data_flz-69-2
_audit_creation_date               2021-04-21
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelxl_version_number             2013-4
_audit_contact_author_address      ?
_audit_contact_author_email        ?
_audit_contact_author_name         ''
_audit_contact_author_phone        ?
_publ_contact_author_id_orcid      ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_chemical_name_common              ?
_chemical_name_systematic
;
 ?
;
_chemical_formula_moiety           'C26 H54 Cu5 I7 N4'
_chemical_formula_sum              'C26 H54 Cu5 I7 N4'
_chemical_formula_weight           1628.73
_chemical_absolute_configuration   ad
_chemical_melting_point            ?
_chemical_oxdiff_formula           c20h20n2Cu1I2
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'I' 'I' -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system        'triclinic'
_space_group_IT_number             1
_space_group_name_H-M_alt          'P 1'
_space_group_name_Hall             'P 1'
loop_
  _space_group_symop_operation_xyz
 'x, y, z'

_cell_length_a                     11.5081(2)
_cell_length_b                     11.6450(3)
_cell_length_c                     16.9677(4)
_cell_angle_alpha                  109.679(2)
_cell_angle_beta                   95.9038(16)
_cell_angle_gamma                  98.0117(19)
_cell_volume                       2092.61(9)
_cell_formula_units_Z              2
_cell_measurement_reflns_used      27652
_cell_measurement_temperature      100.00(10)
_cell_measurement_theta_max        30.2900
_cell_measurement_theta_min        3.9540
_shelx_estimated_absorpt_T_max     0.459
_shelx_estimated_absorpt_T_min     0.338
_exptl_absorpt_coefficient_mu      7.686
_exptl_absorpt_correction_T_max    1.00000
_exptl_absorpt_correction_T_min    0.27708
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.40.53 (Rigaku Oxford Diffraction, 2019)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour              ?
_exptl_crystal_density_diffrn      2.585
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      ?
_exptl_crystal_description         block
_exptl_crystal_F_000               1508
_exptl_crystal_size_max            0.18
_exptl_crystal_size_mid            0.17
_exptl_crystal_size_min            0.12
_exptl_special_details
;
 ?
;
_exptl_transmission_factor_max     ?
_exptl_transmission_factor_min     ?
_diffrn_reflns_av_R_equivalents    0.0318
_diffrn_reflns_av_unetI/netI       0.0440
_diffrn_reflns_Laue_measured_fraction_full  0.998
_diffrn_reflns_Laue_measured_fraction_max  0.852
_diffrn_reflns_limit_h_max         15
_diffrn_reflns_limit_h_min         -16
_diffrn_reflns_limit_k_max         16
_diffrn_reflns_limit_k_min         -16
_diffrn_reflns_limit_l_max         23
_diffrn_reflns_limit_l_min         -22
_diffrn_reflns_number              35607
_diffrn_reflns_point_group_measured_fraction_full  0.987
_diffrn_reflns_point_group_measured_fraction_max  0.788
_diffrn_reflns_theta_full          25.242
_diffrn_reflns_theta_max           30.448
_diffrn_reflns_theta_min           3.206
_diffrn_ambient_environment        N~2~
_diffrn_ambient_temperature        100.00(10)
_diffrn_detector                   'CCD plate'
_diffrn_detector_area_resol_mean   5.2169
_diffrn_detector_type              AtlasS2
_diffrn_measured_fraction_theta_full  0.998
_diffrn_measured_fraction_theta_max  0.852
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  t~exp~   \w     \q     \k     \f   Frames
--------------------------------------------------------------------------
  1  \w    -20.00  31.00   1.00   10.00    --  -10.30 -99.00  37.00   51
  2  \w    -15.00  85.00   1.00   10.00    --   12.02  57.00-120.00  100
  3  \w    -73.00  93.00   1.00   10.00    --   12.02   0.00-150.00  166
  4  \w    -13.00  88.00   1.00   10.00    --   12.02  77.00 -30.00  101
  5  \w     52.00  88.00   1.00   10.00    --   14.00-152.00  14.30   36
  6  \w    -29.00  52.00   1.00   10.00    --   14.00 -91.00  82.37   81
  7  \w    -18.00  57.00   1.00   10.00    --   14.00-102.00-175.51   75
;
_diffrn_measurement_device         'four-circle diffractometer'
_diffrn_measurement_device_type    'SuperNova, Dual, Cu at home/near, AtlasS2'
_diffrn_measurement_method         '\w scans'
_diffrn_orient_matrix_type        
 'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11        -0.0149929000
_diffrn_orient_matrix_UB_12        -0.0615458000
_diffrn_orient_matrix_UB_13        -0.0006805000
_diffrn_orient_matrix_UB_21        -0.0096664000
_diffrn_orient_matrix_UB_22        0.0233420000
_diffrn_orient_matrix_UB_23        0.0426793000
_diffrn_orient_matrix_UB_31        -0.0604858000
_diffrn_orient_matrix_UB_32        -0.0012273000
_diffrn_orient_matrix_UB_33        -0.0141859000
_diffrn_radiation_monochromator    mirror
_diffrn_radiation_probe            x-ray
_diffrn_radiation_type             MoK\a
_diffrn_radiation_wavelength       0.71073
_diffrn_source                     'micro-focus sealed X-ray tube'
_diffrn_source_type                'SuperNova (Mo) X-ray Source'
_reflns_Friedel_coverage           0.848
_reflns_Friedel_fraction_full      0.975
_reflns_Friedel_fraction_max       0.723
_reflns_number_gt                  19665
_reflns_number_total               20050
_reflns_odcompleteness_completeness  99.81
_reflns_odcompleteness_iscentric   1
_reflns_odcompleteness_theta       26.32
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression       'I > 2\s(I)'
_computing_cell_refinement         'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)'
_computing_data_collection         'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)'
_computing_data_reduction          'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)'
_computing_molecular_graphics      'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material    'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement    'ShelXL (Sheldrick, 2015)'
_computing_structure_solution      'ShelXS (Sheldrick, 2008)'
_refine_diff_density_max           2.062
_refine_diff_density_min           -2.001
_refine_diff_density_rms           0.193
_refine_ls_abs_structure_details
;
 Flack x determined using 8751 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons and Flack (2004), Acta Cryst. A60, s61).
;
_refine_ls_abs_structure_Flack     0.056(12)
_refine_ls_extinction_coef         .
_refine_ls_extinction_method       none
_refine_ls_goodness_of_fit_ref     1.075
_refine_ls_hydrogen_treatment      constr
_refine_ls_matrix_type             full
_refine_ls_number_parameters       765
_refine_ls_number_reflns           20050
_refine_ls_number_restraints       3
_refine_ls_R_factor_all            0.0315
_refine_ls_R_factor_gt             0.0307
_refine_ls_restrained_S_all        1.075
_refine_ls_shift/su_max            0.001
_refine_ls_shift/su_mean           0.000
_refine_ls_structure_factor_coef   Fsqd
_refine_ls_weighting_details      
 'w=1/[\s^2^(Fo^2^)+(0.0273P)^2^+5.1117P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme        calc
_refine_ls_wR_factor_gt            0.0719
_refine_ls_wR_factor_ref           0.0724
_refine_special_details
;
 ?
;
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Ternary CH refined with riding coordinates:
 C49(H49), C10(H10), C36(H36), C23(H23)
2.b Secondary CH2 refined with riding coordinates:
 C18(H18A,H18B), C14(H14A,H14B), C41(H41A,H41B), C15(H15A,H15B), C19(H19A,
 H19B), C16(H16A,H16B), C5(H5A,H5B), C22(H22A,H22B), C32(H32A,H32B), C28(H28A,
 H28B), C1(H1A,H1B), C20(H20A,H20B), C17(H17A,H17B), C42(H42A,H42B), C30(H30A,
 H30B), C29(H29A,H29B), C33(H33A,H33B), C2(H2A,H2B), C21(H21A,H21B), C3(H3A,
 H3B), C4(H4A,H4B), C44(H44A,H44B), C34(H34A,H34B), C45(H45A,H45B), C43(H43A,
 H43B), C6(H6A,H6B), C7(H7A,H7B), C9(H9A,H9B), C46(H46A,H46B), C35(H35A,H35B),
 C8(H8A,H8B), C48(H48A,H48B), C51(H51A,H51B), C31(H31A,H31B), C27(H27A,H27B),
 C12(H12A,H12B), C40(H40A,H40B), C47(H47A,H47B), C37(H37A,H37B), C25(H25A,H25B)
2.c Idealised Me refined as rotating group:
 C24(H24A,H24B,H24C), C39(H39A,H39B,H39C), C38(H38A,H38B,H38C), C50(H50A,H50B,
 H50C), C11(H11A,H11B,H11C), C13(H13A,H13B,H13C), C52(H52A,H52B,H52C), C26(H26A,
 H26B,H26C)
;
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary       direct
_atom_sites_solution_secondary     ?
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 I1 I 0.61371(5) 0.55381(6) 0.16122(4) 0.01357(12) Uani 1 1 d . . . . .
 I2 I 0.38948(5) 0.65615(6) -0.01517(4) 0.01451(12) Uani 1 1 d . . . . .
 I3 I -0.16904(5) 0.60715(6) 0.67793(4) 0.01515(12) Uani 1 1 d . . . . .
 I4 I 0.83684(5) 0.29620(6) 0.01782(4) 0.01460(12) Uani 1 1 d . . . . .
 I5 I 0.73977(5) 0.59001(6) -0.06716(4) 0.01341(12) Uani 1 1 d . . . . .
 I6 I 0.46460(5) 0.27741(5) -0.09703(4) 0.01323(12) Uani 1 1 d . . . . .
 I7 I 0.18384(5) 0.55253(5) 0.62797(4) 0.01335(12) Uani 1 1 d . . . . .
 I8 I 0.11273(5) 0.92244(5) 0.68909(4) 0.01264(12) Uani 1 1 d . . . . .
 I9 I -0.05123(5) 0.62314(5) 0.44197(4) 0.01257(12) Uani 1 1 d . . . . .
 I10 I 0.34113(5) 0.80901(6) 0.50025(4) 0.01437(12) Uani 1 1 d . . . . .
 I11 I -0.26826(5) 0.89306(5) 0.59790(4) 0.01327(12) Uani 1 1 d . . . . .
 I12 I 0.22537(5) 0.40029(6) 0.09553(4) 0.01386(12) Uani 1 1 d . . . . .
 Cu5 Cu 0.31061(10) 0.42305(11) -0.03891(7) 0.0134(2) Uani 1 1 d . . . . .
 I14 I 0.49987(5) 0.17610(6) 0.11920(4) 0.01469(12) Uani 1 1 d . . . . .
 Cu1 Cu 0.77590(10) 0.51565(11) 0.06048(7) 0.0132(2) Uani 1 1 d . . . . .
 Cu10 Cu -0.21089(10) 0.66754(11) 0.54532(7) 0.0141(2) Uani 1 1 d . . . . .
 I17 I 0.02200(5) 0.98892(6) 0.46476(4) 0.01438(12) Uani 1 1 d . . . . .
 Cu6 Cu 0.27082(10) 0.77622(11) 0.63531(7) 0.0137(2) Uani 1 1 d . . . . .
 Cu8 Cu 0.01397(11) 0.67604(13) 0.61202(8) 0.0187(3) Uani 1 1 d . . . . .
 Cu3 Cu 0.55167(10) 0.52087(12) -0.00601(8) 0.0181(3) Uani 1 1 d . . . . .
 Cu4 Cu 0.42911(13) 0.35195(17) 0.07331(11) 0.0342(4) Uani 1 1 d . . . . .
 Cu7 Cu 0.13137(13) 0.83779(18) 0.51871(10) 0.0334(4) Uani 1 1 d . . . . .
 Cu2 Cu 0.63275(13) 0.31215(15) 0.05615(14) 0.0441(5) Uani 1 1 d . . . . .
 Cu9 Cu -0.07007(12) 0.86514(15) 0.55195(11) 0.0321(4) Uani 1 1 d . . . . .
 N1 N 0.9327(7) 0.6412(7) 0.1381(5) 0.0107(15) Uani 1 1 d . . . . .
 N5 N 0.4164(7) 0.8335(8) 0.7393(5) 0.0118(15) Uani 1 1 d . . . . .
 N3 N 0.1628(6) 0.3599(7) -0.1386(5) 0.0108(15) Uani 1 1 d . . . . .
 N7 N -0.3713(7) 0.5534(7) 0.4669(5) 0.0121(15) Uani 1 1 d . . . . .
 C18 C 0.0853(8) 0.2465(9) -0.1417(6) 0.0132(18) Uani 1 1 d . . . . .
 H18A H 0.0712 0.2547 -0.0849 0.016 Uiso 1 1 calc R . . . .
 H18B H 0.1252 0.1766 -0.1622 0.016 Uiso 1 1 calc R . . . .
 C14 C 0.0876(8) 0.4587(9) -0.1234(6) 0.0135(18) Uani 1 1 d . . . . .
 H14A H 0.1378 0.5390 -0.1103 0.016 Uiso 1 1 calc R . . . .
 H14B H 0.0477 0.4616 -0.0753 0.016 Uiso 1 1 calc R . . . .
 N6 N 0.5887(6) 0.8971(7) 0.8637(5) 0.0098(15) Uani 1 1 d . . . . .
 N4 N -0.0236(7) 0.2959(8) -0.2564(5) 0.0127(16) Uani 1 1 d . . . . .
 N8 N -0.5727(6) 0.4239(7) 0.3798(5) 0.0117(15) Uani 1 1 d . . . . .
 C41 C -0.5826(9) 0.4781(10) 0.4733(6) 0.016(2) Uani 1 1 d . . . . .
 H41A H -0.5976 0.4120 0.4957 0.019 Uiso 1 1 calc R . . . .
 H41B H -0.6481 0.5229 0.4805 0.019 Uiso 1 1 calc R . . . .
 N2 N 1.1266(6) 0.7922(7) 0.2230(5) 0.0119(16) Uani 1 1 d . . . . .
 C15 C -0.0050(9) 0.4314(9) -0.2021(6) 0.0158(19) Uani 1 1 d . . . . .
 H15A H -0.0796 0.4522 -0.1850 0.019 Uiso 1 1 calc R . . . .
 H15B H 0.0219 0.4818 -0.2343 0.019 Uiso 1 1 calc R . . . .
 C19 C -0.0345(8) 0.2204(9) -0.1996(6) 0.0128(18) Uani 1 1 d . . . . .
 H19A H -0.0559 0.1327 -0.2337 0.015 Uiso 1 1 calc R . . . .
 H19B H -0.0962 0.2428 -0.1655 0.015 Uiso 1 1 calc R . . . .
 C16 C 0.1975(8) 0.3382(9) -0.2238(6) 0.0143(19) Uani 1 1 d . . . . .
 H16A H 0.2572 0.2860 -0.2319 0.017 Uiso 1 1 calc R . . . .
 H16B H 0.2319 0.4169 -0.2275 0.017 Uiso 1 1 calc R . . . .
 C5 C 0.9837(8) 0.6026(9) 0.2064(6) 0.0134(18) Uani 1 1 d . . . . .
 H5A H 1.0085 0.5237 0.1816 0.016 Uiso 1 1 calc R . . . .
 H5B H 0.9232 0.5911 0.2402 0.016 Uiso 1 1 calc R . . . .
 C22 C -0.3437(8) 0.2368(10) -0.3729(6) 0.0157(19) Uani 1 1 d . . . . .
 H22A H -0.3199 0.2932 -0.4018 0.019 Uiso 1 1 calc R . . . .
 H22B H -0.3465 0.1530 -0.4118 0.019 Uiso 1 1 calc R . . . .
 C32 C 0.5765(8) 0.7632(9) 0.8094(6) 0.0147(19) Uani 1 1 d . . . . .
 H32A H 0.5446 0.7106 0.8389 0.018 Uiso 1 1 calc R . . . .
 H32B H 0.6536 0.7447 0.7968 0.018 Uiso 1 1 calc R . . . .
 C28 C 0.6084(8) 0.9767(9) 0.8111(6) 0.0122(18) Uani 1 1 d . . . . .
 H28A H 0.6737 0.9562 0.7804 0.015 Uiso 1 1 calc R . . . .
 H28B H 0.6282 1.0635 0.8473 0.015 Uiso 1 1 calc R . . . .
 C1 C 1.0228(8) 0.6479(10) 0.0831(6) 0.0144(19) Uani 1 1 d . . . . .
 H1A H 0.9949 0.6853 0.0433 0.017 Uiso 1 1 calc R . . . .
 H1B H 1.0323 0.5645 0.0508 0.017 Uiso 1 1 calc R . . . .
 C20 C -0.1284(8) 0.2610(9) -0.3257(6) 0.0138(19) Uani 1 1 d . . . . .
 H20A H -0.1288 0.1782 -0.3652 0.017 Uiso 1 1 calc R . . . .
 H20B H -0.1185 0.3175 -0.3565 0.017 Uiso 1 1 calc R . . . .
 C17 C 0.0890(8) 0.2755(9) -0.2939(6) 0.0121(18) Uani 1 1 d . . . . .
 H17A H 0.0928 0.3103 -0.3382 0.015 Uiso 1 1 calc R . . . .
 H17B H 0.0889 0.1873 -0.3187 0.015 Uiso 1 1 calc R . . . .
 C42 C -0.4061(8) 0.5945(10) 0.3959(6) 0.016(2) Uani 1 1 d . . . . .
 H42A H -0.3507 0.5762 0.3560 0.020 Uiso 1 1 calc R . . . .
 H42B H -0.4027 0.6836 0.4174 0.020 Uiso 1 1 calc R . . . .
 C30 C 0.4725(8) 0.9152(10) 0.8964(6) 0.0146(19) Uani 1 1 d . . . . .
 H30A H 0.4710 1.0030 0.9217 0.017 Uiso 1 1 calc R . . . .
 H30B H 0.4635 0.8779 0.9391 0.017 Uiso 1 1 calc R . . . .
 C29 C 0.3715(8) 0.8527(9) 0.8205(6) 0.0109(17) Uani 1 1 d . . . . .
 H29A H 0.3347 0.7733 0.8218 0.013 Uiso 1 1 calc R . . . .
 H29B H 0.3114 0.9042 0.8248 0.013 Uiso 1 1 calc R . . . .
 C33 C 0.6875(8) 0.9350(9) 0.9394(6) 0.0128(18) Uani 1 1 d . . . . .
 H33A H 0.6807 1.0153 0.9791 0.015 Uiso 1 1 calc R . . . .
 H33B H 0.6762 0.8756 0.9678 0.015 Uiso 1 1 calc R . . . .
 C2 C 1.1428(9) 0.7231(9) 0.1333(6) 0.015(2) Uani 1 1 d . . . . .
 H2A H 1.1991 0.6683 0.1332 0.018 Uiso 1 1 calc R . . . .
 H2B H 1.1737 0.7813 0.1076 0.018 Uiso 1 1 calc R . . . .
 C21 C -0.2482(8) 0.2634(10) -0.2953(6) 0.017(2) Uani 1 1 d . . . . .
 H21A H -0.2483 0.3439 -0.2532 0.020 Uiso 1 1 calc R . . . .
 H21B H -0.2641 0.2008 -0.2699 0.020 Uiso 1 1 calc R . . . .
 C3 C 0.9091(8) 0.7691(9) 0.1789(6) 0.0146(19) Uani 1 1 d . . . . .
 H3A H 0.8594 0.7698 0.2218 0.017 Uiso 1 1 calc R . . . .
 H3B H 0.8669 0.7939 0.1366 0.017 Uiso 1 1 calc R . . . .
 C4 C 1.0257(8) 0.8606(9) 0.2195(6) 0.0146(18) Uani 1 1 d . . . . .
 H4A H 1.0415 0.9135 0.1868 0.018 Uiso 1 1 calc R . . . .
 H4B H 1.0193 0.9128 0.2764 0.018 Uiso 1 1 calc R . . . .
 C44 C -0.3641(8) 0.4193(9) 0.4318(6) 0.0157(19) Uani 1 1 d . . . . .
 H44A H -0.3516 0.3885 0.4778 0.019 Uiso 1 1 calc R . . . .
 H44B H -0.2971 0.4091 0.4014 0.019 Uiso 1 1 calc R . . . .
 C34 C 0.8119(8) 0.9429(9) 0.9173(6) 0.0126(18) Uani 1 1 d . . . . .
 H34A H 0.8290 1.0106 0.8966 0.015 Uiso 1 1 calc R . . . .
 H34B H 0.8174 0.8665 0.8727 0.015 Uiso 1 1 calc R . . . .
 C45 C -0.4786(8) 0.3446(10) 0.3716(6) 0.018(2) Uani 1 1 d . . . . .
 H45A H -0.4632 0.3166 0.3137 0.021 Uiso 1 1 calc R . . . .
 H45B H -0.5063 0.2721 0.3853 0.021 Uiso 1 1 calc R . . . .
 C43 C -0.5342(8) 0.5279(9) 0.3498(6) 0.0146(19) Uani 1 1 d . . . . .
 H43A H -0.5883 0.5862 0.3621 0.017 Uiso 1 1 calc R . . . .
 H43B H -0.5354 0.4957 0.2890 0.017 Uiso 1 1 calc R . . . .
 C6 C 1.0908(8) 0.6990(9) 0.2640(6) 0.0156(19) Uani 1 1 d . . . . .
 H6A H 1.0698 0.7407 0.3190 0.019 Uiso 1 1 calc R . . . .
 H6B H 1.1566 0.6582 0.2720 0.019 Uiso 1 1 calc R . . . .
 C7 C 1.2365(8) 0.8845(10) 0.2729(6) 0.019(2) Uani 1 1 d . . . . .
 H7A H 1.2275 0.9140 0.3322 0.023 Uiso 1 1 calc R . . . .
 H7B H 1.2424 0.9551 0.2545 0.023 Uiso 1 1 calc R . . . .
 C24 C -0.4752(9) 0.3820(10) -0.2987(6) 0.020(2) Uani 1 1 d . . . . .
 H24A H -0.4148 0.4108 -0.2494 0.030 Uiso 1 1 calc GR . . . .
 H24B H -0.5520 0.3841 -0.2815 0.030 Uiso 1 1 calc GR . . . .
 H24C H -0.4629 0.4346 -0.3313 0.030 Uiso 1 1 calc GR . . . .
 C39 C 1.1198(9) 1.0286(11) 1.0651(7) 0.023(2) Uani 1 1 d . . . . .
 H39A H 1.0935 1.0797 1.1148 0.034 Uiso 1 1 calc GR . . . .
 H39B H 1.1966 1.0679 1.0606 0.034 Uiso 1 1 calc GR . . . .
 H39C H 1.1248 0.9491 1.0692 0.034 Uiso 1 1 calc GR . . . .
 C38 C 1.0757(10) 0.7963(10) 0.8979(7) 0.024(2) Uani 1 1 d . . . . .
 H38A H 1.0979 0.7538 0.8441 0.037 Uiso 1 1 calc GR . . . .
 H38B H 0.9992 0.7551 0.9015 0.037 Uiso 1 1 calc GR . . . .
 H38C H 1.1336 0.7957 0.9427 0.037 Uiso 1 1 calc GR . . . .
 C9 C 1.4571(8) 0.9355(9) 0.3207(6) 0.019(2) Uani 1 1 d . . . . .
 H9A H 1.4511 0.9507 0.3798 0.023 Uiso 1 1 calc R . . . .
 H9B H 1.4523 1.0119 0.3105 0.023 Uiso 1 1 calc R . . . .
 C49 C -0.9591(7) 0.2304(9) 0.3126(6) 0.0138(18) Uani 1 1 d . . . . .
 H49 H -0.9015 0.1749 0.3088 0.017 Uiso 1 1 calc R . . . .
 C10 C 1.5783(8) 0.8999(9) 0.3037(6) 0.0172(19) Uani 1 1 d . . . . .
 H10 H 1.5715 0.8123 0.2972 0.021 Uiso 1 1 calc R . . . .
 C36 C 1.0306(8) 1.0111(8) 0.9861(6) 0.0133(17) Uani 1 1 d . . . . .
 H36 H 1.0322 1.0932 0.9819 0.016 Uiso 1 1 calc R . . . .
 C46 C -0.6908(8) 0.3450(9) 0.3293(6) 0.018(2) Uani 1 1 d . . . . .
 H46A H -0.6802 0.3041 0.2711 0.021 Uiso 1 1 calc R . . . .
 H46B H -0.7139 0.2810 0.3523 0.021 Uiso 1 1 calc R . . . .
 C35 C 0.9032(8) 0.9643(9) 0.9960(6) 0.0137(18) Uani 1 1 d . . . . .
 H35A H 0.9006 0.8872 1.0064 0.016 Uiso 1 1 calc R . . . .
 H35B H 0.8817 1.0246 1.0449 0.016 Uiso 1 1 calc R . . . .
 C8 C 1.3526(8) 0.8348(9) 0.2650(7) 0.019(2) Uani 1 1 d . . . . .
 H8A H 1.3479 0.7633 0.2824 0.023 Uiso 1 1 calc R . . . .
 H8B H 1.3650 0.8087 0.2064 0.023 Uiso 1 1 calc R . . . .
 C48 C -0.9090(8) 0.3303(10) 0.2793(6) 0.020(2) Uani 1 1 d . . . . .
 H48A H -0.9684 0.3813 0.2778 0.024 Uiso 1 1 calc R . . . .
 H48B H -0.8974 0.2896 0.2213 0.024 Uiso 1 1 calc R . . . .
 C51 C -1.0757(8) 0.1520(10) 0.2568(7) 0.022(2) Uani 1 1 d . . . . .
 H51A H -1.1074 0.0925 0.2814 0.026 Uiso 1 1 calc R . . . .
 H51B H -1.0593 0.1057 0.2012 0.026 Uiso 1 1 calc R . . . .
 C31 C 0.4929(8) 0.7396(10) 0.7279(6) 0.016(2) Uani 1 1 d . . . . .
 H31A H 0.5391 0.7413 0.6835 0.019 Uiso 1 1 calc R . . . .
 H31B H 0.4436 0.6579 0.7104 0.019 Uiso 1 1 calc R . . . .
 C27 C 0.4924(8) 0.9530(9) 0.7476(6) 0.0134(18) Uani 1 1 d . . . . .
 H27A H 0.4495 1.0205 0.7678 0.016 Uiso 1 1 calc R . . . .
 H27B H 0.5121 0.9494 0.6927 0.016 Uiso 1 1 calc R . . . .
 C12 C 1.6753(9) 0.9731(10) 0.3791(7) 0.027(2) Uani 1 1 d . . . . .
 H12A H 1.6562 0.9523 0.4276 0.033 Uiso 1 1 calc R . . . .
 H12B H 1.7496 0.9466 0.3663 0.033 Uiso 1 1 calc R . . . .
 C23 C -0.4687(8) 0.2498(9) -0.3524(6) 0.0165(19) Uani 1 1 d . . . . .
 H23 H -0.4904 0.1961 -0.3204 0.020 Uiso 1 1 calc R . . . .
 C40 C -0.4662(8) 0.5658(9) 0.5205(6) 0.0155(19) Uani 1 1 d . . . . .
 H40A H -0.4795 0.6506 0.5387 0.019 Uiso 1 1 calc R . . . .
 H40B H -0.4404 0.5480 0.5707 0.019 Uiso 1 1 calc R . . . .
 C50 C -0.9733(10) 0.2847(9) 0.4058(6) 0.021(2) Uani 1 1 d . . . . .
 H50A H -0.8975 0.3279 0.4394 0.032 Uiso 1 1 calc GR . . . .
 H50B H -1.0038 0.2189 0.4245 0.032 Uiso 1 1 calc GR . . . .
 H50C H -1.0277 0.3415 0.4121 0.032 Uiso 1 1 calc GR . . . .
 C47 C -0.7906(8) 0.4172(9) 0.3294(7) 0.020(2) Uani 1 1 d . . . . .
 H47A H -0.7699 0.4791 0.3042 0.024 Uiso 1 1 calc R . . . .
 H47B H -0.8008 0.4601 0.3874 0.024 Uiso 1 1 calc R . . . .
 C11 C 1.6073(9) 0.9103(10) 0.2208(7) 0.024(2) Uani 1 1 d . . . . .
 H11A H 1.5498 0.8522 0.1746 0.036 Uiso 1 1 calc GR . . . .
 H11B H 1.6852 0.8922 0.2133 0.036 Uiso 1 1 calc GR . . . .
 H11C H 1.6053 0.9930 0.2220 0.036 Uiso 1 1 calc GR . . . .
 C37 C 1.0702(8) 0.9305(10) 0.9067(6) 0.020(2) Uani 1 1 d . . . . .
 H37A H 1.1487 0.9704 0.9038 0.024 Uiso 1 1 calc R . . . .
 H37B H 1.0168 0.9288 0.8581 0.024 Uiso 1 1 calc R . . . .
 C13 C 1.6937(9) 1.1127(11) 0.4037(7) 0.030(3) Uani 1 1 d . . . . .
 H13A H 1.6981 1.1338 0.3539 0.045 Uiso 1 1 calc GR . . . .
 H13B H 1.7663 1.1502 0.4430 0.045 Uiso 1 1 calc GR . . . .
 H13C H 1.6283 1.1427 0.4297 0.045 Uiso 1 1 calc GR . . . .
 C52 C -1.1712(9) 0.2299(13) 0.2466(9) 0.037(3) Uani 1 1 d . . . . .
 H52A H -1.2447 0.1754 0.2168 0.055 Uiso 1 1 calc GR . . . .
 H52B H -1.1451 0.2809 0.2153 0.055 Uiso 1 1 calc GR . . . .
 H52C H -1.1828 0.2818 0.3016 0.055 Uiso 1 1 calc GR . . . .
 C25 C -0.5525(9) 0.2015(11) -0.4363(7) 0.027(3) Uani 1 1 d . . . . .
 H25A H -0.5472 0.1156 -0.4656 0.033 Uiso 1 1 calc R . . . .
 H25B H -0.5261 0.2484 -0.4708 0.033 Uiso 1 1 calc R . . . .
 C26 C -0.6835(9) 0.2090(12) -0.4288(9) 0.035(3) Uani 1 1 d . . . . .
 H26A H -0.7296 0.1809 -0.4845 0.053 Uiso 1 1 calc GR . . . .
 H26B H -0.6899 0.2933 -0.3986 0.053 Uiso 1 1 calc GR . . . .
 H26C H -0.7127 0.1573 -0.3987 0.053 Uiso 1 1 calc GR . . . .

loop_
  _atom_site_aniso_label
  _atom_site_aniso_U_11
  _atom_site_aniso_U_22
  _atom_site_aniso_U_33
  _atom_site_aniso_U_23
  _atom_site_aniso_U_13
  _atom_site_aniso_U_12
 I1 0.0136(3) 0.0142(3) 0.0116(3) 0.0028(2) 0.0034(2) 0.0018(2)
 I2 0.0133(3) 0.0115(3) 0.0202(3) 0.0077(2) 0.0023(2) 0.0021(2)
 I3 0.0147(3) 0.0177(3) 0.0167(3) 0.0101(2) 0.0030(2) 0.0045(2)
 I4 0.0122(3) 0.0118(3) 0.0198(3) 0.0043(2) 0.0048(2) 0.0038(2)
 I5 0.0125(3) 0.0152(3) 0.0133(3) 0.0067(2) 0.0008(2) 0.0019(2)
 I6 0.0135(3) 0.0115(3) 0.0134(3) 0.0024(2) 0.0007(2) 0.0044(2)
 I7 0.0127(3) 0.0108(3) 0.0175(3) 0.0063(2) 0.0021(2) 0.0019(2)
 I8 0.0146(3) 0.0116(3) 0.0113(3) 0.0026(2) 0.0014(2) 0.0053(2)
 I9 0.0137(3) 0.0116(3) 0.0121(3) 0.0034(2) 0.0035(2) 0.0025(2)
 I10 0.0131(3) 0.0180(3) 0.0164(3) 0.0095(2) 0.0054(2) 0.0065(2)
 I11 0.0125(3) 0.0116(3) 0.0170(3) 0.0052(2) 0.0051(2) 0.0040(2)
 I12 0.0127(3) 0.0165(3) 0.0157(3) 0.0084(2) 0.0044(2) 0.0053(2)
 Cu5 0.0127(5) 0.0130(6) 0.0142(5) 0.0051(5) 0.0003(4) 0.0020(4)
 I14 0.0146(3) 0.0152(3) 0.0151(3) 0.0060(2) 0.0018(2) 0.0040(2)
 Cu1 0.0127(5) 0.0125(6) 0.0133(5) 0.0035(5) 0.0010(4) 0.0023(4)
 Cu10 0.0129(5) 0.0139(6) 0.0141(5) 0.0042(5) 0.0004(4) 0.0015(4)
 I17 0.0152(3) 0.0144(3) 0.0155(3) 0.0072(2) 0.0029(2) 0.0038(2)
 Cu6 0.0151(5) 0.0127(6) 0.0129(5) 0.0045(5) 0.0003(4) 0.0032(4)
 Cu8 0.0163(6) 0.0207(7) 0.0206(6) 0.0080(5) 0.0029(5) 0.0064(5)
 Cu3 0.0136(5) 0.0199(7) 0.0214(6) 0.0075(5) 0.0035(5) 0.0038(5)
 Cu4 0.0211(7) 0.0548(10) 0.0496(9) 0.0389(9) 0.0153(6) 0.0227(7)
 Cu7 0.0236(7) 0.0619(11) 0.0326(8) 0.0296(8) 0.0138(6) 0.0271(7)
 Cu2 0.0247(7) 0.0290(8) 0.0960(15) 0.0337(9) 0.0358(9) 0.0134(6)
 Cu9 0.0211(6) 0.0339(8) 0.0592(10) 0.0318(8) 0.0233(7) 0.0121(6)
 N1 0.011(3) 0.011(4) 0.009(3) 0.003(3) 0.005(3) 0.000(3)
 N5 0.015(4) 0.013(4) 0.008(3) 0.003(3) 0.003(3) 0.004(3)
 N3 0.010(3) 0.010(4) 0.012(4) 0.002(3) 0.004(3) 0.004(3)
 N7 0.014(4) 0.007(4) 0.012(4) 0.001(3) 0.001(3) 0.001(3)
 C18 0.013(4) 0.014(5) 0.018(5) 0.011(4) 0.005(3) 0.005(4)
 C14 0.016(4) 0.009(4) 0.015(4) 0.002(4) -0.001(3) 0.007(4)
 N6 0.005(3) 0.009(4) 0.012(4) 0.002(3) -0.003(3) 0.002(3)
 N4 0.014(4) 0.015(4) 0.010(4) 0.005(3) 0.003(3) 0.004(3)
 N8 0.010(3) 0.011(4) 0.013(4) 0.003(3) 0.001(3) 0.002(3)
 C41 0.020(5) 0.016(5) 0.012(4) 0.005(4) 0.004(4) 0.006(4)
 N2 0.009(3) 0.013(4) 0.011(4) 0.004(3) -0.001(3) -0.002(3)
 C15 0.020(5) 0.010(5) 0.017(5) 0.004(4) -0.001(4) 0.007(4)
 C19 0.016(4) 0.013(5) 0.011(4) 0.007(4) 0.005(3) 0.002(4)
 C16 0.018(4) 0.015(5) 0.014(4) 0.009(4) 0.007(4) 0.001(4)
 C5 0.014(4) 0.012(5) 0.012(4) 0.002(4) 0.000(3) 0.000(4)
 C22 0.014(4) 0.016(5) 0.013(4) 0.002(4) -0.002(3) 0.005(4)
 C32 0.011(4) 0.013(5) 0.019(5) 0.004(4) 0.001(4) 0.004(4)
 C28 0.010(4) 0.014(5) 0.011(4) 0.004(4) -0.002(3) 0.000(3)
 C1 0.010(4) 0.021(5) 0.011(4) 0.004(4) 0.001(3) 0.003(4)
 C20 0.012(4) 0.016(5) 0.006(4) -0.002(4) -0.006(3) 0.003(4)
 C17 0.013(4) 0.015(5) 0.008(4) 0.004(4) 0.005(3) 0.003(4)
 C42 0.020(5) 0.020(5) 0.009(4) 0.006(4) -0.001(4) 0.001(4)
 C30 0.010(4) 0.018(5) 0.014(4) 0.003(4) 0.006(3) 0.002(4)
 C29 0.010(4) 0.013(4) 0.010(4) 0.004(4) -0.001(3) 0.005(3)
 C33 0.015(4) 0.014(5) 0.011(4) 0.006(4) 0.002(3) 0.004(4)
 C2 0.018(4) 0.014(5) 0.008(4) 0.001(4) 0.003(3) -0.003(4)
 C21 0.012(4) 0.020(5) 0.014(4) 0.001(4) -0.001(3) 0.002(4)
 C3 0.015(4) 0.012(4) 0.015(4) 0.001(4) 0.003(3) 0.003(3)
 C4 0.023(5) 0.011(4) 0.014(4) 0.007(4) 0.006(4) 0.007(4)
 C44 0.014(4) 0.014(5) 0.015(4) 0.001(4) 0.000(3) -0.001(4)
 C34 0.013(4) 0.012(4) 0.011(4) 0.002(4) -0.002(3) 0.004(3)
 C45 0.016(4) 0.016(5) 0.015(4) -0.001(4) -0.002(4) 0.004(4)
 C43 0.016(4) 0.013(5) 0.012(4) 0.006(4) -0.001(3) -0.003(4)
 C6 0.017(4) 0.017(5) 0.011(4) 0.005(4) 0.001(3) 0.000(4)
 C7 0.016(5) 0.022(5) 0.014(4) 0.000(4) 0.004(4) -0.003(4)
 C24 0.017(5) 0.024(6) 0.014(5) -0.001(4) 0.003(4) 0.004(4)
 C39 0.015(5) 0.030(6) 0.023(5) 0.012(5) 0.004(4) 0.000(4)
 C38 0.029(5) 0.020(5) 0.022(5) 0.002(4) 0.009(4) 0.008(4)
 C9 0.015(4) 0.017(5) 0.018(5) -0.001(4) 0.002(4) -0.005(4)
 C49 0.010(4) 0.016(5) 0.017(4) 0.009(4) 0.000(3) 0.003(3)
 C10 0.016(4) 0.012(4) 0.022(5) 0.006(4) 0.000(4) 0.001(4)
 C36 0.014(4) 0.010(4) 0.018(4) 0.007(4) 0.004(3) 0.004(3)
 C46 0.014(4) 0.017(5) 0.016(5) 0.001(4) 0.002(4) -0.006(4)
 C35 0.015(4) 0.017(5) 0.012(4) 0.007(4) 0.002(3) 0.005(4)
 C8 0.018(4) 0.012(5) 0.024(5) 0.005(4) 0.004(4) -0.004(4)
 C48 0.017(4) 0.025(5) 0.013(4) 0.003(4) -0.001(3) 0.003(4)
 C51 0.013(4) 0.023(5) 0.026(5) 0.009(4) 0.002(4) -0.003(4)
 C31 0.013(4) 0.017(5) 0.015(4) 0.001(4) -0.003(3) 0.007(4)
 C27 0.019(4) 0.010(4) 0.009(4) 0.003(4) -0.001(3) 0.000(4)
 C12 0.019(5) 0.024(6) 0.034(6) 0.006(5) -0.007(4) 0.007(4)
 C23 0.011(4) 0.012(5) 0.025(5) 0.008(4) -0.002(4) -0.003(3)
 C40 0.018(4) 0.015(5) 0.012(4) 0.002(4) 0.005(3) 0.004(4)
 C50 0.035(6) 0.010(5) 0.021(5) 0.011(4) 0.000(4) 0.004(4)
 C47 0.017(5) 0.015(5) 0.023(5) 0.003(4) 0.000(4) -0.002(4)
 C11 0.018(5) 0.019(5) 0.027(5) -0.001(4) 0.004(4) 0.001(4)
 C37 0.016(4) 0.026(5) 0.018(5) 0.008(4) 0.002(4) 0.003(4)
 C13 0.018(5) 0.040(7) 0.020(5) -0.002(5) 0.002(4) -0.002(5)
 C52 0.019(5) 0.048(8) 0.054(8) 0.041(7) -0.007(5) -0.007(5)
 C25 0.021(5) 0.029(6) 0.025(6) 0.004(5) -0.004(4) 0.003(5)
 C26 0.015(5) 0.031(7) 0.050(8) 0.006(6) 0.002(5) -0.001(4)

_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 I1 Cu1 2.6418(13) . ?
 I1 Cu3 2.7354(14) . ?
 I1 Cu4 2.8032(19) . ?
 I1 Cu2 2.8318(19) . ?
 I2 Cu5 2.6185(13) . ?
 I2 Cu3 2.6295(14) . ?
 I3 Cu10 2.5935(13) . ?
 I3 Cu8 2.6359(14) . ?
 I4 Cu1 2.6276(14) . ?
 I4 Cu2 2.5156(15) . ?
 I5 Cu1 2.6060(13) . ?
 I5 Cu3 2.6362(14) . ?
 I6 Cu5 2.6571(13) . ?
 I6 Cu3 2.7144(14) . ?
 I6 Cu4 2.8153(18) . ?
 I6 Cu2 2.950(2) . ?
 I7 Cu6 2.6138(13) . ?
 I7 Cu8 2.6269(14) . ?
 I8 Cu6 2.6833(13) . ?
 I8 Cu8 2.7373(15) . ?
 I8 Cu7 2.7645(16) . ?
 I8 Cu9 2.8002(18) . ?
 I9 Cu10 2.6525(13) . ?
 I9 Cu8 2.7379(15) . ?
 I9 Cu7 2.8530(19) . ?
 I9 Cu9 2.8605(18) . ?
 I10 Cu6 2.6338(13) . ?
 I10 Cu7 2.5195(15) . ?
 I11 Cu10 2.6749(14) . ?
 I11 Cu9 2.5134(15) . ?
 I12 Cu5 2.6516(13) . ?
 I12 Cu4 2.5225(15) . ?
 Cu5 Cu3 2.7708(16) . ?
 Cu5 Cu4 2.6483(19) . ?
 Cu5 N3 2.125(8) . ?
 I14 Cu4 2.6212(17) . ?
 I14 Cu2 2.6068(17) . ?
 Cu1 Cu3 2.7251(16) . ?
 Cu1 Cu2 2.6654(19) . ?
 Cu1 N1 2.147(7) . ?
 Cu10 Cu8 2.6902(17) . ?
 Cu10 Cu9 2.5851(19) . ?
 Cu10 N7 2.137(8) . ?
 I17 Cu7 2.6429(17) . ?
 I17 Cu9 2.5926(16) . ?
 Cu6 Cu8 2.9567(17) . ?
 Cu6 Cu7 2.7616(19) . ?
 Cu6 N5 2.157(8) . ?
 Cu8 Cu9 2.954(2) . ?
 Cu3 Cu4 3.012(2) . ?
 Cu4 Cu2 2.479(2) . ?
 Cu7 Cu9 2.4794(19) . ?
 N1 C5 1.474(12) . ?
 N1 C1 1.475(11) . ?
 N1 C3 1.492(12) . ?
 N5 C29 1.479(12) . ?
 N5 C31 1.472(12) . ?
 N5 C27 1.491(12) . ?
 N3 C18 1.468(12) . ?
 N3 C14 1.505(12) . ?
 N3 C16 1.488(11) . ?
 N7 C42 1.476(12) . ?
 N7 C44 1.490(12) . ?
 N7 C40 1.484(12) . ?
 C18 H18A 0.9700 . ?
 C18 H18B 0.9700 . ?
 C18 C19 1.536(13) . ?
 C14 H14A 0.9700 . ?
 C14 H14B 0.9700 . ?
 C14 C15 1.531(13) . ?
 N6 C32 1.498(12) . ?
 N6 C28 1.499(12) . ?
 N6 C30 1.513(11) . ?
 N6 C33 1.521(11) . ?
 N4 C15 1.507(12) . ?
 N4 C19 1.511(12) . ?
 N4 C20 1.501(11) . ?
 N4 C17 1.514(11) . ?
 N8 C41 1.520(12) . ?
 N8 C45 1.506(12) . ?
 N8 C43 1.494(12) . ?
 N8 C46 1.520(11) . ?
 C41 H41A 0.9700 . ?
 C41 H41B 0.9700 . ?
 C41 C40 1.525(13) . ?
 N2 C2 1.508(12) . ?
 N2 C4 1.503(12) . ?
 N2 C6 1.508(12) . ?
 N2 C7 1.503(12) . ?
 C15 H15A 0.9700 . ?
 C15 H15B 0.9700 . ?
 C19 H19A 0.9700 . ?
 C19 H19B 0.9700 . ?
 C16 H16A 0.9700 . ?
 C16 H16B 0.9700 . ?
 C16 C17 1.536(13) . ?
 C5 H5A 0.9700 . ?
 C5 H5B 0.9700 . ?
 C5 C6 1.536(12) . ?
 C22 H22A 0.9700 . ?
 C22 H22B 0.9700 . ?
 C22 C21 1.540(13) . ?
 C22 C23 1.530(13) . ?
 C32 H32A 0.9700 . ?
 C32 H32B 0.9700 . ?
 C32 C31 1.520(13) . ?
 C28 H28A 0.9700 . ?
 C28 H28B 0.9700 . ?
 C28 C27 1.555(12) . ?
 C1 H1A 0.9700 . ?
 C1 H1B 0.9700 . ?
 C1 C2 1.523(12) . ?
 C20 H20A 0.9700 . ?
 C20 H20B 0.9700 . ?
 C20 C21 1.522(13) . ?
 C17 H17A 0.9700 . ?
 C17 H17B 0.9700 . ?
 C42 H42A 0.9700 . ?
 C42 H42B 0.9700 . ?
 C42 C43 1.556(13) . ?
 C30 H30A 0.9700 . ?
 C30 H30B 0.9700 . ?
 C30 C29 1.538(12) . ?
 C29 H29A 0.9700 . ?
 C29 H29B 0.9700 . ?
 C33 H33A 0.9700 . ?
 C33 H33B 0.9700 . ?
 C33 C34 1.515(13) . ?
 C2 H2A 0.9700 . ?
 C2 H2B 0.9700 . ?
 C21 H21A 0.9700 . ?
 C21 H21B 0.9700 . ?
 C3 H3A 0.9700 . ?
 C3 H3B 0.9700 . ?
 C3 C4 1.525(13) . ?
 C4 H4A 0.9700 . ?
 C4 H4B 0.9700 . ?
 C44 H44A 0.9700 . ?
 C44 H44B 0.9700 . ?
 C44 C45 1.530(12) . ?
 C34 H34A 0.9700 . ?
 C34 H34B 0.9700 . ?
 C34 C35 1.537(12) . ?
 C45 H45A 0.9700 . ?
 C45 H45B 0.9700 . ?
 C43 H43A 0.9700 . ?
 C43 H43B 0.9700 . ?
 C6 H6A 0.9700 . ?
 C6 H6B 0.9700 . ?
 C7 H7A 0.9700 . ?
 C7 H7B 0.9700 . ?
 C7 C8 1.530(14) . ?
 C24 H24A 0.9600 . ?
 C24 H24B 0.9600 . ?
 C24 H24C 0.9600 . ?
 C24 C23 1.519(14) . ?
 C39 H39A 0.9600 . ?
 C39 H39B 0.9600 . ?
 C39 H39C 0.9600 . ?
 C39 C36 1.538(13) . ?
 C38 H38A 0.9600 . ?
 C38 H38B 0.9600 . ?
 C38 H38C 0.9600 . ?
 C38 C37 1.531(15) . ?
 C9 H9A 0.9700 . ?
 C9 H9B 0.9700 . ?
 C9 C10 1.537(13) . ?
 C9 C8 1.529(12) . ?
 C49 H49 0.9800 . ?
 C49 C48 1.526(14) . ?
 C49 C51 1.532(12) . ?
 C49 C50 1.529(13) . ?
 C10 H10 0.9800 . ?
 C10 C12 1.523(13) . ?
 C10 C11 1.518(15) . ?
 C36 H36 0.9800 . ?
 C36 C35 1.538(12) . ?
 C36 C37 1.515(13) . ?
 C46 H46A 0.9700 . ?
 C46 H46B 0.9700 . ?
 C46 C47 1.515(14) . ?
 C35 H35A 0.9700 . ?
 C35 H35B 0.9700 . ?
 C8 H8A 0.9700 . ?
 C8 H8B 0.9700 . ?
 C48 H48A 0.9700 . ?
 C48 H48B 0.9700 . ?
 C48 C47 1.549(13) . ?
 C51 H51A 0.9700 . ?
 C51 H51B 0.9700 . ?
 C51 C52 1.551(15) . ?
 C31 H31A 0.9700 . ?
 C31 H31B 0.9700 . ?
 C27 H27A 0.9700 . ?
 C27 H27B 0.9700 . ?
 C12 H12A 0.9700 . ?
 C12 H12B 0.9700 . ?
 C12 C13 1.514(16) . ?
 C23 H23 0.9800 . ?
 C23 C25 1.516(14) . ?
 C40 H40A 0.9700 . ?
 C40 H40B 0.9700 . ?
 C50 H50A 0.9600 . ?
 C50 H50B 0.9600 . ?
 C50 H50C 0.9600 . ?
 C47 H47A 0.9700 . ?
 C47 H47B 0.9700 . ?
 C11 H11A 0.9600 . ?
 C11 H11B 0.9600 . ?
 C11 H11C 0.9600 . ?
 C37 H37A 0.9700 . ?
 C37 H37B 0.9700 . ?
 C13 H13A 0.9600 . ?
 C13 H13B 0.9600 . ?
 C13 H13C 0.9600 . ?
 C52 H52A 0.9600 . ?
 C52 H52B 0.9600 . ?
 C52 H52C 0.9600 . ?
 C25 H25A 0.9700 . ?
 C25 H25B 0.9700 . ?
 C25 C26 1.537(15) . ?
 C26 H26A 0.9600 . ?
 C26 H26B 0.9600 . ?
 C26 H26C 0.9600 . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 Cu1 I1 Cu3 60.87(4) . . ?
 Cu1 I1 Cu4 102.12(5) . . ?
 Cu1 I1 Cu2 58.16(4) . . ?
 Cu3 I1 Cu4 65.87(4) . . ?
 Cu3 I1 Cu2 69.39(5) . . ?
 Cu4 I1 Cu2 52.19(5) . . ?
 Cu5 I2 Cu3 63.74(4) . . ?
 Cu10 I3 Cu8 61.91(4) . . ?
 Cu2 I4 Cu1 62.38(5) . . ?
 Cu1 I5 Cu3 62.64(4) . . ?
 Cu5 I6 Cu3 62.10(4) . . ?
 Cu5 I6 Cu4 57.80(4) . . ?
 Cu5 I6 Cu2 103.87(4) . . ?
 Cu3 I6 Cu4 65.97(5) . . ?
 Cu3 I6 Cu2 67.91(4) . . ?
 Cu4 I6 Cu2 50.86(4) . . ?
 Cu6 I7 Cu8 68.69(4) . . ?
 Cu6 I8 Cu8 66.10(4) . . ?
 Cu6 I8 Cu7 60.90(4) . . ?
 Cu6 I8 Cu9 107.02(5) . . ?
 Cu8 I8 Cu7 68.62(5) . . ?
 Cu8 I8 Cu9 64.46(4) . . ?
 Cu7 I8 Cu9 52.91(4) . . ?
 Cu10 I9 Cu8 59.85(4) . . ?
 Cu10 I9 Cu7 102.46(4) . . ?
 Cu10 I9 Cu9 55.77(4) . . ?
 Cu8 I9 Cu7 67.35(4) . . ?
 Cu8 I9 Cu9 63.65(5) . . ?
 Cu7 I9 Cu9 51.44(4) . . ?
 Cu7 I10 Cu6 64.76(5) . . ?
 Cu9 I11 Cu10 59.67(4) . . ?
 Cu4 I12 Cu5 61.51(5) . . ?
 I2 Cu5 I6 112.82(4) . . ?
 I2 Cu5 I12 111.17(5) . . ?
 I2 Cu5 Cu3 58.33(4) . . ?
 I2 Cu5 Cu4 111.28(6) . . ?
 I6 Cu5 Cu3 59.97(4) . . ?
 I12 Cu5 I6 115.25(5) . . ?
 I12 Cu5 Cu3 113.34(5) . . ?
 Cu4 Cu5 I6 64.10(5) . . ?
 Cu4 Cu5 I12 56.84(4) . . ?
 Cu4 Cu5 Cu3 67.48(5) . . ?
 N3 Cu5 I2 106.8(2) . . ?
 N3 Cu5 I6 104.3(2) . . ?
 N3 Cu5 I12 105.6(2) . . ?
 N3 Cu5 Cu3 141.0(2) . . ?
 N3 Cu5 Cu4 141.7(2) . . ?
 Cu2 I14 Cu4 56.60(5) . . ?
 I1 Cu1 Cu3 61.26(4) . . ?
 I1 Cu1 Cu2 64.49(5) . . ?
 I4 Cu1 I1 116.27(5) . . ?
 I4 Cu1 Cu3 116.01(5) . . ?
 I4 Cu1 Cu2 56.75(4) . . ?
 I5 Cu1 I1 114.06(5) . . ?
 I5 Cu1 I4 113.20(5) . . ?
 I5 Cu1 Cu3 59.22(4) . . ?
 I5 Cu1 Cu2 117.65(6) . . ?
 Cu2 Cu1 Cu3 72.02(6) . . ?
 N1 Cu1 I1 103.3(2) . . ?
 N1 Cu1 I4 104.3(2) . . ?
 N1 Cu1 I5 103.8(2) . . ?
 N1 Cu1 Cu3 139.6(2) . . ?
 N1 Cu1 Cu2 138.4(2) . . ?
 I3 Cu10 I9 114.42(5) . . ?
 I3 Cu10 I11 107.35(5) . . ?
 I3 Cu10 Cu8 59.82(4) . . ?
 I9 Cu10 I11 118.97(5) . . ?
 I9 Cu10 Cu8 61.65(4) . . ?
 I11 Cu10 Cu8 110.91(5) . . ?
 Cu9 Cu10 I3 113.54(6) . . ?
 Cu9 Cu10 I9 66.19(5) . . ?
 Cu9 Cu10 I11 57.06(4) . . ?
 Cu9 Cu10 Cu8 68.07(5) . . ?
 N7 Cu10 I3 109.6(2) . . ?
 N7 Cu10 I9 102.9(2) . . ?
 N7 Cu10 I11 102.6(2) . . ?
 N7 Cu10 Cu8 146.5(2) . . ?
 N7 Cu10 Cu9 136.1(2) . . ?
 Cu9 I17 Cu7 56.52(5) . . ?
 I7 Cu6 I8 108.35(4) . . ?
 I7 Cu6 I10 119.52(5) . . ?
 I7 Cu6 Cu8 55.86(4) . . ?
 I7 Cu6 Cu7 109.65(6) . . ?
 I8 Cu6 Cu8 57.83(4) . . ?
 I8 Cu6 Cu7 61.00(4) . . ?
 I10 Cu6 I8 109.13(5) . . ?
 I10 Cu6 Cu8 113.91(5) . . ?
 I10 Cu6 Cu7 55.62(4) . . ?
 Cu7 Cu6 Cu8 65.59(5) . . ?
 N5 Cu6 I7 101.8(2) . . ?
 N5 Cu6 I8 105.8(2) . . ?
 N5 Cu6 I10 111.3(2) . . ?
 N5 Cu6 Cu8 134.8(2) . . ?
 N5 Cu6 Cu7 148.3(2) . . ?
 I3 Cu8 I8 113.17(5) . . ?
 I3 Cu8 I9 110.30(5) . . ?
 I3 Cu8 Cu10 58.27(4) . . ?
 I3 Cu8 Cu6 148.33(6) . . ?
 I3 Cu8 Cu9 101.45(5) . . ?
 I7 Cu8 I3 110.42(5) . . ?
 I7 Cu8 I8 106.38(5) . . ?
 I7 Cu8 I9 106.85(5) . . ?
 I7 Cu8 Cu10 147.40(6) . . ?
 I7 Cu8 Cu6 55.45(4) . . ?
 I7 Cu8 Cu9 148.13(6) . . ?
 I8 Cu8 I9 109.47(5) . . ?
 I8 Cu8 Cu6 56.07(4) . . ?
 I8 Cu8 Cu9 58.80(5) . . ?
 I9 Cu8 Cu6 101.24(5) . . ?
 I9 Cu8 Cu9 60.20(5) . . ?
 Cu10 Cu8 I8 106.06(5) . . ?
 Cu10 Cu8 I9 58.50(4) . . ?
 Cu10 Cu8 Cu6 149.35(6) . . ?
 Cu10 Cu8 Cu9 54.27(5) . . ?
 Cu9 Cu8 Cu6 96.48(5) . . ?
 I1 Cu3 Cu5 103.18(5) . . ?
 I1 Cu3 Cu4 58.15(4) . . ?
 I2 Cu3 I1 107.44(5) . . ?
 I2 Cu3 I5 110.68(5) . . ?
 I2 Cu3 I6 110.63(5) . . ?
 I2 Cu3 Cu5 57.94(4) . . ?
 I2 Cu3 Cu1 147.06(6) . . ?
 I2 Cu3 Cu4 100.62(5) . . ?
 I5 Cu3 I1 110.09(5) . . ?
 I5 Cu3 I6 108.04(5) . . ?
 I5 Cu3 Cu5 146.72(6) . . ?
 I5 Cu3 Cu1 58.14(4) . . ?
 I5 Cu3 Cu4 148.70(6) . . ?
 I6 Cu3 I1 109.96(5) . . ?
 I6 Cu3 Cu5 57.94(4) . . ?
 I6 Cu3 Cu1 102.27(5) . . ?
 I6 Cu3 Cu4 58.63(5) . . ?
 Cu5 Cu3 Cu4 54.32(4) . . ?
 Cu1 Cu3 I1 57.87(4) . . ?
 Cu1 Cu3 Cu5 148.55(6) . . ?
 Cu1 Cu3 Cu4 95.07(5) . . ?
 I1 Cu4 I6 105.19(5) . . ?
 I1 Cu4 Cu3 55.98(4) . . ?
 I6 Cu4 Cu3 55.40(4) . . ?
 I12 Cu4 I1 113.31(7) . . ?
 I12 Cu4 I6 114.16(6) . . ?
 I12 Cu4 Cu5 61.64(4) . . ?
 I12 Cu4 I14 119.27(6) . . ?
 I12 Cu4 Cu3 109.60(6) . . ?
 Cu5 Cu4 I1 104.61(6) . . ?
 Cu5 Cu4 I6 58.10(4) . . ?
 Cu5 Cu4 Cu3 58.20(5) . . ?
 I14 Cu4 I1 101.50(5) . . ?
 I14 Cu4 I6 101.58(6) . . ?
 I14 Cu4 Cu5 150.35(8) . . ?
 I14 Cu4 Cu3 131.13(6) . . ?
 Cu2 Cu4 I1 64.50(6) . . ?
 Cu2 Cu4 I6 67.38(6) . . ?
 Cu2 Cu4 I12 177.75(10) . . ?
 Cu2 Cu4 Cu5 118.99(8) . . ?
 Cu2 Cu4 I14 61.41(6) . . ?
 Cu2 Cu4 Cu3 69.75(6) . . ?
 I8 Cu7 I9 105.46(5) . . ?
 I10 Cu7 I8 110.07(6) . . ?
 I10 Cu7 I9 116.78(7) . . ?
 I10 Cu7 I17 124.00(7) . . ?
 I10 Cu7 Cu6 59.62(4) . . ?
 I17 Cu7 I8 101.62(6) . . ?
 I17 Cu7 I9 96.48(5) . . ?
 I17 Cu7 Cu6 154.69(8) . . ?
 Cu6 Cu7 I8 58.10(4) . . ?
 Cu6 Cu7 I9 103.31(6) . . ?
 Cu9 Cu7 I8 64.28(6) . . ?
 Cu9 Cu7 I9 64.44(5) . . ?
 Cu9 Cu7 I10 173.97(8) . . ?
 Cu9 Cu7 I17 60.72(5) . . ?
 Cu9 Cu7 Cu6 114.44(7) . . ?
 I1 Cu2 I6 101.04(5) . . ?
 I4 Cu2 I1 113.51(6) . . ?
 I4 Cu2 I6 109.28(7) . . ?
 I4 Cu2 I14 129.31(7) . . ?
 I4 Cu2 Cu1 60.87(4) . . ?
 I14 Cu2 I1 101.11(6) . . ?
 I14 Cu2 I6 98.46(5) . . ?
 I14 Cu2 Cu1 155.26(9) . . ?
 Cu1 Cu2 I1 57.35(4) . . ?
 Cu1 Cu2 I6 97.79(7) . . ?
 Cu4 Cu2 I1 63.31(6) . . ?
 Cu4 Cu2 I4 168.01(10) . . ?
 Cu4 Cu2 I6 61.76(6) . . ?
 Cu4 Cu2 I14 61.99(5) . . ?
 Cu4 Cu2 Cu1 110.83(8) . . ?
 I8 Cu9 I9 104.32(5) . . ?
 I8 Cu9 Cu8 56.74(4) . . ?
 I9 Cu9 Cu8 56.15(4) . . ?
 I11 Cu9 I8 112.59(7) . . ?
 I11 Cu9 I9 117.16(6) . . ?
 I11 Cu9 Cu10 63.27(4) . . ?
 I11 Cu9 I17 120.83(6) . . ?
 I11 Cu9 Cu8 107.58(6) . . ?
 Cu10 Cu9 I8 107.20(6) . . ?
 Cu10 Cu9 I9 58.03(4) . . ?
 Cu10 Cu9 I17 145.57(8) . . ?
 Cu10 Cu9 Cu8 57.65(5) . . ?
 I17 Cu9 I8 101.95(5) . . ?
 I17 Cu9 I9 97.44(6) . . ?
 I17 Cu9 Cu8 131.57(6) . . ?
 Cu7 Cu9 I8 62.80(5) . . ?
 Cu7 Cu9 I9 64.13(6) . . ?
 Cu7 Cu9 I11 175.18(9) . . ?
 Cu7 Cu9 Cu10 115.95(8) . . ?
 Cu7 Cu9 I17 62.76(5) . . ?
 Cu7 Cu9 Cu8 68.98(6) . . ?
 C5 N1 Cu1 113.4(6) . . ?
 C5 N1 C1 108.5(7) . . ?
 C5 N1 C3 107.2(7) . . ?
 C1 N1 Cu1 108.1(5) . . ?
 C1 N1 C3 107.8(7) . . ?
 C3 N1 Cu1 111.7(6) . . ?
 C29 N5 Cu6 110.6(5) . . ?
 C29 N5 C27 107.0(7) . . ?
 C31 N5 Cu6 111.1(6) . . ?
 C31 N5 C29 108.3(7) . . ?
 C31 N5 C27 107.7(8) . . ?
 C27 N5 Cu6 111.8(6) . . ?
 C18 N3 Cu5 113.5(6) . . ?
 C18 N3 C14 106.4(7) . . ?
 C18 N3 C16 108.2(7) . . ?
 C14 N3 Cu5 108.0(5) . . ?
 C16 N3 Cu5 113.3(5) . . ?
 C16 N3 C14 107.1(8) . . ?
 C42 N7 Cu10 111.3(6) . . ?
 C42 N7 C44 108.8(8) . . ?
 C42 N7 C40 108.5(8) . . ?
 C44 N7 Cu10 113.3(6) . . ?
 C40 N7 Cu10 107.3(6) . . ?
 C40 N7 C44 107.5(7) . . ?
 N3 C18 H18A 109.2 . . ?
 N3 C18 H18B 109.2 . . ?
 N3 C18 C19 112.2(8) . . ?
 H18A C18 H18B 107.9 . . ?
 C19 C18 H18A 109.2 . . ?
 C19 C18 H18B 109.2 . . ?
 N3 C14 H14A 109.6 . . ?
 N3 C14 H14B 109.6 . . ?
 N3 C14 C15 110.3(7) . . ?
 H14A C14 H14B 108.1 . . ?
 C15 C14 H14A 109.6 . . ?
 C15 C14 H14B 109.6 . . ?
 C32 N6 C28 109.7(7) . . ?
 C32 N6 C30 108.0(7) . . ?
 C32 N6 C33 111.5(7) . . ?
 C28 N6 C30 107.5(7) . . ?
 C28 N6 C33 111.4(7) . . ?
 C30 N6 C33 108.5(7) . . ?
 C15 N4 C19 108.4(7) . . ?
 C15 N4 C17 106.8(7) . . ?
 C19 N4 C17 106.8(7) . . ?
 C20 N4 C15 111.1(7) . . ?
 C20 N4 C19 113.2(7) . . ?
 C20 N4 C17 110.3(7) . . ?
 C41 N8 C46 110.1(7) . . ?
 C45 N8 C41 107.6(7) . . ?
 C45 N8 C46 109.7(7) . . ?
 C43 N8 C41 108.8(7) . . ?
 C43 N8 C45 109.0(7) . . ?
 C43 N8 C46 111.5(7) . . ?
 N8 C41 H41A 110.0 . . ?
 N8 C41 H41B 110.0 . . ?
 N8 C41 C40 108.5(7) . . ?
 H41A C41 H41B 108.4 . . ?
 C40 C41 H41A 110.0 . . ?
 C40 C41 H41B 110.0 . . ?
 C2 N2 C6 108.6(7) . . ?
 C4 N2 C2 108.2(7) . . ?
 C4 N2 C6 107.5(7) . . ?
 C7 N2 C2 111.8(7) . . ?
 C7 N2 C4 108.7(7) . . ?
 C7 N2 C6 111.8(7) . . ?
 C14 C15 H15A 109.7 . . ?
 C14 C15 H15B 109.7 . . ?
 N4 C15 C14 109.7(8) . . ?
 N4 C15 H15A 109.7 . . ?
 N4 C15 H15B 109.7 . . ?
 H15A C15 H15B 108.2 . . ?
 C18 C19 H19A 109.9 . . ?
 C18 C19 H19B 109.9 . . ?
 N4 C19 C18 108.8(7) . . ?
 N4 C19 H19A 109.9 . . ?
 N4 C19 H19B 109.9 . . ?
 H19A C19 H19B 108.3 . . ?
 N3 C16 H16A 109.5 . . ?
 N3 C16 H16B 109.5 . . ?
 N3 C16 C17 110.7(7) . . ?
 H16A C16 H16B 108.1 . . ?
 C17 C16 H16A 109.5 . . ?
 C17 C16 H16B 109.5 . . ?
 N1 C5 H5A 109.3 . . ?
 N1 C5 H5B 109.3 . . ?
 N1 C5 C6 111.8(8) . . ?
 H5A C5 H5B 107.9 . . ?
 C6 C5 H5A 109.3 . . ?
 C6 C5 H5B 109.3 . . ?
 H22A C22 H22B 107.6 . . ?
 C21 C22 H22A 108.6 . . ?
 C21 C22 H22B 108.6 . . ?
 C23 C22 H22A 108.6 . . ?
 C23 C22 H22B 108.6 . . ?
 C23 C22 C21 114.7(8) . . ?
 N6 C32 H32A 110.1 . . ?
 N6 C32 H32B 110.1 . . ?
 N6 C32 C31 107.9(8) . . ?
 H32A C32 H32B 108.4 . . ?
 C31 C32 H32A 110.1 . . ?
 C31 C32 H32B 110.1 . . ?
 N6 C28 H28A 110.0 . . ?
 N6 C28 H28B 110.0 . . ?
 N6 C28 C27 108.5(7) . . ?
 H28A C28 H28B 108.4 . . ?
 C27 C28 H28A 110.0 . . ?
 C27 C28 H28B 110.0 . . ?
 N1 C1 H1A 109.1 . . ?
 N1 C1 H1B 109.1 . . ?
 N1 C1 C2 112.5(7) . . ?
 H1A C1 H1B 107.8 . . ?
 C2 C1 H1A 109.1 . . ?
 C2 C1 H1B 109.1 . . ?
 N4 C20 H20A 108.6 . . ?
 N4 C20 H20B 108.6 . . ?
 N4 C20 C21 114.6(7) . . ?
 H20A C20 H20B 107.6 . . ?
 C21 C20 H20A 108.6 . . ?
 C21 C20 H20B 108.6 . . ?
 N4 C17 C16 109.4(7) . . ?
 N4 C17 H17A 109.8 . . ?
 N4 C17 H17B 109.8 . . ?
 C16 C17 H17A 109.8 . . ?
 C16 C17 H17B 109.8 . . ?
 H17A C17 H17B 108.2 . . ?
 N7 C42 H42A 109.5 . . ?
 N7 C42 H42B 109.5 . . ?
 N7 C42 C43 110.7(8) . . ?
 H42A C42 H42B 108.1 . . ?
 C43 C42 H42A 109.5 . . ?
 C43 C42 H42B 109.5 . . ?
 N6 C30 H30A 110.2 . . ?
 N6 C30 H30B 110.2 . . ?
 N6 C30 C29 107.5(7) . . ?
 H30A C30 H30B 108.5 . . ?
 C29 C30 H30A 110.2 . . ?
 C29 C30 H30B 110.2 . . ?
 N5 C29 C30 111.2(7) . . ?
 N5 C29 H29A 109.4 . . ?
 N5 C29 H29B 109.4 . . ?
 C30 C29 H29A 109.4 . . ?
 C30 C29 H29B 109.4 . . ?
 H29A C29 H29B 108.0 . . ?
 N6 C33 H33A 108.6 . . ?
 N6 C33 H33B 108.6 . . ?
 H33A C33 H33B 107.6 . . ?
 C34 C33 N6 114.5(7) . . ?
 C34 C33 H33A 108.6 . . ?
 C34 C33 H33B 108.6 . . ?
 N2 C2 C1 108.5(7) . . ?
 N2 C2 H2A 110.0 . . ?
 N2 C2 H2B 110.0 . . ?
 C1 C2 H2A 110.0 . . ?
 C1 C2 H2B 110.0 . . ?
 H2A C2 H2B 108.4 . . ?
 C22 C21 H21A 110.2 . . ?
 C22 C21 H21B 110.2 . . ?
 C20 C21 C22 107.6(8) . . ?
 C20 C21 H21A 110.2 . . ?
 C20 C21 H21B 110.2 . . ?
 H21A C21 H21B 108.5 . . ?
 N1 C3 H3A 109.6 . . ?
 N1 C3 H3B 109.6 . . ?
 N1 C3 C4 110.3(7) . . ?
 H3A C3 H3B 108.1 . . ?
 C4 C3 H3A 109.6 . . ?
 C4 C3 H3B 109.6 . . ?
 N2 C4 C3 110.4(8) . . ?
 N2 C4 H4A 109.6 . . ?
 N2 C4 H4B 109.6 . . ?
 C3 C4 H4A 109.6 . . ?
 C3 C4 H4B 109.6 . . ?
 H4A C4 H4B 108.1 . . ?
 N7 C44 H44A 109.6 . . ?
 N7 C44 H44B 109.6 . . ?
 N7 C44 C45 110.5(8) . . ?
 H44A C44 H44B 108.1 . . ?
 C45 C44 H44A 109.6 . . ?
 C45 C44 H44B 109.6 . . ?
 C33 C34 H34A 109.7 . . ?
 C33 C34 H34B 109.7 . . ?
 C33 C34 C35 110.0(8) . . ?
 H34A C34 H34B 108.2 . . ?
 C35 C34 H34A 109.7 . . ?
 C35 C34 H34B 109.7 . . ?
 N8 C45 C44 109.8(8) . . ?
 N8 C45 H45A 109.7 . . ?
 N8 C45 H45B 109.7 . . ?
 C44 C45 H45A 109.7 . . ?
 C44 C45 H45B 109.7 . . ?
 H45A C45 H45B 108.2 . . ?
 N8 C43 C42 108.9(8) . . ?
 N8 C43 H43A 109.9 . . ?
 N8 C43 H43B 109.9 . . ?
 C42 C43 H43A 109.9 . . ?
 C42 C43 H43B 109.9 . . ?
 H43A C43 H43B 108.3 . . ?
 N2 C6 C5 108.8(7) . . ?
 N2 C6 H6A 109.9 . . ?
 N2 C6 H6B 109.9 . . ?
 C5 C6 H6A 109.9 . . ?
 C5 C6 H6B 109.9 . . ?
 H6A C6 H6B 108.3 . . ?
 N2 C7 H7A 108.5 . . ?
 N2 C7 H7B 108.5 . . ?
 N2 C7 C8 115.0(8) . . ?
 H7A C7 H7B 107.5 . . ?
 C8 C7 H7A 108.5 . . ?
 C8 C7 H7B 108.5 . . ?
 H24A C24 H24B 109.5 . . ?
 H24A C24 H24C 109.5 . . ?
 H24B C24 H24C 109.5 . . ?
 C23 C24 H24A 109.5 . . ?
 C23 C24 H24B 109.5 . . ?
 C23 C24 H24C 109.5 . . ?
 H39A C39 H39B 109.5 . . ?
 H39A C39 H39C 109.5 . . ?
 H39B C39 H39C 109.5 . . ?
 C36 C39 H39A 109.5 . . ?
 C36 C39 H39B 109.5 . . ?
 C36 C39 H39C 109.5 . . ?
 H38A C38 H38B 109.5 . . ?
 H38A C38 H38C 109.5 . . ?
 H38B C38 H38C 109.5 . . ?
 C37 C38 H38A 109.5 . . ?
 C37 C38 H38B 109.5 . . ?
 C37 C38 H38C 109.5 . . ?
 H9A C9 H9B 107.8 . . ?
 C10 C9 H9A 109.1 . . ?
 C10 C9 H9B 109.1 . . ?
 C8 C9 H9A 109.1 . . ?
 C8 C9 H9B 109.1 . . ?
 C8 C9 C10 112.7(8) . . ?
 C48 C49 H49 107.2 . . ?
 C48 C49 C51 111.0(8) . . ?
 C48 C49 C50 112.1(8) . . ?
 C51 C49 H49 107.2 . . ?
 C50 C49 H49 107.2 . . ?
 C50 C49 C51 111.7(8) . . ?
 C9 C10 H10 106.9 . . ?
 C12 C10 C9 111.2(8) . . ?
 C12 C10 H10 106.9 . . ?
 C11 C10 C9 111.2(8) . . ?
 C11 C10 H10 106.9 . . ?
 C11 C10 C12 113.3(8) . . ?
 C39 C36 H36 107.0 . . ?
 C35 C36 C39 111.1(8) . . ?
 C35 C36 H36 107.0 . . ?
 C37 C36 C39 110.4(8) . . ?
 C37 C36 H36 107.0 . . ?
 C37 C36 C35 114.0(8) . . ?
 N8 C46 H46A 108.7 . . ?
 N8 C46 H46B 108.7 . . ?
 H46A C46 H46B 107.6 . . ?
 C47 C46 N8 114.1(8) . . ?
 C47 C46 H46A 108.7 . . ?
 C47 C46 H46B 108.7 . . ?
 C34 C35 C36 112.6(8) . . ?
 C34 C35 H35A 109.1 . . ?
 C34 C35 H35B 109.1 . . ?
 C36 C35 H35A 109.1 . . ?
 C36 C35 H35B 109.1 . . ?
 H35A C35 H35B 107.8 . . ?
 C7 C8 H8A 109.6 . . ?
 C7 C8 H8B 109.6 . . ?
 C9 C8 C7 110.1(8) . . ?
 C9 C8 H8A 109.6 . . ?
 C9 C8 H8B 109.6 . . ?
 H8A C8 H8B 108.1 . . ?
 C49 C48 H48A 108.1 . . ?
 C49 C48 H48B 108.1 . . ?
 C49 C48 C47 116.9(8) . . ?
 H48A C48 H48B 107.3 . . ?
 C47 C48 H48A 108.1 . . ?
 C47 C48 H48B 108.1 . . ?
 C49 C51 H51A 108.9 . . ?
 C49 C51 H51B 108.9 . . ?
 C49 C51 C52 113.4(9) . . ?
 H51A C51 H51B 107.7 . . ?
 C52 C51 H51A 108.9 . . ?
 C52 C51 H51B 108.9 . . ?
 N5 C31 C32 111.3(8) . . ?
 N5 C31 H31A 109.4 . . ?
 N5 C31 H31B 109.4 . . ?
 C32 C31 H31A 109.4 . . ?
 C32 C31 H31B 109.4 . . ?
 H31A C31 H31B 108.0 . . ?
 N5 C27 C28 109.6(8) . . ?
 N5 C27 H27A 109.8 . . ?
 N5 C27 H27B 109.8 . . ?
 C28 C27 H27A 109.8 . . ?
 C28 C27 H27B 109.8 . . ?
 H27A C27 H27B 108.2 . . ?
 C10 C12 H12A 108.5 . . ?
 C10 C12 H12B 108.5 . . ?
 H12A C12 H12B 107.5 . . ?
 C13 C12 C10 115.1(9) . . ?
 C13 C12 H12A 108.5 . . ?
 C13 C12 H12B 108.5 . . ?
 C22 C23 H23 108.2 . . ?
 C24 C23 C22 112.2(8) . . ?
 C24 C23 H23 108.2 . . ?
 C25 C23 C22 107.0(8) . . ?
 C25 C23 C24 113.0(9) . . ?
 C25 C23 H23 108.2 . . ?
 N7 C40 C41 111.9(8) . . ?
 N7 C40 H40A 109.2 . . ?
 N7 C40 H40B 109.2 . . ?
 C41 C40 H40A 109.2 . . ?
 C41 C40 H40B 109.2 . . ?
 H40A C40 H40B 107.9 . . ?
 C49 C50 H50A 109.5 . . ?
 C49 C50 H50B 109.5 . . ?
 C49 C50 H50C 109.5 . . ?
 H50A C50 H50B 109.5 . . ?
 H50A C50 H50C 109.5 . . ?
 H50B C50 H50C 109.5 . . ?
 C46 C47 C48 111.2(8) . . ?
 C46 C47 H47A 109.4 . . ?
 C46 C47 H47B 109.4 . . ?
 C48 C47 H47A 109.4 . . ?
 C48 C47 H47B 109.4 . . ?
 H47A C47 H47B 108.0 . . ?
 C10 C11 H11A 109.5 . . ?
 C10 C11 H11B 109.5 . . ?
 C10 C11 H11C 109.5 . . ?
 H11A C11 H11B 109.5 . . ?
 H11A C11 H11C 109.5 . . ?
 H11B C11 H11C 109.5 . . ?
 C38 C37 H37A 108.0 . . ?
 C38 C37 H37B 108.0 . . ?
 C36 C37 C38 117.3(8) . . ?
 C36 C37 H37A 108.0 . . ?
 C36 C37 H37B 108.0 . . ?
 H37A C37 H37B 107.2 . . ?
 C12 C13 H13A 109.5 . . ?
 C12 C13 H13B 109.5 . . ?
 C12 C13 H13C 109.5 . . ?
 H13A C13 H13B 109.5 . . ?
 H13A C13 H13C 109.5 . . ?
 H13B C13 H13C 109.5 . . ?
 C51 C52 H52A 109.5 . . ?
 C51 C52 H52B 109.5 . . ?
 C51 C52 H52C 109.5 . . ?
 H52A C52 H52B 109.5 . . ?
 H52A C52 H52C 109.5 . . ?
 H52B C52 H52C 109.5 . . ?
 C23 C25 H25A 108.6 . . ?
 C23 C25 H25B 108.6 . . ?
 C23 C25 C26 114.8(9) . . ?
 H25A C25 H25B 107.6 . . ?
 C26 C25 H25A 108.6 . . ?
 C26 C25 H25B 108.6 . . ?
 C25 C26 H26A 109.5 . . ?
 C25 C26 H26B 109.5 . . ?
 C25 C26 H26C 109.5 . . ?
 H26A C26 H26B 109.5 . . ?
 H26A C26 H26C 109.5 . . ?
 H26B C26 H26C 109.5 . . ?

loop_
  _geom_torsion_atom_site_label_1
  _geom_torsion_atom_site_label_2
  _geom_torsion_atom_site_label_3
  _geom_torsion_atom_site_label_4
  _geom_torsion
  _geom_torsion_site_symmetry_1
  _geom_torsion_site_symmetry_2
  _geom_torsion_site_symmetry_3
  _geom_torsion_site_symmetry_4
  _geom_torsion_publ_flag
 Cu5 N3 C18 C19 166.5(6) . . . . ?
 Cu5 N3 C14 C15 168.0(6) . . . . ?
 Cu5 N3 C16 C17 171.9(6) . . . . ?
 Cu1 N1 C5 C6 -176.3(6) . . . . ?
 Cu1 N1 C1 C2 -173.4(7) . . . . ?
 Cu1 N1 C3 C4 -169.3(6) . . . . ?
 Cu10 N7 C42 C43 -169.1(6) . . . . ?
 Cu10 N7 C44 C45 -176.2(6) . . . . ?
 Cu10 N7 C40 C41 -174.3(7) . . . . ?
 Cu6 N5 C29 C30 -170.0(6) . . . . ?
 Cu6 N5 C31 C32 -166.1(6) . . . . ?
 Cu6 N5 C27 C28 -169.0(6) . . . . ?
 N1 C5 C6 N2 -11.2(11) . . . . ?
 N1 C1 C2 N2 -12.5(11) . . . . ?
 N1 C3 C4 N2 -12.1(11) . . . . ?
 N3 C18 C19 N4 17.0(11) . . . . ?
 N3 C14 C15 N4 20.8(11) . . . . ?
 N3 C16 C17 N4 20.0(11) . . . . ?
 N7 C42 C43 N8 -11.8(11) . . . . ?
 N7 C44 C45 N8 -11.5(11) . . . . ?
 C18 N3 C14 C15 -69.8(9) . . . . ?
 C18 N3 C16 C17 45.2(10) . . . . ?
 C14 N3 C18 C19 47.9(10) . . . . ?
 C14 N3 C16 C17 -69.1(9) . . . . ?
 N6 C32 C31 N5 -21.8(11) . . . . ?
 N6 C28 C27 N5 -18.6(10) . . . . ?
 N6 C30 C29 N5 -18.9(11) . . . . ?
 N6 C33 C34 C35 -172.4(8) . . . . ?
 N4 C20 C21 C22 175.1(8) . . . . ?
 N8 C41 C40 N7 -11.6(11) . . . . ?
 N8 C46 C47 C48 -178.1(8) . . . . ?
 C41 N8 C45 C44 -52.5(10) . . . . ?
 C41 N8 C43 C42 65.5(9) . . . . ?
 C41 N8 C46 C47 64.7(11) . . . . ?
 N2 C7 C8 C9 -178.2(8) . . . . ?
 C15 N4 C19 C18 -66.4(9) . . . . ?
 C15 N4 C20 C21 -68.7(11) . . . . ?
 C15 N4 C17 C16 46.6(10) . . . . ?
 C19 N4 C15 C14 45.1(10) . . . . ?
 C19 N4 C20 C21 53.5(11) . . . . ?
 C19 N4 C17 C16 -69.3(9) . . . . ?
 C16 N3 C18 C19 -66.9(10) . . . . ?
 C16 N3 C14 C15 45.7(10) . . . . ?
 C5 N1 C1 C2 -50.1(11) . . . . ?
 C5 N1 C3 C4 65.9(9) . . . . ?
 C22 C23 C25 C26 -179.0(10) . . . . ?
 C32 N6 C28 C27 68.2(9) . . . . ?
 C32 N6 C30 C29 -47.9(10) . . . . ?
 C32 N6 C33 C34 71.1(10) . . . . ?
 C28 N6 C32 C31 -45.7(9) . . . . ?
 C28 N6 C30 C29 70.4(9) . . . . ?
 C28 N6 C33 C34 -51.9(10) . . . . ?
 C1 N1 C5 C6 63.7(10) . . . . ?
 C1 N1 C3 C4 -50.7(10) . . . . ?
 C20 N4 C15 C14 170.1(8) . . . . ?
 C20 N4 C19 C18 169.9(8) . . . . ?
 C20 N4 C17 C16 167.4(8) . . . . ?
 C17 N4 C15 C14 -69.7(9) . . . . ?
 C17 N4 C19 C18 48.4(9) . . . . ?
 C17 N4 C20 C21 173.1(8) . . . . ?
 C42 N7 C44 C45 -51.8(10) . . . . ?
 C42 N7 C40 C41 65.3(10) . . . . ?
 C30 N6 C32 C31 71.2(9) . . . . ?
 C30 N6 C28 C27 -49.0(9) . . . . ?
 C30 N6 C33 C34 -170.1(8) . . . . ?
 C29 N5 C31 C32 -44.3(10) . . . . ?
 C29 N5 C27 C28 69.7(9) . . . . ?
 C33 N6 C32 C31 -169.7(8) . . . . ?
 C33 N6 C28 C27 -167.7(7) . . . . ?
 C33 N6 C30 C29 -168.9(8) . . . . ?
 C33 C34 C35 C36 -163.1(8) . . . . ?
 C2 N2 C4 C3 65.4(9) . . . . ?
 C2 N2 C6 C5 -52.1(9) . . . . ?
 C2 N2 C7 C8 -47.0(12) . . . . ?
 C21 C22 C23 C24 64.1(12) . . . . ?
 C21 C22 C23 C25 -171.5(9) . . . . ?
 C3 N1 C5 C6 -52.5(9) . . . . ?
 C3 N1 C1 C2 65.7(10) . . . . ?
 C4 N2 C2 C1 -51.0(10) . . . . ?
 C4 N2 C6 C5 64.8(9) . . . . ?
 C4 N2 C7 C8 -166.3(8) . . . . ?
 C44 N7 C42 C43 65.4(10) . . . . ?
 C44 N7 C40 C41 -52.1(10) . . . . ?
 C45 N8 C41 C40 65.5(10) . . . . ?
 C45 N8 C43 C42 -51.6(10) . . . . ?
 C45 N8 C46 C47 -177.0(8) . . . . ?
 C43 N8 C41 C40 -52.4(10) . . . . ?
 C43 N8 C45 C44 65.3(10) . . . . ?
 C43 N8 C46 C47 -56.1(11) . . . . ?
 C6 N2 C2 C1 65.4(10) . . . . ?
 C6 N2 C4 C3 -51.8(9) . . . . ?
 C6 N2 C7 C8 75.1(10) . . . . ?
 C7 N2 C2 C1 -170.7(8) . . . . ?
 C7 N2 C4 C3 -173.0(8) . . . . ?
 C7 N2 C6 C5 -176.0(8) . . . . ?
 C24 C23 C25 C26 -55.1(13) . . . . ?
 C39 C36 C35 C34 -178.7(8) . . . . ?
 C39 C36 C37 C38 63.7(11) . . . . ?
 C9 C10 C12 C13 -59.5(12) . . . . ?
 C49 C48 C47 C46 62.0(11) . . . . ?
 C10 C9 C8 C7 -169.6(9) . . . . ?
 C46 N8 C41 C40 -174.9(8) . . . . ?
 C46 N8 C45 C44 -172.3(8) . . . . ?
 C46 N8 C43 C42 -172.9(8) . . . . ?
 C35 C36 C37 C38 -62.1(11) . . . . ?
 C8 C9 C10 C12 -158.0(9) . . . . ?
 C8 C9 C10 C11 74.7(11) . . . . ?
 C48 C49 C51 C52 -55.5(11) . . . . ?
 C51 C49 C48 C47 -180.0(8) . . . . ?
 C31 N5 C29 C30 67.9(10) . . . . ?
 C31 N5 C27 C28 -46.6(9) . . . . ?
 C27 N5 C29 C30 -48.0(10) . . . . ?
 C27 N5 C31 C32 71.2(10) . . . . ?
 C23 C22 C21 C20 -173.6(8) . . . . ?
 C40 N7 C42 C43 -51.3(10) . . . . ?
 C40 N7 C44 C45 65.5(10) . . . . ?
 C50 C49 C48 C47 54.3(11) . . . . ?
 C50 C49 C51 C52 70.4(11) . . . . ?
 C11 C10 C12 C13 66.6(12) . . . . ?
 C37 C36 C35 C34 -53.2(11) . . . . ?

loop_
  _refln_index_h
  _refln_index_k
  _refln_index_l
  _refln_F_squared_meas
  _refln_F_squared_sigma
 0 0 3 416.26 10.82
 0 0 -3 379.03 10.7
 0 0 4 618.63 15.71
 0 0 -4 583.81 15.4
 0 0 -4 592.72 15.73
 0 0 4 597.83 15.6
 0 0 -5 600.67 16.9
 0 0 5 613.87 17.1
 0 0 -5 647.01 17.49
 0 0 5 607.46 17.03
 0 0 6 483.79 15.35
 0 0 -6 470.99 14.95
 0 0 -6 501.88 15.78
 0 0 6 441.88 14.71
 0 0 -7 25.33 3.25
 0 0 7 21.87 3.11
 0 0 -7 25.64 3.39
 0 0 7 25.4 3.04
 0 0 -8 8.68 2.11
 0 0 8 9.33 2.34
 0 0 -8 12.12 2.64
 0 0 8 11.11 2.33
 0 0 8 10.53 2.3
 0 0 9 95.77 7.53
 0 0 9 107.26 7.68
 0 0 -9 98.21 7.66
 0 0 9 102.51 7.16
 0 0 -10 169.91 10.67
 0 0 10 166.42 10.65
 0 0 10 195.86 11.2
 0 0 -10 166.99 10.76
 0 0 10 185.66 10.19
 0 0 11 407.9 18.25
 0 0 -11 449.23 18.88
 0 0 11 459.55 18.97
 0 0 -11 403.03 18.45
 0 0 11 426.81 17.28
 0 0 -12 136.55 10.41
 0 0 12 108.8 9.29
 0 0 12 133.88 10.11
 0 0 -12 112.45 9.72
 0 0 12 118.25 8.85
 0 0 -13 556.33 24.11
 0 0 13 576.96 22.21
 0 0 -14 100.33 10.06
 0 0 14 100.73 8.97
 0 0 -15 44 6.85
 0 0 15 43.21 6.06
 0 0 -16 131.67 12.51
 0 0 16 139.03 11.32
 0 0 -17 270.15 18.85
 0 0 17 279.46 16.89
 0 0 17 258.21 16.17
 0 0 -18 76.81 10.36
 0 0 18 74.2 8.91
 0 0 18 65.57 8.07
 0 0 -19 60.34 9.51
 0 0 19 81.14 9.36
 0 0 19 74.22 9.24
 0 0 -20 12.79 4.87
 0 0 20 12.32 4.56
 0 0 20 13.34 4.09
 0 0 21 146.16 13.82
 0 -1 21 523.66 27.26
 0 -1 21 493.76 26.28
 0 1 -20 292.02 22
 0 -1 20 272.18 18.97
 0 -1 20 274.7 18.7
 0 1 -19 42.48 8.21
 0 -1 19 40.68 6.87
 0 -1 19 60.62 8.39
 0 1 -18 173.38 15.41
 0 -1 18 187.19 14.08
 0 1 -17 610.94 29.05
 0 -1 17 622.41 26.4
 0 -1 16 458.83 23.67
 0 1 -16 462.18 24.02
 0 -1 16 465.23 21.67
 0 1 -15 24.29 5.21
 0 -1 15 24 4.97
 0 -1 15 25.98 4.24
 0 -1 15 28.97 4.83
 0 1 -14 96 9.69
 0 -1 14 94.71 9.66
 0 -1 14 106.18 8.29
 0 -1 14 120.35 9.69
 0 1 -13 47.24 6.36
 0 -1 13 36.23 5.42
 0 -1 13 40.45 4.76
 0 -1 13 41.6 5.43
 0 -1 12 207.28 13.23
 0 1 -12 209.18 12.95
 0 -1 12 253.62 13.72
 0 1 -12 210.01 13.25
 0 -1 12 245.76 12.98
 0 -1 11 141.23 9.61
 0 1 -11 125.77 9.55
 0 -1 11 123.77 7.83
 0 1 -11 123.74 9.23
 0 -1 11 119.49 9.43
 0 -1 10 313.24 14.05
 0 1 -10 290.17 14.33
 0 1 -10 287.42 14.11
 0 -1 10 282.27 14.23
 0 -1 9 208.43 10.77
 0 1 -9 211.09 11.27
 0 -1 9 198.3 11.12
 0 1 -8 330.07 13.81
 0 -1 8 352.79 13.56
 0 -1 8 332.38 14.01
 0 1 -7 219.53 10.2
 0 -1 7 216.6 9.64
 0 -1 7 199.63 10.02
 0 1 -6 1493.25 34.41
 0 -1 6 1573.12 34.23
 0 -1 6 1476.8 34.73
 0 1 -6 1432.56 34.09
 0 1 -5 267.03 9.79
 0 -1 5 270.7 9.58
 0 -1 5 251.69 8.18
 0 -1 5 264 10.09
 0 -1 4 2636.6 49.93
 0 1 -4 2487.22 50.09
 0 -1 4 2450.75 47.78
 0 -1 4 2591.88 50.77
 0 1 -3 596.84 14.81
 0 -1 3 575.86 13.16
 0 -1 -2 433.05 11.5
 0 -1 -2 450.99 11.02
 0 1 2 431.98 10.88
 0 -1 -3 3579.9 69.04
 0 -1 -3 3709.86 70.32
 0 1 3 3691.82 69.05
 0 -1 -3 3751.45 69.24
 0 -1 -4 112.02 5.63
 0 1 4 126.09 6.27
 0 -1 -4 117.86 6.15
 0 -1 -4 115.28 5.47
 0 1 4 118.56 5.53
 0 -1 -5 500.88 15.04
 0 -1 -5 521.34 16.14
 0 1 5 507.14 15.66
 0 1 5 518.55 14.78
 0 -1 -6 304.69 11.59
 0 -1 -6 321.96 12.58
 0 1 6 287.35 10.92
 0 -1 -7 26.13 3.24
 0 -1 -7 21.8 3.33
 0 1 7 28.67 3.4
 0 -1 -8 53.15 5.5
 0 1 8 56.57 5.41
 0 1 8 52.1 4.91
 0 -1 -9 1341.59 37.15
 0 1 9 1393.21 36.89
 0 1 9 1339.47 34.47
 0 -1 -10 277.05 13.86
 0 -1 -10 246.32 13.65
 0 1 10 236.39 13.1
 0 1 10 243.64 12.21
 0 -1 -11 1455.74 41.3
 0 -1 -11 1476.24 42.54
 0 1 11 1476.84 39.38
 0 -1 -12 19.09 4.24
 0 -1 -12 15.25 4.01
 0 1 12 20.35 3.79
 0 -1 -13 700.53 28.21
 0 1 13 733.42 25.89
 0 1 13 698.48 23.93
 0 -1 -14 275.53 17.3
 0 1 14 276.37 14.33
 0 1 14 308.27 16.38
 0 -1 -15 192.86 14.81
 0 1 15 189.12 11.96
 0 1 15 192.9 13.18
 0 -1 -16 210.32 16.29
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 10 0 -10 321.58 17.64
 -10 0 10 337.02 20.74
 10 0 -10 327.96 17.92
 10 0 -9 218.34 13.59
 -10 0 9 216.38 16.19
 10 0 -9 221.99 14.35
 10 0 -8 63.21 6.74
 10 0 -8 76.76 8.32
 -10 0 8 66.36 8.84
 10 0 -7 174.27 10.86
 10 0 -7 176.87 12.89
 10 0 -7 180.22 11.65
 10 0 -7 171.03 12.29
 -10 0 7 171.42 13.84
 10 0 -7 188.49 7.27
 10 0 -6 124.02 8.52
 10 0 -6 127.55 10.86
 10 0 -6 131.26 9.55
 10 0 -6 118.61 10.32
 -10 0 6 120.85 11.51
 10 0 -6 130.72 6.63
 10 0 -5 26.54 3.55
 10 0 -5 25.53 4.58
 10 0 -5 36.11 5.64
 -10 0 5 24.98 5.06
 10 0 -5 28.67 4.22
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 10 0 -4 200.95 9.62
 10 0 -4 208.11 14.05
 10 0 -4 194.95 13.46
 -10 0 4 213.69 14.62
 10 0 -4 203.05 9.87
 10 0 -4 202.5 11.67
 10 0 -3 226.71 9.26
 10 0 -3 212.42 11.26
 10 0 -3 222.25 14.76
 10 0 -3 228.17 14.82
 -10 0 3 210.27 14.36
 10 0 -3 214.92 10.91
 10 0 -2 16.06 2.33
 10 0 -2 16.12 1.93
 10 0 -2 13.03 3.64
 -10 0 2 11.61 3.38
 10 0 -2 14.23 2.79
 10 0 -1 211.07 6.18
 10 0 -1 216.25 6.08
 10 0 -1 238.49 15.26
 10 0 -1 187.81 10.91
 -10 0 1 199.78 13.28
 10 0 -1 212.85 12.03
 10 0 0 872.09 28.04
 -10 0 0 915.91 30.94
 10 0 0 866.62 28.91
 10 0 1 21.07 4
 10 0 1 18 4.12
 -10 0 -1 19.62 4.18
 -10 0 -1 22.05 6.09
 10 0 1 22.78 4.62
 10 0 2 1454.65 40.22
 -10 0 -2 1540.22 43.26
 10 0 2 1518.91 44.21
 -10 0 -2 1419.98 52.27
 10 0 3 109.26 10.36
 10 0 3 100.69 7.76
 -10 0 -3 110.75 9.52
 10 0 3 105.52 10.02
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 10 0 4 58.59 5.47
 10 0 4 52.43 7.06
 -10 0 -4 49.66 8.57
 10 0 4 50.81 7.08
 10 0 5 368.65 14.24
 10 0 5 389.72 20.2
 -10 0 -5 353.11 24.24
 10 0 5 337.24 19.86
 10 0 6 56.09 5.17
 10 0 6 58.09 7.61
 -10 0 -6 54.52 9.64
 10 0 6 46.71 7.63
 10 0 7 185.59 9.88
 10 0 7 194.06 14.18
 10 0 7 164.36 14.34
 -10 0 -7 159.78 16.69
 10 0 8 507.02 18.05
 10 0 8 509.46 24.4
 10 0 8 483.13 26.29
 -10 0 -8 462.13 29.86
 10 0 9 346.35 19.65
 -10 0 -9 296.08 24.01
 10 0 9 303.02 21
 10 0 10 29.65 5.86
 -10 0 -10 38.3 8.97
 10 0 10 41.69 8.03
 10 0 11 281.7 17.5
 -10 0 -11 284.03 24.08
 10 0 11 287.2 21.58
 -10 0 -12 741.11 41.26
 10 0 12 819.16 38.71
 10 1 -18 59.61 10.27
 -10 -1 18 56.46 10.11
 10 1 -17 90.49 12.21
 -10 -1 17 82.9 12.08
 10 1 -16 397.64 25.32
 -10 -1 16 408.12 26.92
 10 1 -16 429.59 21.37
 10 1 -15 80.32 10.65
 -10 -1 15 85.47 11.73
 10 1 -15 76.82 8.99
 10 1 -14 127.09 12.78
 -10 -1 14 131.59 14.29
 10 1 -14 132.66 11.39
 10 1 -13 108.53 11.44
 -10 -1 13 113.34 12.83
 10 1 -13 133.21 11.48
 10 1 -12 910.27 35.04
 -10 -1 12 902.74 38.23
 10 1 -12 979.76 34.41
 10 1 -11 336.47 19.06
 -10 -1 11 333.85 21.39
 10 1 -11 368.28 19.76
 10 1 -10 175.44 12.92
 -10 -1 10 189.14 15.54
 10 1 -10 183.16 13.44
 10 1 -9 663.97 25.79
 10 1 -9 695.75 27.71
 -10 -1 9 672.17 30.32
 10 1 -8 614.53 23.75
 10 1 -8 636.39 26.42
 10 1 -8 650.21 23.88
 10 1 -8 643.61 23.69
 -10 -1 8 616.7 28.39
 10 1 -8 662.81 18.26
 10 1 -7 26.54 4.45
 10 1 -7 25.27 4.9
 10 1 -7 29.68 4.4
 -10 -1 7 28.99 5.84
 10 1 -7 25.36 4.41
 10 1 -7 35.52 3.74
 10 1 -7 32.16 5.05
 10 1 -6 336.62 15.24
 10 1 -6 357.64 18.97
 10 1 -6 341.54 15.42
 10 1 -6 349.63 17.64
 -10 -1 6 347.5 19.92
 10 1 -6 351.42 17.38
 10 1 -6 337.61 13.02
 10 1 -5 196.51 10.47
 10 1 -5 194.13 12.61
 10 1 -5 188.4 13.41
 10 1 -5 194.54 10.83
 10 1 -5 181.59 12.69
 -10 -1 5 192.23 14.22
 10 1 -5 186.7 9.71
 10 1 -4 709.46 21.62
 10 1 -4 750.26 26.17
 10 1 -4 721.28 28.66
 10 1 -4 772.23 23.07
 10 1 -4 704.97 27.62
 -10 -1 4 717.99 29.17
 10 1 -4 715.02 22.52
 10 1 -3 244.92 12.18
 10 1 -3 224.74 9.88
 10 1 -3 238.72 15.39
 10 1 -3 227.54 10.86
 10 1 -3 238.54 15.05
 -10 -1 3 243.59 15.49
 10 1 -3 224.58 11.72
 10 1 -2 287.8 11.35
 10 1 -2 279.81 10.4
 10 1 -2 333.18 18.37
 -10 -1 2 301.67 17.01
 10 1 -2 294.45 14.14
 10 1 -1 422.81 12.34
 10 1 -1 430.08 12.1
 10 1 -1 400.71 15.96
 10 1 -1 465.1 22.01
 -10 -1 1 430.45 20.2
 10 1 -1 401.07 17.83
 -10 -1 1 395.62 24.38
 10 1 0 68.78 3.34
 10 1 0 60.73 3.24
 10 1 0 66.14 8.4
 10 1 0 63.5 5.88
 -10 -1 0 64.35 7.28
 10 1 0 59.94 6.71
 -10 -1 0 77.25 10.59
 10 1 1 1497.15 45.14
 10 1 1 1426.86 35.4
 -10 -1 -1 1431.14 41.19
 10 1 1 1392.05 41.28
 -10 -1 -1 1352.17 50.53
 10 1 2 21.85 2.94
 10 1 2 18.95 4.51
 -10 -1 -2 27.04 4.61
 10 1 2 24.01 4.67
 -10 -1 -2 25.41 6.73
 10 1 3 126.47 6.34
 10 1 3 128.66 11.55
 -10 -1 -3 128.15 10.08
 -10 -1 -3 135.94 14.62
 10 1 3 106.53 10.24
 10 1 4 234.4 8.86
 10 1 4 260.49 16.71
 -10 -1 -4 237.31 20.03
 10 1 4 232.11 15.99
 10 1 5 639.36 27.28
 -10 -1 -5 578.84 32.21
 10 1 5 559.1 26.03
 10 1 6 24.4 2.71
 10 1 6 41.68 6.79
 10 1 6 32.37 6.32
 -10 -1 -6 41.01 8.59
 10 1 7 11.89 4.02
 10 1 7 7.87 3.3
 -10 -1 -7 12.53 5.42
 10 1 8 51.94 7.49
 10 1 8 38.87 7.36
 -10 -1 -8 36.43 8.88
 10 1 9 265.4 17.03
 -10 -1 -9 259.03 22.95
 10 1 9 263.98 19.93
 10 1 10 9.88 4.25
 10 1 10 11.67 4.77
 -10 -1 -10 7.03 4.03
 -10 -1 -11 103.33 14.8
 10 1 11 71.11 10.64
 -10 -1 -12 34.35 8.99
 10 2 -18 102.8 13.71
 -10 -2 18 139.29 16.36
 10 2 -17 94.25 12.49
 -10 -2 17 121.09 15.04
 10 2 -16 848.38 38.8
 -10 -2 16 912.48 42.38
 10 2 -15 313.93 21.88
 -10 -2 15 344.98 24.21
 10 2 -14 233.85 18.01
 -10 -2 14 243.69 19.76
 10 2 -14 247.56 15.97
 10 2 -13 6.69 2.88
 -10 -2 13 11.88 4.46
 10 2 -13 12.92 4.2
 10 2 -12 160.53 13.49
 -10 -2 12 171.08 15.69
 10 2 -12 178.31 13.41
 10 2 -11 352.07 19.83
 -10 -2 11 390.63 23.54
 10 2 -11 374.07 19.82
 10 2 -10 122.07 10.93
 10 2 -10 139.8 11.79
 -10 -2 10 146.29 13.73
 10 2 -9 83.21 8.47
 10 2 -9 80.81 9.1
 -10 -2 9 85.85 10.33
 10 2 -9 67.25 7.22
 10 2 -9 80.06 8.85
 10 2 -8 327.21 16.99
 10 2 -8 367.68 16.5
 10 2 -8 385.93 20.51
 -10 -2 8 385.98 21.83
 10 2 -8 363.43 16.32
 10 2 -8 329.41 16.82
 10 2 -8 374.74 14.7
 10 2 -8 362.93 19.22
 10 2 -7 52.37 6.11
 10 2 -7 77.44 8.94
 10 2 -7 71.48 6.6
 10 2 -7 54.64 6.31
 -10 -2 7 60.66 8.26
 10 2 -7 66.45 7.81
 10 2 -7 55.57 6.56
 10 2 -7 60.79 5.64
 10 2 -6 43.95 5.31
 10 2 -6 40.72 6.31
 10 2 -6 51.39 5.26
 10 2 -6 55.84 7.63
 -10 -2 6 43.94 6.9
 10 2 -6 46.47 6
 10 2 -6 45.14 4.82
 10 2 -5 231.96 12.22
 10 2 -5 267.63 15.66
 10 2 -5 248.72 11.49
 10 2 -5 271.11 16.95
 10 2 -5 243.68 14.67
 -10 -2 5 231.16 15.81
 10 2 -5 258.37 12.35
 10 2 -4 448.45 20.09
 10 2 -4 461.31 17.16
 10 2 -4 509.99 23.85
 10 2 -4 483.69 16.2
 10 2 -4 462.91 21.55
 -10 -2 4 456.44 22.41
 10 2 -4 455 17.89
 10 2 -3 322.33 14.89
 10 2 -3 319.74 13.31
 10 2 -3 361.41 19.97
 10 2 -3 347.97 12.38
 10 2 -3 326.46 18.19
 -10 -2 3 297.89 17.59
 10 2 -3 317.41 14.98
 10 2 -2 729.25 22.24
 10 2 -2 730.22 21.32
 10 2 -2 737.02 21.59
 10 2 -2 824.42 31.65
 10 2 -2 825.23 20.18
 -10 -2 2 722.8 28.42
 10 2 -2 695.64 25
 -10 -2 2 714.66 33.6
 10 2 -1 28.94 3.32
 10 2 -1 27.13 3.17
 10 2 -1 44.01 7.15
 10 2 -1 31.66 3.52
 10 2 -1 33.83 2.88
 -10 -2 1 32.02 5.25
 -10 -2 1 28.86 6.39
 10 2 -1 25.96 4.4
 10 2 0 795.28 21.71
 10 2 0 841 21.73
 10 2 0 924.34 34.6
 10 2 0 903.8 20.82
 10 2 0 915.75 19.36
 -10 -2 0 828.32 29.41
 10 2 0 773.55 28.73
 -10 -2 0 785.55 37.02
 10 2 1 36.76 3.31
 10 2 1 43.32 3.42
 10 2 1 43.68 2.14
 10 2 1 45.95 7.11
 10 2 1 39.15 1.98
 -10 -2 -1 43.53 5.81
 -10 -2 -1 46.04 8.38
 10 2 1 38.11 5.83
 10 2 2 327.33 10.29
 10 2 2 277.54 10.06
 10 2 2 327.59 19.1
 -10 -2 -2 297.92 15.74
 -10 -2 -2 275 21.6
 10 2 2 258.09 16.1
 10 2 3 128.04 11.59
 -10 -2 -3 128.11 10.19
 -10 -2 -3 118.29 14.21
 10 2 3 98.06 9.96
 10 2 4 54.49 7.69
 -10 -2 -4 48.78 9.16
 10 2 4 44.52 6.85
 10 2 5 103.75 10.46
 -10 -2 -5 82.04 12.27
 10 2 5 100.79 10.82
 10 2 6 121.25 11.74
 -10 -2 -6 154.4 17.54
 10 2 6 125.56 12.77
 10 2 7 101.68 10.66
 -10 -2 -7 77.73 12.51
 10 2 7 88.7 10.91
 10 2 8 55.49 8.89
 -10 -2 -8 81.78 12.96
 10 2 9 34.07 7.25
 -10 -2 -9 45.87 10.31
 -10 -2 -10 238.08 23.37
 10 2 10 279.14 21.21
 -10 -2 -11 9.09 4.87
 10 3 -18 117.69 14.81
 10 3 -17 193.68 18.43
 -10 -3 17 174.2 18.51
 10 3 -16 169.12 16.75
 -10 -3 16 194.17 18.99
 10 3 -15 307.24 21.99
 -10 -3 15 320.06 23.93
 10 3 -14 40.68 7.57
 -10 -3 14 51.72 9
 10 3 -13 157.05 14.36
 -10 -3 13 180.19 16.74
 10 3 -12 328.65 20.5
 -10 -3 12 354.74 23.38
 10 3 -12 367.53 19.95
 10 3 -11 96.43 10.38
 -10 -3 11 98.46 11.77
 10 3 -11 108.9 10.54
 10 3 -10 55.73 7.57
 10 3 -10 61.21 8.08
 -10 -3 10 49.4 8.15
 10 3 -9 35 5.67
 10 3 -9 41.46 5.28
 10 3 -9 36.7 6.26
 -10 -3 9 30.62 6.24
 10 3 -9 38.36 4.76
 10 3 -8 369.92 18.98
 10 3 -8 408.7 22.05
 10 3 -8 420.71 17.1
 10 3 -8 427.03 21.6
 -10 -3 8 382.1 22.3
 10 3 -8 398.76 17.13
 10 3 -8 401.69 16.89
 10 3 -7 399.83 19.04
 10 3 -7 447.43 22.95
 10 3 -7 442.15 16.64
 10 3 -7 415.1 21.34
 -10 -3 7 383.56 21.94
 10 3 -7 375.62 17.75
 10 3 -7 391.98 16.66
 10 3 -6 445.92 19.85
 10 3 -6 537.08 24.68
 10 3 -6 516.07 17.41
 10 3 -6 509.75 24.05
 10 3 -6 476.89 21
 -10 -3 6 453.92 23.68
 10 3 -6 467.28 18.77
 10 3 -5 1054.21 35.89
 10 3 -5 941.88 30.72
 10 3 -5 1127.63 27.62
 10 3 -5 1030.69 36.65
 10 3 -5 1035.35 34.57
 -10 -3 5 1054.4 37.48
 10 3 -5 975.01 30.31
 10 3 -4 330.55 17.29
 10 3 -4 309.21 15.07
 10 3 -4 372.9 12.41
 10 3 -4 343.9 19.4
 10 3 -4 333.25 18.2
 -10 -3 4 342.19 19.28
 10 3 -4 334.83 15.89
 10 3 -3 1254.46 36.41
 10 3 -3 1177.17 34.62
 10 3 -3 1322.99 42.84
 -10 -3 3 1256.75 41.1
 10 3 -3 1189.29 36.42
 -10 -3 3 1300.62 47.11
 10 3 -2 64.79 6.11
 10 3 -2 55.59 5.66
 10 3 -2 69.76 3.29
 10 3 -2 72.51 9.03
 10 3 -2 71.52 4.03
 -10 -3 2 63.4 7.79
 10 3 -2 62.56 6.91
 -10 -3 2 59.7 9.14
 10 3 -1 704.14 23.11
 10 3 -1 773.49 23.24
 -10 -3 1 776.69 28.75
 10 3 -1 725.05 27.02
 -10 -3 1 746.45 35.31
 10 3 0 185.99 10.32
 10 3 0 205.59 10.01
 10 3 0 213.71 15.19
 -10 -3 0 205.71 13.1
 -10 -3 0 183.53 17
 10 3 0 190.97 13.15
 10 3 1 198.33 9.57
 10 3 1 208.11 15.12
 -10 -3 -1 202.21 12.77
 -10 -3 -1 180.67 17.39
 10 3 1 194.63 13.63
 10 3 2 306.46 18.5
 -10 -3 -2 295 15.6
 -10 -3 -2 285.43 22.67
 10 3 2 265.55 16.68
 10 3 3 12.96 4.28
 -10 -3 -3 5.75 2.04
 -10 -3 -3 5.12 2.14
 10 3 3 5.17 2.68
 10 3 4 266.96 17.66
 -10 -3 -4 245.44 22.12
 10 3 4 259.76 17.63
 -10 -3 -5 58.38 11.08
 10 3 5 56.27 8.7
 -10 -3 -6 424.45 30.48
 10 3 6 452.64 25
 -10 -3 -7 93.58 14.45
 10 3 7 94.45 11.41
 -10 -3 -8 77.04 13.25
 10 3 8 71.87 10.21
 -10 -3 -9 248.72 24.47
 10 3 9 262.87 20.61
 -10 -3 -10 181.47 21.1
 10 4 -18 65.7 11.39
 10 4 -17 99.53 13.48
 -10 -4 17 142.64 16.81
 10 4 -16 331.08 24.32
 -10 -4 16 376.28 27.2
 10 4 -15 57.21 9.58
 -10 -4 15 46.3 8.67
 10 4 -14 20.24 5.8
 -10 -4 14 8.14 3.82
 10 4 -13 135.57 13.86
 -10 -4 13 149.9 15.58
 10 4 -12 812.61 34.96
 -10 -4 12 874.07 38.94
 10 4 -11 119.76 12.12
 -10 -4 11 134.72 14.24
 10 4 -10 352.65 20.77
 -10 -4 10 391.57 24.06
 10 4 -10 431.45 18.65
 10 4 -9 50.48 7.24
 10 4 -9 67.82 6.55
 -10 -4 9 58.7 8.79
 10 4 -9 61.29 6.72
 10 4 -8 307.81 18.02
 10 4 -8 318.96 18.87
 10 4 -8 357.04 14.87
 -10 -4 8 324.56 20.66
 10 4 -8 307.46 15.66
 -10 -4 8 325.48 15.91
 10 4 -7 164.4 12.53
 10 4 -7 191.74 15.21
 10 4 -7 174.72 13.87
 10 4 -7 209.66 10.41
 -10 -4 7 168.7 14.2
 10 4 -7 176.97 11.79
 10 4 -7 183.2 11.62
 -10 -4 7 169.01 11.6
 10 4 -6 1398.41 44.11
 10 4 -6 1151.71 37.75
 10 4 -6 1347 31.37
 10 4 -6 1187.45 40.95
 10 4 -6 1238.64 38.1
 -10 -4 6 1195.56 41.95
 10 4 -6 1131.37 35.15
 -10 -4 6 1134.07 36.51
 10 4 -5 22.33 4.65
 10 4 -5 21.3 4.7
 10 4 -5 23.04 2.78
 10 4 -5 24.13 6.04
 10 4 -5 25.9 5.02
 -10 -4 5 12.78 4.01
 10 4 -5 22.26 4.18
 -10 -4 5 16.44 3.88
 10 4 -4 542.11 23.47
 10 4 -4 477.96 21.32
 10 4 -4 577.49 14.25
 10 4 -4 558.38 25.86
 10 4 -4 496.03 23.42
 -10 -4 4 526.64 24.78
 10 4 -4 506.12 21.44
 10 4 -3 181.9 12.04
 10 4 -3 172.11 11.83
 10 4 -3 208.04 15.26
 -10 -4 3 191.94 14.04
 -10 -4 3 192.25 16.41
 10 4 -3 187.44 12.45
 10 4 -2 620.87 24.38
 10 4 -2 708.98 24.38
 10 4 -2 709.1 29.83
 -10 -4 2 696.31 27.77
 10 4 -2 681.27 26.24
 -10 -4 2 686.27 33.32
 10 4 -1 18.25 3.51
 -10 -4 1 20.89 4.56
 -10 -4 1 25.79 6.58
 10 4 -1 25.63 5.08
 -10 -4 0 1408.79 40.56
 -10 -4 0 1361.02 52.52
 10 4 0 1294.37 41.5
 -10 -4 -1 1198.18 35.87
 -10 -4 -1 1124.47 48.22
 10 4 1 1098.11 38.05
 -10 -4 -2 70.9 7.37
 -10 -4 -2 56.22 10.62
 10 4 2 68.19 8.63
 -10 -4 -3 181.36 18.91
 10 4 3 161.63 13.69
 -10 -4 -3 181.3 14.47
 -10 -4 -4 267.97 23.8
 10 4 4 281.73 18.8
 -10 -4 -5 744.4 41.82
 10 4 5 782.77 33.77
 -10 -4 -6 244.33 23.74
 10 4 6 195.78 16.8
 -10 -4 -7 476.16 34.12
 10 4 7 472.27 26.88
 -10 -4 -8 184.56 21.29
 10 4 8 136.69 14.56
 -10 -4 -9 11.89 5.38
 10 5 -17 57.97 11.02
 -10 -5 17 61.58 11.65
 10 5 -16 461.06 30.03
 -10 -5 16 582.45 35.12
 10 5 -15 100.22 13.15
 -10 -5 15 111.56 14.62
 10 5 -14 101.77 12.92
 -10 -5 14 116.19 14.38
 10 5 -13 31.91 7.71
 -10 -5 13 45.8 8.8
 10 5 -12 282.24 20.32
 -10 -5 12 319.29 23.05
 10 5 -11 113.37 12.29
 -10 -5 11 107.11 12.94
 10 5 -10 144.39 13.53
 -10 -5 10 150.04 15.07
 10 5 -10 169.59 12.14
 10 5 -9 28.62 5.87
 -10 -5 9 26.24 6.35
 10 5 -9 32.65 5.33
 10 5 -8 96.75 10.53
 -10 -5 8 106.5 11.82
 10 5 -8 104.22 9.47
 10 5 -7 225.32 15.95
 -10 -5 7 238.77 17.4
 10 5 -7 238.36 14.35
 10 5 -6 33.38 5.92
 -10 -5 6 24.27 5.45
 10 5 -6 38.28 5.71
 10 5 -5 56.28 7.65
 10 5 -5 42.39 6.47
 -10 -5 5 50.09 7.4
 10 5 -5 49.44 6.39
 10 5 -4 110.45 10.36
 10 5 -4 91.78 9.51
 -10 -5 4 108.51 10.74
 10 5 -4 89.21 8.76
 -10 -5 4 102.93 11.58
 10 5 -3 37.45 5.67
 10 5 -3 41.81 6.41
 -10 -5 3 40.42 6.53
 10 5 -3 38.43 5.92
 -10 -5 3 53.7 8.86
 -10 -5 2 355.74 19.16
 -10 -5 2 366.25 24.13
 10 5 -2 333.78 18.5
 -10 -5 1 542.22 23.49
 -10 -5 1 582.74 31.96
 10 5 -1 518.76 24.05
 -10 -5 0 19.01 4.61
 -10 -5 0 15.54 6.25
 10 5 0 22.57 5.26
 -10 -5 -1 805.21 27.78
 -10 -5 -1 756.19 39.25
 10 5 1 758.24 31.15
 -10 -5 -2 280.26 14.81
 -10 -5 -2 222.98 21.3
 10 5 2 231.6 16.65
 -10 -5 -2 283.15 19.77
 -10 -5 -3 18.77 5.9
 -10 -5 -3 12.5 5.46
 10 5 3 11.19 3.89
 -10 -5 -4 120.43 16.26
 10 5 4 123.31 12.53
 -10 -5 -5 416 31.64
 10 5 5 415.69 24.43
 -10 -5 -6 6.08 4.72
 10 5 6 10.4 4.27
 -10 -5 -7 421.94 33.7
 -10 -5 -8 70.28 13.83
 10 6 -17 98.38 14.06
 10 6 -16 558.75 34.4
 -10 -6 16 656.06 38.72
 10 6 -15 114.18 14.59
 -10 -6 15 154.72 17.61
 10 6 -14 121.78 14.57
 -10 -6 14 160.4 17.59
 10 6 -13 11.9 4.7
 -10 -6 13 10.31 4.4
 10 6 -12 265.12 20.55
 -10 -6 12 315.5 23.53
 10 6 -11 12.48 5.18
 -10 -6 11 16.67 5.31
 10 6 -10 338 22.51
 -10 -6 10 388.97 25.04
 10 6 -10 410.58 20.65
 10 6 -9 137.39 13.85
 -10 -6 9 167.11 15.74
 10 6 -9 166.7 12.79
 10 6 -8 187.7 15.8
 -10 -6 8 207.25 17.02
 10 6 -8 207.31 14.22
 10 6 -7 339.27 21.47
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 10 6 -7 399.57 20.18
 10 6 -6 79.09 9.77
 -10 -6 6 103.07 11.24
 10 6 -6 93.53 9.38
 10 6 -5 251.45 17.72
 -10 -6 5 280.51 18.52
 10 6 -5 277.62 16.75
 -10 -6 4 3.26 2.39
 -10 -6 4 0.68 1.93
 10 6 -4 -0.56 1.58
 -10 -6 3 328.4 19.12
 10 6 -3 301.77 18.08
 -10 -6 2 67.24 8.1
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 10 6 -2 59.8 7.89
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 10 6 -1 80.52 9.3
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 10 6 4 61.87 9.21
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 -10 -6 -5 149.67 19.62
 -10 -6 -6 45.59 11.02
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 10 7 -16 140.98 17.18
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 10 7 -15 365.26 27.62
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 10 7 -14 173.27 18.28
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 10 7 -13 263.17 22.22
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 10 7 -12 34.69 7.85
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 10 7 -11 202.8 18.55
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 10 7 -11 268.27 17.34
 10 7 -10 38.22 8.03
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 10 7 -10 34.7 6.17
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 10 7 -9 290.38 18.04
 10 7 -8 262.39 20.08
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 10 7 -8 332.07 19.25
 10 7 -7 61.21 9.33
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 10 7 -7 57.34 7.94
 10 7 -6 417.04 25.2
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 10 7 -2 71.98 9.13
 10 7 -1 33.95 6.41
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 10 8 -11 27.73 7.64
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 10 8 -10 51.74 9.76
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 10 8 -10 80.01 9.81
 10 8 -9 99.9 12.99
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 10 8 -9 129.82 12.52
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 10 8 -8 262.4 17.95
 10 8 -7 570.63 31.69
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 10 8 -7 649.06 29.4
 -10 -8 6 206.92 17.07
 10 8 -6 213.85 16.21
 -10 -8 5 134.08 13.36
 10 8 -5 123.84 12.47
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 -10 -8 4 82.68 10.75
 10 8 -4 63.2 8.84
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 10 8 -3 75.66 9.85
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 10 8 -2 276.67 19.29
 10 8 -1 7.72 3.33
 -10 -8 1 19.48 6.54
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 10 8 0 61.66 9.13
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 10 8 1 129.37 13.63
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 -10 -8 -3 37.05 10.38
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 10 9 -14 111.88 15.89
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 10 9 -13 21.55 7.49
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 10 9 -12 38.33 8.81
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 10 9 -11 46.39 9.73
 -10 -9 11 40.77 9.23
 10 9 -11 49.47 8.09
 10 9 -10 133.61 15.93
 -10 -9 10 149.88 16.74
 10 9 -10 169.77 15.2
 10 9 -9 379.11 26.96
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 10 9 -9 426.81 24.61
 10 9 -8 158.27 16.79
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 10 9 -8 167.32 15.09
 10 9 -7 552.75 32.11
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 10 9 -7 593.73 29.5
 -10 -9 6 148.29 14.83
 10 9 -6 129.88 13.19
 10 9 -5 112.91 12.46
 10 9 -4 26.04 6.18
 10 9 -3 31.61 6.88
 -10 -9 2 57.15 10.4
 10 9 -2 47.74 8.42
 -10 -9 1 159.77 18.02
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 -10 -9 0 96.07 14.3
 -10 -9 -1 52.82 11.46
 -10 -9 -2 190.26 21.9
 -10 -9 -3 71.59 14.05
 -10 -10 13 26.48 8.12
 10 10 -12 12.69 5.5
 -10 -10 12 5.7 3.98
 10 10 -11 126.38 16.15
 -10 -10 11 105.22 14.91
 10 10 -11 141.85 14.37
 10 10 -10 146.98 17.05
 -10 -10 10 138.42 16.5
 10 10 -10 156.52 15.21
 10 10 -9 43.42 8.92
 -10 -10 9 39.14 8.43
 10 10 -9 48 8.56
 10 10 -8 143.87 16.45
 -10 -10 8 134.81 15.41
 10 10 -8 128.72 14.09
 10 10 -7 114.82 12.99
 10 10 -6 82.67 11.08
 10 10 -5 40.67 7.84
 -10 -11 12 96.04 14.78
 -10 -11 11 135 17.19
 11 -11 -5 8.45 3.78
 11 -11 -4 35.19 7.28
 -11 11 4 64.1 12.29
 11 -11 -3 115.95 12.71
 -11 11 3 135.2 17.96
 -11 11 2 31.34 8.62
 -11 11 1 1.27 2.91
 -11 11 0 19.2 6.93
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 -11 11 -2 18.27 6.65
 11 -11 2 33.93 8.24
 -11 11 -3 75.83 13.27
 11 -11 3 91.06 12.55
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 11 -11 4 116.84 14.45
 -11 11 -5 11.62 5.32
 11 -11 5 10.14 4.8
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 11 -11 6 90.78 13.45
 -11 11 -7 51.49 11.22
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 11 -10 -8 181.29 17.04
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 11 -10 -7 556.09 30.11
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 11 -10 -6 193.35 16.73
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 11 -10 -5 66.51 9.4
 -11 10 5 69.54 12.51
 11 -10 -4 38.97 7.18
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 11 -10 -3 24.28 5.49
 -11 10 3 29.22 8.32
 11 -10 -2 55.86 8.04
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 11 -10 -1 109.62 10.93
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 11 -10 -1 104.92 12.7
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 11 -10 0 311.23 22.3
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 11 -10 1 38.85 7.98
 -11 10 -2 129.95 16.85
 11 -10 2 116.03 13.68
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 11 -10 3 199.17 18.17
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 11 -10 4 517.32 30.14
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 11 -10 5 85.4 12.45
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 11 -10 6 83.57 12.34
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 11 -10 7 119.77 15.04
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 11 -10 8 395.65 28.18
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 11 -10 9 33.01 8.04
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 11 -10 10 190.8 19.72
 -11 9 11 27.69 6.33
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 11 -9 -9 128.69 14.05
 -11 9 9 120.65 15.71
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 11 -9 -8 357.07 23.1
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 11 -9 -7 8.55 4.05
 -11 9 7 6.62 3.28
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 11 -9 -6 515.52 26.68
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 -11 9 6 528.94 26.01
 11 -9 -5 84.56 9.96
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 11 -9 -4 243.02 16.58
 -11 9 4 198.77 19.72
 11 -9 -3 3.73 2.17
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 11 -9 -2 513.42 23.75
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 11 -9 -1 78.04 8.54
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 11 -9 -1 75.32 10.26
 11 -9 0 221.06 14.29
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 11 -9 1 185.62 16.45
 -11 9 -2 496.38 32.08
 11 -9 2 470.96 27.54
 -11 9 -3 79.69 12.43
 11 -9 3 81.12 11.05
 -11 9 -4 1013.9 48.1
 11 -9 4 1033.71 43.29
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 11 -9 5 315.21 23.28
 -11 9 -6 138.64 16.89
 11 -9 6 110.34 13.92
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 11 -9 7 134.26 15.58
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 11 -9 8 125.97 15.29
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 11 -9 9 42.64 9.22
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 11 -9 10 202.93 19.97
 -11 9 -11 11.15 4.95
 11 -9 11 22.35 6.9
 11 -9 12 98.53 14.3
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 -11 8 12 18.84 4.94
 11 -8 -11 3.96 2.53
 -11 8 11 0.63 2.17
 -11 8 11 -3.4 3.93
 11 -8 -11 -1.2 2.5
 11 -8 -10 61.88 9.67
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 11 -8 -10 61.13 9.23
 11 -8 -9 19.58 5.71
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 11 -8 -9 23.91 5.85
 11 -8 -8 57.74 8.76
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 11 -8 -7 28.37 5.81
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 11 -8 -6 4.84 2.75
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 11 -8 -5 46.14 7.04
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 -11 8 5 33.03 7.48
 11 -8 -4 31.13 5.74
 -11 8 4 22.31 5
 -11 8 4 17.26 6.2
 11 -8 -3 533.41 23.33
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 11 -8 -2 11.57 3.26
 -11 8 2 6.37 3.97
 11 -8 -1 730.79 26.44
 -11 8 1 671.81 35.77
 11 -8 0 71.36 7.26
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 11 -8 0 64.53 9.15
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 11 -8 1 13.64 4.41
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 11 -8 2 68 9.54
 -11 8 -3 506.4 30.86
 11 -8 3 506.41 27.75
 -11 8 -4 75.65 11.79
 11 -8 4 68.19 10
 -11 8 -5 599.14 34.33
 11 -8 5 604.16 31.89
 -11 8 -6 105.97 14.14
 11 -8 6 114.41 13.82
 -11 8 -7 570.02 34.05
 11 -8 7 581.78 32.88
 -11 8 -8 473.2 31.26
 11 -8 8 461.36 29.59
 -11 8 -9 63.21 11.53
 11 -8 9 91.95 12.94
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 11 -8 10 1007.51 46.18
 -11 8 -11 149.39 18.15
 11 -8 11 156.88 17.29
 11 -8 12 30.82 6.31
 11 -8 12 31.52 8.1
 11 -8 13 159.65 17.54
 11 -8 13 146.4 13.85
 11 -8 14 140.79 16.92
 11 -8 14 105.31 11.71
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 11 -7 -12 221.23 18.49
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 11 -7 -11 159.51 15.17
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 11 -7 -11 158.52 14.3
 11 -7 -10 193.66 16.21
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 11 -7 -10 181.17 15.3
 11 -7 -9 15.59 4.78
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 11 -7 -9 8.65 3.22
 11 -7 -8 69.12 8.95
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 11 -7 -8 66.26 9.18
 11 -7 -7 147.49 12.69
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 11 -7 -7 148.43 13.64
 11 -7 -6 120.93 11.02
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 -11 7 6 114.42 11.22
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 -11 7 5 28.15 6.62
 11 -7 -4 56.75 6.93
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 11 -7 -3 124.7 9.94
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 11 -7 -2 247.21 13.46
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 11 -7 -1 5.05 2
 -11 7 1 8.59 3.42
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 11 -7 0 309.65 14.35
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 11 -7 0 302.14 19.51
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 11 -7 1 93.69 10.63
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 11 -7 2 406.51 23.29
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 11 -7 3 148.54 14.23
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 11 -7 4 28.14 6.47
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 11 -7 5 138.7 14.57
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 11 -7 6 83.12 11.91
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 11 -7 7 165.9 16.77
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 11 -7 8 887.36 41.08
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 11 -7 9 260.75 17.78
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 11 -7 11 270.75 22.06
 11 -7 11 243.48 17.32
 11 -7 12 194.5 18.59
 11 -7 12 164.19 14.29
 11 -7 13 31.91 6.37
 11 -7 13 24.27 6.93
 11 -7 14 208.17 19.67
 11 -7 14 188.19 15.57
 11 -7 15 26.38 7.42
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 11 -6 -12 119.69 13.26
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 11 -6 -12 133.78 12.67
 11 -6 -11 49.75 8.1
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 11 -6 -11 59.02 8.51
 11 -6 -10 13.69 4.16
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 11 -6 -10 10.89 3.61
 11 -6 -9 431.05 22.93
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 11 -6 -9 412.36 23.08
 11 -6 -8 461.02 23.01
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 11 -6 -7 62.36 7.64
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 11 -6 -7 47.1 7.59
 11 -6 -6 57.23 7.05
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 11 -6 -5 7.57 2.61
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 11 -6 -4 265.82 17.92
 11 -6 -3 32.34 4.47
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 11 -6 -1 193.08 13.67
 11 -6 0 440 22.66
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 11 -6 1 718.76 29.73
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 11 -6 2 14.06 3.91
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 11 -6 4 234.39 18.01
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 11 -6 6 30.22 6.83
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 11 -6 7 64.27 10.47
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 11 -6 10 60.31 8.28
 11 -6 11 108.03 13.38
 11 -6 11 116.09 11.67
 11 -6 12 97 12.63
 11 -6 12 105.45 11.2
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 11 -6 13 143.77 15.57
 11 -6 13 147.3 13.4
 11 -6 14 17.56 5.81
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 11 -5 -8 600.27 25.8
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 11 -5 0 27.18 2.52
 11 -5 0 18.52 4.25
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 11 -5 1 117.75 11.26
 11 -5 1 130.19 11.79
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 11 -5 2 19.47 4.37
 11 -5 2 21.91 5.08
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 11 -5 3 25.75 5.46
 11 -5 3 22 4.62
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 11 -5 4 162.19 13.31
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 11 -5 5 4.84 2.62
 11 -5 5 1.73 1.83
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 11 -5 6 581.06 26.47
 11 -5 6 551.41 29.71
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 11 -5 7 21.05 4.82
 11 -5 7 22.05 5.88
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 11 -5 8 11.09 3.67
 11 -5 8 5.85 3.23
 11 -5 8 8.16 3.71
 11 -5 9 35.75 6.49
 11 -5 9 41.73 7.94
 11 -5 9 35.49 7.24
 11 -5 10 865.39 37.7
 11 -5 10 830.47 33.41
 11 -5 10 796.42 35.64
 11 -5 11 5.45 2.93
 11 -5 11 14.06 4.28
 -11 5 -11 11.98 4.97
 11 -5 11 13.46 4.86
 11 -5 12 420.05 25.39
 11 -5 12 448.83 23.81
 11 -5 12 370.3 24.61
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 11 -5 13 67.69 9.02
 11 -5 13 64.47 9.86
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 11 -5 14 33.59 7.37
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 11 -4 -12 169.11 13.86
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 11 -4 -11 512.01 25.06
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 11 -4 -10 334.97 19.77
 11 -4 -9 729.33 29.21
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 11 -4 -9 785.89 31.82
 11 -4 -8 76.14 8.11
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 11 -4 -8 70.05 8.83
 11 -4 -7 294.13 15.78
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 14 -3 2 525.24 28.59
 14 -3 2 480.89 24.29
 14 -3 3 44.86 8.55
 14 -3 3 34.86 6.68
 14 -3 4 295.81 21.1
 14 -3 4 251.42 18.23
 14 -3 5 6.83 3.94
 14 -3 5 6.72 3.52
 14 -3 6 209.99 17.83
 14 -3 6 206.57 17.32
 14 -3 7 15.29 5.26
 14 -2 -10 76.85 10.67
 14 -2 -9 26.64 6.03
 -14 2 9 21.41 5.78
 14 -2 -8 46.99 8.14
 -14 2 8 49.87 8.85
 14 -2 -7 257.78 19.74
 -14 2 7 241.64 19.21
 14 -2 -6 98.68 12.12
 -14 2 6 116.18 12.96
 14 -2 -5 11.22 3.79
 -14 2 5 10.01 3.77
 14 -2 -4 325.39 22.49
 -14 2 4 316.51 21.34
 14 -2 -3 4.15 2.05
 -14 2 3 1.47 1.99
 14 -2 -2 1300.36 47.71
 -14 2 2 1228.8 44.62
 14 -2 -1 20.53 5.71
 14 -2 -1 21.87 5.09
 -14 2 1 14.87 4.92
 14 -2 0 240.83 18.98
 -14 2 0 224.26 17.29
 14 -2 0 236.91 15.4
 14 -2 1 0.71 2.54
 -14 2 -1 0.56 2.14
 14 -2 1 -2.19 3.05
 14 -2 2 155.55 15.2
 14 -2 2 152.06 13.25
 14 -2 3 -3.97 3.89
 14 -2 3 2.48 2.06
 14 -2 4 213.53 18.06
 14 -2 4 203.19 16.48
 14 -2 5 16.64 4.7
 14 -2 5 12.88 4.67
 14 -2 6 68.07 10.16
 14 -2 6 65.57 9.84
 14 -1 -10 0.43 2.29
 14 -1 -9 72 10.09
 -14 1 9 71.58 10.92
 14 -1 -8 388.55 24.71
 -14 1 8 374.85 24.92
 14 -1 -7 255.63 19.86
 -14 1 7 316.26 22.28
 14 -1 -6 406.42 25.61
 -14 1 6 565.03 29.53
 14 -1 -5 327.48 22.72
 -14 1 5 349.88 22.77
 14 -1 -4 164.82 15.98
 -14 1 4 178.1 15.82
 14 -1 -3 236.11 19.01
 -14 1 3 240.64 18.35
 14 -1 -2 89.99 11.58
 -14 1 2 63.7 9.21
 14 -1 -1 101.79 12.21
 -14 1 1 118.53 12.43
 14 -1 -1 116 10.29
 14 -1 0 41.74 8.03
 -14 1 0 31.93 6.45
 14 -1 0 37.32 6.14
 14 -1 1 176.87 16.36
 -14 1 -1 171.64 15.03
 14 -1 1 146.37 12.78
 14 -1 2 41.25 7.78
 14 -1 2 33.56 6.41
 14 -1 3 149.63 15.09
 14 -1 3 131.32 13.03
 14 -1 4 158.54 15.7
 14 -1 4 150.89 14.34
 14 -1 5 90.18 11.81
 14 -1 5 82.88 10.83
 14 -1 6 25.37 6.37
 -14 0 10 79.97 11.82
 14 0 -9 131.56 14.13
 -14 0 9 105.19 13.33
 14 0 -8 290.16 21.42
 -14 0 8 271.76 21.45
 14 0 -7 138.92 14.61
 -14 0 7 133.56 14.49
 14 0 -6 1278.35 49.34
 -14 0 6 1383.73 50.64
 14 0 -5 71.75 10.62
 -14 0 5 74.35 10.56
 14 0 -4 1132.98 45.21
 -14 0 4 1083.69 42.83
 14 0 -3 637.88 32.32
 -14 0 3 564.83 29.17
 14 0 -2 54.15 9.17
 -14 0 2 71.84 9.89
 14 0 -2 49.05 6.56
 14 0 -1 176.49 16.64
 -14 0 1 182.2 15.44
 14 0 -1 151.25 12.17
 14 0 0 120.62 13.75
 -14 0 0 109.74 11.9
 14 0 0 113.62 10.95
 14 0 1 61.47 9.84
 -14 0 -1 60.41 8.85
 14 0 1 45.61 7.4
 14 0 2 241.75 19.67
 14 0 2 197.78 15.84
 14 0 3 79 11.58
 14 0 3 70.68 9.7
 14 0 4 141.94 14.27
 14 0 5 1.25 2.53
 -14 -1 10 415.6 27.81
 -14 -1 9 63.14 10.75
 14 1 -8 55.62 9.5
 -14 -1 8 36.86 8
 14 1 -7 305.96 22.72
 -14 -1 7 251.1 20.47
 14 1 -6 492.91 29.4
 -14 -1 6 413.73 26.02
 14 1 -5 963.23 42.47
 -14 -1 5 813.9 37.24
 14 1 -4 11.97 5.76
 -14 -1 4 5.85 3.24
 14 1 -3 564.59 31.67
 -14 -1 3 453.85 26.01
 14 1 -2 432.14 27.63
 -14 -1 2 381.57 23.29
 14 1 -2 389.7 20.01
 14 1 -1 117.95 14.29
 -14 -1 1 126.56 13.02
 14 1 -1 104.75 10.4
 14 1 0 94.44 12.48
 -14 -1 0 79.45 10.14
 14 1 0 74.41 9.11
 14 1 1 26.32 7.16
 -14 -1 -1 19.91 5.17
 14 1 1 10.83 4.08
 14 1 2 57.11 8.61
 -14 -1 -3 11.71 7.01
 14 1 3 18.53 5.44
 -14 -1 -4 29.23 9.32
 14 1 4 35.73 7.29
 -14 -2 10 560.09 33.19
 -14 -2 9 238.94 20.72
 -14 -2 8 147.81 15.9
 -14 -2 7 24.39 6.04
 -14 -2 6 53.61 9.35
 -14 -2 5 65.67 9.96
 -14 -2 4 45.46 8.25
 -14 -2 3 24.11 5.47
 -14 -2 2 156.17 14.66
 14 2 -2 181.36 13.84
 -14 -2 1 75.38 9.98
 14 2 -1 65.78 8.57
 -14 -2 0 97.47 11.35
 14 2 0 75.95 9.73
 -14 -2 -1 28.48 5.97
 14 2 1 24.16 5.79
 -14 -2 -2 7.36 4.37
 14 2 2 7.21 3.57
 -14 -2 -3 74.25 14.33
 14 2 3 69.84 10.05
 -14 -3 9 209.62 19.72
 -14 -3 8 19.06 5.46
 -14 -3 7 351.29 24.77
 -14 -3 6 406.67 26.37
 -14 -3 5 232.15 19.21
 -14 -3 4 438.21 26.19
 -14 -3 3 53.27 8.77
 -14 -3 2 69.41 9.75
 14 3 -2 77.42 9.44
 -14 -3 1 245.03 18.49
 14 3 -1 250.51 17.54
 -14 -3 0 859.37 36.22
 14 3 0 813.99 34.64
 14 3 1 178.34 15.7
 -14 -3 -1 201.69 23.72
 -14 -3 -2 16.14 6.65
 14 3 2 18.15 5.45
 -14 -4 9 46.04 9.55
 -14 -4 8 20.79 6.19
 -14 -4 7 77.44 11.68
 -14 -4 6 589.1 32.8
 -14 -4 5 235.47 19.57
 -14 -4 4 307.3 21.93
 -14 -4 3 136.63 14.03
 14 4 -3 120.1 11.94
 -14 -4 2 233.99 18.28
 14 4 -2 225.15 16.72
 14 4 -1 29.58 6.64
 14 4 0 439.46 25.56
 -14 -4 0 541.38 38.81
 -14 -4 -1 69.16 14.36
 -14 -5 9 71.75 12
 -14 -5 8 235.84 21.3
 -14 -5 7 28.8 7.36
 -14 -5 6 28.78 6.91
 -14 -5 5 115 13.79
 -14 -5 4 18.16 5.12
 14 5 -3 30.21 6.65
 14 5 -2 109.9 12.06
 14 5 -1 44.64 8.04
 -14 -5 0 91.6 15.98
 -14 -6 8 268.93 23.33
 -14 -6 7 50.85 9.71
 -14 -6 6 18.19 5.62
 -15 7 5 124.51 14.2
 -15 7 4 163.91 16.37
 -15 7 3 97.3 12.69
 -15 7 2 19.43 5.89
 -15 7 1 67.07 10.96
 -15 7 0 69.25 11.28
 15 -7 1 17.27 5.43
 15 -7 2 107.21 13.78
 15 -7 3 85.15 12.7
 15 -7 4 -0.01 3.42
 -15 6 5 46.28 8.35
 -15 6 4 17.14 5.55
 15 -6 -3 42.37 7.67
 -15 6 3 59.81 9.43
 15 -6 -2 110.63 12.71
 -15 6 2 137.44 14.64
 15 -6 -1 55.18 9.1
 -15 6 1 49.45 8.9
 15 -6 0 46.89 8.53
 -15 6 0 35.97 7.83
 15 -6 1 49.73 9.21
 -15 6 -1 54.84 9.69
 15 -6 2 -0.59 2.97
 -15 6 -2 5.5 3.75
 15 -6 3 12.63 5.24
 -15 5 5 320.56 21.1
 -15 5 4 1.96 1.63
 15 -5 -3 126.14 13
 -15 5 3 161.36 15.06
 15 -5 -2 20.51 5.5
 -15 5 2 25.23 6.07
 15 -5 -1 58.66 9.32
 -15 5 1 66.19 10.09
 15 -5 0 40.78 7.82
 -15 5 0 50.48 8.84
 15 -5 1 88.94 11.74
 15 -5 4 167.99 14.74
 15 -5 5 66.03 9.46
 15 -5 6 53.93 8.8
 -15 4 5 466.57 25.02
 -15 4 4 497.77 26.38
 15 -4 -3 43.64 7.35
 15 -4 -2 26.01 5.93
 15 -4 -1 5.95 2.86
 -15 4 1 5.4 3.16
 -15 4 0 47.69 8.45
 15 -4 4 22.82 5.81
 15 -4 5 291.18 20.41
 15 -3 -3 22.1 5.13
 -15 3 3 29.27 6.53
 -15 3 2 95.32 11.75
 -15 3 1 17.28 4.91
 -15 3 0 43.85 8.1
 15 -3 3 118.37 12.31
 15 -3 4 170.84 15.36
 15 -3 5 30.01 6.58
 -15 2 4 33.8 7.56
 -15 2 3 246.62 19.35
 -15 2 2 55.83 9.28
 -15 2 1 156.91 15.3
 -15 2 0 5.81 3.34
 15 -2 2 27.53 6.1
 15 -2 3 50.19 8.13
 15 -2 4 16.76 4.88
 15 -2 5 122.9 13.56
 -15 1 5 4.41 3.25
 -15 1 4 157.32 15.51
 -15 1 3 21.04 5.48
 -15 1 2 85.81 11.17
 -15 1 1 9.51 3.77
 -15 1 0 135.1 14.03
 -15 1 -1 22.34 6.01
 15 -1 2 728.05 32.54
 15 -1 3 42.6 7.68
 15 -1 4 433.95 25.81
 -15 0 6 123.37 14.03
 -15 0 5 85.74 11.64
 -15 0 4 83.14 11.32
 -15 0 3 69.04 10.25
 -15 0 2 125.35 13.67
 -15 0 1 40.25 7.64
 -15 0 0 17.13 4.83
 -15 0 -1 356.34 23.33
 15 0 1 338.43 20.88
 15 0 2 71.68 10.05
 15 0 3 1068.67 42.44
 -15 -1 6 4.39 3.78
 -15 -1 5 64.4 10.07
 -15 -1 4 37.57 7.54
 -15 -1 3 38.13 7.7
 -15 -1 2 173.4 16.15
 -15 -1 1 149.23 14.85
 -15 -1 0 307.31 21.66
 -15 -1 -1 30.35 6.8
 15 1 1 30.25 6.04
 15 1 2 180 15.81
 -15 -2 6 14.99 5.18
 -15 -2 5 39.6 7.89
 -15 -2 4 36.12 7.56
 -15 -2 3 42.45 8.26
 -15 -2 2 111.95 12.83
 -15 -2 1 348.4 23.32
 -15 -2 0 39.76 7.68
 -15 -3 6 134.85 15.49
 -15 -3 5 443.47 27.89
 -15 -3 4 130.15 14.73
 -15 -3 3 16.8 5.01
 -15 -3 2 39.03 7.88
 -15 -3 1 324.95 22.57
 -15 -4 5 680.28 35.65
 -15 -4 4 446.48 27.9
 -16 5 3 21.85 5.81

_iucr_refine_instructions_details
;
TITL flz-69-2 in P1 #1
REM reset to P1 #1
CELL 0.71073 11.50808 11.644958 16.967665 109.6791 95.9038 98.0117
ZERR 2 0.000215 0.000323 0.000365 0.0022 0.0016 0.0019
LATT -1
SFAC C H Cu I N
UNIT 52 108 10 14 8
 
L.S. 10
PLAN  20
SIZE 0.18 0.17 0.12
BOND
MORE -1
BOND $H
CONF
fmap 2 53
ACTA
REM <olex2.extras>
REM <HklSrc "%.\\flz-69-2.hkl">
REM </olex2.extras>
 
WGHT    0.027300    5.111700
FVAR       0.19946
I1    4    0.613709    0.553806    0.161222    11.00000    0.01363    0.01419 =
         0.01158    0.00284    0.00342    0.00178
I2    4    0.389483    0.656154   -0.015172    11.00000    0.01327    0.01150 =
         0.02023    0.00772    0.00230    0.00211
I3    4   -0.169038    0.607148    0.677931    11.00000    0.01475    0.01774 =
         0.01665    0.01012    0.00299    0.00450
I4    4    0.836840    0.296200    0.017823    11.00000    0.01223    0.01177 =
         0.01978    0.00435    0.00478    0.00384
I5    4    0.739772    0.590011   -0.067161    11.00000    0.01250    0.01524 =
         0.01326    0.00666    0.00083    0.00194
I6    4    0.464600    0.277413   -0.097030    11.00000    0.01354    0.01147 =
         0.01343    0.00243    0.00074    0.00441
I7    4    0.183840    0.552531    0.627972    11.00000    0.01272    0.01077 =
         0.01746    0.00635    0.00213    0.00192
I8    4    0.112731    0.922442    0.689089    11.00000    0.01462    0.01155 =
         0.01129    0.00258    0.00135    0.00532
I9    4   -0.051234    0.623141    0.441971    11.00000    0.01373    0.01157 =
         0.01213    0.00341    0.00354    0.00248
I10   4    0.341128    0.809006    0.500246    11.00000    0.01315    0.01803 =
         0.01638    0.00949    0.00545    0.00648
I11   4   -0.268259    0.893060    0.597898    11.00000    0.01247    0.01157 =
         0.01697    0.00515    0.00511    0.00397
I12   4    0.225373    0.400290    0.095531    11.00000    0.01271    0.01654 =
         0.01568    0.00840    0.00444    0.00528
CU5   3    0.310607    0.423048   -0.038910    11.00000    0.01271    0.01299 =
         0.01417    0.00508    0.00032    0.00205
I14   4    0.499869    0.176100    0.119198    11.00000    0.01455    0.01517 =
         0.01506    0.00600    0.00179    0.00395
CU1   3    0.775900    0.515646    0.060477    11.00000    0.01272    0.01247 =
         0.01331    0.00350    0.00098    0.00234
CU10  3   -0.210892    0.667539    0.545325    11.00000    0.01286    0.01391 =
         0.01414    0.00419    0.00038    0.00147
I17   4    0.022001    0.988921    0.464765    11.00000    0.01521    0.01436 =
         0.01550    0.00722    0.00292    0.00383
CU6   3    0.270817    0.776224    0.635310    11.00000    0.01514    0.01266 =
         0.01288    0.00447    0.00034    0.00321
CU8   3    0.013967    0.676040    0.612016    11.00000    0.01629    0.02071 =
         0.02059    0.00801    0.00291    0.00636
CU3   3    0.551668    0.520874   -0.006008    11.00000    0.01361    0.01988 =
         0.02139    0.00750    0.00352    0.00380
CU4   3    0.429110    0.351949    0.073312    11.00000    0.02110    0.05476 =
         0.04964    0.03885    0.01532    0.02270
CU7   3    0.131365    0.837786    0.518710    11.00000    0.02356    0.06193 =
         0.03262    0.02965    0.01375    0.02710
CU2   3    0.632749    0.312148    0.056149    11.00000    0.02469    0.02899 =
         0.09595    0.03366    0.03580    0.01345
CU9   3   -0.070070    0.865142    0.551952    11.00000    0.02110    0.03393 =
         0.05923    0.03180    0.02330    0.01205
N1    5    0.932744    0.641203    0.138133    11.00000    0.01150    0.01109 =
         0.00918    0.00313    0.00487   -0.00005
N5    5    0.416408    0.833498    0.739308    11.00000    0.01496    0.01257 =
         0.00832    0.00348    0.00277    0.00419
N3    5    0.162812    0.359866   -0.138607    11.00000    0.00954    0.00996 =
         0.01231    0.00166    0.00350    0.00446
N7    5   -0.371337    0.553411    0.466864    11.00000    0.01441    0.00670 =
         0.01243    0.00058    0.00091    0.00084
C18   1    0.085292    0.246498   -0.141728    11.00000    0.01310    0.01393 =
         0.01781    0.01061    0.00523    0.00487
AFIX  23
H18A  2    0.071154    0.254742   -0.084864    11.00000   -1.20000
H18B  2    0.125222    0.176613   -0.162228    11.00000   -1.20000
AFIX   0
C14   1    0.087560    0.458696   -0.123428    11.00000    0.01586    0.00911 =
         0.01450    0.00231   -0.00135    0.00671
AFIX  23
H14A  2    0.137828    0.538979   -0.110328    11.00000   -1.20000
H14B  2    0.047721    0.461610   -0.075300    11.00000   -1.20000
AFIX   0
 
N6    5    0.588661    0.897145    0.863745    11.00000    0.00494    0.00947 =
         0.01245    0.00182   -0.00329    0.00218
N4    5   -0.023557    0.295873   -0.256391    11.00000    0.01352    0.01530 =
         0.01034    0.00517    0.00347    0.00380
N8    5   -0.572665    0.423942    0.379814    11.00000    0.00958    0.01114 =
         0.01293    0.00274    0.00098    0.00155
C41   1   -0.582574    0.478068    0.473280    11.00000    0.02001    0.01646 =
         0.01197    0.00495    0.00365    0.00562
AFIX  23
H41A  2   -0.597586    0.411967    0.495707    11.00000   -1.20000
H41B  2   -0.648056    0.522891    0.480527    11.00000   -1.20000
AFIX   0
 
N2    5    1.126587    0.792193    0.222951    11.00000    0.00944    0.01321 =
         0.01076    0.00371   -0.00079   -0.00246
C15   1   -0.005047    0.431393   -0.202091    11.00000    0.02048    0.00978 =
         0.01650    0.00364   -0.00134    0.00669
AFIX  23
H15A  2   -0.079606    0.452170   -0.184975    11.00000   -1.20000
H15B  2    0.021937    0.481793   -0.234345    11.00000   -1.20000
AFIX   0
C19   1   -0.034491    0.220402   -0.199553    11.00000    0.01628    0.01348 =
         0.01129    0.00724    0.00490    0.00222
AFIX  23
H19A  2   -0.055923    0.132712   -0.233658    11.00000   -1.20000
H19B  2   -0.096186    0.242800   -0.165478    11.00000   -1.20000
AFIX   0
C16   1    0.197490    0.338236   -0.223836    11.00000    0.01772    0.01471 =
         0.01372    0.00893    0.00717    0.00064
AFIX  23
H16A  2    0.257187    0.285971   -0.231859    11.00000   -1.20000
H16B  2    0.231858    0.416851   -0.227504    11.00000   -1.20000
AFIX   0
C5    1    0.983708    0.602634    0.206408    11.00000    0.01361    0.01211 =
         0.01161    0.00213   -0.00035    0.00015
AFIX  23
H5A   2    1.008537    0.523714    0.181585    11.00000   -1.20000
H5B   2    0.923171    0.591101    0.240234    11.00000   -1.20000
AFIX   0
C22   1   -0.343677    0.236793   -0.372931    11.00000    0.01448    0.01612 =
         0.01341    0.00198   -0.00241    0.00497
AFIX  23
H22A  2   -0.319906    0.293202   -0.401818    11.00000   -1.20000
H22B  2   -0.346535    0.153048   -0.411836    11.00000   -1.20000
AFIX   0
 
C32   1    0.576496    0.763237    0.809440    11.00000    0.01102    0.01281 =
         0.01900    0.00355    0.00095    0.00413
AFIX  23
H32A  2    0.544595    0.710589    0.838859    11.00000   -1.20000
H32B  2    0.653577    0.744711    0.796777    11.00000   -1.20000
AFIX   0
C28   1    0.608354    0.976662    0.811067    11.00000    0.00987    0.01424 =
         0.01098    0.00441   -0.00230    0.00037
AFIX  23
H28A  2    0.673721    0.956167    0.780379    11.00000   -1.20000
H28B  2    0.628220    1.063517    0.847283    11.00000   -1.20000
AFIX   0
 
C1    1    1.022771    0.647935    0.083140    11.00000    0.00986    0.02060 =
         0.01121    0.00419    0.00080    0.00255
AFIX  23
H1A   2    0.994884    0.685322    0.043343    11.00000   -1.20000
H1B   2    1.032340    0.564495    0.050751    11.00000   -1.20000
AFIX   0
C20   1   -0.128373    0.260995   -0.325746    11.00000    0.01231    0.01638 =
         0.00585   -0.00244   -0.00640    0.00293
AFIX  23
H20A  2   -0.128788    0.178194   -0.365173    11.00000   -1.20000
H20B  2   -0.118502    0.317526   -0.356485    11.00000   -1.20000
AFIX   0
C17   1    0.089038    0.275508   -0.293862    11.00000    0.01319    0.01516 =
         0.00817    0.00356    0.00505    0.00253
AFIX  23
H17A  2    0.092842    0.310329   -0.338243    11.00000   -1.20000
H17B  2    0.088922    0.187284   -0.318669    11.00000   -1.20000
AFIX   0
 
C42   1   -0.406118    0.594513    0.395945    11.00000    0.02030    0.02000 =
         0.00854    0.00649   -0.00077    0.00109
AFIX  23
H42A  2   -0.350706    0.576244    0.355999    11.00000   -1.20000
H42B  2   -0.402678    0.683569    0.417441    11.00000   -1.20000
AFIX   0
C30   1    0.472536    0.915222    0.896424    11.00000    0.01042    0.01823 =
         0.01368    0.00323    0.00601    0.00158
AFIX  23
H30A  2    0.470987    1.003014    0.921746    11.00000   -1.20000
H30B  2    0.463489    0.877860    0.939146    11.00000   -1.20000
AFIX   0
C29   1    0.371504    0.852710    0.820503    11.00000    0.01035    0.01258 =
         0.01036    0.00414   -0.00058    0.00528
AFIX  23
H29A  2    0.334734    0.773291    0.821761    11.00000   -1.20000
H29B  2    0.311363    0.904235    0.824847    11.00000   -1.20000
AFIX   0
C33   1    0.687522    0.935037    0.939384    11.00000    0.01539    0.01353 =
         0.01110    0.00586    0.00235    0.00406
AFIX  23
H33A  2    0.680708    1.015323    0.979064    11.00000   -1.20000
H33B  2    0.676186    0.875644    0.967828    11.00000   -1.20000
AFIX   0
 
C2    1    1.142837    0.723090    0.133283    11.00000    0.01793    0.01428 =
         0.00788    0.00054    0.00263   -0.00318
AFIX  23
H2A   2    1.199054    0.668262    0.133197    11.00000   -1.20000
H2B   2    1.173731    0.781345    0.107572    11.00000   -1.20000
AFIX   0
C21   1   -0.248203    0.263357   -0.295310    11.00000    0.01151    0.01997 =
         0.01372    0.00121   -0.00063    0.00222
AFIX  23
H21A  2   -0.248347    0.343950   -0.253160    11.00000   -1.20000
H21B  2   -0.264108    0.200813   -0.269879    11.00000   -1.20000
AFIX   0
C3    1    0.909144    0.769068    0.178878    11.00000    0.01477    0.01190 =
         0.01470    0.00115    0.00338    0.00322
AFIX  23
H3A   2    0.859428    0.769847    0.221814    11.00000   -1.20000
H3B   2    0.866931    0.793900    0.136620    11.00000   -1.20000
AFIX   0
C4    1    1.025724    0.860577    0.219494    11.00000    0.02307    0.01070 =
         0.01394    0.00702    0.00602    0.00667
AFIX  23
H4A   2    1.041491    0.913545    0.186808    11.00000   -1.20000
H4B   2    1.019264    0.912820    0.276446    11.00000   -1.20000
AFIX   0
 
C44   1   -0.364114    0.419327    0.431759    11.00000    0.01367    0.01366 =
         0.01542    0.00127    0.00035   -0.00052
AFIX  23
H44A  2   -0.351584    0.388491    0.477823    11.00000   -1.20000
H44B  2   -0.297053    0.409065    0.401418    11.00000   -1.20000
AFIX   0
C34   1    0.811944    0.942897    0.917297    11.00000    0.01328    0.01225 =
         0.01057    0.00239   -0.00220    0.00387
AFIX  23
H34A  2    0.829008    1.010632    0.896633    11.00000   -1.20000
H34B  2    0.817437    0.866464    0.872689    11.00000   -1.20000
AFIX   0
C45   1   -0.478622    0.344595    0.371625    11.00000    0.01564    0.01637 =
         0.01507   -0.00068   -0.00174    0.00391
AFIX  23
H45A  2   -0.463215    0.316620    0.313665    11.00000   -1.20000
H45B  2   -0.506297    0.272054    0.385290    11.00000   -1.20000
AFIX   0
C43   1   -0.534214    0.527872    0.349843    11.00000    0.01640    0.01341 =
         0.01245    0.00603   -0.00079   -0.00317
AFIX  23
H43A  2   -0.588266    0.586206    0.362127    11.00000   -1.20000
H43B  2   -0.535416    0.495688    0.289018    11.00000   -1.20000
AFIX   0
 
C6    1    1.090752    0.699009    0.263986    11.00000    0.01731    0.01697 =
         0.01144    0.00540    0.00116   -0.00020
AFIX  23
H6A   2    1.069752    0.740745    0.319050    11.00000   -1.20000
H6B   2    1.156570    0.658211    0.272047    11.00000   -1.20000
AFIX   0
C7    1    1.236462    0.884494    0.272895    11.00000    0.01613    0.02194 =
         0.01362    0.00044    0.00401   -0.00298
AFIX  23
H7A   2    1.227527    0.914024    0.332247    11.00000   -1.20000
H7B   2    1.242355    0.955142    0.254484    11.00000   -1.20000
AFIX   0
C24   1   -0.475185    0.382020   -0.298721    11.00000    0.01732    0.02353 =
         0.01400   -0.00082    0.00269    0.00375
AFIX 137
H24A  2   -0.414806    0.410846   -0.249417    11.00000   -1.50000
H24B  2   -0.551987    0.384141   -0.281494    11.00000   -1.50000
H24C  2   -0.462858    0.434634   -0.331319    11.00000   -1.50000
AFIX   0
 
C39   1    1.119772    1.028589    1.065121    11.00000    0.01513    0.03029 =
         0.02346    0.01187    0.00403    0.00010
AFIX 137
H39A  2    1.093523    1.079682    1.114849    11.00000   -1.50000
H39B  2    1.196612    1.067867    1.060627    11.00000   -1.50000
H39C  2    1.124805    0.949130    1.069202    11.00000   -1.50000
AFIX   0
C38   1    1.075723    0.796258    0.897940    11.00000    0.02893    0.02029 =
         0.02174    0.00202    0.00901    0.00793
AFIX 137
H38A  2    1.097852    0.753770    0.844145    11.00000   -1.50000
H38B  2    0.999160    0.755138    0.901455    11.00000   -1.50000
H38C  2    1.133598    0.795666    0.942717    11.00000   -1.50000
AFIX   0
 
C9    1    1.457120    0.935463    0.320680    11.00000    0.01535    0.01715 =
         0.01773   -0.00083    0.00214   -0.00532
AFIX  23
H9A   2    1.451135    0.950715    0.379822    11.00000   -1.20000
H9B   2    1.452260    1.011885    0.310466    11.00000   -1.20000
AFIX   0
 
C49   1   -0.959081    0.230381    0.312582    11.00000    0.01047    0.01634 =
         0.01705    0.00938    0.00020    0.00329
AFIX  13
H49   2   -0.901507    0.174908    0.308758    11.00000   -1.20000
AFIX   0
 
C10   1    1.578261    0.899933    0.303659    11.00000    0.01625    0.01218 =
         0.02197    0.00613    0.00050    0.00056
AFIX  13
H10   2    1.571495    0.812295    0.297208    11.00000   -1.20000
AFIX   0
 
C36   1    1.030627    1.011104    0.986090    11.00000    0.01411    0.00998 =
         0.01830    0.00729    0.00365    0.00430
AFIX  13
H36   2    1.032213    1.093196    0.981902    11.00000   -1.20000
AFIX   0
C46   1   -0.690807    0.345007    0.329263    11.00000    0.01431    0.01664 =
         0.01598    0.00124    0.00181   -0.00629
AFIX  23
H46A  2   -0.680161    0.304083    0.271085    11.00000   -1.20000
H46B  2   -0.713921    0.281012    0.352286    11.00000   -1.20000
AFIX   0
C35   1    0.903225    0.964349    0.996010    11.00000    0.01469    0.01674 =
         0.01211    0.00735    0.00177    0.00543
AFIX  23
H35A  2    0.900629    0.887166    1.006448    11.00000   -1.20000
H35B  2    0.881664    1.024602    1.044901    11.00000   -1.20000
AFIX   0
 
C8    1    1.352643    0.834829    0.265037    11.00000    0.01757    0.01246 =
         0.02442    0.00460    0.00355   -0.00381
AFIX  23
H8A   2    1.347850    0.763258    0.282427    11.00000   -1.20000
H8B   2    1.365023    0.808719    0.206375    11.00000   -1.20000
AFIX   0
 
C48   1   -0.908961    0.330274    0.279298    11.00000    0.01730    0.02483 =
         0.01250    0.00255   -0.00127    0.00306
AFIX  23
H48A  2   -0.968382    0.381269    0.277762    11.00000   -1.20000
H48B  2   -0.897356    0.289578    0.221318    11.00000   -1.20000
AFIX   0
C51   1   -1.075736    0.151969    0.256827    11.00000    0.01342    0.02328 =
         0.02558    0.00850    0.00215   -0.00298
AFIX  23
H51A  2   -1.107411    0.092530    0.281390    11.00000   -1.20000
H51B  2   -1.059295    0.105651    0.201162    11.00000   -1.20000
AFIX   0
C31   1    0.492908    0.739638    0.727928    11.00000    0.01312    0.01669 =
         0.01502    0.00129   -0.00264    0.00691
AFIX  23
H31A  2    0.539121    0.741313    0.683503    11.00000   -1.20000
H31B  2    0.443626    0.657857    0.710351    11.00000   -1.20000
AFIX   0
C27   1    0.492431    0.952958    0.747606    11.00000    0.01900    0.01030 =
         0.00918    0.00312   -0.00098    0.00049
AFIX  23
H27A  2    0.449534    1.020491    0.767757    11.00000   -1.20000
H27B  2    0.512070    0.949385    0.692690    11.00000   -1.20000
AFIX   0
 
C12   1    1.675311    0.973089    0.379140    11.00000    0.01853    0.02375 =
         0.03448    0.00597   -0.00673    0.00689
AFIX  23
H12A  2    1.656167    0.952307    0.427640    11.00000   -1.20000
H12B  2    1.749649    0.946604    0.366325    11.00000   -1.20000
AFIX   0
C23   1   -0.468704    0.249770   -0.352424    11.00000    0.01100    0.01158 =
         0.02525    0.00766   -0.00171   -0.00288
AFIX  13
H23   2   -0.490356    0.196104   -0.320424    11.00000   -1.20000
AFIX   0
 
C40   1   -0.466228    0.565754    0.520493    11.00000    0.01765    0.01533 =
         0.01178    0.00167    0.00455    0.00408
AFIX  23
H40A  2   -0.479457    0.650603    0.538694    11.00000   -1.20000
H40B  2   -0.440399    0.548037    0.570729    11.00000   -1.20000
AFIX   0
C50   1   -0.973336    0.284730    0.405832    11.00000    0.03547    0.01043 =
         0.02106    0.01055   -0.00035    0.00376
AFIX 137
H50A  2   -0.897491    0.327873    0.439418    11.00000   -1.50000
H50B  2   -1.003782    0.218898    0.424466    11.00000   -1.50000
H50C  2   -1.027682    0.341536    0.412147    11.00000   -1.50000
AFIX   0
C47   1   -0.790627    0.417193    0.329429    11.00000    0.01745    0.01499 =
         0.02269    0.00259   -0.00003   -0.00159
AFIX  23
H47A  2   -0.769870    0.479096    0.304196    11.00000   -1.20000
H47B  2   -0.800798    0.460054    0.387444    11.00000   -1.20000
AFIX   0
 
C11   1    1.607287    0.910280    0.220778    11.00000    0.01811    0.01948 =
         0.02699   -0.00102    0.00356    0.00125
AFIX 137
H11A  2    1.549776    0.852212    0.174561    11.00000   -1.50000
H11B  2    1.685161    0.892170    0.213330    11.00000   -1.50000
H11C  2    1.605287    0.993005    0.222017    11.00000   -1.50000
AFIX   0
 
C37   1    1.070233    0.930530    0.906716    11.00000    0.01616    0.02564 =
         0.01838    0.00841    0.00179    0.00341
AFIX  23
H37A  2    1.148651    0.970426    0.903759    11.00000   -1.20000
H37B  2    1.016751    0.928822    0.858095    11.00000   -1.20000
AFIX   0
 
C13   1    1.693674    1.112713    0.403670    11.00000    0.01818    0.04019 =
         0.02033   -0.00182    0.00225   -0.00155
AFIX 137
H13A  2    1.698088    1.133831    0.353895    11.00000   -1.50000
H13B  2    1.766325    1.150161    0.442966    11.00000   -1.50000
H13C  2    1.628255    1.142687    0.429706    11.00000   -1.50000
AFIX   0
 
C52   1   -1.171193    0.229943    0.246649    11.00000    0.01864    0.04768 =
         0.05432    0.04119   -0.00742   -0.00670
AFIX 137
H52A  2   -1.244731    0.175413    0.216765    11.00000   -1.50000
H52B  2   -1.145126    0.280871    0.215252    11.00000   -1.50000
H52C  2   -1.182803    0.281805    0.301632    11.00000   -1.50000
AFIX   0
 
C25   1   -0.552522    0.201495   -0.436253    11.00000    0.02096    0.02904 =
         0.02503    0.00430   -0.00409    0.00345
AFIX  23
H25A  2   -0.547151    0.115585   -0.465642    11.00000   -1.20000
H25B  2   -0.526105    0.248374   -0.470835    11.00000   -1.20000
AFIX   0
C26   1   -0.683469    0.208960   -0.428795    11.00000    0.01493    0.03090 =
         0.05030    0.00551    0.00178   -0.00108
AFIX 137
H26A  2   -0.729599    0.180900   -0.484470    11.00000   -1.50000
H26B  2   -0.689863    0.293298   -0.398577    11.00000   -1.50000
H26C  2   -0.712726    0.157346   -0.398678    11.00000   -1.50000
AFIX   0
HKLF 4
 
REM  flz-69-2 in P1 #1
REM R1 =  0.0307 for   19665 Fo > 4sig(Fo)  and  0.0315 for all   20050 data
REM    765 parameters refined using      3 restraints
 
END  
     
WGHT      0.0273      5.1119 

REM Highest difference peak  2.062,  deepest hole -2.001,  1-sigma level  0.193
Q1    1   0.1746  0.9016  0.5413  11.00000  0.05    2.06
Q2    1  -0.0558  0.6929  0.4412  11.00000  0.05    1.57
Q3    1   0.1779  0.6211  0.6215  11.00000  0.05    1.42
Q4    1   0.3815  0.7251 -0.0246  11.00000  0.05    1.39
Q5    1   0.0165  1.0603  0.4602  11.00000  0.05    1.36
Q6    1  -0.2619  0.8263  0.5988  11.00000  0.05    1.36
Q7    1   0.4810  0.3426  0.0404  11.00000  0.05    1.31
Q8    1   0.3915  0.5780 -0.0146  11.00000  0.05    1.31
Q9    1   0.8763  0.4314  0.1416  11.00000  0.05    1.30
Q10   1   0.1842  0.4686  0.6186  11.00000  0.05    1.27
Q11   1  -0.1732  0.6820  0.6749  11.00000  0.05    1.25
Q12   1  -0.1246  0.4467 -0.0809  11.00000  0.05    1.24
Q13   1   0.0780  0.8682  0.5530  11.00000  0.05    1.24
Q14   1   0.2157  0.4591  0.0822  11.00000  0.05    1.23
Q15   1   0.4998  0.2534  0.1191  11.00000  0.05    1.21
Q16   1   0.7446  0.5215 -0.0637  11.00000  0.05    1.21
Q17   1   0.4667  0.1966 -0.0949  11.00000  0.05    1.21
Q18   1   0.3731  0.9445  0.6333  11.00000  0.05    1.19
Q19   1  -0.1534  0.5732  0.6387  11.00000  0.05    1.17
Q20   1   0.5023  0.1012  0.1187  11.00000  0.05    1.16

  REM The information below was added by Olex2.
  REM
  REM R1 = 0.0307 for 19665 Fo > 4sig(Fo) and 0.0315 for all 35607 data
  REM n/a parameters refined using n/a restraints
  REM Highest difference peak 2.06, deepest hole -2.00
  REM Mean Shift 0, Max Shift -0.001.

  REM +++ Tabular Listing of Refinement Information +++
  REM R1_all = 0.0315
  REM R1_gt = 0.0307
  REM wR_ref = 0.0724
  REM GOOF = 1.075
  REM Shift_max = -0.001
  REM Shift_mean = 0
  REM Reflections_all = 35607
  REM Reflections_gt = 19665
  REM Parameters = n/a
  REM Hole = -2.00
  REM Peak = 2.06
  REM Flack = 0.056(12)

  
;
_olex2_date_sample_data_collection  2020-12-25
_olex2_submission_special_instructions  'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max  1.990
_oxdiff_exptl_absorpt_empirical_full_min  0.665
