      Table 1.  Crystal data and structure refinement for a. 
  
  
      Identification code               a 
  
      Empirical formula                 C84 H71 Au3 Cl3 N9 O4 
  
      Formula weight                    1967.74 
  
      Temperature                       100(2) K 
  
      Wavelength                        1.54184 A 
  
      Crystal system, space group       Monoclinic,  C2 
  
      Unit cell dimensions              a = 24.0503(6) A   alpha = 90 deg. 
                                        b = 12.2870(2) A    beta = 109.212(3) deg. 
                                        c = 30.3447(8) A   gamma = 90 deg. 
  
      Volume                            8467.7(4) A^3 
  
      Z, Calculated density             4,  1.544 Mg/m^3 
  
      Absorption coefficient            10.855 mm^-1 
  
      F(000)                            3832 
  
      Crystal size                      0.160 x 0.150 x 0.140 mm 
  
      Theta range for data collection   3.084 to 75.938 deg. 
  
      Limiting indices                  -28<=h<=29, -13<=k<=15, -37<=l<=37 
  
      Reflections collected / unique    25404 / 12598 [R(int) = 0.0381] 
  
      Completeness to theta = 67.684    98.6 % 
  
      Absorption correction             Semi-empirical from equivalents 
  
      Max. and min. transmission        1.00000 and 0.65968 
  
      Refinement method                 Full-matrix least-squares on F^2 
  
      Data / restraints / parameters    12598 / 8 / 919 
  
      Goodness-of-fit on F^2            0.900 
  
      Final R indices [I>2sigma(I)]     R1 = 0.0562, wR2 = 0.1549 
  
      R indices (all data)              R1 = 0.0714, wR2 = 0.1703 
  
      Absolute structure parameter      -0.027(13) 
  
      Extinction coefficient            0.000116(14) 
  
      Largest diff. peak and hole       2.708 and -2.264 e.A^-3 
  
         Table 2.  Atomic coordinates ( x 10^4) and equivalent isotropic 
         displacement parameters (A^2 x 10^3) for a. 
         U(eq) is defined as one third of the trace of the orthogonalized 
         Uij tensor. 
  
         ________________________________________________________________ 
  
                         x             y             z           U(eq) 
         ________________________________________________________________ 
  
          Au(1)        9725(1)       3487(1)       5440(1)       40(1) 
          C(1)         8374(7)        455(14)      4327(6)       38(3) 
          N(1)         8628(5)       3720(11)      4639(4)       36(3) 
          Cl(1)       10496(2)       4059(4)       6066(2)       51(1) 
          Au(2)        2482(1)       3986(1)        699(1)       50(1) 
          C(2)         8699(8)        345(15)      4017(6)       41(4) 
          N(2)         8859(6)       1932(11)      4869(5)       35(3) 
          Cl(2)        2172(3)       2233(4)        521(2)       66(1) 
          Au(3)        6651(1)       9795(1)       1346(1)       52(1) 
          C(3)         9059(7)       1176(14)      3926(6)       40(4) 
          N(3)         7966(6)       1041(11)      4876(5)       34(3) 
          Cl(3)        6373(4)      11536(4)       1107(3)       84(2) 
          O(38)        7464(5)       -529(10)      4933(4)       45(3) 
          C(38)        3748(10)      7186(16)      1794(7)       52(5) 
          C(37)        1950(11)      6067(17)       152(7)       62(6) 
          C(36)        2226(15)      8310(20)       365(8)       91(9) 
          C(35)        2378(17)      9340(20)       498(8)       97(11) 
          C(34)        2892(13)      9580(30)       870(11)      91(8) 
          C(33)        3264(16)      8819(18)      1123(9)       93(10) 
          C(32)        3134(13)      7690(20)      1016(7)       74(7) 
          C(31)        2614(15)      7440(17)       649(8)       81(8) 
          C(30)        2763(9)       5539(14)       810(7)       48(4) 
          C(29)        3547(11)      6865(19)      1278(7)       60(5) 
          O(39)        5188(8)       4986(15)      2386(5)       76(5) 
          C(39)        4334(11)      7440(18)      1921(9)       68(7) 
          C(49)        3428(9)       7234(15)      2094(6)       48(4) 
          C(9)         7780(7)          1(14)      4763(6)       40(4) 
          N(9)         7161(8)       6810(12)      2541(6)       50(4) 
          C(8)         8678(9)       -720(17)      3797(7)       55(5) 
          N(8)         7272(7)       7947(12)      1923(5)       40(3) 
          C(22)        8131(6)       3430(15)      4298(5)       38(3) 
          C(21)        7940(5)       2348(14)      4250(5)       32(3) 
          C(20)        8991(7)       2973(13)      4932(6)       36(3) 
          O(93)        7503(9)       6335(13)      3316(6)       77(5) 
          C(13)        7782(7)       1721(14)      5193(6)       39(4) 
          C(24)        7271(9)       3861(15)      3625(6)       49(4) 
          C(69)        7650(10)      8802(16)      2206(8)       60(5) 
          C(10)        8045(7)       -386(14)      4416(6)       39(4) 
          C(19)        8529(8)       2740(16)      5876(7)       47(4) 
          C(18)        9000(8)       2717(19)      6315(6)       49(5) 
          C(48)        2830(10)      6886(17)      1997(7)       56(5) 
          C(7)         8293(6)       1480(14)      4586(6)       34(3) 
          N(7)         6428(7)       7450(12)      1304(6)       45(4) 
          C(6)         8994(11)      -870(19)      3497(8)       67(6) 
          N(6)         4086(11)      6880(20)      1157(6)       89(8) 
          C(5)         9330(12)       -20(20)      3401(8)       72(7) 
          N(5)         2458(10)      6327(14)       544(6)       64(5) 
          C(4)         9363(9)        962(19)      3628(7)       56(5) 
          N(4)         3253(9)       5771(15)      1183(7)       60(5) 
          C(11)        8018(9)      -1386(16)      4208(7)       52(4) 
          C(25)        7093(10)      2802(17)      3613(7)       57(5) 
          C(46)        2870(9)       7435(19)      2774(6)       55(5) 
          C(79)        6807(7)       8273(16)      1568(7)       46(4) 
          C(76)        6698(15)      9840(40)      2994(15)     138(17) 
          C(23)        7794(8)       4191(15)      3972(6)       46(4) 
          C(40)        4636(10)      7857(19)      2369(7)       62(6) 
          C(17)        9159(10)      1730(19)      6531(9)       63(6) 
          C(26)        7412(8)       2047(16)      3911(6)       48(4) 
          C(47)        2560(10)      6978(18)      2322(7)       56(5) 
          C(75)        6059(8)       8940(20)      2236(7)       63(6) 
          C(44)        3745(9)       7669(17)      2550(7)       54(5) 
          C(14)        8259(7)       1741(16)      5677(6)       41(4) 
          C(63)        3556(9)       4934(17)      1495(7)       55(5) 
          C(62)        8664(11)      5946(17)      3098(7)       62(5) 
          C(61)        9114(11)      5854(18)      2915(8)       67(5) 
          C(60)        9026(11)      6170(17)      2425(8)       62(5) 
          C(59)        9486(11)      6060(20)      2247(9)       71(7) 
          C(58)        9385(10)      6390(20)      1805(10)      71(7) 
          C(57)        8817(10)      6756(18)      1509(8)       60(5) 
          C(56)        8377(9)       6844(17)      1685(8)       55(5) 
          C(55)        8467(9)       6535(15)      2151(7)       52(5) 
          C(54)        6883(11)      4139(18)      1533(10)      81(8) 
          C(53)        7186(10)      4930(16)      1860(9)       62(6) 
          C(52)        7055(9)       6010(16)      1765(8)       53(5) 
          C(51)        6591(9)       6325(18)      1368(9)       59(5) 
          C(50)        6280(11)      5556(16)      1073(10)      66(6) 
          C(12)        8323(9)      -1524(19)      3890(6)       58(5) 
          O(64)        5083(10)      7310(20)      1522(8)      115(9) 
          C(64)        8127(10)      6305(15)      2816(7)       56(5) 
          C(68)        7581(11)      6471(15)      2937(8)       61(6) 
          C(67)        5949(10)      7751(17)       906(10)      74(7) 
          C(66)        8029(9)       6576(14)      2363(7)       48(4) 
          C(28)        9272(7)       1131(16)      5181(6)       40(4) 
          C(45)        3426(10)      7720(19)      2878(7)       57(5) 
          C(43)        4352(10)      8003(16)      2671(6)       55(5) 
          C(65)        7360(9)       6862(15)      2144(6)       45(4) 
          C(27)        8771(9)       4877(18)      4708(8)       59(5) 
          C(88)        6543(11)      7040(20)      2507(10)      77(7) 
          C(83)        4240(20)      3660(40)       239(14)     460(100) 
          C(82)        4670(20)      3160(20)       607(18)     410(80) 
          C(81)        4947(17)      3740(30)      1015(14)     290(50) 
          C(80)        4789(13)      4810(30)      1056(9)      150(16) 
          C(78)        4358(13)      5310(20)       688(11)     118(12) 
          C(77)        4086(16)      4730(40)       279(11)     260(40) 
          C(70)        6463(7)       8255(18)      2599(6)       52(5) 
          C(15)        8432(9)        746(17)      5910(8)       53(5) 
          C(16)        8878(10)       760(20)      6354(8)       66(6) 
          C(71)        6764(12)      8800(30)      2970(10)      93(10) 
          C(74)        6027(11)     10020(20)      2320(9)       74(7) 
          C(73)        4132(16)      6560(30)       695(11)     115(14) 
          C(72)        6362(14)     10510(30)      2700(14)     102(10) 
          C(42)        4550(12)      7240(20)      1529(9)       82(9) 
          C(41)        6424(14)      4450(20)      1148(12)      96(10) 
         ________________________________________________________________ 
  
           Table 3.  Bond lengths [A] and angles [deg] for a. 
           _____________________________________________________________ 
  
            Au(1)-C(20)                   2.026(17) 
            Au(1)-Cl(1)                   2.285(4) 
            Au(1)-Au(1)#1                 3.3497(13) 
            C(1)-C(10)                    1.38(2) 
            C(1)-C(2)                     1.41(2) 
            C(1)-C(7)                     1.53(2) 
            N(1)-C(22)                    1.345(19) 
            N(1)-C(20)                    1.37(2) 
            N(1)-C(27)                    1.46(3) 
            Au(2)-C(30)                   2.016(17) 
            Au(2)-Cl(2)                   2.285(5) 
            C(2)-C(3)                     1.42(2) 
            C(2)-C(8)                     1.46(3) 
            N(2)-C(20)                    1.32(2) 
            N(2)-C(7)                     1.458(19) 
            N(2)-C(28)                    1.50(2) 
            Au(3)-C(79)                   1.981(19) 
            Au(3)-Cl(3)                   2.286(5) 
            C(3)-C(4)                     1.36(2) 
            C(3)-H(3)                     0.9500 
            N(3)-C(9)                     1.36(2) 
            N(3)-C(13)                    1.45(2) 
            N(3)-C(7)                     1.461(18) 
            O(38)-C(9)                    1.234(19) 
            C(38)-C(39)                   1.37(3) 
            C(38)-C(49)                   1.37(3) 
            C(38)-C(29)                   1.53(3) 
            C(37)-N(5)                    1.43(3) 
            C(37)-H(37A)                  0.9800 
            C(37)-H(37B)                  0.9800 
            C(37)-H(37C)                  0.9800 
            C(36)-C(35)                   1.34(4) 
            C(36)-C(31)                   1.49(4) 
            C(36)-H(36)                   0.9500 
            C(35)-C(34)                   1.40(4) 
            C(35)-H(35)                   0.9500 
            C(34)-C(33)                   1.35(4) 
            C(34)-H(34)                   0.9500 
            C(33)-C(32)                   1.43(3) 
            C(33)-H(33)                   0.9500 
            C(32)-C(31)                   1.41(4) 
            C(32)-C(29)                   1.46(4) 
            C(31)-N(5)                    1.43(3) 
            C(30)-N(5)                    1.32(3) 
            C(30)-N(4)                    1.37(3) 
            C(29)-N(6)                    1.46(3) 
            C(29)-N(4)                    1.50(3) 
            O(39)-H(39A)                  0.87(3) 
            O(39)-H(39B)                  0.88(3) 
            C(39)-C(40)                   1.41(3) 
            C(39)-C(42)                   1.46(3) 
            C(49)-C(48)                   1.43(3) 
            C(49)-C(44)                   1.44(3) 
            C(9)-C(10)                    1.48(2) 
            N(9)-C(68)                    1.36(3) 
            N(9)-C(65)                    1.44(2) 
            N(9)-C(88)                    1.48(3) 
            C(8)-C(6)                     1.38(2) 
            C(8)-C(12)                    1.39(3) 
            N(8)-C(79)                    1.33(2) 
            N(8)-C(69)                    1.47(2) 
            N(8)-C(65)                    1.48(2) 
            C(22)-C(21)                   1.40(2) 
            C(22)-C(23)                   1.41(2) 
            C(21)-C(26)                   1.40(2) 
            C(21)-C(7)                    1.53(2) 
            O(93)-C(68)                   1.24(2) 
            C(13)-C(14)                   1.54(2) 
            C(13)-H(13A)                  0.9900 
            C(13)-H(13B)                  0.9900 
            C(24)-C(25)                   1.37(3) 
            C(24)-C(23)                   1.41(3) 
            C(24)-H(24)                   0.9500 
            C(69)-H(69A)                  0.9800 
            C(69)-H(69B)                  0.9800 
            C(69)-H(69C)                  0.9800 
            C(10)-C(11)                   1.37(2) 
            C(19)-C(14)                   1.43(3) 
            C(19)-C(18)                   1.44(2) 
            C(19)-H(19)                   0.9500 
            C(18)-C(17)                   1.37(3) 
            C(18)-H(18)                   0.9500 
            C(48)-C(47)                   1.35(3) 
            C(48)-H(48)                   0.9500 
            N(7)-C(79)                    1.42(3) 
            N(7)-C(67)                    1.42(3) 
            N(7)-C(51)                    1.43(3) 
            C(6)-C(5)                     1.41(3) 
            C(6)-H(6)                     0.9500 
            N(6)-C(42)                    1.37(3) 
            N(6)-C(73)                    1.49(3) 
            C(5)-C(4)                     1.38(3) 
            C(5)-H(5)                     0.9500 
            C(4)-H(4)                     0.9500 
            N(4)-C(63)                    1.42(3) 
            C(11)-C(12)                   1.40(2) 
            C(11)-H(11)                   0.9500 
            C(25)-C(26)                   1.34(3) 
            C(25)-H(25)                   0.9500 
            C(46)-C(45)                   1.32(3) 
            C(46)-C(47)                   1.44(3) 
            C(46)-H(46)                   0.9500 
            C(76)-C(71)                   1.29(5) 
            C(76)-C(72)                   1.28(5) 
            C(76)-H(76)                   0.9500 
            C(23)-H(23)                   0.9500 
            C(40)-C(43)                   1.32(3) 
            C(40)-H(40)                   0.9500 
            C(17)-C(16)                   1.39(3) 
            C(17)-H(17)                   0.9500 
            C(26)-H(26)                   0.9500 
            C(47)-H(47)                   0.9500 
            C(75)-C(74)                   1.36(4) 
            C(75)-C(70)                   1.47(3) 
            C(75)-H(75)                   0.9500 
            C(44)-C(43)                   1.44(3) 
            C(44)-C(45)                   1.45(3) 
            C(14)-C(15)                   1.40(3) 
            C(63)-H(63A)                  0.9800 
            C(63)-H(63B)                  0.9800 
            C(63)-H(63C)                  0.9800 
            C(62)-C(64)                   1.37(3) 
            C(62)-C(61)                   1.37(3) 
            C(62)-H(62)                   0.9500 
            C(61)-C(60)                   1.48(3) 
            C(61)-H(61)                   0.9500 
            C(60)-C(59)                   1.39(3) 
            C(60)-C(55)                   1.40(3) 
            C(59)-C(58)                   1.34(3) 
            C(59)-H(59)                   0.9500 
            C(58)-C(57)                   1.44(3) 
            C(58)-H(58)                   0.9500 
            C(57)-C(56)                   1.34(3) 
            C(57)-H(57)                   0.9500 
            C(56)-C(55)                   1.41(3) 
            C(56)-H(56)                   0.9500 
            C(55)-C(66)                   1.40(3) 
            C(54)-C(41)                   1.37(4) 
            C(54)-C(53)                   1.41(3) 
            C(54)-H(54)                   0.9500 
            C(53)-C(52)                   1.37(3) 
            C(53)-H(53)                   0.9500 
            C(52)-C(51)                   1.40(3) 
            C(52)-C(65)                   1.55(3) 
            C(51)-C(50)                   1.35(3) 
            C(50)-C(41)                   1.40(3) 
            C(50)-H(50)                   0.9500 
            C(12)-H(12)                   0.9500 
            O(64)-C(42)                   1.29(3) 
            C(64)-C(66)                   1.36(3) 
            C(64)-C(68)                   1.49(3) 
            C(67)-H(67A)                  0.9800 
            C(67)-H(67B)                  0.9800 
            C(67)-H(67C)                  0.9800 
            C(66)-C(65)                   1.57(3) 
            C(28)-H(28A)                  0.9800 
            C(28)-H(28B)                  0.9800 
            C(28)-H(28C)                  0.9800 
            C(45)-H(45)                   0.9500 
            C(43)-H(43)                   0.9500 
            C(27)-H(27A)                  0.9800 
            C(27)-H(27B)                  0.9800 
            C(27)-H(27C)                  0.9800 
            C(88)-C(70)                   1.54(3) 
            C(88)-H(88A)                  0.9900 
            C(88)-H(88B)                  0.9900 
            C(83)-C(82)                   1.3900 
            C(83)-C(77)                   1.3900 
            C(83)-H(83)                   0.9500 
            C(82)-C(81)                   1.3900 
            C(82)-H(82)                   0.9500 
            C(81)-C(80)                   1.3900 
            C(81)-H(81)                   0.9500 
            C(80)-C(78)                   1.3900 
            C(80)-H(80)                   0.9500 
            C(78)-C(77)                   1.3900 
            C(78)-C(73)                   1.63(5) 
            C(77)-H(77)                   0.9500 
            C(70)-C(71)                   1.31(3) 
            C(15)-C(16)                   1.42(3) 
            C(15)-H(15)                   0.9500 
            C(16)-H(16)                   0.9500 
            C(71)-H(71)                   0.9500 
            C(74)-C(72)                   1.32(4) 
            C(74)-H(74)                   0.9500 
            C(73)-H(73A)                  0.9900 
            C(73)-H(73B)                  0.9900 
            C(72)-H(72)                   0.9500 
            C(41)-H(41)                   0.9500 
  
            C(20)-Au(1)-Cl(1)           174.0(4) 
            C(20)-Au(1)-Au(1)#1          82.3(4) 
            Cl(1)-Au(1)-Au(1)#1         103.69(12) 
            C(10)-C(1)-C(2)             122.5(17) 
            C(10)-C(1)-C(7)             109.6(13) 
            C(2)-C(1)-C(7)              127.8(15) 
            C(22)-N(1)-C(20)            122.3(15) 
            C(22)-N(1)-C(27)            118.4(15) 
            C(20)-N(1)-C(27)            119.3(15) 
            C(30)-Au(2)-Cl(2)           175.9(5) 
            C(1)-C(2)-C(3)              124.4(16) 
            C(1)-C(2)-C(8)              116.4(17) 
            C(3)-C(2)-C(8)              119.1(15) 
            C(20)-N(2)-C(7)             126.1(14) 
            C(20)-N(2)-C(28)            118.0(14) 
            C(7)-N(2)-C(28)             114.7(13) 
            C(79)-Au(3)-Cl(3)           173.6(5) 
            C(4)-C(3)-C(2)              118.9(18) 
            C(4)-C(3)-H(3)              120.5 
            C(2)-C(3)-H(3)              120.5 
            C(9)-N(3)-C(13)             124.1(13) 
            C(9)-N(3)-C(7)              113.2(13) 
            C(13)-N(3)-C(7)             121.9(13) 
            C(39)-C(38)-C(49)           124(2) 
            C(39)-C(38)-C(29)           107.2(17) 
            C(49)-C(38)-C(29)           129.2(19) 
            N(5)-C(37)-H(37A)           109.5 
            N(5)-C(37)-H(37B)           109.5 
            H(37A)-C(37)-H(37B)         109.5 
            N(5)-C(37)-H(37C)           109.5 
            H(37A)-C(37)-H(37C)         109.5 
            H(37B)-C(37)-H(37C)         109.5 
            C(35)-C(36)-C(31)           116(3) 
            C(35)-C(36)-H(36)           121.9 
            C(31)-C(36)-H(36)           121.9 
            C(36)-C(35)-C(34)           121(3) 
            C(36)-C(35)-H(35)           119.3 
            C(34)-C(35)-H(35)           119.3 
            C(33)-C(34)-C(35)           124(3) 
            C(33)-C(34)-H(34)           118.1 
            C(35)-C(34)-H(34)           118.1 
            C(34)-C(33)-C(32)           119(3) 
            C(34)-C(33)-H(33)           120.4 
            C(32)-C(33)-H(33)           120.4 
            C(31)-C(32)-C(33)           118(3) 
            C(31)-C(32)-C(29)           123(2) 
            C(33)-C(32)-C(29)           119(2) 
            C(32)-C(31)-N(5)            119(2) 
            C(32)-C(31)-C(36)           122(2) 
            N(5)-C(31)-C(36)            119(3) 
            N(5)-C(30)-N(4)             120.6(17) 
            N(5)-C(30)-Au(2)            120.2(15) 
            N(4)-C(30)-Au(2)            119.1(14) 
            N(6)-C(29)-C(32)            110.8(19) 
            N(6)-C(29)-N(4)             111.5(19) 
            C(32)-C(29)-N(4)            109.1(19) 
            N(6)-C(29)-C(38)            104.3(18) 
            C(32)-C(29)-C(38)           107.8(19) 
            N(4)-C(29)-C(38)            113.4(16) 
            H(39A)-O(39)-H(39B)         103(6) 
            C(38)-C(39)-C(40)           120.5(19) 
            C(38)-C(39)-C(42)           110(2) 
            C(40)-C(39)-C(42)           130(2) 
            C(38)-C(49)-C(48)           126.4(18) 
            C(38)-C(49)-C(44)           114.6(19) 
            C(48)-C(49)-C(44)           118.9(17) 
            O(38)-C(9)-N(3)             126.0(15) 
            O(38)-C(9)-C(10)            126.6(16) 
            N(3)-C(9)-C(10)             107.3(13) 
            C(68)-N(9)-C(65)            113.7(16) 
            C(68)-N(9)-C(88)            123.7(18) 
            C(65)-N(9)-C(88)            122.4(18) 
            C(6)-C(8)-C(12)             123(2) 
            C(6)-C(8)-C(2)              118.6(19) 
            C(12)-C(8)-C(2)             118.3(17) 
            C(79)-N(8)-C(69)            116.8(17) 
            C(79)-N(8)-C(65)            126.5(16) 
            C(69)-N(8)-C(65)            114.4(16) 
            N(1)-C(22)-C(21)            120.7(15) 
            N(1)-C(22)-C(23)            121.6(17) 
            C(21)-C(22)-C(23)           117.6(14) 
            C(26)-C(21)-C(22)           121.2(15) 
            C(26)-C(21)-C(7)            118.7(15) 
            C(22)-C(21)-C(7)            120.1(12) 
            N(2)-C(20)-N(1)             119.0(15) 
            N(2)-C(20)-Au(1)            121.4(12) 
            N(1)-C(20)-Au(1)            119.6(11) 
            N(3)-C(13)-C(14)            110.3(13) 
            N(3)-C(13)-H(13A)           109.6 
            C(14)-C(13)-H(13A)          109.6 
            N(3)-C(13)-H(13B)           109.6 
            C(14)-C(13)-H(13B)          109.6 
            H(13A)-C(13)-H(13B)         108.1 
            C(25)-C(24)-C(23)           119.3(18) 
            C(25)-C(24)-H(24)           120.4 
            C(23)-C(24)-H(24)           120.4 
            N(8)-C(69)-H(69A)           109.5 
            N(8)-C(69)-H(69B)           109.5 
            H(69A)-C(69)-H(69B)         109.5 
            N(8)-C(69)-H(69C)           109.5 
            H(69A)-C(69)-H(69C)         109.5 
            H(69B)-C(69)-H(69C)         109.5 
            C(11)-C(10)-C(1)            121.6(15) 
            C(11)-C(10)-C(9)            130.4(16) 
            C(1)-C(10)-C(9)             108.0(15) 
            C(14)-C(19)-C(18)           119.1(18) 
            C(14)-C(19)-H(19)           120.5 
            C(18)-C(19)-H(19)           120.5 
            C(17)-C(18)-C(19)           118.1(19) 
            C(17)-C(18)-H(18)           120.9 
            C(19)-C(18)-H(18)           120.9 
            C(47)-C(48)-C(49)           121(2) 
            C(47)-C(48)-H(48)           119.5 
            C(49)-C(48)-H(48)           119.5 
            N(2)-C(7)-N(3)              111.8(13) 
            N(2)-C(7)-C(21)             109.5(13) 
            N(3)-C(7)-C(21)             111.6(12) 
            N(2)-C(7)-C(1)              111.3(13) 
            N(3)-C(7)-C(1)              101.0(12) 
            C(21)-C(7)-C(1)             111.6(13) 
            C(79)-N(7)-C(67)            119.1(15) 
            C(79)-N(7)-C(51)            121.1(17) 
            C(67)-N(7)-C(51)            118.4(17) 
            C(8)-C(6)-C(5)              121(2) 
            C(8)-C(6)-H(6)              119.4 
            C(5)-C(6)-H(6)              119.4 
            C(42)-N(6)-C(29)            110.2(18) 
            C(42)-N(6)-C(73)            125(2) 
            C(29)-N(6)-C(73)            125(2) 
            C(4)-C(5)-C(6)              119.2(19) 
            C(4)-C(5)-H(5)              120.4 
            C(6)-C(5)-H(5)              120.4 
            C(30)-N(5)-C(31)            121(2) 
            C(30)-N(5)-C(37)            119.8(16) 
            C(31)-N(5)-C(37)            119(2) 
            C(3)-C(4)-C(5)              123(2) 
            C(3)-C(4)-H(4)              118.5 
            C(5)-C(4)-H(4)              118.5 
            C(30)-N(4)-C(63)            120.8(17) 
            C(30)-N(4)-C(29)            124.6(18) 
            C(63)-N(4)-C(29)            114.4(18) 
            C(10)-C(11)-C(12)           117.9(18) 
            C(10)-C(11)-H(11)           121.1 
            C(12)-C(11)-H(11)           121.1 
            C(26)-C(25)-C(24)           122(2) 
            C(26)-C(25)-H(25)           118.8 
            C(24)-C(25)-H(25)           118.8 
            C(45)-C(46)-C(47)           119.8(18) 
            C(45)-C(46)-H(46)           120.1 
            C(47)-C(46)-H(46)           120.1 
            N(8)-C(79)-N(7)             116.9(17) 
            N(8)-C(79)-Au(3)            125.0(14) 
            N(7)-C(79)-Au(3)            117.8(13) 
            C(71)-C(76)-C(72)           131(4) 
            C(71)-C(76)-H(76)           114.6 
            C(72)-C(76)-H(76)           114.6 
            C(24)-C(23)-C(22)           120.0(17) 
            C(24)-C(23)-H(23)           120.0 
            C(22)-C(23)-H(23)           120.0 
            C(43)-C(40)-C(39)           120(2) 
            C(43)-C(40)-H(40)           120.0 
            C(39)-C(40)-H(40)           120.0 
            C(18)-C(17)-C(16)           123(2) 
            C(18)-C(17)-H(17)           118.3 
            C(16)-C(17)-H(17)           118.3 
            C(25)-C(26)-C(21)           119.4(19) 
            C(25)-C(26)-H(26)           120.3 
            C(21)-C(26)-H(26)           120.3 
            C(48)-C(47)-C(46)           120(2) 
            C(48)-C(47)-H(47)           119.8 
            C(46)-C(47)-H(47)           119.8 
            C(74)-C(75)-C(70)           118.8(19) 
            C(74)-C(75)-H(75)           120.6 
            C(70)-C(75)-H(75)           120.6 
            C(43)-C(44)-C(49)           121.3(19) 
            C(43)-C(44)-C(45)           122.3(18) 
            C(49)-C(44)-C(45)           116.4(19) 
            C(15)-C(14)-C(19)           121.1(17) 
            C(15)-C(14)-C(13)           118.2(17) 
            C(19)-C(14)-C(13)           120.7(17) 
            N(4)-C(63)-H(63A)           109.5 
            N(4)-C(63)-H(63B)           109.5 
            H(63A)-C(63)-H(63B)         109.5 
            N(4)-C(63)-H(63C)           109.5 
            H(63A)-C(63)-H(63C)         109.5 
            H(63B)-C(63)-H(63C)         109.5 
            C(64)-C(62)-C(61)           119(2) 
            C(64)-C(62)-H(62)           120.6 
            C(61)-C(62)-H(62)           120.6 
            C(62)-C(61)-C(60)           121(2) 
            C(62)-C(61)-H(61)           119.6 
            C(60)-C(61)-H(61)           119.6 
            C(59)-C(60)-C(55)           122(2) 
            C(59)-C(60)-C(61)           120(2) 
            C(55)-C(60)-C(61)           118(2) 
            C(58)-C(59)-C(60)           117(2) 
            C(58)-C(59)-H(59)           121.6 
            C(60)-C(59)-H(59)           121.6 
            C(59)-C(58)-C(57)           123(2) 
            C(59)-C(58)-H(58)           118.6 
            C(57)-C(58)-H(58)           118.6 
            C(56)-C(57)-C(58)           119(2) 
            C(56)-C(57)-H(57)           120.3 
            C(58)-C(57)-H(57)           120.3 
            C(57)-C(56)-C(55)           120(2) 
            C(57)-C(56)-H(56)           120.0 
            C(55)-C(56)-H(56)           120.0 
            C(60)-C(55)-C(66)           117(2) 
            C(60)-C(55)-C(56)           119(2) 
            C(66)-C(55)-C(56)           124.1(19) 
            C(41)-C(54)-C(53)           119(2) 
            C(41)-C(54)-H(54)           120.3 
            C(53)-C(54)-H(54)           120.3 
            C(52)-C(53)-C(54)           119(2) 
            C(52)-C(53)-H(53)           120.4 
            C(54)-C(53)-H(53)           120.4 
            C(53)-C(52)-C(51)           121(2) 
            C(53)-C(52)-C(65)           119(2) 
            C(51)-C(52)-C(65)           120.0(18) 
            C(50)-C(51)-C(52)           119(2) 
            C(50)-C(51)-N(7)            121(2) 
            C(52)-C(51)-N(7)            119(2) 
            C(51)-C(50)-C(41)           121(3) 
            C(51)-C(50)-H(50)           119.4 
            C(41)-C(50)-H(50)           119.4 
            C(8)-C(12)-C(11)            123.2(19) 
            C(8)-C(12)-H(12)            118.4 
            C(11)-C(12)-H(12)           118.4 
            C(66)-C(64)-C(62)           122(2) 
            C(66)-C(64)-C(68)           110.0(19) 
            C(62)-C(64)-C(68)           128(2) 
            O(93)-C(68)-N(9)            125(2) 
            O(93)-C(68)-C(64)           129(2) 
            N(9)-C(68)-C(64)            106.4(16) 
            N(7)-C(67)-H(67A)           109.5 
            N(7)-C(67)-H(67B)           109.5 
            H(67A)-C(67)-H(67B)         109.5 
            N(7)-C(67)-H(67C)           109.5 
            H(67A)-C(67)-H(67C)         109.5 
            H(67B)-C(67)-H(67C)         109.5 
            C(64)-C(66)-C(55)           123(2) 
            C(64)-C(66)-C(65)           107.3(17) 
            C(55)-C(66)-C(65)           129.4(17) 
            N(2)-C(28)-H(28A)           109.5 
            N(2)-C(28)-H(28B)           109.5 
            H(28A)-C(28)-H(28B)         109.5 
            N(2)-C(28)-H(28C)           109.5 
            H(28A)-C(28)-H(28C)         109.5 
            H(28B)-C(28)-H(28C)         109.5 
            C(46)-C(45)-C(44)           123.5(18) 
            C(46)-C(45)-H(45)           118.3 
            C(44)-C(45)-H(45)           118.3 
            C(40)-C(43)-C(44)           119.7(18) 
            C(40)-C(43)-H(43)           120.2 
            C(44)-C(43)-H(43)           120.2 
            N(9)-C(65)-N(8)             112.5(14) 
            N(9)-C(65)-C(52)            112.7(16) 
            N(8)-C(65)-C(52)            108.2(15) 
            N(9)-C(65)-C(66)            102.3(15) 
            N(8)-C(65)-C(66)            111.7(15) 
            C(52)-C(65)-C(66)           109.5(14) 
            N(1)-C(27)-H(27A)           109.5 
            N(1)-C(27)-H(27B)           109.5 
            H(27A)-C(27)-H(27B)         109.5 
            N(1)-C(27)-H(27C)           109.5 
            H(27A)-C(27)-H(27C)         109.5 
            H(27B)-C(27)-H(27C)         109.5 
            N(9)-C(88)-C(70)            110.9(18) 
            N(9)-C(88)-H(88A)           109.5 
            C(70)-C(88)-H(88A)          109.5 
            N(9)-C(88)-H(88B)           109.5 
            C(70)-C(88)-H(88B)          109.5 
            H(88A)-C(88)-H(88B)         108.1 
            C(82)-C(83)-C(77)           120.0 
            C(82)-C(83)-H(83)           120.0 
            C(77)-C(83)-H(83)           120.0 
            C(81)-C(82)-C(83)           120.0 
            C(81)-C(82)-H(82)           120.0 
            C(83)-C(82)-H(82)           120.0 
            C(82)-C(81)-C(80)           120.0 
            C(82)-C(81)-H(81)           120.0 
            C(80)-C(81)-H(81)           120.0 
            C(81)-C(80)-C(78)           120.0 
            C(81)-C(80)-H(80)           120.0 
            C(78)-C(80)-H(80)           120.0 
            C(80)-C(78)-C(77)           120.0 
            C(80)-C(78)-C(73)           125(3) 
            C(77)-C(78)-C(73)           115(3) 
            C(78)-C(77)-C(83)           120.0 
            C(78)-C(77)-H(77)           120.0 
            C(83)-C(77)-H(77)           120.0 
            C(71)-C(70)-C(75)           113(2) 
            C(71)-C(70)-C(88)           126(2) 
            C(75)-C(70)-C(88)           120.7(19) 
            C(14)-C(15)-C(16)           118.1(19) 
            C(14)-C(15)-H(15)           120.9 
            C(16)-C(15)-H(15)           120.9 
            C(17)-C(16)-C(15)           120(2) 
            C(17)-C(16)-H(16)           120.0 
            C(15)-C(16)-H(16)           120.0 
            C(76)-C(71)-C(70)           121(3) 
            C(76)-C(71)-H(71)           119.6 
            C(70)-C(71)-H(71)           119.6 
            C(72)-C(74)-C(75)           124(2) 
            C(72)-C(74)-H(74)           118.1 
            C(75)-C(74)-H(74)           118.1 
            N(6)-C(73)-C(78)            113(3) 
            N(6)-C(73)-H(73A)           109.0 
            C(78)-C(73)-H(73A)          109.0 
            N(6)-C(73)-H(73B)           109.0 
            C(78)-C(73)-H(73B)          109.0 
            H(73A)-C(73)-H(73B)         107.8 
            C(76)-C(72)-C(74)           112(3) 
            C(76)-C(72)-H(72)           123.9 
            C(74)-C(72)-H(72)           123.9 
            O(64)-C(42)-N(6)            123(2) 
            O(64)-C(42)-C(39)           128(2) 
            N(6)-C(42)-C(39)            108(2) 
            C(54)-C(41)-C(50)           120(3) 
            C(54)-C(41)-H(41)           120.1 
            C(50)-C(41)-H(41)           120.1 
           _____________________________________________________________ 
  
           Symmetry transformations used to generate equivalent atoms: 
           #1 -x+2,y,-z+1     
  
    Table 4.  Anisotropic displacement parameters (A^2 x 10^3) for a. 
    The anisotropic displacement factor exponent takes the form: 
    -2 pi^2 [ h^2 a*^2 U11 + ... + 2 h k a* b* U12 ] 
  
    _______________________________________________________________________ 
  
              U11        U22        U33        U23        U13        U12 
    _______________________________________________________________________ 
  
    Au(1)    39(1)      38(1)      45(1)      -6(1)      16(1)      -8(1) 
    C(1)     44(8)      34(9)      33(8)       6(7)      10(7)      -2(7) 
    N(1)     38(6)      35(8)      39(7)     -11(5)      18(5)       2(5) 
    Cl(1)    50(2)      53(3)      44(2)     -10(2)       9(2)     -13(2) 
    Au(2)    78(1)      29(1)      42(1)      -4(1)      18(1)      -8(1) 
    C(2)     50(9)      38(9)      34(9)      -1(7)      15(7)       7(7) 
    N(2)     40(7)      30(7)      28(7)      -1(5)       3(5)      -5(6) 
    Cl(2)   109(4)      31(2)      52(3)      -3(2)      20(3)     -12(3) 
    Au(3)    69(1)      24(1)      64(1)      -1(1)      23(1)      -1(1) 
    C(3)     53(9)      37(9)      45(9)       9(7)      35(8)      11(7) 
    N(3)     44(7)      30(7)      33(7)      -3(6)      18(6)      -1(6) 
    Cl(3)   123(5)      24(2)      80(4)       3(3)       1(4)       4(3) 
    O(38)    53(6)      36(7)      51(7)       0(5)      22(6)     -11(5) 
    C(38)    79(13)     36(10)     48(11)     -5(8)      31(10)    -24(9) 
    C(37)   112(17)     34(10)     35(10)      1(8)      18(10)     23(11) 
    C(36)   150(20)     56(15)     44(12)      8(11)      4(14)    -27(13) 
    C(35)   190(30)     56(16)     32(11)    -13(11)     27(15)    -14(18) 
    C(33)   190(30)     33(12)     62(15)      6(10)     47(17)    -21(15) 
    C(32)   140(20)     47(12)     33(10)    -12(9)      27(12)    -32(14) 
    C(31)   180(30)     21(10)     55(14)     -5(8)      51(15)     -6(11) 
    C(30)    79(13)     24(9)      49(11)    -13(8)      33(10)    -11(8) 
    C(29)    88(15)     51(12)     47(12)      5(10)     30(11)    -16(11) 
    O(39)    88(11)     79(12)     40(8)     -15(8)      -8(7)     -12(9) 
    C(39)   103(17)     48(12)     74(15)    -32(11)     56(14)    -36(12) 
    C(49)    78(12)     31(9)      40(10)      1(8)      26(9)      -4(9) 
    C(9)     44(8)      42(10)     39(9)      -6(7)      21(7)      -3(7) 
    N(9)     80(10)     26(7)      58(10)      7(7)      41(8)      -7(7) 
    C(8)     70(12)     46(11)     55(11)      6(9)      32(10)      3(9) 
    N(8)     67(9)      26(7)      42(8)       5(6)      36(7)      -5(6) 
    C(22)    31(6)      37(9)      43(8)      -6(8)       7(6)       2(7) 
    C(21)    15(5)      45(9)      31(7)      -3(7)      -2(5)     -13(6) 
    C(20)    50(9)      30(8)      37(9)      -8(7)      25(7)      -3(7) 
    O(93)   131(14)     45(9)      60(10)      8(7)      40(10)     -6(9) 
    C(13)    39(8)      37(9)      45(9)      -3(7)      21(7)      -2(7) 
    C(24)    72(11)     35(10)     47(10)     -3(8)      29(9)      -1(8) 
    C(69)    75(12)     39(12)     72(14)     -4(9)      33(11)     -9(9) 
    C(10)    41(8)      35(9)      45(9)      -9(7)      18(7)       5(7) 
    C(19)    64(11)     37(10)     48(10)     -7(8)      31(9)      -6(8) 
    C(18)    50(10)     62(13)     22(8)      -2(8)      -6(7)      -7(9) 
    C(48)    83(14)     48(11)     41(10)     -4(9)      27(10)     -6(10) 
    C(7)     29(7)      40(9)      37(8)      -2(7)      17(6)      -9(6) 
    N(7)     49(8)      23(7)      65(10)      5(7)      24(7)       6(6) 
    C(6)    103(16)     47(12)     73(14)    -14(11)     60(13)      0(12) 
    N(6)    135(19)    107(18)     45(10)    -31(11)     57(12)    -76(16) 
    C(5)    106(18)     66(16)     61(14)    -11(12)     49(13)      8(13) 
    N(5)    122(15)     33(9)      28(8)      -8(7)      12(9)     -26(9) 
    C(4)     52(10)     67(14)     58(12)     12(11)     28(9)      18(10) 
    N(4)     84(12)     43(10)     63(12)     -2(8)      40(10)    -16(9) 
    C(11)    72(11)     30(9)      59(11)     -1(8)      30(9)      -6(8) 
    C(25)    76(13)     41(11)     46(11)      9(9)      11(9)      -2(9) 
    C(46)    67(12)     65(14)     33(9)     -12(9)      17(9)      11(10) 
    C(79)    43(8)      42(11)     64(12)      6(9)      30(8)       9(7) 
    C(76)   100(20)    130(30)    150(40)    -80(30)      0(20)     40(20) 
    C(23)    65(10)     39(10)     39(9)       8(8)      25(8)       8(8) 
    C(40)    82(14)     59(14)     52(12)    -11(10)     34(11)    -26(11) 
    C(17)    58(12)     55(14)     80(16)      3(12)     29(11)     -2(10) 
    C(26)    55(10)     38(10)     46(10)      7(8)      11(8)       2(8) 
    C(47)    65(12)     55(13)     52(12)      8(10)     26(10)     12(10) 
    C(75)    48(10)     93(18)     42(10)    -17(12)      8(8)     -15(11) 
    C(44)    67(11)     39(10)     47(11)      8(9)       8(9)       1(9) 
    C(14)    44(8)      45(10)     35(9)      -5(8)      12(7)       0(7) 
    C(63)    75(13)     42(11)     41(10)     -3(9)      11(9)     -11(10) 
    C(62)   107(15)     37(10)     34(10)      3(9)      12(9)       8(11) 
    C(61)    90(14)     43(11)     58(13)     12(10)      9(10)     11(11) 
    C(60)    96(16)     32(10)     48(12)      6(9)      12(11)      5(10) 
    C(59)    70(13)     86(18)     61(14)     11(13)     27(11)     21(13) 
    C(58)    63(13)     71(16)     91(19)      3(13)     40(13)      9(11) 
    C(57)    79(14)     54(13)     51(12)      4(10)     27(11)     18(11) 
    C(56)    65(12)     38(10)     64(14)     -4(9)      22(10)      4(9) 
    C(55)    71(12)     32(9)      51(11)    -13(8)      17(9)       7(8) 
    C(54)    97(17)     24(10)    104(19)     10(12)      7(15)     14(11) 
    C(53)    74(13)     26(10)     77(15)      7(10)     15(11)     -6(9) 
    C(52)    55(10)     28(9)      72(14)      5(9)      15(10)     -4(8) 
    C(51)    65(12)     36(11)     78(16)      8(10)     26(11)     -1(9) 
    C(50)    87(16)     21(9)      90(18)     -3(10)     31(13)     -5(9) 
    C(12)    83(12)     53(11)     44(10)    -21(10)     29(9)      -6(11) 
    O(64)   137(17)    128(19)    109(16)    -60(14)     81(14)    -87(16) 
    C(64)    95(15)     26(9)      50(12)      8(8)      28(11)     10(9) 
    C(68)   110(17)     29(9)      62(13)      5(9)      53(13)    -14(10) 
    C(67)    66(13)     26(10)    110(20)     -1(11)      2(13)    -12(9) 
    C(66)    75(12)     26(8)      50(11)     -3(7)      31(9)      -9(8) 
    C(28)    32(7)      55(11)     36(9)       2(8)      16(7)      -9(7) 
    C(45)    89(15)     57(13)     30(9)     -10(9)      25(9)      -1(11) 
    C(43)    88(14)     50(11)     24(8)     -14(8)      13(8)     -21(10) 
    C(65)    69(11)     37(9)      42(10)     -6(7)      38(9)       0(8) 
    C(27)    60(11)     48(12)     61(13)      6(11)     10(10)    -15(10) 
    C(88)    87(16)     74(17)     96(19)    -10(14)     65(15)    -13(13) 
    C(82)   700(200)   190(80)    440(150)  -240(100)   310(160)  -130(110) 
    C(81)   370(90)    120(40)    530(130)   -90(60)    370(100)     0(50) 
    C(80)   240(50)    120(30)    120(30)    -20(20)     90(30)    -20(30) 
    C(78)   120(30)    140(30)    130(30)    -60(20)     80(20)    -30(20) 
    C(77)   270(70)    270(90)    130(40)    -20(50)    -70(40)    -80(70) 
    C(70)    40(8)      72(15)     42(10)    -31(10)     13(7)     -20(9) 
    C(15)    57(11)     42(11)     63(13)     10(9)      24(9)     -12(8) 
    C(16)    64(12)     80(17)     58(14)     28(12)     25(11)      3(11) 
    C(71)    93(18)     80(20)     78(17)    -35(15)     -3(14)     30(15) 
    C(74)    72(13)    100(20)     72(14)     33(11)     45(10)     61(13) 
    C(73)   130(30)    160(40)     70(20)    -30(20)     59(19)    -80(30) 
    C(72)   100(20)     60(18)    160(30)    -17(19)     61(19)      2(16) 
    C(42)   105(19)     77(18)     81(17)    -34(14)     53(15)    -58(15) 
    C(41)   110(20)     42(14)    110(20)     -6(15)      6(19)      6(14) 
    _______________________________________________________________________ 
  
         Table 5.  Hydrogen coordinates ( x 10^4) and isotropic 
         displacement parameters (A^2 x 10^3) for a. 
  
         ________________________________________________________________ 
  
                         x             y             z           U(eq) 
         ________________________________________________________________ 
  
          H(3)         9087          1868          4071          48 
          H(37A)       1854          5295           162          93 
          H(37B)       2032          6219          -138          93 
          H(37C)       1616          6511           162          93 
          H(36)        1889          8138           104         109 
          H(35)        2132          9916           338         117 
          H(34)        2983         10323           947         109 
          H(33)        3608          9026          1370         112 
          H(39A)       5340(110)     4990(190)     2160(70)     102 
          H(39B)       5110(120)     4300(60)      2410(90)     102 
          H(13A)       7410          1437          5221          46 
          H(13B)       7709          2471          5067          46 
          H(24)        7045          4368          3401          59 
          H(69A)       7500          9517          2078          90 
          H(69B)       8052          8710          2199          90 
          H(69C)       7651          8750          2528          90 
          H(19)        8399          3412          5721          56 
          H(18)        9196          3367          6452          59 
          H(48)        2621          6586          1700          67 
          H(6)         8985         -1559          3353          80 
          H(5)         9532          -126          3183          87 
          H(4)         9608          1516          3574          67 
          H(11)        7800         -1967          4279          62 
          H(25)        6731          2592          3386          68 
          H(46)        2673          7530          2997          66 
          H(76)        6938         10163          3277         165 
          H(23)        7920          4928          3985          55 
          H(40)        5042          8032          2454          74 
          H(17)        9478          1709          6817          75 
          H(26)        7279          1314          3890          57 
          H(47)        2164          6741          2252          67 
          H(75)        5823          8631          1948          75 
          H(63A)       3415          4907          1763          82 
          H(63B)       3980          5087          1603          82 
          H(63C)       3482          4232          1332          82 
          H(62)        8726          5764          3415          75 
          H(61)        9486          5585          3105          80 
          H(59)        9855          5764          2429          85 
          H(58)        9701          6382          1684          86 
          H(57)        8755          6933          1192          72 
          H(56)        8005          7114          1497          67 
          H(54)        6994          3395          1579          98 
          H(53)        7479          4718          2142          74 
          H(50)        5957          5767           809          79 
          H(12)        8286         -2199          3730          70 
          H(67A)       5876          8533           916         111 
          H(67B)       5597          7346           903         111 
          H(67C)       6045          7580           623         111 
          H(28A)       9375           571          4991          60 
          H(28B)       9082           788          5386          60 
          H(28C)       9630          1507          5371          60 
          H(45)        3628          7971          3185          69 
          H(43)        4547          8326          2966          66 
          H(27A)       8948          5122          4476          70 
          H(27B)       9050          4993          5022          70 
          H(27C)       8410          5293          4670          70 
          H(88A)       6436          6594          2738          93 
          H(88B)       6277          6844          2192          93 
          H(83)        4058          3266           -40         552 
          H(82)        4782          2429           580         494 
          H(81)        5241          3400          1267         343 
          H(80)        4975          5208          1335         180 
          H(77)        3791          5075            28         308 
          H(15)        8256            81          5774          64 
          H(16)        8984           110          6530          80 
          H(71)        7035          8428          3225         111 
          H(74)        5747         10443          2092          89 
          H(73A)       4408          7061           616         138 
          H(73B)       3741          6644           452         138 
          H(72)        6356         11270          2752         122 
          H(41)        6204          3923           933         116 
         ________________________________________________________________ 
  
         Table 6.  Torsion angles [deg] for a. 
         ________________________________________________________________ 
  
          C(10)-C(1)-C(2)-C(3)                               -177.8(16) 
          C(7)-C(1)-C(2)-C(3)                                   6(3) 
          C(10)-C(1)-C(2)-C(8)                                 -1(3) 
          C(7)-C(1)-C(2)-C(8)                                -176.9(16) 
          C(1)-C(2)-C(3)-C(4)                                 178.4(17) 
          C(8)-C(2)-C(3)-C(4)                                   2(3) 
          C(31)-C(36)-C(35)-C(34)                               3(5) 
          C(36)-C(35)-C(34)-C(33)                              -1(5) 
          C(35)-C(34)-C(33)-C(32)                              -1(5) 
          C(34)-C(33)-C(32)-C(31)                              -1(4) 
          C(34)-C(33)-C(32)-C(29)                             178(3) 
          C(33)-C(32)-C(31)-N(5)                             -178(2) 
          C(29)-C(32)-C(31)-N(5)                                4(4) 
          C(33)-C(32)-C(31)-C(36)                               3(4) 
          C(29)-C(32)-C(31)-C(36)                            -175(2) 
          C(35)-C(36)-C(31)-C(32)                              -4(4) 
          C(35)-C(36)-C(31)-N(5)                              176(3) 
          C(31)-C(32)-C(29)-N(6)                              108(3) 
          C(33)-C(32)-C(29)-N(6)                              -70(3) 
          C(31)-C(32)-C(29)-N(4)                              -15(3) 
          C(33)-C(32)-C(29)-N(4)                              167(2) 
          C(31)-C(32)-C(29)-C(38)                            -139(2) 
          C(33)-C(32)-C(29)-C(38)                              43(3) 
          C(39)-C(38)-C(29)-N(6)                                5(3) 
          C(49)-C(38)-C(29)-N(6)                             -176(2) 
          C(39)-C(38)-C(29)-C(32)                            -113(2) 
          C(49)-C(38)-C(29)-C(32)                              67(3) 
          C(39)-C(38)-C(29)-N(4)                              126(2) 
          C(49)-C(38)-C(29)-N(4)                              -54(3) 
          C(49)-C(38)-C(39)-C(40)                              -5(4) 
          C(29)-C(38)-C(39)-C(40)                             175(2) 
          C(49)-C(38)-C(39)-C(42)                             177(2) 
          C(29)-C(38)-C(39)-C(42)                              -4(3) 
          C(39)-C(38)-C(49)-C(48)                            -174(2) 
          C(29)-C(38)-C(49)-C(48)                               6(4) 
          C(39)-C(38)-C(49)-C(44)                               5(3) 
          C(29)-C(38)-C(49)-C(44)                            -174(2) 
          C(13)-N(3)-C(9)-O(38)                                -5(3) 
          C(7)-N(3)-C(9)-O(38)                               -175.0(16) 
          C(13)-N(3)-C(9)-C(10)                               177.4(15) 
          C(7)-N(3)-C(9)-C(10)                                  7.3(19) 
          C(1)-C(2)-C(8)-C(6)                                -179.1(19) 
          C(3)-C(2)-C(8)-C(6)                                  -2(3) 
          C(1)-C(2)-C(8)-C(12)                                  3(3) 
          C(3)-C(2)-C(8)-C(12)                                180.0(18) 
          C(20)-N(1)-C(22)-C(21)                                5(2) 
          C(27)-N(1)-C(22)-C(21)                             -172.9(16) 
          C(20)-N(1)-C(22)-C(23)                             -173.6(14) 
          C(27)-N(1)-C(22)-C(23)                                9(2) 
          N(1)-C(22)-C(21)-C(26)                              177.2(15) 
          C(23)-C(22)-C(21)-C(26)                              -4(2) 
          N(1)-C(22)-C(21)-C(7)                                 0(2) 
          C(23)-C(22)-C(21)-C(7)                              178.6(14) 
          C(7)-N(2)-C(20)-N(1)                                -15(2) 
          C(28)-N(2)-C(20)-N(1)                               177.8(13) 
          C(7)-N(2)-C(20)-Au(1)                               166.3(11) 
          C(28)-N(2)-C(20)-Au(1)                               -0.7(19) 
          C(22)-N(1)-C(20)-N(2)                                 2(2) 
          C(27)-N(1)-C(20)-N(2)                               179.9(15) 
          C(22)-N(1)-C(20)-Au(1)                             -179.3(11) 
          C(27)-N(1)-C(20)-Au(1)                               -1.6(19) 
          C(9)-N(3)-C(13)-C(14)                               100.4(18) 
          C(7)-N(3)-C(13)-C(14)                               -90.3(18) 
          C(2)-C(1)-C(10)-C(11)                                 0(3) 
          C(7)-C(1)-C(10)-C(11)                               177.1(16) 
          C(2)-C(1)-C(10)-C(9)                                178.4(15) 
          C(7)-C(1)-C(10)-C(9)                                 -4.9(19) 
          O(38)-C(9)-C(10)-C(11)                               -1(3) 
          N(3)-C(9)-C(10)-C(11)                               176.6(18) 
          O(38)-C(9)-C(10)-C(1)                              -178.9(17) 
          N(3)-C(9)-C(10)-C(1)                                 -1.2(19) 
          C(14)-C(19)-C(18)-C(17)                              -2(3) 
          C(38)-C(49)-C(48)-C(47)                            -180(2) 
          C(44)-C(49)-C(48)-C(47)                               1(3) 
          C(20)-N(2)-C(7)-N(3)                               -105.8(18) 
          C(28)-N(2)-C(7)-N(3)                                 61.6(17) 
          C(20)-N(2)-C(7)-C(21)                                18(2) 
          C(28)-N(2)-C(7)-C(21)                              -174.3(13) 
          C(20)-N(2)-C(7)-C(1)                                142.1(15) 
          C(28)-N(2)-C(7)-C(1)                                -50.5(18) 
          C(9)-N(3)-C(7)-N(2)                                -128.1(15) 
          C(13)-N(3)-C(7)-N(2)                                 61.5(19) 
          C(9)-N(3)-C(7)-C(21)                                109.0(16) 
          C(13)-N(3)-C(7)-C(21)                               -61.4(18) 
          C(9)-N(3)-C(7)-C(1)                                  -9.6(17) 
          C(13)-N(3)-C(7)-C(1)                                180.0(14) 
          C(26)-C(21)-C(7)-N(2)                               172.7(14) 
          C(22)-C(21)-C(7)-N(2)                               -10.2(19) 
          C(26)-C(21)-C(7)-N(3)                               -63.1(19) 
          C(22)-C(21)-C(7)-N(3)                               114.0(16) 
          C(26)-C(21)-C(7)-C(1)                                49.0(19) 
          C(22)-C(21)-C(7)-C(1)                              -133.9(15) 
          C(10)-C(1)-C(7)-N(2)                                127.3(15) 
          C(2)-C(1)-C(7)-N(2)                                 -56(2) 
          C(10)-C(1)-C(7)-N(3)                                  8.5(17) 
          C(2)-C(1)-C(7)-N(3)                                -175.0(16) 
          C(10)-C(1)-C(7)-C(21)                              -110.1(15) 
          C(2)-C(1)-C(7)-C(21)                                 66(2) 
          C(12)-C(8)-C(6)-C(5)                                178(2) 
          C(2)-C(8)-C(6)-C(5)                                   0(3) 
          C(32)-C(29)-N(6)-C(42)                              112(3) 
          N(4)-C(29)-N(6)-C(42)                              -127(2) 
          C(38)-C(29)-N(6)-C(42)                               -4(3) 
          C(32)-C(29)-N(6)-C(73)                              -68(4) 
          N(4)-C(29)-N(6)-C(73)                                54(4) 
          C(38)-C(29)-N(6)-C(73)                              176(3) 
          C(8)-C(6)-C(5)-C(4)                                   3(4) 
          N(4)-C(30)-N(5)-C(31)                                -3(3) 
          Au(2)-C(30)-N(5)-C(31)                              173.0(18) 
          N(4)-C(30)-N(5)-C(37)                               179.4(19) 
          Au(2)-C(30)-N(5)-C(37)                               -5(3) 
          C(32)-C(31)-N(5)-C(30)                                6(4) 
          C(36)-C(31)-N(5)-C(30)                             -174(2) 
          C(32)-C(31)-N(5)-C(37)                             -176(2) 
          C(36)-C(31)-N(5)-C(37)                                3(4) 
          C(2)-C(3)-C(4)-C(5)                                   1(3) 
          C(6)-C(5)-C(4)-C(3)                                  -3(4) 
          N(5)-C(30)-N(4)-C(63)                               174.8(19) 
          Au(2)-C(30)-N(4)-C(63)                               -1(2) 
          N(5)-C(30)-N(4)-C(29)                               -11(3) 
          Au(2)-C(30)-N(4)-C(29)                              173.1(15) 
          N(6)-C(29)-N(4)-C(30)                              -104(2) 
          C(32)-C(29)-N(4)-C(30)                               19(3) 
          C(38)-C(29)-N(4)-C(30)                              139(2) 
          N(6)-C(29)-N(4)-C(63)                                71(2) 
          C(32)-C(29)-N(4)-C(63)                             -166.4(18) 
          C(38)-C(29)-N(4)-C(63)                              -46(3) 
          C(1)-C(10)-C(11)-C(12)                               -2(3) 
          C(9)-C(10)-C(11)-C(12)                             -179.4(18) 
          C(23)-C(24)-C(25)-C(26)                              -3(3) 
          C(69)-N(8)-C(79)-N(7)                              -177.8(15) 
          C(65)-N(8)-C(79)-N(7)                               -16(2) 
          C(69)-N(8)-C(79)-Au(3)                                8(2) 
          C(65)-N(8)-C(79)-Au(3)                              170.2(11) 
          C(67)-N(7)-C(79)-N(8)                              -176.1(19) 
          C(51)-N(7)-C(79)-N(8)                               -10(2) 
          C(67)-N(7)-C(79)-Au(3)                               -2(2) 
          C(51)-N(7)-C(79)-Au(3)                              164.1(15) 
          C(25)-C(24)-C(23)-C(22)                               1(3) 
          N(1)-C(22)-C(23)-C(24)                             -178.9(14) 
          C(21)-C(22)-C(23)-C(24)                               3(2) 
          C(38)-C(39)-C(40)-C(43)                               0(4) 
          C(42)-C(39)-C(40)-C(43)                             178(3) 
          C(19)-C(18)-C(17)-C(16)                              -2(3) 
          C(24)-C(25)-C(26)-C(21)                               1(3) 
          C(22)-C(21)-C(26)-C(25)                               3(3) 
          C(7)-C(21)-C(26)-C(25)                              179.7(17) 
          C(49)-C(48)-C(47)-C(46)                               0(3) 
          C(45)-C(46)-C(47)-C(48)                              -3(3) 
          C(38)-C(49)-C(44)-C(43)                              -1(3) 
          C(48)-C(49)-C(44)-C(43)                             178.2(19) 
          C(38)-C(49)-C(44)-C(45)                            -179(2) 
          C(48)-C(49)-C(44)-C(45)                               0(3) 
          C(18)-C(19)-C(14)-C(15)                               2(3) 
          C(18)-C(19)-C(14)-C(13)                            -176.0(15) 
          N(3)-C(13)-C(14)-C(15)                              -58(2) 
          N(3)-C(13)-C(14)-C(19)                              120.1(17) 
          C(64)-C(62)-C(61)-C(60)                               2(3) 
          C(62)-C(61)-C(60)-C(59)                            -179(2) 
          C(62)-C(61)-C(60)-C(55)                              -2(3) 
          C(55)-C(60)-C(59)-C(58)                               4(4) 
          C(61)-C(60)-C(59)-C(58)                            -178(2) 
          C(60)-C(59)-C(58)-C(57)                              -5(4) 
          C(59)-C(58)-C(57)-C(56)                               5(4) 
          C(58)-C(57)-C(56)-C(55)                              -3(3) 
          C(59)-C(60)-C(55)-C(66)                             178(2) 
          C(61)-C(60)-C(55)-C(66)                               0(3) 
          C(59)-C(60)-C(55)-C(56)                              -3(3) 
          C(61)-C(60)-C(55)-C(56)                             179.6(18) 
          C(57)-C(56)-C(55)-C(60)                               2(3) 
          C(57)-C(56)-C(55)-C(66)                            -178.6(19) 
          C(41)-C(54)-C(53)-C(52)                              -6(4) 
          C(54)-C(53)-C(52)-C(51)                               5(4) 
          C(54)-C(53)-C(52)-C(65)                             176(2) 
          C(53)-C(52)-C(51)-C(50)                              -1(3) 
          C(65)-C(52)-C(51)-C(50)                            -171(2) 
          C(53)-C(52)-C(51)-N(7)                              174(2) 
          C(65)-C(52)-C(51)-N(7)                                4(3) 
          C(79)-N(7)-C(51)-C(50)                             -170(2) 
          C(67)-N(7)-C(51)-C(50)                               -4(3) 
          C(79)-N(7)-C(51)-C(52)                               15(3) 
          C(67)-N(7)-C(51)-C(52)                             -179(2) 
          C(52)-C(51)-C(50)-C(41)                              -2(4) 
          N(7)-C(51)-C(50)-C(41)                             -177(3) 
          C(6)-C(8)-C(12)-C(11)                               177(2) 
          C(2)-C(8)-C(12)-C(11)                                -5(3) 
          C(10)-C(11)-C(12)-C(8)                                4(3) 
          C(61)-C(62)-C(64)-C(66)                               0(3) 
          C(61)-C(62)-C(64)-C(68)                            -180(2) 
          C(65)-N(9)-C(68)-O(93)                             -177.7(19) 
          C(88)-N(9)-C(68)-O(93)                               -1(3) 
          C(65)-N(9)-C(68)-C(64)                                2(2) 
          C(88)-N(9)-C(68)-C(64)                              178.4(19) 
          C(66)-C(64)-C(68)-O(93)                            -178(2) 
          C(62)-C(64)-C(68)-O(93)                               1(4) 
          C(66)-C(64)-C(68)-N(9)                                2(2) 
          C(62)-C(64)-C(68)-N(9)                             -179(2) 
          C(62)-C(64)-C(66)-C(55)                              -1(3) 
          C(68)-C(64)-C(66)-C(55)                             178.1(17) 
          C(62)-C(64)-C(66)-C(65)                             175.8(18) 
          C(68)-C(64)-C(66)-C(65)                              -5(2) 
          C(60)-C(55)-C(66)-C(64)                               1(3) 
          C(56)-C(55)-C(66)-C(64)                            -178.0(19) 
          C(60)-C(55)-C(66)-C(65)                            -175.2(18) 
          C(56)-C(55)-C(66)-C(65)                               5(3) 
          C(47)-C(46)-C(45)-C(44)                               4(4) 
          C(43)-C(44)-C(45)-C(46)                             179(2) 
          C(49)-C(44)-C(45)-C(46)                              -3(3) 
          C(39)-C(40)-C(43)-C(44)                               4(4) 
          C(49)-C(44)-C(43)-C(40)                              -4(3) 
          C(45)-C(44)-C(43)-C(40)                             175(2) 
          C(68)-N(9)-C(65)-N(8)                              -124.5(17) 
          C(88)-N(9)-C(65)-N(8)                                59(2) 
          C(68)-N(9)-C(65)-C(52)                              112.8(18) 
          C(88)-N(9)-C(65)-C(52)                              -64(2) 
          C(68)-N(9)-C(65)-C(66)                               -5(2) 
          C(88)-N(9)-C(65)-C(66)                              179.0(17) 
          C(79)-N(8)-C(65)-N(9)                               -93(2) 
          C(69)-N(8)-C(65)-N(9)                                69(2) 
          C(79)-N(8)-C(65)-C(52)                               32(2) 
          C(69)-N(8)-C(65)-C(52)                             -166.0(15) 
          C(79)-N(8)-C(65)-C(66)                              152.3(16) 
          C(69)-N(8)-C(65)-C(66)                              -45.4(19) 
          C(53)-C(52)-C(65)-N(9)                              -69(3) 
          C(51)-C(52)-C(65)-N(9)                              101(2) 
          C(53)-C(52)-C(65)-N(8)                              165.6(19) 
          C(51)-C(52)-C(65)-N(8)                              -24(2) 
          C(53)-C(52)-C(65)-C(66)                              44(2) 
          C(51)-C(52)-C(65)-C(66)                            -146.0(19) 
          C(64)-C(66)-C(65)-N(9)                                5.5(19) 
          C(55)-C(66)-C(65)-N(9)                             -177.4(17) 
          C(64)-C(66)-C(65)-N(8)                              126.0(16) 
          C(55)-C(66)-C(65)-N(8)                              -57(2) 
          C(64)-C(66)-C(65)-C(52)                            -114.2(17) 
          C(55)-C(66)-C(65)-C(52)                              63(2) 
          C(68)-N(9)-C(88)-C(70)                               93(2) 
          C(65)-N(9)-C(88)-C(70)                              -91(2) 
          C(77)-C(83)-C(82)-C(81)                               0.0 
          C(83)-C(82)-C(81)-C(80)                               0.0 
          C(82)-C(81)-C(80)-C(78)                               0.0 
          C(81)-C(80)-C(78)-C(77)                               0.0 
          C(81)-C(80)-C(78)-C(73)                             179(3) 
          C(80)-C(78)-C(77)-C(83)                               0.0 
          C(73)-C(78)-C(77)-C(83)                            -179(2) 
          C(82)-C(83)-C(77)-C(78)                               0.0 
          C(74)-C(75)-C(70)-C(71)                              -1(3) 
          C(74)-C(75)-C(70)-C(88)                            -176.0(19) 
          N(9)-C(88)-C(70)-C(71)                              -56(3) 
          N(9)-C(88)-C(70)-C(75)                              118(2) 
          C(19)-C(14)-C(15)-C(16)                               1(3) 
          C(13)-C(14)-C(15)-C(16)                             179.2(16) 
          C(18)-C(17)-C(16)-C(15)                               5(3) 
          C(14)-C(15)-C(16)-C(17)                              -5(3) 
          C(72)-C(76)-C(71)-C(70)                               0(8) 
          C(75)-C(70)-C(71)-C(76)                              -1(5) 
          C(88)-C(70)-C(71)-C(76)                             174(3) 
          C(70)-C(75)-C(74)-C(72)                               4(4) 
          C(42)-N(6)-C(73)-C(78)                               83(3) 
          C(29)-N(6)-C(73)-C(78)                              -97(4) 
          C(80)-C(78)-C(73)-N(6)                              -39(3) 
          C(77)-C(78)-C(73)-N(6)                              141(2) 
          C(71)-C(76)-C(72)-C(74)                               2(7) 
          C(75)-C(74)-C(72)-C(76)                              -4(5) 
          C(29)-N(6)-C(42)-O(64)                              178(3) 
          C(73)-N(6)-C(42)-O(64)                               -2(5) 
          C(29)-N(6)-C(42)-C(39)                                2(3) 
          C(73)-N(6)-C(42)-C(39)                             -178(3) 
          C(38)-C(39)-C(42)-O(64)                            -175(3) 
          C(40)-C(39)-C(42)-O(64)                               7(5) 
          C(38)-C(39)-C(42)-N(6)                                1(3) 
          C(40)-C(39)-C(42)-N(6)                             -177(3) 
          C(53)-C(54)-C(41)-C(50)                               3(5) 
          C(51)-C(50)-C(41)-C(54)                               1(5) 
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         Symmetry transformations used to generate equivalent atoms: 
         #1 -x+2,y,-z+1     
  
 Table 7.  Hydrogen bonds for a [A and deg.]. 
 ____________________________________________________________________________ 
  
 D-H...A                      d(D-H)      d(H...A)    d(D...A)    <(DHA) 
  
