 O31 Mo8 -30(8) . . . . ?
 O34 P8 O31 Mo8 64(3) . . . . ?
 N1 Mo1 Mo5 Mo4 130.8(6) . . . . ?
 N1 Mo1 Mo5 Mo6 134.9(4) . . . . ?
 N1 Mo1 Mo5 O4 40(2) . . . . ?
 N1 Mo1 Mo5 O5 90.5(10) . . . . ?
 N1 Mo1 Mo5 O7 -175.3(4) . . . . ?
 N1 Mo1 Mo5 O9 -79.3(5) . . . . ?
 N1 Mo1 Mo5 O10 -133.0(14) . . . . ?
 N1 C1 C2 C3 -1(2) . . . . ?
 N2 C6 C7 C8 1(2) . . . . ?
 N3 C11 C12 C13 -1(2) . . . . ?
 N4 C16 C17 C18 -1(3) . . . . ?
 N5 Mo5 O5 Mo6 179(2) . . . . ?
 N5 C21 C22 C23 1(3) . . . . ?
 N6 Mo6 O6 Mo4 -175(3) . . . . ?
 N6 C26 C27 C28 0(3) . . . . ?
 C1 N1 C5 C4 -1(3) . . . . ?
 C1 C2 C3 C4 2(3) . . . . ?
 C2 C3 C4 C5 -2(4) . . . . ?
 C3 C4 C5 N1 1(4) . . . . ?
 C5 N1 C1 C2 0.7(18) . . . . ?
 C6 N2 C10 C9 0(3) . . . . ?
 C6 C7 C8 C9 -3(3) . . . . ?
 C7 C8 C9 C10 3(4) . . . . ?
 C8 C9 C10 N2 -1(4) . . . . ?
 C10 N2 C6 C7 0.3(19) . . . . ?
 C11 N3 C15 C14 1(3) . . . . ?
 C11 C12 C13 C14 0(3) . . . . ?
 C12 C13 C14 C15 1(4) . . . . ?
 C13 C14 C15 N3 -2(4) . . . . ?
 C15 N3 C11 C12 0.3(18) . . . . ?
 C16 N4 C20 C19 3(7) . . . . ?
 C16 C17 C18 C19 1(7) . . . . ?
 C17 C18 C19 C20 1(9) . . . . ?
 C18 C19 C20 N4 -2(9) . . . . ?
 C20 N4 C16 C17 -1(3) . . . . ?
 C21 N5 C25 C24 0(7) . . . . ?
 C21 C22 C23 C24 -2(7) . . . . ?
 C22 C23 C24 C25 2(9) . . . . ?
 C23 C24 C25 N5 -2(9) . . . . ?
 C25 N5 C21 C22 0(3) . . . . ?
 C26 N6 C30 C29 2(7) . . . . ?
 C26 C27 C28 C29 0(7) . . . . ?
 C27 C28 C29 C30 1(9) . . . . ?
 C28 C29 C30 N6 -2(9) . . . . ?
 C30 N6 C26 C27 -1(3) . . . . ?
 N7 C31 C32 C33 0(2) . . . . ?
 C31 N7 C35 C34 3(5) . . . . ?
 C31 C32 C33 C34 0(5) . . . . ?
 C32 C33 C34 C35 2(6) . . . . ?
 C33 C34 C35 N7 -3(6) . . . . ?
 C35 N7 C31 C32 -1(3) . . . . ?
 N8 C36 C37 C38 1(3) . . . . ?
 C36 N8 C40 C39 -1(7) . . . . ?
 C36 C37 C38 C39 -2(6) . . . . ?
 C37 C38 C39 C40 2(9) . . . . ?
 C38 C39 C40 N8 0(9) . . . . ?
 C40 N8 C36 C37 1(3) . . . . ?
 N9 C41 C42 C43 -0.1(6) . . . . ?
 C41 N9 C45 C44 -0.3(14) . . . . ?
 C41 C42 C43 C44 0.3(14) . . . . ?
 C42 C43 C44 C45 -0.5(19) . . . . ?
 C43 C44 C45 N9 0.5(19) . . . . ?
 C45 N9 C41 C42 0.1(7) . . . . ?
 N10 C51 C52 C53 0(3) . . . . ?
 C51 N10 C55 C54 0(7) . . . . ?
 C51 C52 C53 C54 0(7) . . . . ?
 C52 C53 C54 C55 0(9) . . . . ?
 C53 C54 C55 N10 0(9) . . . . ?
 C55 N10 C51 C52 0(3) . . . . ?
 N11 C46 C47 C48 0(4) . . . . ?
 C46 N11 C50 C49 -0.1(13) . . . . ?
 C46 C47 C48 C49 -1(4) . . . . ?
 C47 C48 C49 C50 1(3) . . . . ?
 C48 C49 C50 N11 -0.3(13) . . . . ?
 C50 N11 C46 C47 0(3) . . . . ?
 N12 C56 C57 C58 0(3) . . . . ?
 C56 N12 C60 C59 1(7) . . . . ?
 C56 C57 C58 C59 -1(7) . . . . ?
 C57 C58 C59 C60 2(9) . . . . ?
 C58 C59 C60 N12 -2(9) . . . . ?
 C60 N12 C56 C57 0(3) . . . . ?

_olex2_submission_special_instructions  'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max  1.373
_oxdiff_exptl_absorpt_empirical_full_min  0.720
loop_
  _twin_individual_id
  _twin_individual_mass_fraction_refined
 1 0.9611(10)
 2 0.0389(10)

