TPD/R/O 1100             Thermo 
	Standard Data Report 

	Run Nr.:478 
	File: C:\Users\PUTRACat\Desktop\Data\TYRAA\TPD-NH3\CU (I).110 
	Comment:  
	Operator: TYRAA 
	Room Temperature 26°C 		Atmospheric Pressure 1000hPa 

	Sample 
	Producer: TYRAA 		Sample-Code: 0
	Name: CU (I) 		Customer-Code: 0
	Mass: 0.0462 g 		Support: 
	Info:  		Metals: 0
	Preparation:  	 

	Pretreatment 
	Name: NH3 PRETREATMENT 2 		Info: 
	On Instrument: Instrument 1  with Ser.Nr.20180140 on Right Oven 
	Started: 19/12/2022 at 4:14:13 PM finished 4:56:39 PM 

	Phase	With Gas	Flow [ccm/min]	Start at T [°C]	Ramp[°C/min]	Stop at T [°C]	Hold for [min]
	Cleaning	Nitrogen	20	Off			0
	1:	Nitrogen	20	Off	 	0 	30
	2:	Off	  	  	  	  	 
	3:	Off	  	 			 
	4:	Off	  	 			 
	End Pretreatment with Oven Off

	TPD/R/O 
	Method Name: TPD NH3 		Info: 
	On Instrument: Instrument 1  with Ser.Nr.20180140 on Right Oven 
	Started: 19/12/2022 at 6:59:56 PM finished 9:00:31 PM 
	Gas Port when Ready: 	(a) Helium
	Gas Port when End: 	(a) Helium
	Sample rate: 	1 s
	Gain: 	10	 
	Polarity: 	Positive	 

 	With Gas	Flow [ccm/min]	Start at T [°C]	Ramp°C/min	Stop at T [°C]	Hold for [min]
	Helium	20	50	10	950	30

	Results 
	Amount gas adsorbed: 	5013.88248	µmol/g

	Baseline 
	Start at 0.0000 min -184.38438 mV. Stop at 120.2564 min -51.65165 mV 

	Calibration 
	Use Calibration Factor: 7.711065 *10e-7 mmol/mVs 

	Peaks 
	#	Start [min] 	Stop [min]	Maximum [min] 	T [°C]	Integral [mVs]	[µmol/g] 	[%] 
	1	75.1500 	120.1333 	92.5833	952 	300401.26 	5013.88250 	100.00