      Table 1.  Crystal data and structure refinement for t. 
  
  
      Identification code               t 
  
      Empirical formula                 C26 H18 Cl N3 O 
  
      Formula weight                    423.88 
  
      Temperature                       173(2) K 
  
      Wavelength                        1.54178 A 
  
      Crystal system, space group       Triclinic,  P1 
  
      Unit cell dimensions              a = 9.8911(4) A   alpha = 87.166(2) deg. 
                                        b = 15.4147(6) A    beta = 80.070(3) deg. 
                                        c = 15.4438(7) A   gamma = 86.647(3) deg. 
  
      Volume                            2313.59(17) A^3 
  
      Z, Calculated density             4,  1.217 Mg/m^3 
  
      Absorption coefficient            1.627 mm^-1 
  
      F(000)                            880 
  
      Crystal size                      0.150 x 0.140 x 0.120 mm 
  
      Theta range for data collection   2.874 to 63.657 deg. 
  
      Limiting indices                  -11<=h<=11, -17<=k<=17, -17<=l<=17 
  
      Reflections collected / unique    41599 / 14698 [R(int) = 0.0656] 
  
      Completeness to theta = 63.657    99.9 % 
  
      Absorption correction             Semi-empirical from equivalents 
  
      Max. and min. transmission        0.7531 and 0.6781 
  
      Refinement method                 Full-matrix least-squares on F^2 
  
      Data / restraints / parameters    14698 / 9 / 1121 
  
      Goodness-of-fit on F^2            0.940 
  
      Final R indices [I>2sigma(I)]     R1 = 0.0665, wR2 = 0.1576 
  
      R indices (all data)              R1 = 0.1129, wR2 = 0.1856 
  
      Absolute structure parameter      0.057(9) 
  
      Extinction coefficient            n/a 
  
      Largest diff. peak and hole       0.364 and -0.347 e.A^-3 
  
         Table 2.  Atomic coordinates ( x 10^4) and equivalent isotropic 
         displacement parameters (A^2 x 10^3) for t. 
         U(eq) is defined as one third of the trace of the orthogonalized 
         Uij tensor. 
  
         ________________________________________________________________ 
  
                         x             y             z           U(eq) 
         ________________________________________________________________ 
  
          Cl(2)        3115(6)      10088(2)       8194(2)      194(3) 
          Cl(3)        4878(6)        977(3)      10090(2)      192(2) 
          Cl(4)       10193(3)        -72(2)       1754(2)      116(1) 
          O(1)         9901(5)       6049(3)       4943(3)       57(1) 
          Cl(1)       12119(4)       8740(2)        -70(2)      125(1) 
          N(1)         8243(7)       5958(4)       2517(4)       60(2) 
          N(10)        5773(6)       2434(3)       4370(4)       50(2) 
          N(11)        5748(7)       1426(4)       3281(4)       61(2) 
          N(12)        7375(6)       3484(3)       3699(4)       46(1) 
          C(1)         7598(11)      6382(6)       1900(6)       76(3) 
          O(2)         2164(5)       5109(3)       6189(3)       51(1) 
          O(3)         5040(5)       3986(3)       5316(3)       53(1) 
          O(4)         7704(5)       4886(3)       4047(3)       59(1) 
          N(2)         9493(6)       6515(3)       3566(4)       48(2) 
          N(3)          -27(7)       7609(4)       5835(4)       58(2) 
          N(4)         1375(6)       6512(3)       6483(4)       49(2) 
          C(2)         1152(11)      3538(6)       8252(6)       73(3) 
          C(12)        8071(11)      8764(5)       3957(7)       77(3) 
          C(13)        6811(10)      8630(5)       4474(6)       66(2) 
          C(14)        6463(9)       7788(5)       4679(6)       65(2) 
          C(15)        7334(9)       7094(5)       4367(6)       63(2) 
          C(16)        5838(11)      9383(5)       4823(8)       90(3) 
          C(17)       10018(8)       5946(5)       4142(5)       54(2) 
          C(18)       10447(8)       5312(4)       2794(5)       52(2) 
          C(19)       10687(8)       5223(4)       3648(5)       50(2) 
          C(20)       11381(8)       4465(5)       3963(5)       59(2) 
          C(21)       11739(9)       3807(5)       3392(6)       66(2) 
          C(22)       11441(8)       3876(5)       2511(6)       59(2) 
          C(23)       10800(8)       4628(5)       2197(5)       58(2) 
          C(24)       10523(9)       4684(6)       1332(6)       70(2) 
          C(3)         9465(11)      7160(5)       1351(6)       71(2) 
          C(25)       10831(11)      3991(7)        801(7)       87(3) 
          C(26)       11456(12)      3217(7)       1121(8)       91(3) 
          C(27)       11771(10)      3174(6)       1938(7)       81(3) 
          C(28)        -842(12)      8230(6)       6258(7)       93(3) 
          C(29)         808(15)      8708(5)       6930(6)       94(4) 
          C(30)        1250(20)      9343(6)       7430(8)      128(6) 
          C(31)        2590(20)      9311(7)       7563(7)      123(5) 
          C(32)        3547(14)      8698(7)       7201(7)      102(4) 
          C(33)        3155(12)      8065(6)       6681(6)       81(3) 
          C(34)        1777(11)      8086(5)       6535(5)       66(2) 
          C(35)        1352(8)       7383(4)       5990(5)       52(2) 
          C(36)         468(8)       6301(4)       7277(5)       52(2) 
          C(37)         706(9)       6515(5)       8094(5)       64(2) 
          C(38)        -162(10)      6275(6)       8857(6)       73(2) 
          C(39)       -1282(10)      5781(6)       8812(6)       73(2) 
          C(40)       -1507(9)       5555(6)       7982(6)       70(2) 
          C(41)        -641(9)       5818(5)       7229(5)       59(2) 
          C(42)       -2238(12)      5493(9)       9642(7)      105(4) 
          C(43)        2125(8)       5890(4)       5997(5)       49(2) 
          C(44)        2827(8)       6333(4)       5188(5)       50(2) 
          C(45)        3769(8)       5970(5)       4500(6)       61(2) 
          C(46)        4210(9)       6507(5)       3786(6)       64(2) 
          C(47)        3742(9)       7375(5)       3719(6)       67(2) 
          C(48)        4202(12)      7924(6)       2981(7)       86(3) 
          C(49)        3742(12)      8764(6)       2914(6)       88(3) 
          C(50)        2695(12)      9110(6)       3583(6)       88(3) 
          C(51)        2223(10)      8626(5)       4329(6)       68(2) 
          C(52)        2756(8)       7743(4)       4416(5)       55(2) 
          C(53)        2351(8)       7183(4)       5166(5)       51(2) 
          C(54)        2817(13)      2709(5)       8748(6)       79(2) 
          C(55)        3145(15)      2001(5)       9320(6)       95(3) 
          C(56)        4518(19)      1855(8)       9379(7)      118(5) 
          C(57)        5556(17)      2316(9)       8901(8)      132(6) 
          C(58)        5214(13)      2983(7)       8343(6)       91(3) 
          C(59)        3847(11)      3183(5)       8263(5)       70(2) 
          C(60)        3511(9)       3850(5)       7577(5)       56(2) 
          C(61)        3360(8)       2786(4)       6361(5)       52(2) 
          C(62)        3851(9)       1949(4)       6525(5)       62(2) 
          C(63)        3295(10)      1279(5)       6163(6)       71(2) 
          C(64)        2211(11)      1394(5)       5697(6)       71(2) 
          C(65)        1741(9)       2254(5)       5554(6)       67(2) 
          C(66)        2298(9)       2935(5)       5885(5)       62(2) 
          C(67)        1644(12)       653(6)       5318(8)       98(3) 
          C(68)        4697(8)       4080(4)       6111(5)       50(2) 
          C(69)        4990(8)       4791(5)       6631(5)       51(2) 
          C(70)        5721(8)       5539(5)       6349(5)       61(2) 
          C(71)        5710(9)       6172(5)       6942(6)       68(2) 
          C(72)        4977(9)       6094(5)       7808(6)       64(2) 
          C(73)        4233(8)       5332(5)       8095(5)       56(2) 
          C(74)        4290(8)       4694(4)       7470(5)       52(2) 
          C(75)        4951(11)      6750(6)       8418(7)       84(3) 
          C(76)        4190(13)      6694(7)       9236(7)       94(3) 
          C(77)        3428(10)      5956(6)       9506(6)       76(3) 
          C(78)        3456(9)       5292(5)       8967(5)       65(2) 
          C(79)        5160(8)       1934(4)       3886(5)       54(2) 
          C(80)        7205(8)       1383(4)       3155(5)       54(2) 
          C(81)        7920(11)       764(5)       2580(6)       70(2) 
          C(82)        9347(11)       703(5)       2458(6)       73(2) 
          C(83)       10076(9)       1211(5)       2889(6)       65(2) 
          C(84)        9385(8)       1810(5)       3459(5)       58(2) 
          C(85)        7953(8)       1900(4)       3593(4)       47(2) 
          C(86)        7220(7)       2613(4)       4163(4)       46(2) 
          C(87)        6795(8)       3688(4)       2904(5)       52(2) 
          C(88)        7502(9)       3376(5)       2107(5)       59(2) 
          C(89)        6875(11)      3527(7)       1368(6)       82(2) 
          C(90)        5616(12)      4010(7)       1424(7)       87(3) 
          C(91)        5003(10)      4304(6)       2205(7)       78(3) 
          C(92)        5543(9)       4150(5)       2967(6)       65(2) 
          C(93)        4909(14)      4129(10)       606(7)      127(5) 
          C(94)        7707(7)       4095(4)       4217(5)       50(2) 
          C(95)        8055(7)       3633(4)       5013(5)       50(2) 
          C(96)        7770(8)       2778(4)       4999(5)       50(2) 
          C(97)        7904(8)       2188(4)       5718(5)       53(2) 
          C(98)        7578(9)       1308(5)       5758(6)       65(2) 
          C(99)        7750(11)       779(6)       6478(6)       83(3) 
          C(100)       8203(12)      1139(8)       7196(6)       92(3) 
          C(101)       8530(11)      1975(7)       7175(6)       88(3) 
          C(102)       8367(9)       2548(5)       6443(5)       63(2) 
          C(103)       8679(9)       3439(6)       6418(6)       68(2) 
          C(104)       8542(8)       3979(5)       5721(6)       63(2) 
          C(4)        10062(13)      7747(6)        739(6)       86(3) 
          C(5)        11380(13)      7968(5)        723(6)       83(2) 
          C(6)        12205(12)      7610(6)       1306(6)       83(3) 
          C(7)        11598(11)      6985(6)       1932(6)       77(3) 
          C(8)        10237(10)      6772(5)       1961(5)       63(2) 
          C(9)         9592(8)       6161(4)       2671(5)       55(2) 
          C(10)        8591(8)       7243(4)       3843(5)       52(2) 
          C(11)        8974(9)       8082(5)       3638(6)       64(2) 
          N(5)         -552(14)      8765(6)       6792(7)      135(5) 
          N(6)         8098(10)      6960(6)       1345(6)       87(2) 
          N(7)         2027(7)       4054(4)       7730(4)       58(2) 
          N(8)         1419(10)      2885(5)       8726(5)       83(2) 
          N(9)         3950(6)       3518(3)       6666(4)       50(2) 
         ________________________________________________________________ 
  
           Table 3.  Bond lengths [A] and angles [deg] for t. 
           _____________________________________________________________ 
  
            Cl(2)-C(31)                   1.734(11) 
            Cl(3)-C(56)                   1.760(11) 
            Cl(4)-C(82)                   1.734(8) 
            O(1)-C(17)                    1.240(8) 
            Cl(1)-C(5)                    1.761(9) 
            N(1)-C(1)                     1.357(11) 
            N(1)-C(9)                     1.450(10) 
            N(10)-C(79)                   1.338(9) 
            N(10)-C(86)                   1.451(9) 
            N(11)-C(79)                   1.286(9) 
            N(11)-C(80)                   1.419(10) 
            N(12)-C(94)                   1.354(8) 
            N(12)-C(87)                   1.456(9) 
            N(12)-C(86)                   1.493(9) 
            C(1)-N(6)                     1.266(12) 
            O(2)-C(43)                    1.226(8) 
            O(3)-C(68)                    1.230(8) 
            O(4)-C(94)                    1.235(8) 
            N(2)-C(17)                    1.362(9) 
            N(2)-C(10)                    1.427(9) 
            N(2)-C(9)                     1.497(9) 
            N(3)-C(28)                    1.335(10) 
            N(3)-C(35)                    1.445(10) 
            N(4)-C(43)                    1.352(9) 
            N(4)-C(36)                    1.424(10) 
            N(4)-C(35)                    1.511(9) 
            C(2)-N(8)                     1.257(11) 
            C(2)-N(7)                     1.345(10) 
            C(12)-C(13)                   1.380(13) 
            C(12)-C(11)                   1.390(12) 
            C(13)-C(14)                   1.371(11) 
            C(13)-C(16)                   1.522(12) 
            C(14)-C(15)                   1.385(11) 
            C(15)-C(10)                   1.386(11) 
            C(17)-C(19)                   1.444(10) 
            C(18)-C(19)                   1.380(10) 
            C(18)-C(23)                   1.423(10) 
            C(18)-C(9)                    1.538(11) 
            C(19)-C(20)                   1.428(10) 
            C(20)-C(21)                   1.368(11) 
            C(21)-C(22)                   1.439(12) 
            C(22)-C(23)                   1.395(11) 
            C(22)-C(27)                   1.418(11) 
            C(23)-C(24)                   1.407(12) 
            C(24)-C(25)                   1.367(12) 
            C(3)-C(4)                     1.359(13) 
            C(3)-C(8)                     1.403(12) 
            C(3)-N(6)                     1.406(13) 
            C(25)-C(26)                   1.418(15) 
            C(26)-C(27)                   1.349(15) 
            C(28)-N(5)                    1.272(13) 
            C(29)-N(5)                    1.395(16) 
            C(29)-C(34)                   1.399(14) 
            C(29)-C(30)                   1.407(15) 
            C(30)-C(31)                   1.38(2) 
            C(31)-C(32)                   1.36(2) 
            C(32)-C(33)                   1.405(12) 
            C(33)-C(34)                   1.418(14) 
            C(34)-C(35)                   1.525(10) 
            C(35)-C(53)                   1.504(10) 
            C(36)-C(41)                   1.375(11) 
            C(36)-C(37)                   1.382(10) 
            C(37)-C(38)                   1.381(12) 
            C(38)-C(39)                   1.394(13) 
            C(39)-C(40)                   1.402(12) 
            C(39)-C(42)                   1.518(14) 
            C(40)-C(41)                   1.379(12) 
            C(43)-C(44)                   1.477(10) 
            C(44)-C(53)                   1.367(10) 
            C(44)-C(45)                   1.403(11) 
            C(45)-C(46)                   1.369(11) 
            C(46)-C(47)                   1.395(11) 
            C(47)-C(48)                   1.412(12) 
            C(47)-C(52)                   1.437(11) 
            C(48)-C(49)                   1.352(13) 
            C(49)-C(50)                   1.430(14) 
            C(50)-C(51)                   1.369(12) 
            C(51)-C(52)                   1.439(11) 
            C(52)-C(53)                   1.423(10) 
            C(54)-C(59)                   1.379(14) 
            C(54)-N(8)                    1.400(13) 
            C(54)-C(55)                   1.428(13) 
            C(55)-C(56)                   1.381(19) 
            C(56)-C(57)                   1.37(2) 
            C(57)-C(58)                   1.374(15) 
            C(58)-C(59)                   1.395(14) 
            C(59)-C(60)                   1.505(11) 
            C(60)-N(7)                    1.464(10) 
            C(60)-N(9)                    1.504(9) 
            C(60)-C(74)                   1.537(11) 
            C(61)-C(62)                   1.380(10) 
            C(61)-C(66)                   1.385(11) 
            C(61)-N(9)                    1.435(9) 
            C(62)-C(63)                   1.383(11) 
            C(63)-C(64)                   1.389(13) 
            C(64)-C(65)                   1.400(12) 
            C(64)-C(67)                   1.488(12) 
            C(65)-C(66)                   1.372(11) 
            C(68)-N(9)                    1.347(9) 
            C(68)-C(69)                   1.461(10) 
            C(69)-C(74)                   1.366(10) 
            C(69)-C(70)                   1.407(11) 
            C(70)-C(71)                   1.369(11) 
            C(71)-C(72)                   1.411(12) 
            C(72)-C(75)                   1.411(11) 
            C(72)-C(73)                   1.433(11) 
            C(73)-C(74)                   1.404(9) 
            C(73)-C(78)                   1.431(12) 
            C(75)-C(76)                   1.356(15) 
            C(76)-C(77)                   1.407(15) 
            C(77)-C(78)                   1.348(11) 
            C(80)-C(85)                   1.391(10) 
            C(80)-C(81)                   1.409(11) 
            C(81)-C(82)                   1.390(13) 
            C(82)-C(83)                   1.364(12) 
            C(83)-C(84)                   1.377(10) 
            C(84)-C(85)                   1.395(11) 
            C(85)-C(86)                   1.514(9) 
            C(86)-C(96)                   1.522(10) 
            C(87)-C(92)                   1.382(11) 
            C(87)-C(88)                   1.400(10) 
            C(88)-C(89)                   1.395(12) 
            C(89)-C(90)                   1.404(15) 
            C(90)-C(91)                   1.342(14) 
            C(90)-C(93)                   1.544(14) 
            C(91)-C(92)                   1.379(12) 
            C(94)-C(95)                   1.473(10) 
            C(95)-C(96)                   1.366(9) 
            C(95)-C(104)                  1.408(11) 
            C(96)-C(97)                   1.419(10) 
            C(97)-C(98)                   1.409(10) 
            C(97)-C(102)                  1.429(10) 
            C(98)-C(99)                   1.375(12) 
            C(99)-C(100)                  1.413(14) 
            C(100)-C(101)                 1.345(14) 
            C(101)-C(102)                 1.425(13) 
            C(102)-C(103)                 1.422(12) 
            C(103)-C(104)                 1.349(12) 
            C(4)-C(5)                     1.362(15) 
            C(5)-C(6)                     1.390(15) 
            C(6)-C(7)                     1.415(12) 
            C(7)-C(8)                     1.397(13) 
            C(8)-C(9)                     1.491(11) 
            C(10)-C(11)                   1.376(10) 
  
            C(1)-N(1)-C(9)              123.5(7) 
            C(79)-N(10)-C(86)           123.2(6) 
            C(79)-N(11)-C(80)           114.7(6) 
            C(94)-N(12)-C(87)           123.6(6) 
            C(94)-N(12)-C(86)           112.6(5) 
            C(87)-N(12)-C(86)           121.0(5) 
            N(6)-C(1)-N(1)              126.1(10) 
            C(17)-N(2)-C(10)            122.8(6) 
            C(17)-N(2)-C(9)             113.0(5) 
            C(10)-N(2)-C(9)             121.7(6) 
            C(28)-N(3)-C(35)            123.5(7) 
            C(43)-N(4)-C(36)            121.6(5) 
            C(43)-N(4)-C(35)            112.5(6) 
            C(36)-N(4)-C(35)            124.3(5) 
            N(8)-C(2)-N(7)              128.8(10) 
            C(13)-C(12)-C(11)           122.5(8) 
            C(14)-C(13)-C(12)           117.7(8) 
            C(14)-C(13)-C(16)           120.4(9) 
            C(12)-C(13)-C(16)           121.9(8) 
            C(13)-C(14)-C(15)           121.3(8) 
            C(14)-C(15)-C(10)           120.2(7) 
            O(1)-C(17)-N(2)             124.5(7) 
            O(1)-C(17)-C(19)            127.9(7) 
            N(2)-C(17)-C(19)            107.6(6) 
            C(19)-C(18)-C(23)           121.6(7) 
            C(19)-C(18)-C(9)            109.8(6) 
            C(23)-C(18)-C(9)            128.0(7) 
            C(18)-C(19)-C(20)           121.8(6) 
            C(18)-C(19)-C(17)           109.5(7) 
            C(20)-C(19)-C(17)           128.4(7) 
            C(21)-C(20)-C(19)           117.0(7) 
            C(20)-C(21)-C(22)           121.6(8) 
            C(23)-C(22)-C(27)           117.9(8) 
            C(23)-C(22)-C(21)           121.2(7) 
            C(27)-C(22)-C(21)           120.9(8) 
            C(22)-C(23)-C(24)           120.3(7) 
            C(22)-C(23)-C(18)           116.7(7) 
            C(24)-C(23)-C(18)           123.0(8) 
            C(25)-C(24)-C(23)           120.4(10) 
            C(4)-C(3)-C(8)              118.8(10) 
            C(4)-C(3)-N(6)              118.7(9) 
            C(8)-C(3)-N(6)              122.5(8) 
            C(24)-C(25)-C(26)           119.6(10) 
            C(27)-C(26)-C(25)           120.0(9) 
            C(26)-C(27)-C(22)           121.6(10) 
            N(5)-C(28)-N(3)             128.5(11) 
            N(5)-C(29)-C(34)            122.5(8) 
            N(5)-C(29)-C(30)            118.5(11) 
            C(34)-C(29)-C(30)           118.8(14) 
            C(31)-C(30)-C(29)           119.7(12) 
            C(32)-C(31)-C(30)           122.3(10) 
            C(32)-C(31)-Cl(2)           118.3(14) 
            C(30)-C(31)-Cl(2)           119.3(13) 
            C(31)-C(32)-C(33)           119.5(12) 
            C(32)-C(33)-C(34)           119.1(11) 
            C(29)-C(34)-C(33)           120.4(8) 
            C(29)-C(34)-C(35)           120.7(9) 
            C(33)-C(34)-C(35)           118.7(8) 
            N(3)-C(35)-C(53)            113.4(6) 
            N(3)-C(35)-N(4)             109.4(6) 
            C(53)-C(35)-N(4)            100.5(5) 
            N(3)-C(35)-C(34)            108.2(6) 
            C(53)-C(35)-C(34)           114.9(7) 
            N(4)-C(35)-C(34)            110.1(6) 
            C(41)-C(36)-C(37)           118.9(8) 
            C(41)-C(36)-N(4)            118.4(7) 
            C(37)-C(36)-N(4)            122.6(7) 
            C(36)-C(37)-C(38)           121.5(8) 
            C(37)-C(38)-C(39)           119.8(8) 
            C(38)-C(39)-C(40)           118.4(9) 
            C(38)-C(39)-C(42)           120.9(9) 
            C(40)-C(39)-C(42)           120.7(9) 
            C(41)-C(40)-C(39)           120.7(8) 
            C(36)-C(41)-C(40)           120.7(7) 
            O(2)-C(43)-N(4)             125.9(7) 
            O(2)-C(43)-C(44)            127.4(6) 
            N(4)-C(43)-C(44)            106.7(6) 
            C(53)-C(44)-C(45)           122.7(7) 
            C(53)-C(44)-C(43)           109.1(6) 
            C(45)-C(44)-C(43)           128.1(7) 
            C(46)-C(45)-C(44)           117.1(7) 
            C(45)-C(46)-C(47)           122.8(8) 
            C(46)-C(47)-C(48)           122.4(8) 
            C(46)-C(47)-C(52)           120.1(8) 
            C(48)-C(47)-C(52)           117.4(8) 
            C(49)-C(48)-C(47)           122.4(10) 
            C(48)-C(49)-C(50)           119.8(9) 
            C(51)-C(50)-C(49)           121.1(9) 
            C(50)-C(51)-C(52)           118.8(9) 
            C(53)-C(52)-C(47)           116.1(7) 
            C(53)-C(52)-C(51)           123.7(7) 
            C(47)-C(52)-C(51)           120.2(7) 
            C(44)-C(53)-C(52)           121.1(7) 
            C(44)-C(53)-C(35)           110.6(6) 
            C(52)-C(53)-C(35)           128.3(6) 
            C(59)-C(54)-N(8)            123.5(9) 
            C(59)-C(54)-C(55)           120.4(11) 
            N(8)-C(54)-C(55)            116.1(10) 
            C(56)-C(55)-C(54)           116.2(11) 
            C(57)-C(56)-C(55)           124.3(10) 
            C(57)-C(56)-Cl(3)           120.8(12) 
            C(55)-C(56)-Cl(3)           114.8(12) 
            C(56)-C(57)-C(58)           118.2(14) 
            C(57)-C(58)-C(59)           120.8(13) 
            C(54)-C(59)-C(58)           120.0(9) 
            C(54)-C(59)-C(60)           119.9(9) 
            C(58)-C(59)-C(60)           119.7(9) 
            N(7)-C(60)-N(9)             109.4(6) 
            N(7)-C(60)-C(59)            108.9(7) 
            N(9)-C(60)-C(59)            111.0(6) 
            N(7)-C(60)-C(74)            110.1(6) 
            N(9)-C(60)-C(74)             99.3(6) 
            C(59)-C(60)-C(74)           117.6(7) 
            C(62)-C(61)-C(66)           120.3(7) 
            C(62)-C(61)-N(9)            120.9(7) 
            C(66)-C(61)-N(9)            118.8(6) 
            C(61)-C(62)-C(63)           117.8(8) 
            C(62)-C(63)-C(64)           123.9(7) 
            C(63)-C(64)-C(65)           116.0(7) 
            C(63)-C(64)-C(67)           122.1(9) 
            C(65)-C(64)-C(67)           121.7(10) 
            C(66)-C(65)-C(64)           121.3(9) 
            C(65)-C(66)-C(61)           120.5(7) 
            O(3)-C(68)-N(9)             124.4(6) 
            O(3)-C(68)-C(69)            128.3(7) 
            N(9)-C(68)-C(69)            107.3(6) 
            C(74)-C(69)-C(70)           121.4(6) 
            C(74)-C(69)-C(68)           109.3(6) 
            C(70)-C(69)-C(68)           128.9(7) 
            C(71)-C(70)-C(69)           118.0(8) 
            C(70)-C(71)-C(72)           121.7(8) 
            C(75)-C(72)-C(71)           121.8(8) 
            C(75)-C(72)-C(73)           117.9(8) 
            C(71)-C(72)-C(73)           120.2(7) 
            C(74)-C(73)-C(78)           125.3(7) 
            C(74)-C(73)-C(72)           116.1(7) 
            C(78)-C(73)-C(72)           118.6(7) 
            C(69)-C(74)-C(73)           122.5(7) 
            C(69)-C(74)-C(60)           110.3(6) 
            C(73)-C(74)-C(60)           127.0(7) 
            C(76)-C(75)-C(72)           121.8(9) 
            C(75)-C(76)-C(77)           120.0(8) 
            C(78)-C(77)-C(76)           121.0(9) 
            C(77)-C(78)-C(73)           120.6(9) 
            N(11)-C(79)-N(10)           127.1(7) 
            C(85)-C(80)-C(81)           118.8(7) 
            C(85)-C(80)-N(11)           123.2(6) 
            C(81)-C(80)-N(11)           118.0(7) 
            C(82)-C(81)-C(80)           118.9(7) 
            C(83)-C(82)-C(81)           122.1(7) 
            C(83)-C(82)-Cl(4)           120.2(8) 
            C(81)-C(82)-Cl(4)           117.7(7) 
            C(82)-C(83)-C(84)           119.3(8) 
            C(83)-C(84)-C(85)           120.4(7) 
            C(80)-C(85)-C(84)           120.5(6) 
            C(80)-C(85)-C(86)           119.9(6) 
            C(84)-C(85)-C(86)           119.5(6) 
            N(10)-C(86)-N(12)           109.3(5) 
            N(10)-C(86)-C(85)           108.1(5) 
            N(12)-C(86)-C(85)           111.3(5) 
            N(10)-C(86)-C(96)           110.3(6) 
            N(12)-C(86)-C(96)           100.5(5) 
            C(85)-C(86)-C(96)           117.1(6) 
            C(92)-C(87)-C(88)           122.4(7) 
            C(92)-C(87)-N(12)           119.1(7) 
            C(88)-C(87)-N(12)           118.5(7) 
            C(89)-C(88)-C(87)           117.2(8) 
            C(88)-C(89)-C(90)           120.7(9) 
            C(91)-C(90)-C(89)           119.1(9) 
            C(91)-C(90)-C(93)           121.2(11) 
            C(89)-C(90)-C(93)           119.5(11) 
            C(90)-C(91)-C(92)           123.1(10) 
            C(91)-C(92)-C(87)           117.5(8) 
            O(4)-C(94)-N(12)            126.0(7) 
            O(4)-C(94)-C(95)            127.2(6) 
            N(12)-C(94)-C(95)           106.8(6) 
            C(96)-C(95)-C(104)          122.6(7) 
            C(96)-C(95)-C(94)           109.2(6) 
            C(104)-C(95)-C(94)          128.2(7) 
            C(95)-C(96)-C(97)           121.6(7) 
            C(95)-C(96)-C(86)           110.0(7) 
            C(97)-C(96)-C(86)           128.2(6) 
            C(98)-C(97)-C(96)           124.4(7) 
            C(98)-C(97)-C(102)          120.1(7) 
            C(96)-C(97)-C(102)          115.5(6) 
            C(99)-C(98)-C(97)           120.5(8) 
            C(98)-C(99)-C(100)          119.1(9) 
            C(101)-C(100)-C(99)         121.7(9) 
            C(100)-C(101)-C(102)        121.2(9) 
            C(103)-C(102)-C(101)        122.0(8) 
            C(103)-C(102)-C(97)         120.7(8) 
            C(101)-C(102)-C(97)         117.3(8) 
            C(104)-C(103)-C(102)        122.0(8) 
            C(103)-C(104)-C(95)         117.5(7) 
            C(3)-C(4)-C(5)              120.9(10) 
            C(4)-C(5)-C(6)              123.4(9) 
            C(4)-C(5)-Cl(1)             119.8(9) 
            C(6)-C(5)-Cl(1)             116.8(9) 
            C(5)-C(6)-C(7)              115.9(10) 
            C(8)-C(7)-C(6)              120.7(9) 
            C(7)-C(8)-C(3)              120.2(8) 
            C(7)-C(8)-C(9)              119.5(8) 
            C(3)-C(8)-C(9)              120.2(8) 
            N(1)-C(9)-C(8)              110.0(7) 
            N(1)-C(9)-N(2)              110.3(6) 
            C(8)-C(9)-N(2)              112.3(5) 
            N(1)-C(9)-C(18)             109.4(6) 
            C(8)-C(9)-C(18)             114.8(7) 
            N(2)-C(9)-C(18)              99.6(5) 
            C(11)-C(10)-C(15)           119.7(7) 
            C(11)-C(10)-N(2)            121.4(7) 
            C(15)-C(10)-N(2)            118.8(6) 
            C(10)-C(11)-C(12)           118.7(8) 
            C(28)-N(5)-C(29)            115.3(9) 
            C(1)-N(6)-C(3)              116.8(8) 
            C(2)-N(7)-C(60)             121.5(7) 
            C(2)-N(8)-C(54)             115.0(9) 
            C(68)-N(9)-C(61)            122.1(6) 
            C(68)-N(9)-C(60)            113.3(5) 
            C(61)-N(9)-C(60)            122.9(6) 
           _____________________________________________________________ 
  
           Symmetry transformations used to generate equivalent atoms: 
            
  
    Table 4.  Anisotropic displacement parameters (A^2 x 10^3) for t. 
    The anisotropic displacement factor exponent takes the form: 
    -2 pi^2 [ h^2 a*^2 U11 + ... + 2 h k a* b* U12 ] 
  
    _______________________________________________________________________ 
  
              U11        U22        U33        U23        U13        U12 
    _______________________________________________________________________ 
  
    Cl(2)   455(8)      85(2)      72(2)      10(2)     -93(3)    -136(3) 
    Cl(3)   329(6)     135(3)      83(2)      22(2)      -5(3)     125(4) 
    Cl(4)   108(2)      99(2)     134(2)     -70(2)       7(2)      14(2) 
    O(1)     70(3)      53(3)      51(3)      -7(2)     -14(3)     -14(2) 
    Cl(1)   192(3)      66(2)      89(2)      19(1)      44(2)       5(2) 
    N(1)     74(5)      60(4)      50(4)      -6(3)     -18(3)      -7(3) 
    N(10)    61(4)      41(3)      48(4)     -15(3)      -3(3)      -9(3) 
    N(11)    61(5)      53(4)      75(5)     -27(3)     -21(3)      -5(3) 
    N(12)    57(4)      38(3)      43(3)      -8(2)      -6(3)     -11(3) 
    C(1)     91(7)      74(6)      67(6)      -9(5)     -23(5)      13(5) 
    O(2)     62(3)      36(3)      56(3)      -7(2)      -8(2)      -3(2) 
    O(3)     65(3)      42(3)      51(3)      -9(2)      -3(2)       1(2) 
    O(4)     65(3)      44(3)      69(3)     -12(2)      -8(3)     -13(2) 
    N(2)     67(4)      40(3)      40(3)      -6(3)      -8(3)      -7(3) 
    N(3)     72(5)      53(4)      52(4)     -20(3)     -15(3)      10(3) 
    N(4)     66(4)      30(3)      53(4)      -7(3)     -11(3)      -2(3) 
    C(2)    100(7)      61(5)      55(5)     -14(4)       4(5)     -29(5) 
    C(12)    93(7)      42(5)      97(7)      -8(4)     -17(6)      -3(5) 
    C(13)    78(6)      46(5)      73(6)     -16(4)      -9(5)      -1(4) 
    C(14)    64(5)      44(4)      88(6)     -14(4)     -14(4)      -3(4) 
    C(15)    69(6)      45(4)      77(6)     -12(4)     -10(5)     -14(4) 
    C(16)    94(7)      49(5)     129(9)     -19(5)     -16(6)      -5(5) 
    C(17)    68(5)      49(4)      45(5)      -7(4)      -6(4)     -20(4) 
    C(18)    68(5)      43(4)      49(5)      -8(3)     -13(4)      -9(3) 
    C(19)    66(5)      43(4)      43(4)     -10(3)      -9(4)      -9(3) 
    C(20)    68(5)      52(4)      57(5)       6(4)     -11(4)     -13(4) 
    C(21)    65(5)      48(4)      84(7)      -1(4)      -4(5)      -3(4) 
    C(22)    59(5)      49(4)      64(5)     -16(4)       8(4)     -13(4) 
    C(23)    70(5)      51(5)      52(5)     -14(4)       2(4)     -14(4) 
    C(24)    84(6)      69(5)      61(6)     -18(4)      -7(5)     -28(5) 
    C(3)    105(8)      55(5)      50(5)      -2(4)      -4(5)      -2(5) 
    C(25)   100(7)      87(7)      73(6)     -34(6)       2(5)     -26(6) 
    C(26)   102(8)      80(7)      84(8)     -36(6)      21(6)     -21(6) 
    C(27)    76(6)      53(5)     104(8)     -21(5)      19(6)     -11(4) 
    C(28)   126(9)      78(6)      77(7)     -36(5)     -33(6)      48(6) 
    C(29)   194(13)     38(5)      54(5)     -21(4)     -39(6)      26(6) 
    C(30)   276(18)     34(5)      91(8)     -25(5)     -79(11)     19(8) 
    C(31)   284(19)     39(5)      61(7)      10(4)     -54(9)     -54(7) 
    C(32)   158(10)     94(7)      71(7)      14(5)     -43(7)     -79(7) 
    C(33)   109(8)      74(6)      70(6)     -12(5)     -26(6)     -37(5) 
    C(34)   116(8)      37(4)      46(5)      -2(3)     -17(5)     -15(4) 
    C(35)    85(6)      29(3)      45(4)     -12(3)     -16(4)      -1(3) 
    C(36)    68(5)      30(3)      60(5)     -11(3)     -13(4)      -1(3) 
    C(37)    86(6)      54(5)      60(6)      -9(4)     -28(5)     -11(4) 
    C(38)    98(7)      73(6)      47(5)      -3(4)     -10(5)     -11(5) 
    C(39)    78(6)      75(6)      62(6)       1(4)      -5(5)       1(5) 
    C(40)    74(6)      71(5)      66(6)     -15(4)     -12(5)     -10(4) 
    C(41)    72(5)      58(5)      51(5)     -13(4)     -19(4)      -6(4) 
    C(42)    97(8)     140(10)     71(7)      11(7)       5(6)     -10(7) 
    C(43)    69(5)      33(4)      49(4)      -9(3)     -15(4)     -11(3) 
    C(44)    67(5)      35(4)      53(5)     -13(3)     -16(4)      -6(3) 
    C(45)    69(5)      39(4)      77(6)     -11(4)     -17(4)      -7(4) 
    C(46)    78(6)      48(5)      67(6)     -11(4)      -9(4)     -14(4) 
    C(47)    89(6)      56(5)      59(5)      -6(4)     -15(5)     -15(4) 
    C(48)   115(8)      64(6)      77(7)       7(5)      -5(6)     -21(5) 
    C(49)   145(9)      59(6)      58(6)       0(4)     -13(6)     -10(6) 
    C(50)   150(10)     48(5)      69(6)      -3(5)     -21(6)     -15(5) 
    C(51)   103(7)      38(4)      64(6)      -3(4)     -20(5)     -11(4) 
    C(52)    79(6)      38(4)      52(5)      -8(3)     -19(4)     -13(4) 
    C(53)    73(5)      38(4)      46(4)      -5(3)     -14(4)     -13(3) 
    C(54)   143(6)      36(4)      54(5)     -16(4)      -5(6)       5(5) 
    C(55)   185(10)     40(5)      51(5)      -6(4)       3(6)       3(6) 
    C(56)   203(11)     83(7)      51(6)       7(5)      -7(8)      69(9) 
    C(57)   183(14)    135(11)     62(7)      14(7)      -9(8)      87(10) 
    C(58)   123(9)      91(7)      55(6)     -12(5)     -21(6)      44(6) 
    C(59)   114(8)      42(4)      49(5)     -10(4)      -4(5)       9(5) 
    C(60)    80(6)      43(4)      46(4)     -13(3)     -10(4)       3(4) 
    C(61)    71(5)      35(4)      47(4)     -11(3)      -1(4)      -4(3) 
    C(62)    89(6)      37(4)      59(5)      -6(3)      -7(4)       4(4) 
    C(63)    98(7)      33(4)      74(6)      -2(4)       5(5)      -1(4) 
    C(64)    98(7)      49(5)      61(5)     -18(4)       5(5)     -16(5) 
    C(65)    76(6)      50(5)      76(6)     -16(4)     -12(4)      -6(4) 
    C(66)    77(6)      44(4)      64(5)     -12(4)      -6(5)       3(4) 
    C(67)   128(9)      51(5)     116(8)     -20(5)     -13(7)     -21(5) 
    C(68)    54(5)      38(4)      57(5)      -7(3)     -12(4)       9(3) 
    C(69)    54(5)      49(4)      52(5)      -9(3)     -11(4)       3(3) 
    C(70)    63(5)      61(5)      61(5)     -10(4)     -16(4)      -9(4) 
    C(71)    72(6)      58(5)      80(7)     -14(4)     -17(5)     -15(4) 
    C(72)    71(6)      59(5)      67(6)     -22(4)     -24(5)       1(4) 
    C(73)    64(5)      55(4)      55(5)     -13(4)     -23(4)       2(4) 
    C(74)    64(5)      45(4)      52(5)     -11(3)     -25(4)       3(3) 
    C(75)   114(8)      66(6)      80(7)     -25(5)     -26(6)     -16(5) 
    C(76)   145(10)     75(7)      73(7)     -36(5)     -42(7)       1(6) 
    C(77)    92(7)      72(6)      70(6)     -32(5)     -25(5)      10(5) 
    C(78)    82(6)      61(5)      56(5)     -18(4)     -24(4)       9(4) 
    C(79)    57(5)      38(4)      69(5)      -9(4)     -15(4)      -3(3) 
    C(80)    65(6)      42(4)      56(5)     -12(3)      -8(4)      -4(3) 
    C(81)    97(7)      45(4)      70(6)     -23(4)      -9(5)     -10(4) 
    C(82)    88(7)      58(5)      67(6)     -22(4)       3(5)      13(5) 
    C(83)    62(5)      52(5)      79(6)     -17(4)      -3(4)       0(4) 
    C(84)    62(6)      48(4)      64(5)      -5(4)      -6(4)      -6(4) 
    C(85)    61(5)      34(4)      44(4)       0(3)      -5(3)      -3(3) 
    C(86)    52(5)      42(4)      45(4)     -14(3)      -9(3)      -4(3) 
    C(87)    66(5)      45(4)      48(5)       1(3)     -17(4)     -16(4) 
    C(88)    67(5)      63(5)      47(5)      -5(4)     -11(4)      -2(4) 
    C(89)   108(7)      94(7)      45(5)      -1(5)      -8(5)     -25(5) 
    C(90)   101(6)      99(7)      67(7)      28(6)     -34(6)     -35(5) 
    C(91)    75(6)      90(7)      72(7)      20(5)     -22(5)     -17(5) 
    C(92)    66(6)      58(5)      70(6)      -2(4)      -9(4)      -1(4) 
    C(93)   131(10)    179(12)     82(8)      59(8)     -50(7)     -68(9) 
    C(94)    58(5)      35(4)      56(5)     -11(3)      -4(4)     -10(3) 
    C(95)    46(4)      39(4)      63(5)      -8(3)      -5(4)      -3(3) 
    C(96)    54(5)      41(4)      57(5)     -14(3)      -9(4)       6(3) 
    C(97)    59(5)      48(4)      54(5)     -13(4)     -15(4)       4(3) 
    C(98)    83(6)      49(5)      61(5)       1(4)      -9(4)       0(4) 
    C(99)   106(8)      65(6)      76(7)       7(5)     -16(6)      10(5) 
    C(100)  123(9)      93(8)      61(6)       7(5)     -31(6)      29(7) 
    C(101)  110(8)      94(8)      64(6)      -4(5)     -28(6)      15(6) 
    C(102)   74(6)      66(5)      50(5)     -13(4)     -13(4)      17(4) 
    C(103)   70(6)      64(5)      76(6)     -24(5)     -25(5)       1(4) 
    C(104)   68(5)      49(4)      73(6)     -23(4)     -14(4)       0(4) 
    C(4)    143(7)      62(5)      50(5)       2(4)     -12(6)       8(6) 
    C(5)    145(7)      41(4)      51(5)       3(4)      16(5)      -8(5) 
    C(6)    109(8)      71(6)      65(6)     -10(4)       8(4)     -24(5) 
    C(7)     91(7)      70(6)      69(6)      -3(5)      -7(5)     -28(5) 
    C(8)    104(7)      45(4)      42(5)      -9(3)     -14(5)       0(4) 
    C(9)     73(5)      47(4)      45(4)      -3(3)     -11(4)     -12(4) 
    C(10)    67(5)      43(4)      46(4)      -6(3)      -8(4)      -5(4) 
    C(11)    64(5)      55(5)      71(6)      -2(4)      -6(4)      -5(4) 
    N(5)    197(11)    102(7)     119(8)     -70(6)     -74(8)      85(8) 
    N(6)    101(7)      93(6)      69(5)      11(5)     -28(5)       2(5) 
    N(7)     62(4)      46(3)      63(4)      -8(3)      -6(3)      -1(3) 
    N(8)    135(6)      57(5)      51(4)      -5(4)       1(5)     -17(5) 
    N(9)     72(4)      32(3)      46(4)     -11(3)     -11(3)       5(3) 
    _______________________________________________________________________ 
  
         Table 5.  Hydrogen coordinates ( x 10^4) and isotropic 
         displacement parameters (A^2 x 10^3) for t. 
  
         ________________________________________________________________ 
  
                         x             y             z           U(eq) 
         ________________________________________________________________ 
  
          H(1)         7819          5537          2841          72 
          H(10)        5275          2666          4838          60 
          H(1A)        6685          6232          1883          92 
          H(3)         -346          7323          5441          70 
          H(2)          203          3687          8265          88 
          H(12)        8332          9344          3814          92 
          H(14)        5608          7677          5042          78 
          H(15)        7070          6515          4512          76 
          H(16A)       4917          9172          5025         135 
          H(16B)       5802          9831          4353         135 
          H(16C)       6170          9631          5315         135 
          H(20)       11586          4420          4543          71 
          H(21)       12196          3291          3582          80 
          H(24)       10119          5207          1115          85 
          H(25)       10628          4028           221         104 
          H(26)       11652          2729           760         109 
          H(27)       12226          2661          2135          97 
          H(28)       -1758          8280          6145         111 
          H(30)         617          9791          7674         154 
          H(32)        4469          8700          7298         123 
          H(33)        3804          7630          6431          98 
          H(37)        1485          6835          8132          77 
          H(38)           3          6446          9410          87 
          H(40)       -2264          5218          7938          84 
          H(41)        -811          5664          6671          71 
          H(42A)      -2781          5021          9509         158 
          H(42B)      -2855          5985          9859         158 
          H(42C)      -1694          5289         10092         158 
          H(45)        4088          5378          4528          73 
          H(46)        4862          6278          3317          77 
          H(48)        4858          7695          2515         104 
          H(49)        4113          9124          2423         105 
          H(50)        2321          9685          3509         106 
          H(51)        1555          8868          4782          81 
          H(55)        2457          1650          9643         114 
          H(57)        6488          2178          8955         159 
          H(58)        5919          3312          8006         109 
          H(62)        4547          1836          6876          75 
          H(63)        3678           706          6236          85 
          H(65)        1022          2370          5222          80 
          H(66)        1953          3513          5786          75 
          H(67A)       1597           790          4698         147 
          H(67B)        720           551          5642         147 
          H(67C)       2241           129          5367         147 
          H(70)        6206          5603          5764          73 
          H(71)        6209          6678          6765          82 
          H(75)        5482          7244          8251         101 
          H(76)        4171          7153          9627         113 
          H(77)        2885          5927         10077          92 
          H(78)        2956          4792          9167          78 
          H(79)        4184          1957          4000          65 
          H(81)        7434           396          2280          84 
          H(83)       11051          1152          2796          78 
          H(84)        9886          2165          3763          70 
          H(88)        8373          3073          2071          70 
          H(89)        7303          3302           821          98 
          H(91)        4156          4635          2235          94 
          H(92)        5073          4353          3515          78 
          H(93A)       3912          4112           788         190 
          H(93B)       5235          3660           204         190 
          H(93C)       5134          4691           306         190 
          H(98)        7237          1077          5283          78 
          H(99)        7568           180          6494         100 
          H(100)       8277           781          7706         110 
          H(101)       8877          2187          7656         106 
          H(103)       8994          3660          6907          81 
          H(104)       8766          4572          5708          75 
          H(4)         9554          8007           317         103 
          H(6)        13121          7775          1284         100 
          H(7)        12121          6708          2338          92 
          H(11)        9837          8194          3286          77 
          H(7A)        1700          4524          7474          69 
         ________________________________________________________________ 
  
         Table 6.  Torsion angles [deg] for t. 
         ________________________________________________________________ 
  
          C(9)-N(1)-C(1)-N(6)                                   4.9(13) 
          C(11)-C(12)-C(13)-C(14)                               0.6(14) 
          C(11)-C(12)-C(13)-C(16)                             179.6(9) 
          C(12)-C(13)-C(14)-C(15)                              -1.0(13) 
          C(16)-C(13)-C(14)-C(15)                             179.9(8) 
          C(13)-C(14)-C(15)-C(10)                               0.6(13) 
          C(10)-N(2)-C(17)-O(1)                                -8.4(11) 
          C(9)-N(2)-C(17)-O(1)                               -170.8(7) 
          C(10)-N(2)-C(17)-C(19)                              170.6(6) 
          C(9)-N(2)-C(17)-C(19)                                 8.2(8) 
          C(23)-C(18)-C(19)-C(20)                               4.1(11) 
          C(9)-C(18)-C(19)-C(20)                              175.9(7) 
          C(23)-C(18)-C(19)-C(17)                            -170.0(7) 
          C(9)-C(18)-C(19)-C(17)                                1.7(9) 
          O(1)-C(17)-C(19)-C(18)                              172.9(7) 
          N(2)-C(17)-C(19)-C(18)                               -6.1(8) 
          O(1)-C(17)-C(19)-C(20)                               -0.7(13) 
          N(2)-C(17)-C(19)-C(20)                             -179.7(7) 
          C(18)-C(19)-C(20)-C(21)                              -3.2(11) 
          C(17)-C(19)-C(20)-C(21)                             169.7(7) 
          C(19)-C(20)-C(21)-C(22)                               0.5(11) 
          C(20)-C(21)-C(22)-C(23)                               1.5(12) 
          C(20)-C(21)-C(22)-C(27)                            -177.6(8) 
          C(27)-C(22)-C(23)-C(24)                              -1.3(11) 
          C(21)-C(22)-C(23)-C(24)                             179.7(7) 
          C(27)-C(22)-C(23)-C(18)                             178.3(7) 
          C(21)-C(22)-C(23)-C(18)                              -0.7(11) 
          C(19)-C(18)-C(23)-C(22)                              -2.0(11) 
          C(9)-C(18)-C(23)-C(22)                             -172.1(7) 
          C(19)-C(18)-C(23)-C(24)                             177.6(8) 
          C(9)-C(18)-C(23)-C(24)                                7.5(12) 
          C(22)-C(23)-C(24)-C(25)                               2.5(12) 
          C(18)-C(23)-C(24)-C(25)                            -177.1(8) 
          C(23)-C(24)-C(25)-C(26)                              -1.1(14) 
          C(24)-C(25)-C(26)-C(27)                              -1.5(15) 
          C(25)-C(26)-C(27)-C(22)                               2.8(14) 
          C(23)-C(22)-C(27)-C(26)                              -1.4(13) 
          C(21)-C(22)-C(27)-C(26)                             177.7(8) 
          C(35)-N(3)-C(28)-N(5)                                 6.3(17) 
          N(5)-C(29)-C(30)-C(31)                             -178.9(12) 
          C(34)-C(29)-C(30)-C(31)                              -3.7(16) 
          C(29)-C(30)-C(31)-C(32)                               2.4(19) 
          C(29)-C(30)-C(31)-Cl(2)                            -179.1(8) 
          C(30)-C(31)-C(32)-C(33)                              -1.0(17) 
          Cl(2)-C(31)-C(32)-C(33)                            -179.5(7) 
          C(31)-C(32)-C(33)-C(34)                               0.9(14) 
          N(5)-C(29)-C(34)-C(33)                              178.7(10) 
          C(30)-C(29)-C(34)-C(33)                               3.7(13) 
          N(5)-C(29)-C(34)-C(35)                               -5.3(14) 
          C(30)-C(29)-C(34)-C(35)                             179.8(8) 
          C(32)-C(33)-C(34)-C(29)                              -2.4(13) 
          C(32)-C(33)-C(34)-C(35)                            -178.5(8) 
          C(28)-N(3)-C(35)-C(53)                             -141.0(8) 
          C(28)-N(3)-C(35)-N(4)                               107.7(8) 
          C(28)-N(3)-C(35)-C(34)                              -12.3(11) 
          C(43)-N(4)-C(35)-N(3)                               113.6(6) 
          C(36)-N(4)-C(35)-N(3)                               -52.2(8) 
          C(43)-N(4)-C(35)-C(53)                               -6.0(7) 
          C(36)-N(4)-C(35)-C(53)                             -171.8(6) 
          C(43)-N(4)-C(35)-C(34)                             -127.6(7) 
          C(36)-N(4)-C(35)-C(34)                               66.6(9) 
          C(29)-C(34)-C(35)-N(3)                               11.6(10) 
          C(33)-C(34)-C(35)-N(3)                             -172.3(7) 
          C(29)-C(34)-C(35)-C(53)                             139.5(8) 
          C(33)-C(34)-C(35)-C(53)                             -44.4(10) 
          C(29)-C(34)-C(35)-N(4)                             -107.9(8) 
          C(33)-C(34)-C(35)-N(4)                               68.2(9) 
          C(43)-N(4)-C(36)-C(41)                              -63.9(9) 
          C(35)-N(4)-C(36)-C(41)                              100.6(8) 
          C(43)-N(4)-C(36)-C(37)                              111.9(8) 
          C(35)-N(4)-C(36)-C(37)                              -83.5(9) 
          C(41)-C(36)-C(37)-C(38)                              -1.7(12) 
          N(4)-C(36)-C(37)-C(38)                             -177.6(7) 
          C(36)-C(37)-C(38)-C(39)                               2.2(13) 
          C(37)-C(38)-C(39)-C(40)                              -1.3(13) 
          C(37)-C(38)-C(39)-C(42)                             178.9(9) 
          C(38)-C(39)-C(40)-C(41)                              -0.1(13) 
          C(42)-C(39)-C(40)-C(41)                             179.8(9) 
          C(37)-C(36)-C(41)-C(40)                               0.4(11) 
          N(4)-C(36)-C(41)-C(40)                              176.4(7) 
          C(39)-C(40)-C(41)-C(36)                               0.5(13) 
          C(36)-N(4)-C(43)-O(2)                                -3.3(11) 
          C(35)-N(4)-C(43)-O(2)                              -169.6(7) 
          C(36)-N(4)-C(43)-C(44)                              174.4(6) 
          C(35)-N(4)-C(43)-C(44)                                8.2(8) 
          O(2)-C(43)-C(44)-C(53)                              170.5(7) 
          N(4)-C(43)-C(44)-C(53)                               -7.2(8) 
          O(2)-C(43)-C(44)-C(45)                               -5.6(12) 
          N(4)-C(43)-C(44)-C(45)                              176.8(7) 
          C(53)-C(44)-C(45)-C(46)                               0.0(11) 
          C(43)-C(44)-C(45)-C(46)                             175.6(7) 
          C(44)-C(45)-C(46)-C(47)                              -1.2(12) 
          C(45)-C(46)-C(47)-C(48)                             180.0(8) 
          C(45)-C(46)-C(47)-C(52)                               0.0(12) 
          C(46)-C(47)-C(48)-C(49)                             179.6(9) 
          C(52)-C(47)-C(48)-C(49)                              -0.5(14) 
          C(47)-C(48)-C(49)-C(50)                              -3.6(16) 
          C(48)-C(49)-C(50)-C(51)                               5.3(16) 
          C(49)-C(50)-C(51)-C(52)                              -2.6(14) 
          C(46)-C(47)-C(52)-C(53)                               2.2(11) 
          C(48)-C(47)-C(52)-C(53)                            -177.7(8) 
          C(46)-C(47)-C(52)-C(51)                            -177.0(7) 
          C(48)-C(47)-C(52)-C(51)                               3.0(11) 
          C(50)-C(51)-C(52)-C(53)                             179.3(8) 
          C(50)-C(51)-C(52)-C(47)                              -1.5(12) 
          C(45)-C(44)-C(53)-C(52)                               2.4(11) 
          C(43)-C(44)-C(53)-C(52)                            -174.0(6) 
          C(45)-C(44)-C(53)-C(35)                             179.7(7) 
          C(43)-C(44)-C(53)-C(35)                               3.4(8) 
          C(47)-C(52)-C(53)-C(44)                              -3.4(10) 
          C(51)-C(52)-C(53)-C(44)                             175.8(7) 
          C(47)-C(52)-C(53)-C(35)                             179.7(7) 
          C(51)-C(52)-C(53)-C(35)                              -1.0(12) 
          N(3)-C(35)-C(53)-C(44)                             -115.4(7) 
          N(4)-C(35)-C(53)-C(44)                                1.2(7) 
          C(34)-C(35)-C(53)-C(44)                             119.4(7) 
          N(3)-C(35)-C(53)-C(52)                               61.7(9) 
          N(4)-C(35)-C(53)-C(52)                              178.4(7) 
          C(34)-C(35)-C(53)-C(52)                             -63.5(10) 
          C(59)-C(54)-C(55)-C(56)                               2.6(12) 
          N(8)-C(54)-C(55)-C(56)                             -176.6(8) 
          C(54)-C(55)-C(56)-C(57)                              -2.9(16) 
          C(54)-C(55)-C(56)-Cl(3)                            -180.0(6) 
          C(55)-C(56)-C(57)-C(58)                               1.8(19) 
          Cl(3)-C(56)-C(57)-C(58)                             178.6(8) 
          C(56)-C(57)-C(58)-C(59)                              -0.2(17) 
          N(8)-C(54)-C(59)-C(58)                              177.9(8) 
          C(55)-C(54)-C(59)-C(58)                              -1.2(11) 
          N(8)-C(54)-C(59)-C(60)                               -8.7(11) 
          C(55)-C(54)-C(59)-C(60)                             172.1(7) 
          C(57)-C(58)-C(59)-C(54)                               0.0(13) 
          C(57)-C(58)-C(59)-C(60)                            -173.4(9) 
          C(54)-C(59)-C(60)-N(7)                               16.6(9) 
          C(58)-C(59)-C(60)-N(7)                             -170.0(7) 
          C(54)-C(59)-C(60)-N(9)                             -103.9(8) 
          C(58)-C(59)-C(60)-N(9)                               69.5(9) 
          C(54)-C(59)-C(60)-C(74)                             142.8(7) 
          C(58)-C(59)-C(60)-C(74)                             -43.8(10) 
          C(66)-C(61)-C(62)-C(63)                               3.1(12) 
          N(9)-C(61)-C(62)-C(63)                             -175.8(7) 
          C(61)-C(62)-C(63)-C(64)                              -4.7(13) 
          C(62)-C(63)-C(64)-C(65)                               4.2(13) 
          C(62)-C(63)-C(64)-C(67)                            -179.9(9) 
          C(63)-C(64)-C(65)-C(66)                              -2.1(13) 
          C(67)-C(64)-C(65)-C(66)                            -178.1(9) 
          C(64)-C(65)-C(66)-C(61)                               0.9(13) 
          C(62)-C(61)-C(66)-C(65)                              -1.4(12) 
          N(9)-C(61)-C(66)-C(65)                              177.6(7) 
          O(3)-C(68)-C(69)-C(74)                              173.1(7) 
          N(9)-C(68)-C(69)-C(74)                               -6.6(8) 
          O(3)-C(68)-C(69)-C(70)                                0.6(12) 
          N(9)-C(68)-C(69)-C(70)                             -179.1(7) 
          C(74)-C(69)-C(70)-C(71)                               0.0(11) 
          C(68)-C(69)-C(70)-C(71)                             171.7(7) 
          C(69)-C(70)-C(71)-C(72)                              -1.0(12) 
          C(70)-C(71)-C(72)-C(75)                            -179.2(8) 
          C(70)-C(71)-C(72)-C(73)                               0.9(13) 
          C(75)-C(72)-C(73)-C(74)                            -179.7(8) 
          C(71)-C(72)-C(73)-C(74)                               0.1(11) 
          C(75)-C(72)-C(73)-C(78)                               2.7(11) 
          C(71)-C(72)-C(73)-C(78)                            -177.5(8) 
          C(70)-C(69)-C(74)-C(73)                               1.1(11) 
          C(68)-C(69)-C(74)-C(73)                            -172.1(6) 
          C(70)-C(69)-C(74)-C(60)                             176.1(7) 
          C(68)-C(69)-C(74)-C(60)                               3.0(8) 
          C(78)-C(73)-C(74)-C(69)                             176.3(7) 
          C(72)-C(73)-C(74)-C(69)                              -1.1(10) 
          C(78)-C(73)-C(74)-C(60)                               2.1(12) 
          C(72)-C(73)-C(74)-C(60)                            -175.3(7) 
          N(7)-C(60)-C(74)-C(69)                             -113.4(7) 
          N(9)-C(60)-C(74)-C(69)                                1.3(8) 
          C(59)-C(60)-C(74)-C(69)                             121.0(7) 
          N(7)-C(60)-C(74)-C(73)                               61.3(9) 
          N(9)-C(60)-C(74)-C(73)                              176.1(7) 
          C(59)-C(60)-C(74)-C(73)                             -64.2(10) 
          C(71)-C(72)-C(75)-C(76)                             176.5(9) 
          C(73)-C(72)-C(75)-C(76)                              -3.6(14) 
          C(72)-C(75)-C(76)-C(77)                               1.8(16) 
          C(75)-C(76)-C(77)-C(78)                               1.0(15) 
          C(76)-C(77)-C(78)-C(73)                              -1.8(13) 
          C(74)-C(73)-C(78)-C(77)                            -177.4(8) 
          C(72)-C(73)-C(78)-C(77)                              -0.1(11) 
          C(80)-N(11)-C(79)-N(10)                               2.5(11) 
          C(86)-N(10)-C(79)-N(11)                              13.0(12) 
          C(79)-N(11)-C(80)-C(85)                              -5.2(11) 
          C(79)-N(11)-C(80)-C(81)                             172.7(7) 
          C(85)-C(80)-C(81)-C(82)                              -1.1(12) 
          N(11)-C(80)-C(81)-C(82)                            -179.0(8) 
          C(80)-C(81)-C(82)-C(83)                               1.2(14) 
          C(80)-C(81)-C(82)-Cl(4)                             179.3(6) 
          C(81)-C(82)-C(83)-C(84)                              -0.5(14) 
          Cl(4)-C(82)-C(83)-C(84)                            -178.6(6) 
          C(82)-C(83)-C(84)-C(85)                              -0.2(12) 
          C(81)-C(80)-C(85)-C(84)                               0.4(10) 
          N(11)-C(80)-C(85)-C(84)                             178.2(7) 
          C(81)-C(80)-C(85)-C(86)                             175.5(7) 
          N(11)-C(80)-C(85)-C(86)                              -6.6(10) 
          C(83)-C(84)-C(85)-C(80)                               0.3(11) 
          C(83)-C(84)-C(85)-C(86)                            -174.9(7) 
          C(79)-N(10)-C(86)-N(12)                              99.1(7) 
          C(79)-N(10)-C(86)-C(85)                             -22.1(9) 
          C(79)-N(10)-C(86)-C(96)                            -151.3(6) 
          C(94)-N(12)-C(86)-N(10)                             106.4(6) 
          C(87)-N(12)-C(86)-N(10)                             -55.1(8) 
          C(94)-N(12)-C(86)-C(85)                            -134.3(6) 
          C(87)-N(12)-C(86)-C(85)                              64.2(8) 
          C(94)-N(12)-C(86)-C(96)                              -9.6(7) 
          C(87)-N(12)-C(86)-C(96)                            -171.2(6) 
          C(80)-C(85)-C(86)-N(10)                              18.6(9) 
          C(84)-C(85)-C(86)-N(10)                            -166.2(6) 
          C(80)-C(85)-C(86)-N(12)                            -101.4(7) 
          C(84)-C(85)-C(86)-N(12)                              73.8(8) 
          C(80)-C(85)-C(86)-C(96)                             143.9(7) 
          C(84)-C(85)-C(86)-C(96)                             -40.9(9) 
          C(94)-N(12)-C(87)-C(92)                             -61.1(9) 
          C(86)-N(12)-C(87)-C(92)                              98.4(8) 
          C(94)-N(12)-C(87)-C(88)                             121.6(8) 
          C(86)-N(12)-C(87)-C(88)                             -78.9(8) 
          C(92)-C(87)-C(88)-C(89)                              -1.7(11) 
          N(12)-C(87)-C(88)-C(89)                             175.5(7) 
          C(87)-C(88)-C(89)-C(90)                               2.9(13) 
          C(88)-C(89)-C(90)-C(91)                              -1.8(14) 
          C(88)-C(89)-C(90)-C(93)                            -177.0(9) 
          C(89)-C(90)-C(91)-C(92)                              -0.6(15) 
          C(93)-C(90)-C(91)-C(92)                             174.5(9) 
          C(90)-C(91)-C(92)-C(87)                               1.8(13) 
          C(88)-C(87)-C(92)-C(91)                              -0.6(12) 
          N(12)-C(87)-C(92)-C(91)                            -177.7(7) 
          C(87)-N(12)-C(94)-O(4)                               -8.0(11) 
          C(86)-N(12)-C(94)-O(4)                             -169.0(7) 
          C(87)-N(12)-C(94)-C(95)                             171.6(6) 
          C(86)-N(12)-C(94)-C(95)                              10.6(8) 
          O(4)-C(94)-C(95)-C(96)                              172.5(7) 
          N(12)-C(94)-C(95)-C(96)                              -7.0(8) 
          O(4)-C(94)-C(95)-C(104)                              -4.6(13) 
          N(12)-C(94)-C(95)-C(104)                            175.9(7) 
          C(104)-C(95)-C(96)-C(97)                              2.2(11) 
          C(94)-C(95)-C(96)-C(97)                            -175.0(7) 
          C(104)-C(95)-C(96)-C(86)                            178.2(7) 
          C(94)-C(95)-C(96)-C(86)                               0.9(8) 
          N(10)-C(86)-C(96)-C(95)                            -110.4(7) 
          N(12)-C(86)-C(96)-C(95)                               4.9(7) 
          C(85)-C(86)-C(96)-C(95)                             125.4(7) 
          N(10)-C(86)-C(96)-C(97)                              65.2(9) 
          N(12)-C(86)-C(96)-C(97)                            -179.5(7) 
          C(85)-C(86)-C(96)-C(97)                             -59.0(10) 
          C(95)-C(96)-C(97)-C(98)                             177.6(7) 
          C(86)-C(96)-C(97)-C(98)                               2.5(12) 
          C(95)-C(96)-C(97)-C(102)                             -0.6(10) 
          C(86)-C(96)-C(97)-C(102)                           -175.8(7) 
          C(96)-C(97)-C(98)-C(99)                             179.4(8) 
          C(102)-C(97)-C(98)-C(99)                             -2.4(12) 
          C(97)-C(98)-C(99)-C(100)                              2.7(14) 
          C(98)-C(99)-C(100)-C(101)                            -3.2(16) 
          C(99)-C(100)-C(101)-C(102)                            3.3(17) 
          C(100)-C(101)-C(102)-C(103)                         178.6(9) 
          C(100)-C(101)-C(102)-C(97)                           -2.9(14) 
          C(98)-C(97)-C(102)-C(103)                          -179.1(8) 
          C(96)-C(97)-C(102)-C(103)                            -0.8(11) 
          C(98)-C(97)-C(102)-C(101)                             2.4(12) 
          C(96)-C(97)-C(102)-C(101)                          -179.3(8) 
          C(101)-C(102)-C(103)-C(104)                         179.1(9) 
          C(97)-C(102)-C(103)-C(104)                            0.6(12) 
          C(102)-C(103)-C(104)-C(95)                            0.8(12) 
          C(96)-C(95)-C(104)-C(103)                            -2.3(11) 
          C(94)-C(95)-C(104)-C(103)                           174.4(7) 
          C(8)-C(3)-C(4)-C(5)                                  -1.0(13) 
          N(6)-C(3)-C(4)-C(5)                                 179.3(8) 
          C(3)-C(4)-C(5)-C(6)                                   1.1(14) 
          C(3)-C(4)-C(5)-Cl(1)                               -179.3(7) 
          C(4)-C(5)-C(6)-C(7)                                   0.2(13) 
          Cl(1)-C(5)-C(6)-C(7)                               -179.4(6) 
          C(5)-C(6)-C(7)-C(8)                                  -1.6(13) 
          C(6)-C(7)-C(8)-C(3)                                   1.7(12) 
          C(6)-C(7)-C(8)-C(9)                                -175.4(7) 
          C(4)-C(3)-C(8)-C(7)                                  -0.4(12) 
          N(6)-C(3)-C(8)-C(7)                                 179.3(8) 
          C(4)-C(3)-C(8)-C(9)                                 176.7(7) 
          N(6)-C(3)-C(8)-C(9)                                  -3.7(12) 
          C(1)-N(1)-C(9)-C(8)                                 -10.2(9) 
          C(1)-N(1)-C(9)-N(2)                                 114.2(8) 
          C(1)-N(1)-C(9)-C(18)                               -137.2(7) 
          C(7)-C(8)-C(9)-N(1)                                -173.6(7) 
          C(3)-C(8)-C(9)-N(1)                                   9.3(9) 
          C(7)-C(8)-C(9)-N(2)                                  63.2(9) 
          C(3)-C(8)-C(9)-N(2)                                -113.9(7) 
          C(7)-C(8)-C(9)-C(18)                                -49.7(9) 
          C(3)-C(8)-C(9)-C(18)                                133.3(7) 
          C(17)-N(2)-C(9)-N(1)                                108.2(7) 
          C(10)-N(2)-C(9)-N(1)                                -54.4(8) 
          C(17)-N(2)-C(9)-C(8)                               -128.7(7) 
          C(10)-N(2)-C(9)-C(8)                                 68.7(9) 
          C(17)-N(2)-C(9)-C(18)                                -6.8(7) 
          C(10)-N(2)-C(9)-C(18)                              -169.4(6) 
          C(19)-C(18)-C(9)-N(1)                              -112.8(7) 
          C(23)-C(18)-C(9)-N(1)                                58.2(10) 
          C(19)-C(18)-C(9)-C(8)                               122.9(7) 
          C(23)-C(18)-C(9)-C(8)                               -66.1(10) 
          C(19)-C(18)-C(9)-N(2)                                 2.8(8) 
          C(23)-C(18)-C(9)-N(2)                               173.8(7) 
          C(14)-C(15)-C(10)-C(11)                               0.3(12) 
          C(14)-C(15)-C(10)-N(2)                              177.1(7) 
          C(17)-N(2)-C(10)-C(11)                              115.0(8) 
          C(9)-N(2)-C(10)-C(11)                               -84.1(9) 
          C(17)-N(2)-C(10)-C(15)                              -61.7(9) 
          C(9)-N(2)-C(10)-C(15)                                99.2(8) 
          C(15)-C(10)-C(11)-C(12)                              -0.8(12) 
          N(2)-C(10)-C(11)-C(12)                             -177.4(7) 
          C(13)-C(12)-C(11)-C(10)                               0.3(14) 
          N(3)-C(28)-N(5)-C(29)                                 2.2(19) 
          C(34)-C(29)-N(5)-C(28)                               -2.3(17) 
          C(30)-C(29)-N(5)-C(28)                              172.6(11) 
          N(1)-C(1)-N(6)-C(3)                                   2.2(14) 
          C(4)-C(3)-N(6)-C(1)                                 177.0(8) 
          C(8)-C(3)-N(6)-C(1)                                  -2.7(13) 
          N(8)-C(2)-N(7)-C(60)                                  6.3(12) 
          N(9)-C(60)-N(7)-C(2)                                105.7(7) 
          C(59)-C(60)-N(7)-C(2)                               -15.8(9) 
          C(74)-C(60)-N(7)-C(2)                              -146.1(6) 
          N(7)-C(2)-N(8)-C(54)                                  4.1(12) 
          C(59)-C(54)-N(8)-C(2)                                -2.6(11) 
          C(55)-C(54)-N(8)-C(2)                               176.6(7) 
          O(3)-C(68)-N(9)-C(61)                                -6.3(11) 
          C(69)-C(68)-N(9)-C(61)                              173.4(6) 
          O(3)-C(68)-N(9)-C(60)                              -172.0(7) 
          C(69)-C(68)-N(9)-C(60)                                7.7(8) 
          C(62)-C(61)-N(9)-C(68)                              110.6(8) 
          C(66)-C(61)-N(9)-C(68)                              -68.4(9) 
          C(62)-C(61)-N(9)-C(60)                              -85.2(9) 
          C(66)-C(61)-N(9)-C(60)                               95.8(8) 
          N(7)-C(60)-N(9)-C(68)                               109.6(7) 
          C(59)-C(60)-N(9)-C(68)                             -130.1(7) 
          C(74)-C(60)-N(9)-C(68)                               -5.7(8) 
          N(7)-C(60)-N(9)-C(61)                               -55.9(8) 
          C(59)-C(60)-N(9)-C(61)                               64.3(9) 
          C(74)-C(60)-N(9)-C(61)                             -171.2(6) 
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         Symmetry transformations used to generate equivalent atoms: 
          
  
 Table 7.  Hydrogen bonds for t [A and deg.]. 
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 D-H...A                      d(D-H)      d(H...A)    d(D...A)    <(DHA) 
  
