data_4
_audit_creation_date               2024-05-22
_audit_creation_method
;
Olex2 1.3
(compiled Nov 21 2019 18:26:39 for OlexSys, GUI svn.r6003)
;
_shelx_SHELXL_version_number       '2018/3'
_audit_contact_author_address      ?
_audit_contact_author_email        ?
_audit_contact_author_name         ''
_audit_contact_author_phone        ?
_publ_contact_author_id_orcid      ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8.
;
_chemical_name_common              ?
_chemical_name_systematic          ?
_chemical_formula_moiety           '3(C136 H120 N16 Rh4), 16(C F3 O3 S)'
_chemical_formula_sum              'C424 H360 F48 N48 O48 Rh12 S16'
_chemical_formula_weight           9555.46
_chemical_melting_point            ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'F' 'F' 0.0583 0.0400 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N' 'N' 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'O' 'O' 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Rh' 'Rh' -0.0161 2.8414
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'S' 'S' 0.2925 0.4295 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system        'triclinic'
_space_group_IT_number             2
_space_group_name_H-M_alt          'P -1'
_space_group_name_Hall             '-P 1'
loop_
  _space_group_symop_operation_xyz
 'x, y, z'
 '-x, -y, -z'

_cell_length_a                     23.7694(14)
_cell_length_b                     24.0535(14)
_cell_length_c                     25.6350(15)
_cell_angle_alpha                  89.044(3)
_cell_angle_beta                   74.188(2)
_cell_angle_gamma                  71.864(3)
_cell_volume                       13364.1(14)
_cell_formula_units_Z              1
_cell_measurement_reflns_used      9747
_cell_measurement_temperature      170.00
_cell_measurement_theta_max        54.328
_cell_measurement_theta_min        3.131
_shelx_estimated_absorpt_T_max     0.769
_shelx_estimated_absorpt_T_min     0.471
_exptl_absorpt_coefficient_mu      2.771
_exptl_absorpt_correction_T_max    0.7508
_exptl_absorpt_correction_T_min    0.3424
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1678 before and 0.0883 after correction.
The Ratio of minimum to maximum transmission is 0.4560.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details     ?
_exptl_crystal_colour              yellow
_exptl_crystal_colour_primary      yellow
_exptl_crystal_density_diffrn      1.187
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      ?
_exptl_crystal_description         block
_exptl_crystal_F_000               4852
_exptl_crystal_size_max            0.32
_exptl_crystal_size_mid            0.1
_exptl_crystal_size_min            0.1
_exptl_transmission_factor_max     ?
_exptl_transmission_factor_min     ?
_diffrn_reflns_av_R_equivalents    0.1273
_diffrn_reflns_av_unetI/netI       0.1405
_diffrn_reflns_Laue_measured_fraction_full  0.992
_diffrn_reflns_Laue_measured_fraction_max  0.985
_diffrn_reflns_limit_h_max         24
_diffrn_reflns_limit_h_min         -28
_diffrn_reflns_limit_k_max         29
_diffrn_reflns_limit_k_min         -29
_diffrn_reflns_limit_l_max         31
_diffrn_reflns_limit_l_min         -30
_diffrn_reflns_number              140844
_diffrn_reflns_point_group_measured_fraction_full  0.992
_diffrn_reflns_point_group_measured_fraction_max  0.985
_diffrn_reflns_theta_full          53.594
_diffrn_reflns_theta_max           54.925
_diffrn_reflns_theta_min           2.673
_diffrn_ambient_temperature        170.00
_diffrn_detector_area_resol_mean   ?
_diffrn_measured_fraction_theta_full  0.992
_diffrn_measured_fraction_theta_max  0.985
_diffrn_measurement_device_type    'CCD area detector'
_diffrn_measurement_method         'phi and omega scans'
_diffrn_radiation_type             GaK\a
_diffrn_radiation_wavelength       1.34139
_diffrn_source                     ?
_diffrn_source_current             2.86
_diffrn_source_power               0.1999426
_diffrn_source_voltage             69.91
_reflns_Friedel_coverage           0.000
_reflns_Friedel_fraction_full      .
_reflns_Friedel_fraction_max       .
_reflns_number_gt                  22257
_reflns_number_total               50110
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression       'I > 2σ(I)'
_computing_cell_refinement         'SAINT V8.40B (?, 2016)'
_computing_data_collection         ?
_computing_data_reduction          'SAINT V8.40B (?, 2016)'
_computing_molecular_graphics      'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement    'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution      'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max           1.679
_refine_diff_density_min           -0.769
_refine_diff_density_rms           0.109
_refine_ls_extinction_coef         .
_refine_ls_extinction_method       none
_refine_ls_goodness_of_fit_ref     1.024
_refine_ls_hydrogen_treatment      constr
_refine_ls_matrix_type             full
_refine_ls_number_parameters       2710
_refine_ls_number_reflns           50110
_refine_ls_number_restraints       296
_refine_ls_R_factor_all            0.1689
_refine_ls_R_factor_gt             0.0973
_refine_ls_restrained_S_all        1.044
_refine_ls_shift/su_max            0.001
_refine_ls_shift/su_mean           0.000
_refine_ls_structure_factor_coef   Fsqd
_refine_ls_weighting_details      
 'w=1/[σ²(Fo²)+(0.1606P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme        calc
_refine_ls_wR_factor_gt            0.2650
_refine_ls_wR_factor_ref           0.3163
_refine_special_details            ?
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 F19-C211 = F21-C211 = F20-C211
 1.39 with sigma of 0.01
 S8-C211
 1.78 with sigma of 0.01
 S8-O30 = S8-O29 = S8-O28
 1.45 with sigma of 0.01
 S6-C205
 1.78 with sigma of 0.01
 S6-O14 = S6-O15 = S6-O13
 1.45 with sigma of 0.01
 F15-C205 = F13-C205 = F14-C205
 1.39 with sigma of 0.01
 O29-O28
 2.369 with sigma of 0.01
 O30-O28
 2.369 with sigma of 0.01
 F21-F20
 2.273 with sigma of 0.01
 F19-F20
 2.273 with sigma of 0.01
 O30-O29
 2.369 with sigma of 0.01
 F19-F21
 2.273 with sigma of 0.01
 O15-O13
 2.369 with sigma of 0.01
 S6-F15
 2.603 with sigma of 0.01
 F13-S6
 2.603 with sigma of 0.01
 O13-C205
 2.647 with sigma of 0.01
 O13-O14
 2.369 with sigma of 0.01
 O15-C205
 2.647 with sigma of 0.01
 S6-F14
 2.603 with sigma of 0.01
 F14-F15
 2.273 with sigma of 0.01
 C205-O14
 2.647 with sigma of 0.01
 F13-F15
 2.273 with sigma of 0.01
 O14-O15
 2.369 with sigma of 0.01
 F13-F14
 2.273 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
S8 \\sim C211: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
C209 \\sim S3: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
S6 \\sim O14: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02
within 2A
C205 \\sim S6: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
O15 \\sim S6: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02
within 2A
O13 \\sim S6: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02
within 2A
C205 \\sim F13: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
F15 \\sim C205: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
C205 \\sim F14: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
C142 \\sim C141: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
C143 \\sim C148: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
C146 \\sim C141: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
C149 \\sim C144: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
C145 \\sim C150: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
Uanis(C153) \\sim Ueq, Uanis(C158) \\sim Ueq, Uanis(C157) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
Uanis(O30) \\sim Ueq, Uanis(O28) \\sim Ueq, Uanis(O29) \\sim Ueq, Uanis(F20)
\\sim Ueq, Uanis(F21) \\sim Ueq: with sigma of 0.01 and sigma for terminal
atoms of 0.02
Uanis(S3) \\sim Ueq, Uanis(O9) \\sim Ueq, Uanis(O7) \\sim Ueq, Uanis(O8) \\sim
Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F3) \\sim Ueq, Uanis(F1) \\sim Ueq, Uanis(F2) \\sim Ueq, Uanis(C209)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C148) \\sim Ueq, Uanis(C149) \\sim Ueq, Uanis(C150) \\sim Ueq,
Uanis(C146) \\sim Ueq, Uanis(C142) \\sim Ueq, Uanis(C147) \\sim Ueq: with sigma
of 0.01 and sigma for terminal atoms of 0.02
Uanis(F18) \\sim Ueq, Uanis(O18) \\sim Ueq, Uanis(O16) \\sim Ueq: with sigma of
0.01 and sigma for terminal atoms of 0.02
Uanis(C59) \\sim Ueq, Uanis(C58) \\sim Ueq, Uanis(C57) \\sim Ueq, Uanis(C55)
\\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C128) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
4.a Me refined with riding coordinates:
 C189(H18A,H18B,H18C), C126(H12J,H12K,H12L), C158(H15D,H15E,H15F)
4.b Aromatic/amide H refined with riding coordinates:
 C71(H71), C1(H1), C119(H119), C66(H66), C63(H63), C93(H93), C89(H89),
 C47(H47), C9(H9), C17(H17), C168(H168), C55(H55), C169(H169), C48(H48),
 C94(H94), C67(H67), C87(H87), C30(H30), C43(H43), C79(H79), C120(H120),
 C45(H45), C25(H25), C7(H7), C64(H64), C72(H72), C8(H8), C101(H101), C117(H117),
  C52(H52), C28(H28), C54(H54), C15(H15), C88(H88), C31(H31), C33(H33),
 C92(H92), C22(H22), C29(H29), C46(H46), C53(H53), C35(H35), C170(H170),
 C58(H58), C16(H16), C74(H74), C115(H115), C178(H178), C38(H38), C100(H100),
 C62(H62), C81(H81), C20(H20), C49(H49), C40(H40), C26(H26), C75(H75), C80(H80),
  C163(H163), C107(H107), C114(H114), C42(H42), C118(H118), C2(H2), C21(H21),
 C106(H106), C3(H3), C182(H182), C59(H59), C73(H73), C105(H105), C112(H112),
 C39(H39), C50(H50), C70(H70), C110(H110), C57(H57), C183(H183), C181(H181),
 C176(H176), C103(H103), C162(H162), C102(H102), C98(H98), C69(H69), C34(H34),
 C177(H177), C111(H111), C161(H161), C97(H97)
4.c Idealised Me refined as rotating group:
 C202(H20A,H20B,H20C), C129(H12A,H12B,H12C), C130(H13A,H13B,H13C), C140(H14A,
 H14B,H14C), C193(H19A,H19B,H19C), C192(H19D,H19E,H19F), C139(H13D,H13E,H13F),
 C190(H19G,H19H,H19I), C159(H15A,H15B,H15C), C138(H13G,H13H,H13I), C137(H13J,
 H13K,H13L), C128(H12D,H12E,H12F), C191(H19J,H19K,H19L), C199(H19M,H19N,H19O),
 C201(H20D,H20E,H20F), C203(H20G,H20H,H20I), C200(H20J,H20K,H20L), C127(H12G,
 H12H,H12I), C160(H16A,H16B,H16C), C136(H13M,H13N,H13O), C157(H15G,H15H,H15I),
 C156(H15J,H15K,H15L), C148(H14D,H14E,H14F), C147(H14G,H14H,H14I), C146(H14J,
 H14K,H14L), C149(H14M,H14N,H14O), C150(H15M,H15N,H15O)
;
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary       ?
_atom_sites_solution_secondary     ?
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 Rh3 Rh 0.71409(3) 1.34155(3) 0.57478(3) 0.0702(2) Uani 1 1 d . . . . .
 Rh4 Rh 0.32098(3) 1.23944(3) 0.99061(3) 0.0697(2) Uani 1 1 d . . . . .
 Rh5 Rh 0.05844(3) 0.48010(3) 0.76164(3) 0.0731(2) Uani 1 1 d . . . . .
 Rh6 Rh 0.09905(3) 0.15380(3) 0.35095(3) 0.0720(2) Uani 1 1 d . . . . .
 Rh1 Rh 0.52668(4) 1.33601(3) 0.19263(3) 0.0768(2) Uani 1 1 d . . . . .
 Rh2 Rh 1.01165(4) 0.87797(4) 0.09813(3) 0.0799(2) Uani 1 1 d . . . . .
 S2 S 0.91973(11) 0.68797(12) 0.05230(10) 0.0792(7) Uani 1 1 d . . . . .
 S7 S 0.15043(13) -0.10800(12) 0.51748(12) 0.0907(8) Uani 1 1 d . . . . .
 S5 S 0.53562(13) 0.60766(12) 0.57841(10) 0.0863(7) Uani 1 1 d . . . . .
 S4 S 0.24312(13) 0.32984(13) 0.20675(11) 0.0904(8) Uani 1 1 d . . . . .
 S1 S -0.04688(13) 0.38068(13) 0.44759(13) 0.0938(8) Uani 1 1 d . . . . .
 S3 S 0.7582(2) 1.2611(3) 0.04700(19) 0.1617(17) Uani 1 1 d . U . . .
 S6 S 0.3026(3) 0.5298(2) 0.7147(2) 0.1764(18) Uani 1 1 d D U . . .
 C211 C -0.0877(3) 0.1717(2) 0.6933(2) 0.0397(14) Uani 1 1 d D U . . .
 S8 S -0.0715(3) 0.0974(2) 0.6889(2) 0.190(2) Uani 1 1 d D U . . .
 F7 F 1.0282(3) 0.6546(3) -0.0204(3) 0.113(2) Uani 1 1 d . . . . .
 N16 N 0.3263(3) 1.2977(3) 0.9277(3) 0.0708(19) Uani 1 1 d . . . . .
 N17 N 0.0346(3) 0.4074(3) 0.7427(3) 0.0706(19) Uani 1 1 d . . . . .
 N15 N 0.4141(3) 1.2041(3) 0.9424(3) 0.0681(18) Uani 1 1 d . . . . .
 O5 O 0.9497(3) 0.6709(3) 0.0942(3) 0.0917(19) Uani 1 1 d . . . . .
 N10 N 0.6890(3) 1.2990(3) 0.5190(3) 0.072(2) Uani 1 1 d . . . . .
 F9 F 0.9874(3) 0.5871(3) 0.0002(3) 0.117(2) Uani 1 1 d . . . . .
 N11 N 0.7048(3) 1.2758(3) 0.6290(3) 0.0705(19) Uani 1 1 d . . . . .
 N7 N 0.9579(3) 0.8458(4) 0.1659(3) 0.074(2) Uani 1 1 d . . . . .
 N19 N 0.0501(3) 0.2792(3) 0.5942(3) 0.0737(19) Uani 1 1 d . . . . .
 N18 N 0.0991(3) 0.4648(3) 0.6764(3) 0.0674(18) Uani 1 1 d . . . . .
 N21 N 0.0625(3) 0.1645(3) 0.4366(3) 0.0708(19) Uani 1 1 d . . . . .
 F8 F 0.9533(3) 0.6526(4) -0.0512(3) 0.131(3) Uani 1 1 d . . . . .
 N14 N 0.4690(3) 1.3346(3) 0.7684(3) 0.0716(19) Uani 1 1 d . . . . .
 F26 F 0.1156(4) 0.0034(3) 0.4997(3) 0.119(2) Uani 1 1 d . . . . .
 O6 O 0.8663(3) 0.6701(3) 0.0574(3) 0.0831(18) Uani 1 1 d . . . . .
 N22 N 0.1423(4) 0.2085(3) 0.3739(3) 0.075(2) Uani 1 1 d . . . . .
 F30 F 0.0590(4) 0.3973(4) 0.4056(4) 0.138(3) Uani 1 1 d . . . . .
 O12 O 0.4793(3) 0.6482(4) 0.6103(3) 0.102(2) Uani 1 1 d . . . . .
 O4 O 0.9113(3) 0.7479(3) 0.0393(3) 0.095(2) Uani 1 1 d . . . . .
 F17 F 0.2677(4) 0.3705(4) 0.2879(3) 0.127(2) Uani 1 1 d . . . . .
 N9 N 0.7013(3) 0.8137(3) 0.0608(3) 0.0678(18) Uani 1 1 d . . . . .
 N1 N 0.9271(4) 0.9128(4) 0.0758(3) 0.079(2) Uani 1 1 d . . . . .
 N6 N 0.5684(4) 1.2550(4) 0.1448(3) 0.078(2) Uani 1 1 d . . . . .
 N24 N 0.8586(3) -0.4179(3) 0.2311(3) 0.077(2) Uani 1 1 d . . . . .
 N23 N 0.1713(3) 0.0801(4) 0.3606(3) 0.074(2) Uani 1 1 d . . . . .
 O25 O 0.1986(3) -0.1193(3) 0.4679(3) 0.109(3) Uani 1 1 d . . . . .
 F11 F 0.4899(3) 0.6054(4) 0.4980(3) 0.139(3) Uani 1 1 d . . . . .
 O11 O 0.5666(4) 0.5629(4) 0.6070(3) 0.110(2) Uani 1 1 d . . . . .
 O21 O -0.0572(4) 0.3829(3) 0.3953(3) 0.103(2) Uani 1 1 d . . . . .
 N12 N 0.6182(3) 1.3727(3) 0.6182(3) 0.078(2) Uani 1 1 d . . . . .
 N13 N 0.5612(3) 1.2342(3) 0.7835(3) 0.077(2) Uani 1 1 d . . . . .
 N3 N 0.7454(4) 1.0814(4) 0.1090(3) 0.075(2) Uani 1 1 d . . . . .
 N8 N 0.5226(4) 0.7087(4) 0.7485(3) 0.082(2) Uani 1 1 d . . . . .
 N4 N 0.7905(4) 1.1315(4) 0.1816(3) 0.082(2) Uani 1 1 d . . . . .
 N20 N 0.1264(4) 0.3345(4) 0.5245(3) 0.075(2) Uani 1 1 d . . . . .
 C83 C 0.0721(4) 0.2640(4) 0.5406(3) 0.064(2) Uani 1 1 d . . . . .
 F27 F 0.0439(3) -0.0257(4) 0.5483(3) 0.154(3) Uani 1 1 d . . . . .
 F28 F -0.0156(4) 0.4765(3) 0.4274(4) 0.141(3) Uani 1 1 d . . . . .
 O26 O 0.1175(4) -0.1493(4) 0.5294(3) 0.115(3) Uani 1 1 d . . . . .
 F12 F 0.5650(4) 0.5298(4) 0.4987(3) 0.148(3) Uani 1 1 d . . . . .
 N2 N 0.9708(4) 0.9619(4) 0.1424(3) 0.085(2) Uani 1 1 d . . . . .
 F25 F 0.0784(4) -0.0488(4) 0.4621(3) 0.129(2) Uani 1 1 d . . . . .
 C85 C 0.1014(4) 0.3511(4) 0.5772(3) 0.069(2) Uani 1 1 d . . . . .
 C91 C 0.0529(4) 0.3880(4) 0.6912(3) 0.064(2) Uani 1 1 d . . . . .
 C96 C 0.0627(4) 0.3232(4) 0.6127(4) 0.069(2) Uani 1 1 d . . . . .
 O19 O -0.0998(4) 0.4129(4) 0.4899(3) 0.118(3) Uani 1 1 d . . . . .
 O18 O 0.3083(4) 0.3099(4) 0.1838(3) 0.126(3) Uani 1 1 d . U . . .
 O10 O 0.5755(4) 0.6364(4) 0.5445(4) 0.125(3) Uani 1 1 d . . . . .
 C18 C 0.6013(4) 1.3396(3) 0.6573(4) 0.065(2) Uani 1 1 d . . . . .
 C71 C 0.5251(4) 0.7059(4) 0.6965(3) 0.075(2) Uani 1 1 d . . . . .
 H71 H 0.499431 0.687162 0.686436 0.090 Uiso 1 1 calc R U . . .
 C1 C 0.2800(4) 1.3458(4) 0.9192(4) 0.078(3) Uani 1 1 d . . . . .
 H1 H 0.239356 1.354272 0.942829 0.093 Uiso 1 1 calc R U . . .
 C116 C 0.7522(4) -0.3264(4) 0.2270(4) 0.068(2) Uani 1 1 d . . . . .
 N5 N 0.6058(4) 1.2962(4) 0.2195(3) 0.083(2) Uani 1 1 d . . . . .
 C13 C 0.5258(4) 1.3179(4) 0.7349(4) 0.064(2) Uani 1 1 d . . . . .
 C14 C 0.5408(4) 1.3535(4) 0.6914(4) 0.073(2) Uani 1 1 d . . . . .
 C173 C 0.7356(5) 1.1592(4) 0.1710(3) 0.068(2) Uani 1 1 d . . . . .
 C84 C 0.1121(4) 0.2910(5) 0.5066(4) 0.074(2) Uani 1 1 d . . . . .
 C166 C 0.8931(5) 0.9673(4) 0.0996(3) 0.071(2) Uani 1 1 d . . . . .
 O17 O 0.2078(4) 0.3585(4) 0.1715(3) 0.121(3) Uani 1 1 d . . . . .
 C188 C -0.0108(5) 0.5628(5) 0.7641(4) 0.088(3) Uani 1 1 d . . . . .
 C12 C 0.4564(4) 1.3018(4) 0.8101(4) 0.069(2) Uani 1 1 d . . . . .
 C119 C 0.8612(4) -0.3750(4) 0.1955(4) 0.072(2) Uani 1 1 d . . . . .
 H119 H 0.900281 -0.375075 0.173086 0.086 Uiso 1 1 calc R U . . .
 C56 C 0.7907(4) 0.7658(4) 0.3872(3) 0.074(2) Uani 1 1 d . . . . .
 C108 C 0.5313(4) -0.2036(4) 0.3005(4) 0.071(2) Uani 1 1 d . . . . .
 C66 C 0.6545(5) 0.7701(5) 0.5757(4) 0.083(3) Uani 1 1 d . . . . .
 H66 H 0.632847 0.750025 0.561107 0.100 Uiso 1 1 calc R U . . .
 C109 C 0.4820(4) -0.1516(4) 0.3002(4) 0.078(3) Uani 1 1 d . . . . .
 C167 C 0.8350(4) 0.9968(4) 0.0900(4) 0.070(2) Uani 1 1 d . . . . .
 C24 C 0.5726(4) 1.2665(4) 0.7423(4) 0.074(2) Uani 1 1 d . . . . .
 O20 O -0.0134(4) 0.3246(4) 0.4601(4) 0.122(3) Uani 1 1 d . . . . .
 C171 C 0.8005(5) 1.0539(4) 0.1173(3) 0.071(2) Uani 1 1 d . . . . .
 C95 C 0.0407(4) 0.3418(4) 0.6715(4) 0.069(2) Uani 1 1 d . . . . .
 C86 C 0.1119(5) 0.4008(4) 0.5988(4) 0.078(3) Uani 1 1 d . . . . .
 C10 C 0.4900(4) 1.2159(4) 0.8640(3) 0.068(2) Uani 1 1 d . . . . .
 C63 C 0.7583(5) 0.8588(5) 0.5131(4) 0.093(3) Uani 1 1 d . . . . .
 H63 H 0.770082 0.889794 0.524633 0.111 Uiso 1 1 calc R U . . .
 C19 C 0.6479(4) 1.2860(4) 0.6658(4) 0.066(2) Uani 1 1 d . . . . .
 O27 O 0.1674(5) -0.0910(4) 0.5646(4) 0.129(3) Uani 1 1 d . . . . .
 F29 F 0.0181(4) 0.4265(4) 0.4905(5) 0.159(3) Uani 1 1 d . . . . .
 C93 C -0.0135(5) 0.3324(5) 0.7611(4) 0.081(3) Uani 1 1 d . . . . .
 H93 H -0.037597 0.314132 0.787062 0.097 Uiso 1 1 calc R U . . .
 C65 C 0.7000(4) 0.7930(4) 0.5367(4) 0.075(3) Uani 1 1 d . . . . .
 C172 C 0.8226(5) 1.0791(5) 0.1536(3) 0.073(2) Uani 1 1 d . . . . .
 C89 C 0.1332(5) 0.4923(4) 0.6431(4) 0.082(3) Uani 1 1 d . . . . .
 H89 H 0.140398 0.524698 0.657604 0.099 Uiso 1 1 calc R U . . .
 C6 C 0.4298(4) 1.2352(4) 0.8991(4) 0.068(2) Uani 1 1 d . . . . .
 C165 C 0.9176(5) 0.9929(5) 0.1344(4) 0.071(2) Uani 1 1 d . . . . .
 C77 C 0.1212(4) 0.2287(5) 0.4266(4) 0.084(3) Uani 1 1 d . . . . .
 C124 C 0.3052(5) 1.2984(5) 1.0583(4) 0.087(3) Uani 1 1 d . . . . .
 C47 C 0.6687(5) 0.8717(4) 0.0745(4) 0.076(2) Uani 1 1 d . . . . .
 H47 H 0.636290 0.889080 0.058480 0.091 Uiso 1 1 calc R U . . .
 C179 C 0.6212(5) 1.2201(5) 0.1524(4) 0.083(3) Uani 1 1 d . . . . .
 C125 C 0.3416(5) 1.2418(5) 1.0677(4) 0.078(3) Uani 1 1 d . . . . .
 C37 C 0.7031(4) 1.0832(4) 0.2977(4) 0.075(2) Uani 1 1 d . . . . .
 C36 C 0.6876(4) 1.0566(4) 0.2570(3) 0.069(2) Uani 1 1 d . . . . .
 C9 C 0.5331(4) 1.1651(4) 0.8740(4) 0.075(2) Uani 1 1 d . . . . .
 H9 H 0.573819 1.151651 0.850233 0.090 Uiso 1 1 calc R U . . .
 C134 C 0.7841(4) 1.3630(5) 0.5123(4) 0.079(3) Uani 1 1 d . . . . .
 C164 C 0.8831(5) 1.0485(4) 0.1608(3) 0.071(2) Uani 1 1 d . . . . .
 C175 C 0.6563(5) 1.1660(4) 0.1248(4) 0.073(2) Uani 1 1 d . . . . .
 C5 C 0.3823(4) 1.2854(4) 0.8914(4) 0.071(2) Uani 1 1 d . . . . .
 C17 C 0.5758(4) 1.4214(4) 0.6082(4) 0.075(2) Uani 1 1 d . . . . .
 H17 H 0.587953 1.445495 0.580522 0.090 Uiso 1 1 calc R U . . .
 C154 C 0.4645(5) 1.3929(5) 0.1544(4) 0.087(3) Uani 1 1 d . . . . .
 C168 C 0.8162(5) 0.9680(4) 0.0554(4) 0.078(3) Uani 1 1 d . . . . .
 H168 H 0.778422 0.986263 0.047034 0.093 Uiso 1 1 calc R U . . .
 C4 C 0.3958(4) 1.3194(4) 0.8476(3) 0.064(2) Uani 1 1 d . . . . .
 C55 C 0.8301(4) 0.7907(4) 0.3470(4) 0.081(3) Uani 1 1 d . U . . .
 H55 H 0.848033 0.816323 0.359133 0.097 Uiso 1 1 calc R U . . .
 C169 C 0.8525(5) 0.9126(5) 0.0330(4) 0.080(3) Uani 1 1 d . . . . .
 H169 H 0.838861 0.892107 0.010138 0.095 Uiso 1 1 calc R U . . .
 F19 F -0.1120(3) 0.1953(4) 0.6504(3) 0.132(2) Uani 1 1 d D . . . .
 C48 C 0.6794(4) 0.9059(4) 0.1094(3) 0.071(2) Uani 1 1 d . . . . .
 H48 H 0.654447 0.945744 0.118229 0.085 Uiso 1 1 calc R U . . .
 C82 C 0.0557(4) 0.2189(4) 0.5186(4) 0.072(2) Uani 1 1 d . . . . .
 C11 C 0.5034(4) 1.2509(4) 0.8173(4) 0.072(2) Uani 1 1 d . . . . .
 C94 C 0.0053(4) 0.3131(4) 0.7087(4) 0.081(3) Uani 1 1 d . . . . .
 H94 H -0.004822 0.281178 0.696801 0.097 Uiso 1 1 calc R U . . .
 C67 C 0.6426(5) 0.7758(4) 0.6287(4) 0.080(3) Uani 1 1 d . . . . .
 H67 H 0.663781 0.797504 0.641876 0.096 Uiso 1 1 calc R U . . .
 C113 C 0.5891(4) -0.2142(4) 0.2602(4) 0.076(3) Uani 1 1 d . . . . .
 C87 C 0.1506(4) 0.4318(4) 0.5648(4) 0.081(3) Uani 1 1 d . . . . .
 H87 H 0.169344 0.420661 0.527131 0.097 Uiso 1 1 calc R U . . .
 C76 C 0.1387(4) 0.2712(4) 0.4483(3) 0.074(2) Uani 1 1 d . . . . .
 C30 C 0.6480(5) 1.2194(5) 0.3911(5) 0.091(3) Uani 1 1 d . . . . .
 H30 H 0.619068 1.244399 0.374720 0.110 Uiso 1 1 calc R U . . .
 C43 C 0.7439(4) 0.9141(4) 0.1709(4) 0.076(2) Uani 1 1 d . . . . .
 H43 H 0.777560 0.893916 0.184543 0.091 Uiso 1 1 calc R U . . .
 C79 C 0.0234(4) 0.1387(4) 0.4685(4) 0.072(2) Uani 1 1 d . . . . .
 H79 H 0.011147 0.111399 0.451492 0.087 Uiso 1 1 calc R U . . .
 C23 C 0.6345(4) 1.2513(4) 0.7065(4) 0.068(2) Uani 1 1 d . . . . .
 C187 C -0.0329(5) 0.5310(4) 0.8077(5) 0.089(3) Uani 1 1 d . . . . .
 C120 C 0.8092(4) -0.3317(5) 0.1912(4) 0.080(3) Uani 1 1 d . . . . .
 H120 H 0.812537 -0.305271 0.163433 0.096 Uiso 1 1 calc R U . . .
 C78 C 0.0788(4) 0.2019(4) 0.4617(4) 0.074(2) Uani 1 1 d . . . . .
 C123 C 0.2460(4) 1.2948(5) 1.0557(4) 0.079(3) Uani 1 1 d . . . . .
 C41 C 0.7306(4) 1.0021(4) 0.2294(3) 0.071(2) Uani 1 1 d . . . . .
 C51 C 0.8848(4) 0.8019(4) 0.2508(4) 0.072(2) Uani 1 1 d . . . . .
 C45 C 0.7636(4) 0.8241(4) 0.1156(4) 0.078(3) Uani 1 1 d . . . . .
 H45 H 0.798318 0.805969 0.128582 0.093 Uiso 1 1 calc R U . . .
 C27 C 0.6619(4) 1.2457(4) 0.4358(4) 0.074(2) Uani 1 1 d . . . . .
 C25 C 0.7092(4) 1.2411(4) 0.5074(4) 0.081(3) Uani 1 1 d . . . . .
 H25 H 0.733988 1.217516 0.528197 0.097 Uiso 1 1 calc R U . . .
 F16 F 0.2513(6) 0.4316(4) 0.2295(5) 0.186(4) Uani 1 1 d . . . . .
 C61 C 0.7662(4) 0.7904(5) 0.4414(4) 0.077(3) Uani 1 1 d . . . . .
 C7 C 0.4559(4) 1.1565(4) 0.9505(4) 0.080(3) Uani 1 1 d . . . . .
 H7 H 0.444438 1.135094 0.980783 0.096 Uiso 1 1 calc R U . . .
 C32 C 0.6606(5) 1.1372(4) 0.3280(4) 0.075(2) Uani 1 1 d . . . . .
 C202 C 0.0599(5) 0.2741(5) 0.2903(5) 0.092(3) Uani 1 1 d . . . . .
 H20A H 0.045938 0.295570 0.326064 0.139 Uiso 1 1 calc R U . . .
 H20B H 0.031606 0.292860 0.268847 0.139 Uiso 1 1 calc R U . . .
 H20C H 0.101488 0.274683 0.271412 0.139 Uiso 1 1 calc R U . . .
 C64 C 0.7168(5) 0.8369(5) 0.5507(4) 0.082(3) Uani 1 1 d . . . . .
 H64 H 0.700292 0.853979 0.587011 0.099 Uiso 1 1 calc R U . . .
 C90 C 0.0886(4) 0.4189(4) 0.6536(4) 0.070(2) Uani 1 1 d . . . . .
 C048 C 0.6984(5) 1.2153(5) 0.2030(3) 0.079(3) Uani 1 1 d . . . . .
 C72 C 0.5608(5) 0.7271(5) 0.6567(4) 0.086(3) Uani 1 1 d . . . . .
 H72 H 0.558816 0.724425 0.620324 0.104 Uiso 1 1 calc R U . . .
 C104 C 0.4233(4) -0.1390(5) 0.3424(4) 0.084(3) Uani 1 1 d . . . . .
 C44 C 0.7281(4) 0.8814(4) 0.1322(4) 0.065(2) Uani 1 1 d . . . . .
 C8 C 0.5169(4) 1.1359(4) 0.9164(4) 0.073(2) Uani 1 1 d . . . . .
 H8 H 0.545853 1.101679 0.923874 0.088 Uiso 1 1 calc R U . . .
 C101 C 0.2291(4) 0.0793(4) 0.3469(4) 0.074(2) Uani 1 1 d . . . . .
 H101 H 0.237742 0.114340 0.335850 0.088 Uiso 1 1 calc R U . . .
 C117 C 0.7508(5) -0.3727(5) 0.2619(4) 0.084(3) Uani 1 1 d . . . . .
 H117 H 0.712851 -0.373050 0.286275 0.101 Uiso 1 1 calc R U . . .
 C194 C 0.0317(5) 0.1304(4) 0.3208(4) 0.077(3) Uani 1 1 d . . . . .
 C52 C 0.8955(4) 0.7850(4) 0.1966(4) 0.079(3) Uani 1 1 d . . . . .
 H52 H 0.877801 0.757300 0.187879 0.095 Uiso 1 1 calc R U . . .
 C28 C 0.6410(5) 1.3054(4) 0.4463(4) 0.085(3) Uani 1 1 d . . . . .
 H28 H 0.616532 1.329417 0.425639 0.101 Uiso 1 1 calc R U . . .
 C54 C 0.8425(5) 0.7787(5) 0.2920(4) 0.082(3) Uani 1 1 d . . . . .
 H54 H 0.823076 0.754421 0.279960 0.099 Uiso 1 1 calc R U . . .
 C15 C 0.4966(4) 1.4048(4) 0.6806(4) 0.071(2) Uani 1 1 d . . . . .
 H15 H 0.455031 1.416987 0.702730 0.085 Uiso 1 1 calc R U . . .
 C88 C 0.1585(5) 0.4760(4) 0.5886(4) 0.081(3) Uani 1 1 d . . . . .
 H88 H 0.182805 0.497321 0.567109 0.097 Uiso 1 1 calc R U . . .
 C135 C 0.8107(4) 1.3304(4) 0.5513(4) 0.078(3) Uani 1 1 d . . . . .
 C174 C 0.7125(5) 1.1345(5) 0.1349(4) 0.086(3) Uani 1 1 d . . . . .
 C153 C 0.4504(5) 1.4162(5) 0.2086(4) 0.089(3) Uani 1 1 d . U . . .
 C31 C 0.6730(4) 1.1629(4) 0.3718(4) 0.082(3) Uani 1 1 d . . . . .
 H31 H 0.701468 1.137878 0.388660 0.098 Uiso 1 1 calc R U . . .
 C33 C 0.6052(5) 1.1623(4) 0.3127(4) 0.091(3) Uani 1 1 d . . . . .
 H33 H 0.577170 1.198776 0.330233 0.109 Uiso 1 1 calc R U . . .
 C92 C 0.0018(4) 0.3782(4) 0.7777(4) 0.077(3) Uani 1 1 d . . . . .
 H92 H -0.011174 0.390075 0.815412 0.092 Uiso 1 1 calc R U . . .
 C133 C 0.7395(4) 1.4160(4) 0.5418(5) 0.082(3) Uani 1 1 d . . . . .
 C22 C 0.6822(5) 1.1999(4) 0.7113(4) 0.089(3) Uani 1 1 d . . . . .
 H22 H 0.674775 1.174756 0.739517 0.106 Uiso 1 1 calc R U . . .
 C29 C 0.6549(5) 1.3303(4) 0.4861(5) 0.094(3) Uani 1 1 d . . . . .
 H29 H 0.640269 1.371874 0.491598 0.112 Uiso 1 1 calc R U . . .
 C46 C 0.7477(4) 0.7926(4) 0.0793(4) 0.072(2) Uani 1 1 d . . . . .
 H46 H 0.772997 0.753264 0.067844 0.087 Uiso 1 1 calc R U . . .
 C53 C 0.9314(5) 0.8073(5) 0.1547(4) 0.082(3) Uani 1 1 d . . . . .
 H53 H 0.937213 0.795239 0.117936 0.099 Uiso 1 1 calc R U . . .
 C35 C 0.6313(5) 1.0831(4) 0.2459(4) 0.080(3) Uani 1 1 d . . . . .
 H35 H 0.620377 1.065188 0.219132 0.096 Uiso 1 1 calc R U . . .
 C170 C 0.9088(5) 0.8863(5) 0.0433(4) 0.081(3) Uani 1 1 d . . . . .
 H170 H 0.934084 0.848648 0.026355 0.097 Uiso 1 1 calc R U . . .
 F10 F 0.4761(5) 0.5434(5) 0.5556(4) 0.171(4) Uani 1 1 d . . . . .
 C68 C 0.6017(4) 0.7537(4) 0.6698(4) 0.073(2) Uani 1 1 d . . . . .
 C58 C 0.7335(6) 0.6954(5) 0.4100(5) 0.098(3) Uani 1 1 d . U . . .
 H58 H 0.721770 0.664253 0.398966 0.117 Uiso 1 1 calc R U . . .
 C16 C 0.5149(4) 1.4355(4) 0.6386(4) 0.076(2) Uani 1 1 d . . . . .
 H16 H 0.485020 1.467908 0.629668 0.091 Uiso 1 1 calc R U . . .
 C74 C 0.2046(4) 0.2723(5) 0.3601(4) 0.085(3) Uani 1 1 d . . . . .
 H74 H 0.235411 0.285334 0.336103 0.102 Uiso 1 1 calc R U . . .
 C115 C 0.6994(4) -0.2767(5) 0.2268(4) 0.084(3) Uani 1 1 d . . . . .
 H115 H 0.705571 -0.248775 0.201057 0.101 Uiso 1 1 calc R U . . .
 C178 C 0.5475(5) 1.2348(5) 0.1087(4) 0.085(3) Uani 1 1 d . . . . .
 H178 H 0.510329 1.258490 0.101909 0.101 Uiso 1 1 calc R U . . .
 C184 C 0.0428(5) 0.5736(5) 0.7733(4) 0.085(3) Uani 1 1 d . . . . .
 C38 C 0.7621(5) 1.0576(5) 0.3063(4) 0.084(3) Uani 1 1 d . . . . .
 H38 H 0.773682 1.076315 0.332117 0.100 Uiso 1 1 calc R U . . .
 C197 C 0.0607(5) 0.2132(5) 0.2971(4) 0.085(3) Uani 1 1 d . . . . .
 C100 C 0.2774(5) 0.0304(5) 0.3477(4) 0.086(3) Uani 1 1 d . . . . .
 H100 H 0.318430 0.031738 0.335632 0.103 Uiso 1 1 calc R U . . .
 O16 O 0.2186(6) 0.2906(5) 0.2392(4) 0.145(4) Uani 1 1 d . U . . .
 C62 C 0.7816(5) 0.8367(5) 0.4611(4) 0.080(3) Uani 1 1 d . . . . .
 H62 H 0.809386 0.852731 0.436617 0.096 Uiso 1 1 calc R U . . .
 C81 C 0.0162(4) 0.1896(4) 0.5500(3) 0.068(2) Uani 1 1 d . . . . .
 H81 H 0.000792 0.197233 0.588337 0.081 Uiso 1 1 calc R U . . .
 C20 C 0.7489(4) 1.2249(4) 0.6353(4) 0.082(3) Uani 1 1 d . . . . .
 H20 H 0.789074 1.215096 0.610660 0.099 Uiso 1 1 calc R U . . .
 C60 C 0.7232(5) 0.7679(5) 0.4813(4) 0.085(3) Uani 1 1 d . . . . .
 C180 C 0.6433(5) 1.2434(4) 0.1935(3) 0.071(2) Uani 1 1 d . . . . .
 C186 C 0.0081(5) 0.5182(4) 0.8423(5) 0.089(3) Uani 1 1 d . . . . .
 C49 C 0.9502(4) 0.8607(4) 0.2176(3) 0.074(2) Uani 1 1 d . . . . .
 H49 H 0.971315 0.885756 0.225420 0.089 Uiso 1 1 calc R U . . .
 C40 C 0.7851(4) 0.9800(4) 0.2411(4) 0.076(2) Uani 1 1 d . . . . .
 H40 H 0.813125 0.943919 0.222708 0.091 Uiso 1 1 calc R U . . .
 C26 C 0.6970(5) 1.2128(4) 0.4677(4) 0.079(3) Uani 1 1 d . . . . .
 H26 H 0.712354 1.171261 0.462050 0.095 Uiso 1 1 calc R U . . .
 C75 C 0.1817(4) 0.2943(4) 0.4142(4) 0.079(3) Uani 1 1 d . . . . .
 H75 H 0.194581 0.323511 0.427434 0.094 Uiso 1 1 calc R U . . .
 C80 C 0.0008(5) 0.1496(5) 0.5230(4) 0.081(3) Uani 1 1 d . . . . .
 H80 H -0.025867 0.129616 0.543098 0.097 Uiso 1 1 calc R U . . .
 C207 C 0.9756(5) 0.6437(5) -0.0065(4) 0.086(3) Uani 1 1 d . . . . .
 C163 C 0.9078(5) 1.0724(5) 0.1952(4) 0.087(3) Uani 1 1 d . . . . .
 H163 H 0.886489 1.110058 0.213799 0.104 Uiso 1 1 calc R U . . .
 C107 C 0.5214(5) -0.2422(4) 0.3414(4) 0.083(3) Uani 1 1 d . . . . .
 H107 H 0.553774 -0.277190 0.341915 0.100 Uiso 1 1 calc R U . . .
 C114 C 0.6421(4) -0.2666(5) 0.2601(4) 0.082(3) Uani 1 1 d . . . . .
 H114 H 0.635193 -0.294988 0.285119 0.098 Uiso 1 1 calc R U . . .
 C42 C 0.7137(4) 0.9712(4) 0.1883(4) 0.078(3) Uani 1 1 d . . . . .
 H42 H 0.680835 0.992428 0.174112 0.094 Uiso 1 1 calc R U . . .
 C189 C 0.0774(5) 0.6109(5) 0.7383(6) 0.104(4) Uani 1 1 d . . . . .
 H18A H 0.059419 0.624030 0.708304 0.156 Uiso 1 1 calc R U . . .
 H18B H 0.074208 0.645136 0.760491 0.156 Uiso 1 1 calc R U . . .
 H18C H 0.120950 0.587589 0.723524 0.156 Uiso 1 1 calc R U . . .
 C118 C 0.8038(4) -0.4167(5) 0.2605(4) 0.085(3) Uani 1 1 d . . . . .
 H118 H 0.800783 -0.448570 0.282319 0.102 Uiso 1 1 calc R U . . .
 C196 C 0.1104(5) 0.1613(5) 0.2651(3) 0.078(3) Uani 1 1 d . . . . .
 C198 C 0.0135(5) 0.1923(5) 0.3300(4) 0.086(3) Uani 1 1 d . . . . .
 C2 C 0.2906(4) 1.3809(4) 0.8785(4) 0.076(2) Uani 1 1 d . . . . .
 H2 H 0.258159 1.414691 0.875443 0.091 Uiso 1 1 calc R U . . .
 C121 C 0.3061(5) 1.2024(5) 1.0694(4) 0.081(3) Uani 1 1 d . . . . .
 C21 C 0.7380(4) 1.1880(4) 0.6750(4) 0.080(3) Uani 1 1 d . . . . .
 H21 H 0.770242 1.153501 0.676982 0.095 Uiso 1 1 calc R U . . .
 C106 C 0.4664(5) -0.2302(4) 0.3802(4) 0.085(3) Uani 1 1 d . . . . .
 H106 H 0.460373 -0.256367 0.407766 0.102 Uiso 1 1 calc R U . . .
 C3 C 0.3479(4) 1.3685(4) 0.8413(4) 0.078(3) Uani 1 1 d . . . . .
 H3 H 0.354814 1.392607 0.812039 0.093 Uiso 1 1 calc R U . . .
 C129 C 0.3216(5) 1.3540(5) 1.0559(4) 0.086(3) Uani 1 1 d . . . . .
 H12A H 0.366041 1.344988 1.039085 0.130 Uiso 1 1 calc R U . . .
 H12B H 0.310632 1.372043 1.092778 0.130 Uiso 1 1 calc R U . . .
 H12C H 0.298911 1.381212 1.034186 0.130 Uiso 1 1 calc R U . . .
 C99 C 0.2670(4) -0.0210(4) 0.3659(4) 0.083(3) Uani 1 1 d . . . . .
 C182 C 0.6800(6) 1.2910(5) 0.2699(4) 0.093(3) Uani 1 1 d . . . . .
 H182 H 0.691239 1.307943 0.297083 0.111 Uiso 1 1 calc R U . . .
 C59 C 0.7120(5) 0.7183(5) 0.4640(4) 0.085(3) Uani 1 1 d . U . . .
 H59 H 0.688816 0.699579 0.490240 0.102 Uiso 1 1 calc R U . . .
 C73 C 0.1828(5) 0.2307(5) 0.3403(4) 0.088(3) Uani 1 1 d . . . . .
 H73 H 0.196940 0.218410 0.302644 0.106 Uiso 1 1 calc R U . . .
 C105 C 0.4184(4) -0.1783(5) 0.3789(4) 0.086(3) Uani 1 1 d . . . . .
 H105 H 0.380047 -0.170977 0.405900 0.103 Uiso 1 1 calc R U . . .
 C130 C 0.4023(5) 1.2248(5) 1.0780(4) 0.095(3) Uani 1 1 d . . . . .
 H13A H 0.419854 1.181942 1.074854 0.142 Uiso 1 1 calc R U . . .
 H13B H 0.397721 1.239833 1.114773 0.142 Uiso 1 1 calc R U . . .
 H13C H 0.429775 1.241327 1.051407 0.142 Uiso 1 1 calc R U . . .
 C112 C 0.5937(4) -0.1747(4) 0.2187(4) 0.083(3) Uani 1 1 d . . . . .
 H112 H 0.630962 -0.182701 0.190198 0.100 Uiso 1 1 calc R U . . .
 C39 C 0.8020(5) 1.0071(5) 0.2783(4) 0.085(3) Uani 1 1 d . . . . .
 H39 H 0.841300 0.990525 0.284397 0.103 Uiso 1 1 calc R U . . .
 C50 C 0.9125(4) 0.8412(4) 0.2614(4) 0.076(2) Uani 1 1 d . . . . .
 H50 H 0.906244 0.854982 0.297694 0.091 Uiso 1 1 calc R U . . .
 C140 C 0.8665(5) 1.2735(5) 0.5392(5) 0.089(3) Uani 1 1 d . . . . .
 H14A H 0.868404 1.254336 0.573028 0.134 Uiso 1 1 calc R U . . .
 H14B H 0.904536 1.283039 0.523707 0.134 Uiso 1 1 calc R U . . .
 H14C H 0.861829 1.246939 0.513253 0.134 Uiso 1 1 calc R U . . .
 C70 C 0.5617(6) 0.7329(5) 0.7624(4) 0.095(3) Uani 1 1 d . . . . .
 H70 H 0.562993 0.733755 0.799102 0.113 Uiso 1 1 calc R U . . .
 C110 C 0.4907(5) -0.1131(5) 0.2598(4) 0.092(3) Uani 1 1 d . . . . .
 H110 H 0.458041 -0.077900 0.260656 0.110 Uiso 1 1 calc R U . . .
 C57 C 0.7728(5) 0.7194(5) 0.3726(4) 0.089(3) Uani 1 1 d . U . . .
 H57 H 0.787922 0.703668 0.335854 0.106 Uiso 1 1 calc R U . . .
 C183 C 0.7169(5) 1.2395(5) 0.2425(4) 0.092(3) Uani 1 1 d . . . . .
 H183 H 0.755116 1.219817 0.249675 0.110 Uiso 1 1 calc R U . . .
 C155 C 0.5249(5) 1.3940(5) 0.1272(4) 0.087(3) Uani 1 1 d . . . . .
 C132 C 0.7359(4) 1.4157(5) 0.5961(5) 0.088(3) Uani 1 1 d . . . . .
 F18 F 0.1762(4) 0.4092(5) 0.2845(4) 0.182(4) Uani 1 1 d . U . . .
 C181 C 0.6233(6) 1.3195(6) 0.2573(4) 0.095(3) Uani 1 1 d . . . . .
 H181 H 0.597179 1.356027 0.276119 0.114 Uiso 1 1 calc R U . . .
 C176 C 0.6322(5) 1.1462(5) 0.0890(4) 0.088(3) Uani 1 1 d . . . . .
 H176 H 0.653406 1.108649 0.070075 0.105 Uiso 1 1 calc R U . . .
 C193 C -0.0413(5) 0.5810(5) 0.7210(5) 0.105(4) Uani 1 1 d . . . . .
 H19A H -0.011250 0.586012 0.688098 0.157 Uiso 1 1 calc R U . . .
 H19B H -0.074732 0.618258 0.733077 0.157 Uiso 1 1 calc R U . . .
 H19C H -0.058408 0.550925 0.713234 0.157 Uiso 1 1 calc R U . . .
 C212 C 0.0945(6) -0.0424(5) 0.5061(5) 0.099(4) Uani 1 1 d . . . . .
 C152 C 0.5020(7) 1.4271(5) 0.2161(4) 0.102(4) Uani 1 1 d . . . . .
 C103 C 0.3745(4) -0.0854(5) 0.3441(4) 0.087(3) Uani 1 1 d . . . . .
 H103 H 0.385798 -0.053674 0.326846 0.105 Uiso 1 1 calc R U . . .
 C162 C 0.9658(6) 1.0383(6) 0.2012(5) 0.100(3) Uani 1 1 d . . . . .
 H162 H 0.984726 1.052693 0.223756 0.120 Uiso 1 1 calc R U . . .
 C192 C -0.0905(5) 0.5153(5) 0.8186(5) 0.095(3) Uani 1 1 d . . . . .
 H19D H -0.096864 0.505720 0.784067 0.143 Uiso 1 1 calc R U . . .
 H19E H -0.125595 0.548513 0.838454 0.143 Uiso 1 1 calc R U . . .
 H19F H -0.087162 0.481199 0.840481 0.143 Uiso 1 1 calc R U . . .
 C122 C 0.2466(5) 1.2374(5) 1.0612(4) 0.087(3) Uani 1 1 d . . . . .
 C102 C 0.3152(4) -0.0763(4) 0.3675(4) 0.079(3) Uani 1 1 d . . . . .
 H102 H 0.303207 -0.107043 0.386215 0.095 Uiso 1 1 calc R U . . .
 C98 C 0.2052(5) -0.0197(5) 0.3815(4) 0.092(3) Uani 1 1 d . . . . .
 H98 H 0.194715 -0.053499 0.394219 0.110 Uiso 1 1 calc R U . . .
 F3 F 0.7636(5) 1.2393(7) -0.0530(4) 0.218(5) Uani 1 1 d . U . . .
 C69 C 0.5997(5) 0.7563(5) 0.7236(4) 0.094(3) Uani 1 1 d . . . . .
 H69 H 0.625113 0.774634 0.734712 0.112 Uiso 1 1 calc R U . . .
 C34 C 0.5910(5) 1.1360(5) 0.2740(4) 0.088(3) Uani 1 1 d . . . . .
 H34 H 0.553039 1.153810 0.265787 0.105 Uiso 1 1 calc R U . . .
 C139 C 0.8010(5) 1.3441(5) 0.4524(4) 0.096(3) Uani 1 1 d . . . . .
 H13D H 0.805567 1.302343 0.448191 0.144 Uiso 1 1 calc R U . . .
 H13E H 0.840012 1.350482 0.433422 0.144 Uiso 1 1 calc R U . . .
 H13F H 0.768388 1.367135 0.436879 0.144 Uiso 1 1 calc R U . . .
 C177 C 0.5783(6) 1.1796(5) 0.0801(4) 0.093(3) Uani 1 1 d . . . . .
 H177 H 0.561824 1.165780 0.055009 0.111 Uiso 1 1 calc R U . . .
 C111 C 0.5448(5) -0.1244(5) 0.2188(4) 0.089(3) Uani 1 1 d . . . . .
 H111 H 0.548856 -0.098203 0.190941 0.107 Uiso 1 1 calc R U . . .
 C190 C 0.1043(6) 0.5493(5) 0.8410(5) 0.110(4) Uani 1 1 d . . . . .
 H19G H 0.109464 0.520321 0.868107 0.166 Uiso 1 1 calc R U . . .
 H19H H 0.094382 0.588591 0.858066 0.166 Uiso 1 1 calc R U . . .
 H19I H 0.142661 0.540446 0.811373 0.166 Uiso 1 1 calc R U . . .
 O9 O 0.7068(5) 1.2892(6) 0.0916(5) 0.173(4) Uani 1 1 d . U . . .
 C159 C 0.4197(5) 1.3808(5) 0.1278(5) 0.101(3) Uani 1 1 d . . . . .
 H15A H 0.442207 1.350459 0.097920 0.151 Uiso 1 1 calc R U . . .
 H15B H 0.398120 1.416861 0.113656 0.151 Uiso 1 1 calc R U . . .
 H15C H 0.389555 1.367328 0.154712 0.151 Uiso 1 1 calc R U . . .
 F2 F 0.6979(6) 1.3170(7) -0.0191(4) 0.214(5) Uani 1 1 d . U . . .
 C142 C 1.0937(6) 0.8063(6) 0.0912(6) 0.109(3) Uani 1 1 d . U . . .
 O8 O 0.8008(5) 1.2916(7) 0.0252(5) 0.187(5) Uani 1 1 d . U . . .
 C206 C 0.5161(6) 0.5692(7) 0.5313(5) 0.107(4) Uani 1 1 d . . . . .
 C138 C 0.7036(5) 1.4643(5) 0.5105(5) 0.102(4) Uani 1 1 d . . . . .
 H13G H 0.699780 1.445959 0.478419 0.152 Uiso 1 1 calc R U . . .
 H13H H 0.726186 1.492368 0.499171 0.152 Uiso 1 1 calc R U . . .
 H13I H 0.662464 1.484919 0.534447 0.152 Uiso 1 1 calc R U . . .
 C137 C 0.6980(5) 1.4625(5) 0.6416(4) 0.093(3) Uani 1 1 d . . . . .
 H13J H 0.656654 1.458897 0.655559 0.140 Uiso 1 1 calc R U . . .
 H13K H 0.694692 1.501263 0.627797 0.140 Uiso 1 1 calc R U . . .
 H13L H 0.717951 1.457597 0.670879 0.140 Uiso 1 1 calc R U . . .
 C144 C 1.0950(7) 0.8879(7) 0.0453(6) 0.119(4) Uani 1 1 d . U . . .
 C185 C 0.0531(6) 0.5469(5) 0.8188(5) 0.094(3) Uani 1 1 d . . . . .
 C151 C 0.5482(5) 1.4141(5) 0.1646(4) 0.093(3) Uani 1 1 d . . . . .
 C128 C 0.1917(5) 1.3470(5) 1.0526(5) 0.102(3) Uani 1 1 d . U . . .
 H12D H 0.206524 1.379423 1.038043 0.152 Uiso 1 1 calc R U . . .
 H12E H 0.163121 1.359347 1.089048 0.152 Uiso 1 1 calc R U . . .
 H12F H 0.170364 1.336093 1.028680 0.152 Uiso 1 1 calc R U . . .
 O28 O -0.1255(4) 0.0830(5) 0.6879(5) 0.179(5) Uani 1 1 d D U . . .
 C161 C 0.9931(6) 0.9855(6) 0.1746(5) 0.094(3) Uani 1 1 d . . . . .
 H161 H 1.031866 0.963057 0.179282 0.113 Uiso 1 1 calc R U . . .
 O15 O 0.3442(5) 0.4705(4) 0.7102(5) 0.206(5) Uani 1 1 d D U . . .
 O30 O -0.0234(4) 0.0769(5) 0.6395(3) 0.188(5) Uani 1 1 d D U . . .
 C195 C 0.0902(5) 0.1122(5) 0.2802(4) 0.087(3) Uani 1 1 d . . . . .
 C205 C 0.3037(5) 0.5484(5) 0.6459(3) 0.204(5) Uani 1 1 d D U . . .
 C131 C 0.7827(5) 1.3636(5) 0.6040(5) 0.085(3) Uani 1 1 d . . . . .
 F14 F 0.2808(7) 0.6087(4) 0.6468(5) 0.248(5) Uani 1 1 d D U . . .
 C143 C 1.1082(5) 0.8572(8) 0.0921(6) 0.117(4) Uani 1 1 d . U . . .
 C204 C 0.2336(7) 0.3865(7) 0.2521(6) 0.115(4) Uani 1 1 d . . . . .
 O29 O -0.0505(5) 0.0754(5) 0.7351(4) 0.171(4) Uani 1 1 d D U . . .
 C191 C 0.0014(7) 0.4898(5) 0.8934(5) 0.117(4) Uani 1 1 d . . . . .
 H19J H -0.024562 0.464862 0.894657 0.176 Uiso 1 1 calc R U . . .
 H19K H -0.017974 0.519814 0.923938 0.176 Uiso 1 1 calc R U . . .
 H19L H 0.042093 0.465774 0.895911 0.176 Uiso 1 1 calc R U . . .
 F1 F 0.6783(6) 1.2377(6) 0.0062(5) 0.208(5) Uani 1 1 d . U . . .
 C97 C 0.1602(5) 0.0314(5) 0.3781(5) 0.104(4) Uani 1 1 d . . . . .
 H97 H 0.118523 0.031838 0.389032 0.124 Uiso 1 1 calc R U . . .
 C199 C -0.0063(5) 0.0923(5) 0.3452(5) 0.092(3) Uani 1 1 d . . . . .
 H19M H 0.020669 0.054413 0.351795 0.138 Uiso 1 1 calc R U . . .
 H19N H -0.028734 0.085978 0.320079 0.138 Uiso 1 1 calc R U . . .
 H19O H -0.035894 0.111454 0.379649 0.138 Uiso 1 1 calc R U . . .
 C201 C 0.1645(6) 0.1632(6) 0.2216(5) 0.112(4) Uani 1 1 d . . . . .
 H20D H 0.177216 0.196298 0.229874 0.167 Uiso 1 1 calc R U . . .
 H20E H 0.154091 0.167960 0.187017 0.167 Uiso 1 1 calc R U . . .
 H20F H 0.198383 0.126529 0.218953 0.167 Uiso 1 1 calc R U . . .
 C210 C 0.0064(6) 0.4212(6) 0.4423(7) 0.111(4) Uani 1 1 d . . . . .
 C145 C 1.0755(7) 0.8536(9) 0.0193(5) 0.132(5) Uani 1 1 d . U . . .
 C203 C -0.0441(5) 0.2314(6) 0.3684(4) 0.103(4) Uani 1 1 d . . . . .
 H20G H -0.058874 0.209238 0.398630 0.154 Uiso 1 1 calc R U . . .
 H20H H -0.075796 0.246046 0.349327 0.154 Uiso 1 1 calc R U . . .
 H20I H -0.035615 0.264563 0.382625 0.154 Uiso 1 1 calc R U . . .
 C200 C 0.1272(7) 0.0500(6) 0.2547(4) 0.114(4) Uani 1 1 d . . . . .
 H20J H 0.170803 0.042295 0.252358 0.171 Uiso 1 1 calc R U . . .
 H20K H 0.122733 0.046256 0.218117 0.171 Uiso 1 1 calc R U . . .
 H20L H 0.111692 0.021676 0.277181 0.171 Uiso 1 1 calc R U . . .
 C127 C 0.1912(6) 1.2148(6) 1.0625(5) 0.110(4) Uani 1 1 d . . . . .
 H12G H 0.165496 1.239775 1.041546 0.166 Uiso 1 1 calc R U . . .
 H12H H 0.166469 1.216255 1.100164 0.166 Uiso 1 1 calc R U . . .
 H12I H 0.207029 1.174339 1.046427 0.166 Uiso 1 1 calc R U . . .
 C126 C 0.3244(6) 1.1397(5) 1.0787(5) 0.100(3) Uani 1 1 d . . . . .
 H12J H 0.291055 1.124180 1.077709 0.151 Uiso 1 1 calc R U . . .
 H12K H 0.361835 1.118557 1.050200 0.151 Uiso 1 1 calc R U . . .
 H12L H 0.332352 1.134379 1.114270 0.151 Uiso 1 1 calc R U . . .
 C160 C 0.5588(6) 1.3752(6) 0.0685(4) 0.113(4) Uani 1 1 d . . . . .
 H16A H 0.597861 1.344186 0.065989 0.169 Uiso 1 1 calc R U . . .
 H16B H 0.567275 1.408864 0.049759 0.169 Uiso 1 1 calc R U . . .
 H16C H 0.533566 1.360440 0.051447 0.169 Uiso 1 1 calc R U . . .
 C141 C 1.0713(5) 0.8053(7) 0.0447(7) 0.118(4) Uani 1 1 d . U . . .
 C136 C 0.7967(6) 1.3481(6) 0.6576(5) 0.108(4) Uani 1 1 d . . . . .
 H13M H 0.758383 1.350624 0.685650 0.162 Uiso 1 1 calc R U . . .
 H13N H 0.815324 1.375620 0.668217 0.162 Uiso 1 1 calc R U . . .
 H13O H 0.825489 1.308097 0.653730 0.162 Uiso 1 1 calc R U . . .
 F20 F -0.0391(5) 0.1858(7) 0.6945(5) 0.265(7) Uani 1 1 d D U . . .
 C158 C 0.3883(6) 1.4282(6) 0.2524(5) 0.118(4) Uani 1 1 d . U . . .
 H15D H 0.359388 1.416920 0.237312 0.176 Uiso 1 1 calc R U . . .
 H15E H 0.394554 1.405321 0.283493 0.176 Uiso 1 1 calc R U . . .
 H15F H 0.371439 1.470094 0.264272 0.176 Uiso 1 1 calc R U . . .
 F21 F -0.1378(5) 0.1926(6) 0.7408(3) 0.253(6) Uani 1 1 d D U . . .
 C157 C 0.5037(8) 1.4580(6) 0.2670(5) 0.125(4) Uani 1 1 d . U . . .
 H15G H 0.482144 1.442853 0.299418 0.188 Uiso 1 1 calc R U . . .
 H15H H 0.483416 1.500292 0.267325 0.188 Uiso 1 1 calc R U . . .
 H15I H 0.546689 1.450635 0.266863 0.188 Uiso 1 1 calc R U . . .
 O14 O 0.3264(6) 0.5698(5) 0.7371(5) 0.210(5) Uani 1 1 d D U . . .
 C156 C 0.6118(6) 1.4225(6) 0.1534(6) 0.115(4) Uani 1 1 d . . . . .
 H15J H 0.621831 1.424688 0.187802 0.172 Uiso 1 1 calc R U . . .
 H15K H 0.611141 1.458967 0.135491 0.172 Uiso 1 1 calc R U . . .
 H15L H 0.643128 1.389311 0.129714 0.172 Uiso 1 1 calc R U . . .
 C209 C 0.7255(10) 1.2599(11) -0.0054(8) 0.161(5) Uani 1 1 d . U . . .
 C148 C 1.1372(6) 0.8743(8) 0.1334(7) 0.153(5) Uani 1 1 d . U . . .
 H14D H 1.129496 0.916749 0.134766 0.229 Uiso 1 1 calc R U . . .
 H14E H 1.181711 0.853876 0.122343 0.229 Uiso 1 1 calc R U . . .
 H14F H 1.118770 0.863107 0.169393 0.229 Uiso 1 1 calc R U . . .
 C147 C 1.1016(8) 0.7592(8) 0.1305(8) 0.180(8) Uani 1 1 d . U . . .
 H14G H 1.099996 0.776477 0.165451 0.271 Uiso 1 1 calc R U . . .
 H14H H 1.141614 0.728823 0.115954 0.271 Uiso 1 1 calc R U . . .
 H14I H 1.068509 0.741819 0.135629 0.271 Uiso 1 1 calc R U . . .
 F15 F 0.2670(7) 0.5210(6) 0.6307(5) 0.295(7) Uani 1 1 d D U . . .
 C146 C 1.0579(7) 0.7567(8) 0.0193(8) 0.169(6) Uani 1 1 d . U . . .
 H14J H 1.046479 0.730662 0.047124 0.253 Uiso 1 1 calc R U . . .
 H14K H 1.094673 0.734229 -0.009217 0.253 Uiso 1 1 calc R U . . .
 H14L H 1.023747 0.773488 0.003297 0.253 Uiso 1 1 calc R U . . .
 C149 C 1.1079(9) 0.9419(8) 0.0297(8) 0.176(6) Uani 1 1 d . U . . .
 H14M H 1.073927 0.967818 0.017281 0.264 Uiso 1 1 calc R U . . .
 H14N H 1.146359 0.932997 0.000230 0.264 Uiso 1 1 calc R U . . .
 H14O H 1.111963 0.961478 0.061053 0.264 Uiso 1 1 calc R U . . .
 F13 F 0.3637(5) 0.5276(7) 0.6137(4) 0.316(8) Uani 1 1 d D U . . .
 C150 C 1.0632(9) 0.8748(10) -0.0367(7) 0.183(6) Uani 1 1 d . U . . .
 H15M H 1.027808 0.864629 -0.041152 0.274 Uiso 1 1 calc R U . . .
 H15N H 1.099768 0.855343 -0.066703 0.274 Uiso 1 1 calc R U . . .
 H15O H 1.054380 0.917357 -0.036843 0.274 Uiso 1 1 calc R U . . .
 O7 O 0.7833(5) 1.2024(6) 0.0519(5) 0.172(5) Uani 1 1 d . U . . .
 O13 O 0.2415(4) 0.5345(6) 0.7435(5) 0.248(7) Uani 1 1 d D U . . .


_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 Rh3 N10 2.082(8) . ?
 Rh3 N11 2.112(8) . ?
 Rh3 N12 2.140(7) . ?
 Rh3 C134 2.158(9) . ?
 Rh3 C135 2.140(9) . ?
 Rh3 C133 2.153(10) . ?
 Rh3 C132 2.125(10) . ?
 Rh3 C131 2.173(11) . ?
 Rh4 N16 2.122(8) . ?
 Rh4 N15 2.127(7) . ?
 Rh4 N9 2.123(8) 2_676 ?
 Rh4 C124 2.135(10) . ?
 Rh4 C125 2.167(10) . ?
 Rh4 C123 2.171(9) . ?
 Rh4 C121 2.179(9) . ?
 Rh4 C122 2.171(10) . ?
 Rh5 N17 2.101(8) . ?
 Rh5 N18 2.120(7) . ?
 Rh5 N24 2.125(8) 2_656 ?
 Rh5 C188 2.140(11) . ?
 Rh5 C187 2.145(10) . ?
 Rh5 C184 2.174(11) . ?
 Rh5 C186 2.140(9) . ?
 Rh5 C185 2.143(11) . ?
 Rh6 N21 2.117(8) . ?
 Rh6 N22 2.083(8) . ?
 Rh6 N23 2.116(8) . ?
 Rh6 C194 2.175(10) . ?
 Rh6 C197 2.142(10) . ?
 Rh6 C196 2.155(8) . ?
 Rh6 C198 2.165(10) . ?
 Rh6 C195 2.176(10) . ?
 Rh1 N6 2.121(8) . ?
 Rh1 N8 2.139(8) 2_676 ?
 Rh1 N5 2.119(9) . ?
 Rh1 C154 2.122(12) . ?
 Rh1 C153 2.149(11) . ?
 Rh1 C155 2.165(10) . ?
 Rh1 C152 2.136(11) . ?
 Rh1 C151 2.159(10) . ?
 Rh2 N7 2.148(7) . ?
 Rh2 N1 2.152(9) . ?
 Rh2 N2 2.137(10) . ?
 Rh2 C142 2.130(13) . ?
 Rh2 C144 2.155(12) . ?
 Rh2 C143 2.152(12) . ?
 Rh2 C145 2.132(12) . ?
 Rh2 C141 2.102(13) . ?
 S2 O5 1.431(8) . ?
 S2 O6 1.437(7) . ?
 S2 O4 1.438(7) . ?
 S2 C207 1.803(10) . ?
 S7 O25 1.423(7) . ?
 S7 O26 1.427(8) . ?
 S7 O27 1.474(9) . ?
 S7 C212 1.798(12) . ?
 S5 O12 1.424(7) . ?
 S5 O11 1.419(8) . ?
 S5 O10 1.439(9) . ?
 S5 C206 1.771(13) . ?
 S4 O18 1.423(8) . ?
 S4 O17 1.425(8) . ?
 S4 O16 1.405(9) . ?
 S4 C204 1.724(15) . ?
 S1 O21 1.424(8) . ?
 S1 O19 1.428(8) . ?
 S1 O20 1.418(8) . ?
 S1 C210 1.800(13) . ?
 S3 O9 1.417(11) . ?
 S3 O8 1.418(12) . ?
 S3 C209 1.73(2) . ?
 S3 O7 1.370(13) . ?
 S6 O15 1.446(7) . ?
 S6 C205 1.808(7) . ?
 S6 O14 1.452(7) . ?
 S6 O13 1.408(7) . ?
 C211 S8 1.706(7) . ?
 C211 F19 1.410(7) . ?
 C211 F20 1.309(8) . ?
 C211 F21 1.419(7) . ?
 S8 O28 1.437(7) . ?
 S8 O30 1.426(7) . ?
 S8 O29 1.438(7) . ?
 F7 C207 1.310(12) . ?
 N16 C1 1.389(11) . ?
 N16 C5 1.346(10) . ?
 N17 C91 1.316(11) . ?
 N17 C92 1.359(11) . ?
 N15 C6 1.361(11) . ?
 N15 C7 1.318(12) . ?
 N10 C25 1.335(11) . ?
 N10 C29 1.383(13) . ?
 F9 C207 1.319(12) . ?
 N11 C19 1.372(10) . ?
 N11 C20 1.383(12) . ?
 N7 C53 1.346(12) . ?
 N7 C49 1.326(11) . ?
 N19 C83 1.342(10) . ?
 N19 C96 1.314(11) . ?
 N18 C89 1.328(11) . ?
 N18 C90 1.376(11) . ?
 N21 C79 1.358(11) . ?
 N21 C78 1.320(12) . ?
 F8 C207 1.374(12) . ?
 N14 C13 1.327(10) . ?
 N14 C12 1.342(11) . ?
 F26 C212 1.338(14) . ?
 N22 C77 1.346(13) . ?
 N22 C73 1.344(11) . ?
 F30 C210 1.306(15) . ?
 F17 C204 1.360(16) . ?
 N9 C47 1.366(11) . ?
 N9 C46 1.275(11) . ?
 N1 C166 1.357(12) . ?
 N1 C170 1.297(12) . ?
 N6 C179 1.337(13) . ?
 N6 C178 1.326(12) . ?
 N24 C119 1.372(12) . ?
 N24 C118 1.306(11) . ?
 N23 C101 1.316(11) . ?
 N23 C97 1.323(13) . ?
 F11 C206 1.344(15) . ?
 N12 C18 1.323(11) . ?
 N12 C17 1.359(12) . ?
 N13 C24 1.319(12) . ?
 N13 C11 1.350(10) . ?
 N3 C171 1.344(12) . ?
 N3 C174 1.344(13) . ?
 N8 C71 1.318(11) . ?
 N8 C70 1.362(13) . ?
 N4 C173 1.369(12) . ?
 N4 C172 1.348(12) . ?
 N20 C85 1.330(11) . ?
 N20 C84 1.321(12) . ?
 C83 C84 1.415(12) . ?
 C83 C82 1.433(13) . ?
 F27 C212 1.336(11) . ?
 F28 C210 1.360(14) . ?
 F12 C206 1.327(14) . ?
 N2 C165 1.319(12) . ?
 N2 C161 1.313(14) . ?
 F25 C212 1.310(14) . ?
 C85 C96 1.426(12) . ?
 C85 C86 1.442(13) . ?
 C91 C95 1.369(13) . ?
 C91 C90 1.458(12) . ?
 C96 C95 1.480(12) . ?
 C18 C14 1.404(12) . ?
 C18 C19 1.474(12) . ?
 C71 H71 0.9500 . ?
 C71 C72 1.342(13) . ?
 C1 H1 0.9500 . ?
 C1 C2 1.352(13) . ?
 C116 C120 1.385(12) . ?
 C116 C117 1.419(13) . ?
 C116 C115 1.440(13) . ?
 N5 C180 1.359(12) . ?
 N5 C181 1.345(13) . ?
 C13 C14 1.429(13) . ?
 C13 C24 1.434(12) . ?
 C14 C15 1.429(12) . ?
 C173 C048 1.474(13) . ?
 C173 C174 1.417(14) . ?
 C84 C76 1.476(13) . ?
 C166 C167 1.428(13) . ?
 C166 C165 1.429(13) . ?
 C188 C187 1.418(15) . ?
 C188 C184 1.455(16) . ?
 C188 C193 1.470(16) . ?
 C12 C4 1.432(11) . ?
 C12 C11 1.427(12) . ?
 C119 H119 0.9500 . ?
 C119 C120 1.374(13) . ?
 C56 C55 1.448(12) . ?
 C56 C61 1.412(12) . ?
 C56 C57 1.401(14) . ?
 C108 C109 1.426(13) . ?
 C108 C113 1.428(12) . ?
 C108 C107 1.408(14) . ?
 C66 H66 0.9500 . ?
 C66 C65 1.498(13) . ?
 C66 C67 1.310(12) . ?
 C109 C104 1.462(12) . ?
 C109 C110 1.392(14) . ?
 C167 C171 1.438(13) . ?
 C167 C168 1.377(13) . ?
 C24 C23 1.444(12) . ?
 C171 C172 1.412(13) . ?
 C95 C94 1.411(13) . ?
 C86 C87 1.460(12) . ?
 C86 C90 1.384(12) . ?
 C10 C6 1.404(12) . ?
 C10 C9 1.401(13) . ?
 C10 C11 1.471(13) . ?
 C63 H63 0.9500 . ?
 C63 C64 1.402(14) . ?
 C63 C62 1.345(13) . ?
 C19 C23 1.357(12) . ?
 F29 C210 1.355(16) . ?
 C93 H93 0.9500 . ?
 C93 C94 1.336(13) . ?
 C93 C92 1.370(14) . ?
 C65 C64 1.325(14) . ?
 C65 C60 1.441(13) . ?
 C172 C164 1.458(14) . ?
 C89 H89 0.9500 . ?
 C89 C88 1.370(13) . ?
 C6 C5 1.427(12) . ?
 C165 C164 1.401(13) . ?
 C77 C76 1.391(14) . ?
 C77 C78 1.461(13) . ?
 C124 C125 1.427(14) . ?
 C124 C123 1.455(15) . ?
 C124 C129 1.500(15) . ?
 C47 H47 0.9500 . ?
 C47 C48 1.348(13) . ?
 C179 C175 1.387(14) . ?
 C179 C180 1.486(14) . ?
 C125 C121 1.444(15) . ?
 C125 C130 1.467(14) . ?
 C37 C36 1.418(13) . ?
 C37 C32 1.451(13) . ?
 C37 C38 1.421(14) . ?
 C36 C41 1.438(12) . ?
 C36 C35 1.396(13) . ?
 C9 H9 0.9500 . ?
 C9 C8 1.317(12) . ?
 C134 C135 1.423(15) . ?
 C134 C133 1.440(13) . ?
 C134 C139 1.517(14) . ?
 C164 C163 1.402(13) . ?
 C175 C174 1.406(15) . ?
 C175 C176 1.366(14) . ?
 C5 C4 1.405(12) . ?
 C17 H17 0.9500 . ?
 C17 C16 1.380(12) . ?
 C154 C153 1.416(14) . ?
 C154 C155 1.423(14) . ?
 C154 C159 1.510(16) . ?
 C168 H168 0.9500 . ?
 C168 C169 1.374(14) . ?
 C4 C3 1.405(12) . ?
 C55 H55 0.9500 . ?
 C55 C54 1.374(13) . ?
 C169 H169 0.9500 . ?
 C169 C170 1.385(14) . ?
 C48 H48 0.9500 . ?
 C48 C44 1.402(13) . ?
 C82 C78 1.428(12) . ?
 C82 C81 1.415(12) . ?
 C94 H94 0.9500 . ?
 C67 H67 0.9500 . ?
 C67 C68 1.444(13) . ?
 C113 C114 1.477(13) . ?
 C113 C112 1.420(14) . ?
 C87 H87 0.9500 . ?
 C87 C88 1.322(13) . ?
 C76 C75 1.403(12) . ?
 C30 H30 0.9500 . ?
 C30 C27 1.477(14) . ?
 C30 C31 1.343(14) . ?
 C43 H43 0.9500 . ?
 C43 C44 1.468(12) . ?
 C43 C42 1.354(12) . ?
 C79 H79 0.9500 . ?
 C79 C80 1.352(13) . ?
 C23 C22 1.423(13) . ?
 C187 C186 1.450(16) . ?
 C187 C192 1.487(15) . ?
 C120 H120 0.9500 . ?
 C123 C122 1.379(15) . ?
 C123 C128 1.515(14) . ?
 C41 C40 1.352(13) . ?
 C41 C42 1.505(13) . ?
 C51 C52 1.386(13) . ?
 C51 C54 1.480(13) . ?
 C51 C50 1.376(13) . ?
 C45 H45 0.9500 . ?
 C45 C44 1.376(12) . ?
 C45 C46 1.406(13) . ?
 C27 C28 1.370(13) . ?
 C27 C26 1.388(13) . ?
 C25 H25 0.9500 . ?
 C25 C26 1.377(13) . ?
 F16 C204 1.350(16) . ?
 C61 C62 1.414(14) . ?
 C61 C60 1.463(13) . ?
 C7 H7 0.9500 . ?
 C7 C8 1.410(12) . ?
 C32 C31 1.432(14) . ?
 C32 C33 1.425(14) . ?
 C202 H20A 0.9800 . ?
 C202 H20B 0.9800 . ?
 C202 H20C 0.9800 . ?
 C202 C197 1.469(14) . ?
 C64 H64 0.9500 . ?
 C048 C180 1.359(14) . ?
 C048 C183 1.408(14) . ?
 C72 H72 0.9500 . ?
 C72 C68 1.429(14) . ?
 C104 C105 1.326(14) . ?
 C104 C103 1.432(14) . ?
 C8 H8 0.9500 . ?
 C101 H101 0.9500 . ?
 C101 C100 1.368(13) . ?
 C117 H117 0.9500 . ?
 C117 C118 1.362(14) . ?
 C194 C198 1.421(14) . ?
 C194 C195 1.434(13) . ?
 C194 C199 1.495(14) . ?
 C52 H52 0.9500 . ?
 C52 C53 1.392(13) . ?
 C28 H28 0.9500 . ?
 C28 C29 1.354(14) . ?
 C54 H54 0.9500 . ?
 C15 H15 0.9500 . ?
 C15 C16 1.347(13) . ?
 C88 H88 0.9500 . ?
 C135 C140 1.544(13) . ?
 C135 C131 1.457(13) . ?
 C153 C152 1.394(16) . ?
 C153 C158 1.538(15) . ?
 C31 H31 0.9500 . ?
 C33 H33 0.9500 . ?
 C33 C34 1.353(14) . ?
 C92 H92 0.9500 . ?
 C133 C132 1.373(15) . ?
 C133 C138 1.563(16) . ?
 C22 H22 0.9500 . ?
 C22 C21 1.346(12) . ?
 C29 H29 0.9500 . ?
 C46 H46 0.9500 . ?
 C53 H53 0.9500 . ?
 C35 H35 0.9500 . ?
 C35 C34 1.395(13) . ?
 C170 H170 0.9500 . ?
 F10 C206 1.308(14) . ?
 C68 C69 1.369(13) . ?
 C58 H58 0.9500 . ?
 C58 C59 1.395(14) . ?
 C58 C57 1.398(14) . ?
 C16 H16 0.9500 . ?
 C74 H74 0.9500 . ?
 C74 C75 1.389(13) . ?
 C74 C73 1.419(15) . ?
 C115 H115 0.9500 . ?
 C115 C114 1.346(13) . ?
 C178 H178 0.9500 . ?
 C178 C177 1.404(14) . ?
 C184 C189 1.523(15) . ?
 C184 C185 1.365(15) . ?
 C38 H38 0.9500 . ?
 C38 C39 1.353(13) . ?
 C197 C196 1.488(13) . ?
 C197 C198 1.428(14) . ?
 C100 H100 0.9500 . ?
 C100 C99 1.385(14) . ?
 C62 H62 0.9500 . ?
 C81 H81 0.9500 . ?
 C81 C80 1.385(13) . ?
 C20 H20 0.9500 . ?
 C20 C21 1.362(14) . ?
 C60 C59 1.403(14) . ?
 C186 C185 1.441(15) . ?
 C186 C191 1.460(16) . ?
 C49 H49 0.9500 . ?
 C49 C50 1.407(12) . ?
 C40 H40 0.9500 . ?
 C40 C39 1.374(13) . ?
 C26 H26 0.9500 . ?
 C75 H75 0.9500 . ?
 C80 H80 0.9500 . ?
 C163 H163 0.9500 . ?
 C163 C162 1.415(16) . ?
 C107 H107 0.9500 . ?
 C107 C106 1.359(13) . ?
 C114 H114 0.9500 . ?
 C42 H42 0.9500 . ?
 C189 H18A 0.9800 . ?
 C189 H18B 0.9800 . ?
 C189 H18C 0.9800 . ?
 C118 H118 0.9500 . ?
 C196 C195 1.421(15) . ?
 C196 C201 1.466(13) . ?
 C198 C203 1.492(13) . ?
 C2 H2 0.9500 . ?
 C2 C3 1.379(12) . ?
 C121 C122 1.474(15) . ?
 C121 C126 1.469(15) . ?
 C21 H21 0.9500 . ?
 C106 H106 0.9500 . ?
 C106 C105 1.413(14) . ?
 C3 H3 0.9500 . ?
 C129 H12A 0.9800 . ?
 C129 H12B 0.9800 . ?
 C129 H12C 0.9800 . ?
 C99 C102 1.471(14) . ?
 C99 C98 1.402(14) . ?
 C182 H182 0.9500 . ?
 C182 C183 1.347(15) . ?
 C182 C181 1.431(17) . ?
 C59 H59 0.9500 . ?
 C73 H73 0.9500 . ?
 C105 H105 0.9500 . ?
 C130 H13A 0.9800 . ?
 C130 H13B 0.9800 . ?
 C130 H13C 0.9800 . ?
 C112 H112 0.9500 . ?
 C112 C111 1.390(14) . ?
 C39 H39 0.9500 . ?
 C50 H50 0.9500 . ?
 C140 H14A 0.9800 . ?
 C140 H14B 0.9800 . ?
 C140 H14C 0.9800 . ?
 C70 H70 0.9500 . ?
 C70 C69 1.390(14) . ?
 C110 H110 0.9500 . ?
 C110 C111 1.375(13) . ?
 C57 H57 0.9500 . ?
 C183 H183 0.9500 . ?
 C155 C151 1.393(15) . ?
 C155 C160 1.501(14) . ?
 C132 C137 1.507(13) . ?
 C132 C131 1.449(16) . ?
 F18 C204 1.334(15) . ?
 C181 H181 0.9500 . ?
 C176 H176 0.9500 . ?
 C176 C177 1.361(15) . ?
 C193 H19A 0.9800 . ?
 C193 H19B 0.9800 . ?
 C193 H19C 0.9800 . ?
 C152 C151 1.434(14) . ?
 C152 C157 1.528(15) . ?
 C103 H103 0.9500 . ?
 C103 C102 1.321(13) . ?
 C162 H162 0.9500 . ?
 C162 C161 1.332(16) . ?
 C192 H19D 0.9800 . ?
 C192 H19E 0.9800 . ?
 C192 H19F 0.9800 . ?
 C122 C127 1.565(16) . ?
 C102 H102 0.9500 . ?
 C98 H98 0.9500 . ?
 C98 C97 1.377(14) . ?
 F3 C209 1.302(19) . ?
 C69 H69 0.9500 . ?
 C34 H34 0.9500 . ?
 C139 H13D 0.9800 . ?
 C139 H13E 0.9800 . ?
 C139 H13F 0.9800 . ?
 C177 H177 0.9500 . ?
 C111 H111 0.9500 . ?
 C190 H19G 0.9800 . ?
 C190 H19H 0.9800 . ?
 C190 H19I 0.9800 . ?
 C190 C185 1.495(17) . ?
 C159 H15A 0.9800 . ?
 C159 H15B 0.9800 . ?
 C159 H15C 0.9800 . ?
 F2 C209 1.41(2) . ?
 C142 C143 1.374(19) . ?
 C142 C141 1.43(2) . ?
 C142 C147 1.504(19) . ?
 C138 H13G 0.9800 . ?
 C138 H13H 0.9800 . ?
 C138 H13I 0.9800 . ?
 C137 H13J 0.9800 . ?
 C137 H13K 0.9800 . ?
 C137 H13L 0.9800 . ?
 C144 C143 1.45(2) . ?
 C144 C145 1.33(2) . ?
 C144 C149 1.45(2) . ?
 C151 C156 1.537(16) . ?
 C128 H12D 0.9800 . ?
 C128 H12E 0.9800 . ?
 C128 H12F 0.9800 . ?
 C161 H161 0.9500 . ?
 C195 C200 1.528(15) . ?
 C205 F14 1.380(8) . ?
 C205 F15 1.379(8) . ?
 C205 F13 1.377(8) . ?
 C131 C136 1.515(16) . ?
 C143 C148 1.534(19) . ?
 C191 H19J 0.9800 . ?
 C191 H19K 0.9800 . ?
 C191 H19L 0.9800 . ?
 F1 C209 1.35(2) . ?
 C97 H97 0.9500 . ?
 C199 H19M 0.9800 . ?
 C199 H19N 0.9800 . ?
 C199 H19O 0.9800 . ?
 C201 H20D 0.9800 . ?
 C201 H20E 0.9800 . ?
 C201 H20F 0.9800 . ?
 C145 C141 1.34(2) . ?
 C145 C150 1.59(2) . ?
 C203 H20G 0.9800 . ?
 C203 H20H 0.9800 . ?
 C203 H20I 0.9800 . ?
 C200 H20J 0.9800 . ?
 C200 H20K 0.9800 . ?
 C200 H20L 0.9800 . ?
 C127 H12G 0.9800 . ?
 C127 H12H 0.9800 . ?
 C127 H12I 0.9800 . ?
 C126 H12J 0.9800 . ?
 C126 H12K 0.9800 . ?
 C126 H12L 0.9800 . ?
 C160 H16A 0.9800 . ?
 C160 H16B 0.9800 . ?
 C160 H16C 0.9800 . ?
 C141 C146 1.51(2) . ?
 C136 H13M 0.9800 . ?
 C136 H13N 0.9800 . ?
 C136 H13O 0.9800 . ?
 C158 H15D 0.9800 . ?
 C158 H15E 0.9800 . ?
 C158 H15F 0.9800 . ?
 C157 H15G 0.9800 . ?
 C157 H15H 0.9800 . ?
 C157 H15I 0.9800 . ?
 C156 H15J 0.9800 . ?
 C156 H15K 0.9800 . ?
 C156 H15L 0.9800 . ?
 C148 H14D 0.9800 . ?
 C148 H14E 0.9800 . ?
 C148 H14F 0.9800 . ?
 C147 H14G 0.9800 . ?
 C147 H14H 0.9800 . ?
 C147 H14I 0.9800 . ?
 C146 H14J 0.9800 . ?
 C146 H14K 0.9800 . ?
 C146 H14L 0.9800 . ?
 C149 H14M 0.9800 . ?
 C149 H14N 0.9800 . ?
 C149 H14O 0.9800 . ?
 C150 H15M 0.9800 . ?
 C150 H15N 0.9800 . ?
 C150 H15O 0.9800 . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 N10 Rh3 N11 90.0(3) . . ?
 N10 Rh3 N12 86.6(3) . . ?
 N10 Rh3 C134 93.0(3) . . ?
 N10 Rh3 C135 112.4(3) . . ?
 N10 Rh3 C133 111.4(4) . . ?
 N10 Rh3 C132 148.1(4) . . ?
 N10 Rh3 C131 151.7(3) . . ?
 N11 Rh3 N12 77.3(3) . . ?
 N11 Rh3 C134 139.9(4) . . ?
 N11 Rh3 C135 104.3(4) . . ?
 N11 Rh3 C133 158.1(4) . . ?
 N11 Rh3 C132 121.8(4) . . ?
 N11 Rh3 C131 95.4(4) . . ?
 N12 Rh3 C134 142.8(4) . . ?
 N12 Rh3 C133 107.4(3) . . ?
 N12 Rh3 C131 121.6(3) . . ?
 C134 Rh3 C131 65.5(4) . . ?
 C135 Rh3 N12 160.8(3) . . ?
 C135 Rh3 C134 38.7(4) . . ?
 C135 Rh3 C133 64.2(4) . . ?
 C135 Rh3 C131 39.5(4) . . ?
 C133 Rh3 C134 39.0(3) . . ?
 C133 Rh3 C131 63.7(4) . . ?
 C132 Rh3 N12 96.6(3) . . ?
 C132 Rh3 C134 65.6(4) . . ?
 C132 Rh3 C135 66.0(3) . . ?
 C132 Rh3 C133 37.4(4) . . ?
 C132 Rh3 C131 39.4(4) . . ?
 N16 Rh4 N15 77.3(3) . . ?
 N16 Rh4 N9 87.8(3) . 2_676 ?
 N16 Rh4 C124 99.4(4) . . ?
 N16 Rh4 C125 129.6(4) . . ?
 N16 Rh4 C123 101.7(3) . . ?
 N16 Rh4 C121 164.0(3) . . ?
 N16 Rh4 C122 132.3(4) . . ?
 N15 Rh4 C124 115.9(4) . . ?
 N15 Rh4 C125 96.2(3) . . ?
 N15 Rh4 C123 155.3(4) . . ?
 N15 Rh4 C121 111.7(3) . . ?
 N15 Rh4 C122 150.4(4) . . ?
 N9 Rh4 N15 87.1(3) 2_676 . ?
 N9 Rh4 C124 156.8(4) 2_676 . ?
 N9 Rh4 C125 142.4(4) 2_676 . ?
 N9 Rh4 C123 117.6(3) 2_676 . ?
 N9 Rh4 C121 105.5(4) 2_676 . ?
 N9 Rh4 C122 94.2(3) 2_676 . ?
 C124 Rh4 C125 38.7(4) . . ?
 C124 Rh4 C123 39.5(4) . . ?
 C124 Rh4 C121 64.9(4) . . ?
 C124 Rh4 C122 64.7(4) . . ?
 C125 Rh4 C123 65.1(4) . . ?
 C125 Rh4 C121 38.8(4) . . ?
 C125 Rh4 C122 65.4(4) . . ?
 C123 Rh4 C121 64.4(4) . . ?
 C123 Rh4 C122 37.1(4) . . ?
 C122 Rh4 C121 39.6(4) . . ?
 N17 Rh5 N18 77.4(3) . . ?
 N17 Rh5 N24 86.0(3) . 2_656 ?
 N17 Rh5 C188 114.2(4) . . ?
 N17 Rh5 C187 95.8(4) . . ?
 N17 Rh5 C184 153.4(4) . . ?
 N17 Rh5 C186 111.8(3) . . ?
 N17 Rh5 C185 150.8(4) . . ?
 N18 Rh5 N24 86.1(3) . 2_656 ?
 N18 Rh5 C188 99.6(3) . . ?
 N18 Rh5 C187 130.6(4) . . ?
 N18 Rh5 C184 101.3(3) . . ?
 N18 Rh5 C186 165.2(4) . . ?
 N18 Rh5 C185 131.7(4) . . ?
 N24 Rh5 C188 159.8(4) 2_656 . ?
 N24 Rh5 C187 142.8(4) 2_656 . ?
 N24 Rh5 C184 120.5(4) 2_656 . ?
 N24 Rh5 C186 105.6(4) 2_656 . ?
 N24 Rh5 C185 97.4(4) 2_656 . ?
 C188 Rh5 C187 38.7(4) . . ?
 C188 Rh5 C184 39.4(4) . . ?
 C188 Rh5 C186 66.4(4) . . ?
 C188 Rh5 C185 64.3(5) . . ?
 C187 Rh5 C184 64.5(4) . . ?
 C186 Rh5 C187 39.5(4) . . ?
 C186 Rh5 C184 65.2(4) . . ?
 C186 Rh5 C185 39.3(4) . . ?
 C185 Rh5 C187 64.3(4) . . ?
 C185 Rh5 C184 36.9(4) . . ?
 N21 Rh6 C194 105.4(3) . . ?
 N21 Rh6 C197 123.5(3) . . ?
 N21 Rh6 C196 163.2(3) . . ?
 N21 Rh6 C198 98.1(3) . . ?
 N21 Rh6 C195 140.2(4) . . ?
 N22 Rh6 N21 77.0(3) . . ?
 N22 Rh6 N23 89.4(3) . . ?
 N22 Rh6 C194 157.3(3) . . ?
 N22 Rh6 C197 94.3(4) . . ?
 N22 Rh6 C196 105.9(4) . . ?
 N22 Rh6 C198 119.3(4) . . ?
 N22 Rh6 C195 142.6(4) . . ?
 N23 Rh6 N21 88.5(3) . . ?
 N23 Rh6 C194 113.1(4) . . ?
 N23 Rh6 C197 147.8(3) . . ?
 N23 Rh6 C196 107.9(3) . . ?
 N23 Rh6 C198 151.3(4) . . ?
 N23 Rh6 C195 93.3(4) . . ?
 C194 Rh6 C195 38.5(4) . . ?
 C197 Rh6 C194 65.1(4) . . ?
 C197 Rh6 C196 40.5(4) . . ?
 C197 Rh6 C198 38.7(4) . . ?
 C197 Rh6 C195 65.1(4) . . ?
 C196 Rh6 C194 65.4(4) . . ?
 C196 Rh6 C198 65.8(4) . . ?
 C196 Rh6 C195 38.3(4) . . ?
 C198 Rh6 C194 38.2(4) . . ?
 C198 Rh6 C195 64.0(4) . . ?
 N6 Rh1 N8 87.1(3) . 2_676 ?
 N6 Rh1 C154 107.9(4) . . ?
 N6 Rh1 C153 144.2(4) . . ?
 N6 Rh1 C155 98.3(4) . . ?
 N6 Rh1 C152 160.3(4) . . ?
 N6 Rh1 C151 121.4(4) . . ?
 N8 Rh1 C153 93.3(4) 2_676 . ?
 N8 Rh1 C155 147.3(4) 2_676 . ?
 N8 Rh1 C151 151.6(4) 2_676 . ?
 N5 Rh1 N6 77.0(3) . . ?
 N5 Rh1 N8 88.7(3) . 2_676 ?
 N5 Rh1 C154 161.8(4) . . ?
 N5 Rh1 C153 138.7(4) . . ?
 N5 Rh1 C155 124.0(4) . . ?
 N5 Rh1 C152 104.3(4) . . ?
 N5 Rh1 C151 97.8(4) . . ?
 C154 Rh1 N8 108.9(4) . 2_676 ?
 C154 Rh1 C153 38.7(4) . . ?
 C154 Rh1 C155 38.7(4) . . ?
 C154 Rh1 C152 65.0(5) . . ?
 C154 Rh1 C151 64.4(4) . . ?
 C153 Rh1 C155 63.9(4) . . ?
 C153 Rh1 C151 63.8(4) . . ?
 C152 Rh1 N8 112.6(4) . 2_676 ?
 C152 Rh1 C153 38.0(5) . . ?
 C152 Rh1 C155 64.3(4) . . ?
 C152 Rh1 C151 39.0(4) . . ?
 C151 Rh1 C155 37.6(4) . . ?
 N7 Rh2 N1 85.6(3) . . ?
 N7 Rh2 C144 155.5(5) . . ?
 N7 Rh2 C143 116.2(5) . . ?
 N1 Rh2 C144 118.8(5) . . ?
 N2 Rh2 N7 86.6(3) . . ?
 N2 Rh2 N1 77.4(3) . . ?
 N2 Rh2 C144 101.0(5) . . ?
 N2 Rh2 C143 103.7(5) . . ?
 C142 Rh2 N7 93.9(4) . . ?
 C142 Rh2 N1 147.5(5) . . ?
 C142 Rh2 N2 135.1(5) . . ?
 C142 Rh2 C144 64.2(5) . . ?
 C142 Rh2 C143 37.4(5) . . ?
 C142 Rh2 C145 62.9(6) . . ?
 C143 Rh2 N1 158.2(5) . . ?
 C143 Rh2 C144 39.5(6) . . ?
 C145 Rh2 N7 143.9(6) . . ?
 C145 Rh2 N1 99.8(5) . . ?
 C145 Rh2 N2 129.5(6) . . ?
 C145 Rh2 C144 36.1(6) . . ?
 C145 Rh2 C143 62.4(6) . . ?
 C141 Rh2 N7 107.7(5) . . ?
 C141 Rh2 N1 109.9(5) . . ?
 C141 Rh2 N2 164.1(4) . . ?
 C141 Rh2 C142 39.6(6) . . ?
 C141 Rh2 C144 63.1(5) . . ?
 C141 Rh2 C143 64.2(5) . . ?
 C141 Rh2 C145 36.9(6) . . ?
 O5 S2 O6 115.2(4) . . ?
 O5 S2 O4 114.1(5) . . ?
 O5 S2 C207 102.4(5) . . ?
 O6 S2 O4 114.0(4) . . ?
 O6 S2 C207 103.5(5) . . ?
 O4 S2 C207 105.8(5) . . ?
 O25 S7 O26 116.9(5) . . ?
 O25 S7 O27 113.9(6) . . ?
 O25 S7 C212 102.8(5) . . ?
 O26 S7 O27 112.9(6) . . ?
 O26 S7 C212 104.1(6) . . ?
 O27 S7 C212 104.3(6) . . ?
 O12 S5 O10 112.5(6) . . ?
 O12 S5 C206 106.5(6) . . ?
 O11 S5 O12 115.5(5) . . ?
 O11 S5 O10 113.2(6) . . ?
 O11 S5 C206 104.1(6) . . ?
 O10 S5 C206 103.8(6) . . ?
 O18 S4 O17 116.0(5) . . ?
 O18 S4 C204 101.6(7) . . ?
 O17 S4 C204 102.8(7) . . ?
 O16 S4 O18 115.5(7) . . ?
 O16 S4 O17 114.0(7) . . ?
 O16 S4 C204 104.4(7) . . ?
 O21 S1 O19 113.6(5) . . ?
 O21 S1 C210 103.6(6) . . ?
 O19 S1 C210 104.1(7) . . ?
 O20 S1 O21 115.3(6) . . ?
 O20 S1 O19 115.5(6) . . ?
 O20 S1 C210 102.5(6) . . ?
 O9 S3 O8 117.7(9) . . ?
 O9 S3 C209 103.4(9) . . ?
 O8 S3 C209 102.1(9) . . ?
 O7 S3 O9 113.0(8) . . ?
 O7 S3 O8 116.0(8) . . ?
 O7 S3 C209 101.5(11) . . ?
 O15 S6 C205 105.9(5) . . ?
 O15 S6 O14 109.9(6) . . ?
 O14 S6 C205 107.1(5) . . ?
 O13 S6 O15 112.3(6) . . ?
 O13 S6 C205 107.9(6) . . ?
 O13 S6 O14 113.2(6) . . ?
 F19 C211 S8 109.2(5) . . ?
 F19 C211 F21 104.5(6) . . ?
 F20 C211 S8 111.0(8) . . ?
 F20 C211 F19 113.0(6) . . ?
 F20 C211 F21 113.3(7) . . ?
 F21 C211 S8 105.4(7) . . ?
 O28 S8 C211 110.1(6) . . ?
 O28 S8 O29 111.4(6) . . ?
 O30 S8 C211 105.2(6) . . ?
 O30 S8 O28 111.3(7) . . ?
 O30 S8 O29 111.0(6) . . ?
 O29 S8 C211 107.5(6) . . ?
 C1 N16 Rh4 128.5(6) . . ?
 C5 N16 Rh4 114.7(6) . . ?
 C5 N16 C1 116.8(8) . . ?
 C91 N17 Rh5 116.8(6) . . ?
 C91 N17 C92 116.0(8) . . ?
 C92 N17 Rh5 127.2(6) . . ?
 C6 N15 Rh4 114.1(5) . . ?
 C7 N15 Rh4 126.7(7) . . ?
 C7 N15 C6 119.1(8) . . ?
 C25 N10 Rh3 124.4(7) . . ?
 C25 N10 C29 114.0(9) . . ?
 C29 N10 Rh3 121.2(6) . . ?
 C19 N11 Rh3 116.3(6) . . ?
 C19 N11 C20 114.3(8) . . ?
 C20 N11 Rh3 129.4(6) . . ?
 C53 N7 Rh2 117.1(6) . . ?
 C49 N7 Rh2 124.3(7) . . ?
 C49 N7 C53 118.5(8) . . ?
 C96 N19 C83 117.5(8) . . ?
 C89 N18 Rh5 129.4(7) . . ?
 C89 N18 C90 116.8(8) . . ?
 C90 N18 Rh5 113.8(5) . . ?
 C79 N21 Rh6 127.9(7) . . ?
 C78 N21 Rh6 115.6(6) . . ?
 C78 N21 C79 116.4(8) . . ?
 C13 N14 C12 117.9(7) . . ?
 C77 N22 Rh6 115.4(7) . . ?
 C73 N22 Rh6 126.1(7) . . ?
 C73 N22 C77 118.0(9) . . ?
 C47 N9 Rh4 122.7(6) . 2_676 ?
 C46 N9 Rh4 120.6(6) . 2_676 ?
 C46 N9 C47 116.6(8) . . ?
 C166 N1 Rh2 112.8(7) . . ?
 C170 N1 Rh2 125.6(8) . . ?
 C170 N1 C166 121.6(9) . . ?
 C179 N6 Rh1 116.5(7) . . ?
 C178 N6 Rh1 127.1(7) . . ?
 C178 N6 C179 116.3(9) . . ?
 C119 N24 Rh5 119.8(6) . 2_656 ?
 C118 N24 Rh5 123.4(7) . 2_656 ?
 C118 N24 C119 116.8(8) . . ?
 C101 N23 Rh6 122.0(6) . . ?
 C101 N23 C97 117.2(9) . . ?
 C97 N23 Rh6 120.6(7) . . ?
 C18 N12 Rh3 114.1(6) . . ?
 C18 N12 C17 120.2(7) . . ?
 C17 N12 Rh3 125.7(6) . . ?
 C24 N13 C11 117.0(8) . . ?
 C171 N3 C174 118.4(8) . . ?
 C71 N8 Rh1 122.9(7) . 2_676 ?
 C71 N8 C70 117.0(8) . . ?
 C70 N8 Rh1 119.2(7) . 2_676 ?
 C172 N4 C173 114.8(8) . . ?
 C84 N20 C85 115.8(8) . . ?
 N19 C83 C84 120.6(8) . . ?
 N19 C83 C82 118.9(8) . . ?
 C84 C83 C82 120.4(8) . . ?
 C165 N2 Rh2 114.0(7) . . ?
 C161 N2 Rh2 127.6(8) . . ?
 C161 N2 C165 118.4(10) . . ?
 N20 C85 C96 122.6(9) . . ?
 N20 C85 C86 118.7(8) . . ?
 C96 C85 C86 118.7(8) . . ?
 N17 C91 C95 124.6(8) . . ?
 N17 C91 C90 116.0(8) . . ?
 C95 C91 C90 119.4(8) . . ?
 N19 C96 C85 120.6(8) . . ?
 N19 C96 C95 120.4(8) . . ?
 C85 C96 C95 118.9(9) . . ?
 N12 C18 C14 122.9(8) . . ?
 N12 C18 C19 118.9(8) . . ?
 C14 C18 C19 118.2(8) . . ?
 N8 C71 H71 117.2 . . ?
 N8 C71 C72 125.7(10) . . ?
 C72 C71 H71 117.2 . . ?
 N16 C1 H1 118.9 . . ?
 C2 C1 N16 122.2(8) . . ?
 C2 C1 H1 118.9 . . ?
 C120 C116 C117 115.3(9) . . ?
 C120 C116 C115 120.1(9) . . ?
 C117 C116 C115 124.6(9) . . ?
 C180 N5 Rh1 115.7(7) . . ?
 C181 N5 Rh1 126.1(8) . . ?
 C181 N5 C180 118.1(10) . . ?
 N14 C13 C14 118.7(8) . . ?
 N14 C13 C24 121.7(8) . . ?
 C14 C13 C24 119.5(8) . . ?
 C18 C14 C13 120.6(8) . . ?
 C18 C14 C15 116.5(8) . . ?
 C15 C14 C13 122.9(8) . . ?
 N4 C173 C048 115.7(8) . . ?
 N4 C173 C174 123.2(9) . . ?
 C174 C173 C048 120.9(10) . . ?
 N20 C84 C83 122.6(8) . . ?
 N20 C84 C76 117.7(8) . . ?
 C83 C84 C76 119.7(9) . . ?
 N1 C166 C167 120.4(9) . . ?
 N1 C166 C165 117.2(9) . . ?
 C167 C166 C165 122.4(9) . . ?
 C187 C188 Rh5 70.8(6) . . ?
 C187 C188 C184 106.7(10) . . ?
 C187 C188 C193 122.8(11) . . ?
 C184 C188 Rh5 71.5(6) . . ?
 C184 C188 C193 130.4(10) . . ?
 C193 C188 Rh5 124.2(8) . . ?
 N14 C12 C4 119.1(8) . . ?
 N14 C12 C11 119.9(8) . . ?
 C11 C12 C4 121.0(9) . . ?
 N24 C119 H119 118.8 . . ?
 N24 C119 C120 122.4(8) . . ?
 C120 C119 H119 118.8 . . ?
 C61 C56 C55 120.5(9) . . ?
 C57 C56 C55 121.0(9) . . ?
 C57 C56 C61 118.4(8) . . ?
 C109 C108 C113 118.9(9) . . ?
 C107 C108 C109 118.6(8) . . ?
 C107 C108 C113 122.5(8) . . ?
 C65 C66 H66 117.9 . . ?
 C67 C66 H66 117.9 . . ?
 C67 C66 C65 124.2(10) . . ?
 C108 C109 C104 119.6(9) . . ?
 C110 C109 C108 119.5(8) . . ?
 C110 C109 C104 120.9(9) . . ?
 C166 C167 C171 117.7(9) . . ?
 C168 C167 C166 117.2(9) . . ?
 C168 C167 C171 125.1(9) . . ?
 N13 C24 C13 121.2(8) . . ?
 N13 C24 C23 118.6(8) . . ?
 C13 C24 C23 120.1(9) . . ?
 N3 C171 C167 117.9(8) . . ?
 N3 C171 C172 121.0(9) . . ?
 C172 C171 C167 121.0(9) . . ?
 C91 C95 C96 120.9(8) . . ?
 C91 C95 C94 118.2(8) . . ?
 C94 C95 C96 120.9(9) . . ?
 C85 C86 C87 121.7(9) . . ?
 C90 C86 C85 121.2(8) . . ?
 C90 C86 C87 117.0(9) . . ?
 C6 C10 C11 116.5(8) . . ?
 C9 C10 C6 119.7(8) . . ?
 C9 C10 C11 123.7(8) . . ?
 C64 C63 H63 119.5 . . ?
 C62 C63 H63 119.5 . . ?
 C62 C63 C64 121.0(10) . . ?
 N11 C19 C18 113.2(8) . . ?
 C23 C19 N11 124.7(8) . . ?
 C23 C19 C18 122.1(8) . . ?
 C94 C93 H93 119.7 . . ?
 C94 C93 C92 120.5(9) . . ?
 C92 C93 H93 119.7 . . ?
 C64 C65 C66 122.4(9) . . ?
 C64 C65 C60 119.9(9) . . ?
 C60 C65 C66 117.7(10) . . ?
 N4 C172 C171 122.8(9) . . ?
 N4 C172 C164 117.8(8) . . ?
 C171 C172 C164 119.4(9) . . ?
 N18 C89 H89 118.6 . . ?
 N18 C89 C88 122.9(10) . . ?
 C88 C89 H89 118.6 . . ?
 N15 C6 C10 119.4(8) . . ?
 N15 C6 C5 116.8(8) . . ?
 C10 C6 C5 123.8(8) . . ?
 N2 C165 C166 118.5(10) . . ?
 N2 C165 C164 122.6(9) . . ?
 C164 C165 C166 118.8(9) . . ?
 N22 C77 C76 123.9(9) . . ?
 N22 C77 C78 115.8(10) . . ?
 C76 C77 C78 120.3(10) . . ?
 C125 C124 Rh4 71.9(6) . . ?
 C125 C124 C123 108.2(10) . . ?
 C125 C124 C129 126.9(10) . . ?
 C123 C124 Rh4 71.6(6) . . ?
 C123 C124 C129 124.8(10) . . ?
 C129 C124 Rh4 126.1(7) . . ?
 N9 C47 H47 117.9 . . ?
 C48 C47 N9 124.3(9) . . ?
 C48 C47 H47 117.9 . . ?
 N6 C179 C175 125.8(10) . . ?
 N6 C179 C180 115.3(10) . . ?
 C175 C179 C180 118.9(10) . . ?
 C124 C125 Rh4 69.4(5) . . ?
 C124 C125 C121 107.6(9) . . ?
 C124 C125 C130 128.3(11) . . ?
 C121 C125 Rh4 71.0(5) . . ?
 C121 C125 C130 124.0(10) . . ?
 C130 C125 Rh4 128.3(7) . . ?
 C36 C37 C32 120.4(9) . . ?
 C36 C37 C38 118.9(8) . . ?
 C38 C37 C32 120.6(9) . . ?
 C37 C36 C41 118.0(8) . . ?
 C35 C36 C37 119.5(9) . . ?
 C35 C36 C41 122.5(8) . . ?
 C10 C9 H9 120.1 . . ?
 C8 C9 C10 119.8(8) . . ?
 C8 C9 H9 120.1 . . ?
 C135 C134 Rh3 70.0(5) . . ?
 C135 C134 C133 105.7(9) . . ?
 C135 C134 C139 125.5(9) . . ?
 C133 C134 Rh3 70.3(5) . . ?
 C133 C134 C139 128.8(11) . . ?
 C139 C134 Rh3 124.4(7) . . ?
 C165 C164 C172 120.5(8) . . ?
 C165 C164 C163 117.8(10) . . ?
 C163 C164 C172 121.6(10) . . ?
 C179 C175 C174 120.4(9) . . ?
 C176 C175 C179 115.8(10) . . ?
 C176 C175 C174 123.8(9) . . ?
 N16 C5 C6 117.1(9) . . ?
 N16 C5 C4 123.6(8) . . ?
 C4 C5 C6 119.4(8) . . ?
 N12 C17 H17 120.3 . . ?
 N12 C17 C16 119.5(9) . . ?
 C16 C17 H17 120.3 . . ?
 C153 C154 Rh1 71.7(7) . . ?
 C153 C154 C155 107.0(10) . . ?
 C153 C154 C159 126.1(10) . . ?
 C155 C154 Rh1 72.3(6) . . ?
 C155 C154 C159 125.9(10) . . ?
 C159 C154 Rh1 130.3(8) . . ?
 C167 C168 H168 120.2 . . ?
 C169 C168 C167 119.6(10) . . ?
 C169 C168 H168 120.2 . . ?
 C5 C4 C12 119.4(8) . . ?
 C3 C4 C12 122.8(8) . . ?
 C3 C4 C5 117.7(8) . . ?
 C56 C55 H55 118.6 . . ?
 C54 C55 C56 122.7(10) . . ?
 C54 C55 H55 118.6 . . ?
 C168 C169 H169 119.6 . . ?
 C168 C169 C170 120.7(9) . . ?
 C170 C169 H169 119.6 . . ?
 C47 C48 H48 120.7 . . ?
 C47 C48 C44 118.6(9) . . ?
 C44 C48 H48 120.7 . . ?
 C78 C82 C83 119.9(8) . . ?
 C81 C82 C83 123.8(8) . . ?
 C81 C82 C78 116.3(9) . . ?
 N13 C11 C12 122.2(9) . . ?
 N13 C11 C10 117.9(8) . . ?
 C12 C11 C10 119.8(8) . . ?
 C95 C94 H94 121.1 . . ?
 C93 C94 C95 117.8(10) . . ?
 C93 C94 H94 121.1 . . ?
 C66 C67 H67 115.6 . . ?
 C66 C67 C68 128.9(10) . . ?
 C68 C67 H67 115.6 . . ?
 C108 C113 C114 120.8(9) . . ?
 C112 C113 C108 118.4(8) . . ?
 C112 C113 C114 120.8(8) . . ?
 C86 C87 H87 121.4 . . ?
 C88 C87 C86 117.2(9) . . ?
 C88 C87 H87 121.4 . . ?
 C77 C76 C84 119.8(9) . . ?
 C77 C76 C75 119.1(9) . . ?
 C75 C76 C84 121.1(10) . . ?
 C27 C30 H30 117.4 . . ?
 C31 C30 H30 117.4 . . ?
 C31 C30 C27 125.1(10) . . ?
 C44 C43 H43 117.9 . . ?
 C42 C43 H43 117.9 . . ?
 C42 C43 C44 124.2(9) . . ?
 N21 C79 H79 118.1 . . ?
 C80 C79 N21 123.8(10) . . ?
 C80 C79 H79 118.1 . . ?
 C19 C23 C24 119.5(8) . . ?
 C19 C23 C22 118.3(8) . . ?
 C22 C23 C24 122.2(9) . . ?
 C188 C187 Rh5 70.5(6) . . ?
 C188 C187 C186 109.5(10) . . ?
 C188 C187 C192 126.0(12) . . ?
 C186 C187 Rh5 70.1(5) . . ?
 C186 C187 C192 124.4(11) . . ?
 C192 C187 Rh5 128.1(7) . . ?
 C116 C120 H120 119.8 . . ?
 C119 C120 C116 120.4(9) . . ?
 C119 C120 H120 119.8 . . ?
 N21 C78 C77 115.4(9) . . ?
 N21 C78 C82 124.7(9) . . ?
 C82 C78 C77 119.8(10) . . ?
 C124 C123 Rh4 68.9(5) . . ?
 C124 C123 C128 124.4(11) . . ?
 C122 C123 Rh4 71.5(6) . . ?
 C122 C123 C124 108.7(9) . . ?
 C122 C123 C128 126.7(10) . . ?
 C128 C123 Rh4 129.5(7) . . ?
 C36 C41 C42 119.1(8) . . ?
 C40 C41 C36 119.0(8) . . ?
 C40 C41 C42 121.9(8) . . ?
 C52 C51 C54 117.7(9) . . ?
 C50 C51 C52 116.7(9) . . ?
 C50 C51 C54 125.6(9) . . ?
 C44 C45 H45 120.4 . . ?
 C44 C45 C46 119.1(9) . . ?
 C46 C45 H45 120.4 . . ?
 C28 C27 C30 119.7(10) . . ?
 C28 C27 C26 117.1(9) . . ?
 C26 C27 C30 123.2(9) . . ?
 N10 C25 H25 117.6 . . ?
 N10 C25 C26 124.9(10) . . ?
 C26 C25 H25 117.6 . . ?
 C56 C61 C62 123.5(8) . . ?
 C56 C61 C60 120.7(9) . . ?
 C62 C61 C60 115.8(8) . . ?
 N15 C7 H7 118.4 . . ?
 N15 C7 C8 123.2(9) . . ?
 C8 C7 H7 118.4 . . ?
 C31 C32 C37 121.6(9) . . ?
 C33 C32 C37 116.3(9) . . ?
 C33 C32 C31 122.1(9) . . ?
 H20A C202 H20B 109.5 . . ?
 H20A C202 H20C 109.5 . . ?
 H20B C202 H20C 109.5 . . ?
 C197 C202 H20A 109.5 . . ?
 C197 C202 H20B 109.5 . . ?
 C197 C202 H20C 109.5 . . ?
 C63 C64 H64 119.3 . . ?
 C65 C64 C63 121.5(10) . . ?
 C65 C64 H64 119.3 . . ?
 N18 C90 C91 116.0(8) . . ?
 N18 C90 C86 123.3(8) . . ?
 C86 C90 C91 120.7(9) . . ?
 C180 C048 C173 116.8(9) . . ?
 C180 C048 C183 120.0(10) . . ?
 C183 C048 C173 123.2(10) . . ?
 C71 C72 H72 120.5 . . ?
 C71 C72 C68 119.0(9) . . ?
 C68 C72 H72 120.5 . . ?
 C105 C104 C109 117.2(9) . . ?
 C105 C104 C103 122.6(9) . . ?
 C103 C104 C109 120.1(9) . . ?
 C48 C44 C43 123.6(8) . . ?
 C45 C44 C48 117.1(8) . . ?
 C45 C44 C43 119.3(8) . . ?
 C9 C8 C7 118.8(9) . . ?
 C9 C8 H8 120.6 . . ?
 C7 C8 H8 120.6 . . ?
 N23 C101 H101 118.4 . . ?
 N23 C101 C100 123.3(10) . . ?
 C100 C101 H101 118.4 . . ?
 C116 C117 H117 119.9 . . ?
 C118 C117 C116 120.2(10) . . ?
 C118 C117 H117 119.9 . . ?
 C198 C194 Rh6 70.5(6) . . ?
 C198 C194 C195 107.4(9) . . ?
 C198 C194 C199 125.9(9) . . ?
 C195 C194 Rh6 70.8(6) . . ?
 C195 C194 C199 126.5(9) . . ?
 C199 C194 Rh6 128.4(7) . . ?
 C51 C52 H52 119.0 . . ?
 C51 C52 C53 122.1(10) . . ?
 C53 C52 H52 119.0 . . ?
 C27 C28 H28 119.8 . . ?
 C29 C28 C27 120.5(10) . . ?
 C29 C28 H28 119.8 . . ?
 C55 C54 C51 123.0(10) . . ?
 C55 C54 H54 118.5 . . ?
 C51 C54 H54 118.5 . . ?
 C14 C15 H15 120.6 . . ?
 C16 C15 C14 118.8(8) . . ?
 C16 C15 H15 120.6 . . ?
 C89 C88 H88 118.6 . . ?
 C87 C88 C89 122.8(9) . . ?
 C87 C88 H88 118.6 . . ?
 C134 C135 Rh3 71.4(5) . . ?
 C134 C135 C140 126.3(9) . . ?
 C134 C135 C131 108.8(9) . . ?
 C140 C135 Rh3 129.7(7) . . ?
 C131 C135 Rh3 71.5(5) . . ?
 C131 C135 C140 124.4(10) . . ?
 N3 C174 C173 119.8(10) . . ?
 N3 C174 C175 119.9(9) . . ?
 C175 C174 C173 120.3(10) . . ?
 C154 C153 Rh1 69.6(6) . . ?
 C154 C153 C158 126.2(11) . . ?
 C152 C153 Rh1 70.5(7) . . ?
 C152 C153 C154 109.1(9) . . ?
 C152 C153 C158 124.8(10) . . ?
 C158 C153 Rh1 126.4(8) . . ?
 C30 C31 C32 125.5(10) . . ?
 C30 C31 H31 117.2 . . ?
 C32 C31 H31 117.2 . . ?
 C32 C33 H33 118.8 . . ?
 C34 C33 C32 122.4(9) . . ?
 C34 C33 H33 118.8 . . ?
 N17 C92 C93 122.9(9) . . ?
 N17 C92 H92 118.5 . . ?
 C93 C92 H92 118.5 . . ?
 C134 C133 Rh3 70.6(5) . . ?
 C134 C133 C138 119.6(10) . . ?
 C132 C133 Rh3 70.2(6) . . ?
 C132 C133 C134 111.1(10) . . ?
 C132 C133 C138 129.3(9) . . ?
 C138 C133 Rh3 126.7(7) . . ?
 C23 C22 H22 120.9 . . ?
 C21 C22 C23 118.3(9) . . ?
 C21 C22 H22 120.9 . . ?
 N10 C29 H29 118.0 . . ?
 C28 C29 N10 124.1(9) . . ?
 C28 C29 H29 118.0 . . ?
 N9 C46 C45 124.0(8) . . ?
 N9 C46 H46 118.0 . . ?
 C45 C46 H46 118.0 . . ?
 N7 C53 C52 120.2(9) . . ?
 N7 C53 H53 119.9 . . ?
 C52 C53 H53 119.9 . . ?
 C36 C35 H35 119.9 . . ?
 C34 C35 C36 120.3(10) . . ?
 C34 C35 H35 119.9 . . ?
 N1 C170 C169 120.4(10) . . ?
 N1 C170 H170 119.8 . . ?
 C169 C170 H170 119.8 . . ?
 C72 C68 C67 121.8(9) . . ?
 C69 C68 C67 122.5(9) . . ?
 C69 C68 C72 115.6(8) . . ?
 C59 C58 H58 120.8 . . ?
 C59 C58 C57 118.5(11) . . ?
 C57 C58 H58 120.8 . . ?
 C17 C16 H16 119.0 . . ?
 C15 C16 C17 122.0(9) . . ?
 C15 C16 H16 119.0 . . ?
 C75 C74 H74 119.5 . . ?
 C75 C74 C73 120.9(9) . . ?
 C73 C74 H74 119.5 . . ?
 C116 C115 H115 117.3 . . ?
 C114 C115 C116 125.3(10) . . ?
 C114 C115 H115 117.3 . . ?
 N6 C178 H178 118.8 . . ?
 N6 C178 C177 122.3(10) . . ?
 C177 C178 H178 118.8 . . ?
 C188 C184 Rh5 69.1(6) . . ?
 C188 C184 C189 123.9(11) . . ?
 C189 C184 Rh5 128.2(7) . . ?
 C185 C184 Rh5 70.3(6) . . ?
 C185 C184 C188 107.7(9) . . ?
 C185 C184 C189 128.3(12) . . ?
 C37 C38 H38 119.5 . . ?
 C39 C38 C37 121.0(10) . . ?
 C39 C38 H38 119.5 . . ?
 C202 C197 Rh6 128.1(8) . . ?
 C202 C197 C196 124.2(9) . . ?
 C196 C197 Rh6 70.2(5) . . ?
 C198 C197 Rh6 71.5(6) . . ?
 C198 C197 C202 128.3(9) . . ?
 C198 C197 C196 107.2(9) . . ?
 C101 C100 H100 119.7 . . ?
 C101 C100 C99 120.5(10) . . ?
 C99 C100 H100 119.7 . . ?
 C63 C62 C61 122.3(9) . . ?
 C63 C62 H62 118.8 . . ?
 C61 C62 H62 118.8 . . ?
 C82 C81 H81 121.0 . . ?
 C80 C81 C82 117.9(8) . . ?
 C80 C81 H81 121.0 . . ?
 N11 C20 H20 118.2 . . ?
 C21 C20 N11 123.6(9) . . ?
 C21 C20 H20 118.2 . . ?
 C65 C60 C61 119.5(9) . . ?
 C59 C60 C65 123.5(9) . . ?
 C59 C60 C61 116.7(9) . . ?
 N5 C180 C179 115.4(10) . . ?
 C048 C180 N5 122.1(9) . . ?
 C048 C180 C179 122.5(9) . . ?
 C187 C186 Rh5 70.4(6) . . ?
 C187 C186 C191 128.4(11) . . ?
 C185 C186 Rh5 70.4(6) . . ?
 C185 C186 C187 104.1(10) . . ?
 C185 C186 C191 127.0(12) . . ?
 C191 C186 Rh5 128.9(7) . . ?
 N7 C49 H49 118.3 . . ?
 N7 C49 C50 123.4(9) . . ?
 C50 C49 H49 118.3 . . ?
 C41 C40 H40 118.3 . . ?
 C41 C40 C39 123.3(9) . . ?
 C39 C40 H40 118.3 . . ?
 C27 C26 H26 120.3 . . ?
 C25 C26 C27 119.4(9) . . ?
 C25 C26 H26 120.3 . . ?
 C76 C75 H75 121.6 . . ?
 C74 C75 C76 116.9(10) . . ?
 C74 C75 H75 121.6 . . ?
 C79 C80 C81 120.7(9) . . ?
 C79 C80 H80 119.6 . . ?
 C81 C80 H80 119.6 . . ?
 F7 C207 S2 114.2(8) . . ?
 F7 C207 F9 107.9(9) . . ?
 F7 C207 F8 106.2(8) . . ?
 F9 C207 S2 111.9(7) . . ?
 F9 C207 F8 105.3(10) . . ?
 F8 C207 S2 110.7(7) . . ?
 C164 C163 H163 121.3 . . ?
 C164 C163 C162 117.5(11) . . ?
 C162 C163 H163 121.3 . . ?
 C108 C107 H107 119.4 . . ?
 C106 C107 C108 121.2(9) . . ?
 C106 C107 H107 119.4 . . ?
 C113 C114 H114 117.9 . . ?
 C115 C114 C113 124.2(10) . . ?
 C115 C114 H114 117.9 . . ?
 C43 C42 C41 121.9(9) . . ?
 C43 C42 H42 119.0 . . ?
 C41 C42 H42 119.0 . . ?
 C184 C189 H18A 109.5 . . ?
 C184 C189 H18B 109.5 . . ?
 C184 C189 H18C 109.5 . . ?
 H18A C189 H18B 109.5 . . ?
 H18A C189 H18C 109.5 . . ?
 H18B C189 H18C 109.5 . . ?
 N24 C118 C117 124.2(11) . . ?
 N24 C118 H118 117.9 . . ?
 C117 C118 H118 117.9 . . ?
 C197 C196 Rh6 69.3(5) . . ?
 C195 C196 Rh6 71.7(5) . . ?
 C195 C196 C197 105.9(8) . . ?
 C195 C196 C201 127.9(9) . . ?
 C201 C196 Rh6 129.9(8) . . ?
 C201 C196 C197 125.7(10) . . ?
 C194 C198 Rh6 71.3(6) . . ?
 C194 C198 C197 109.3(8) . . ?
 C194 C198 C203 127.3(10) . . ?
 C197 C198 Rh6 69.8(6) . . ?
 C197 C198 C203 123.3(10) . . ?
 C203 C198 Rh6 123.8(8) . . ?
 C1 C2 H2 119.5 . . ?
 C1 C2 C3 121.1(9) . . ?
 C3 C2 H2 119.5 . . ?
 C125 C121 Rh4 70.1(5) . . ?
 C125 C121 C122 106.9(9) . . ?
 C125 C121 C126 127.4(10) . . ?
 C122 C121 Rh4 69.9(6) . . ?
 C126 C121 Rh4 125.9(7) . . ?
 C126 C121 C122 125.7(10) . . ?
 C22 C21 C20 120.8(9) . . ?
 C22 C21 H21 119.6 . . ?
 C20 C21 H21 119.6 . . ?
 C107 C106 H106 120.5 . . ?
 C107 C106 C105 119.0(10) . . ?
 C105 C106 H106 120.5 . . ?
 C4 C3 H3 120.7 . . ?
 C2 C3 C4 118.5(9) . . ?
 C2 C3 H3 120.7 . . ?
 C124 C129 H12A 109.5 . . ?
 C124 C129 H12B 109.5 . . ?
 C124 C129 H12C 109.5 . . ?
 H12A C129 H12B 109.5 . . ?
 H12A C129 H12C 109.5 . . ?
 H12B C129 H12C 109.5 . . ?
 C100 C99 C102 125.2(9) . . ?
 C100 C99 C98 116.1(10) . . ?
 C98 C99 C102 118.7(9) . . ?
 C183 C182 H182 120.8 . . ?
 C183 C182 C181 118.5(10) . . ?
 C181 C182 H182 120.8 . . ?
 C58 C59 C60 122.8(9) . . ?
 C58 C59 H59 118.6 . . ?
 C60 C59 H59 118.6 . . ?
 N22 C73 C74 121.0(9) . . ?
 N22 C73 H73 119.5 . . ?
 C74 C73 H73 119.5 . . ?
 C104 C105 C106 124.4(9) . . ?
 C104 C105 H105 117.8 . . ?
 C106 C105 H105 117.8 . . ?
 C125 C130 H13A 109.5 . . ?
 C125 C130 H13B 109.5 . . ?
 C125 C130 H13C 109.5 . . ?
 H13A C130 H13B 109.5 . . ?
 H13A C130 H13C 109.5 . . ?
 H13B C130 H13C 109.5 . . ?
 C113 C112 H112 119.2 . . ?
 C111 C112 C113 121.6(8) . . ?
 C111 C112 H112 119.2 . . ?
 C38 C39 C40 119.5(10) . . ?
 C38 C39 H39 120.3 . . ?
 C40 C39 H39 120.3 . . ?
 C51 C50 C49 119.0(9) . . ?
 C51 C50 H50 120.5 . . ?
 C49 C50 H50 120.5 . . ?
 C135 C140 H14A 109.5 . . ?
 C135 C140 H14B 109.5 . . ?
 C135 C140 H14C 109.5 . . ?
 H14A C140 H14B 109.5 . . ?
 H14A C140 H14C 109.5 . . ?
 H14B C140 H14C 109.5 . . ?
 N8 C70 H70 119.6 . . ?
 N8 C70 C69 120.7(10) . . ?
 C69 C70 H70 119.6 . . ?
 C109 C110 H110 118.9 . . ?
 C111 C110 C109 122.2(9) . . ?
 C111 C110 H110 118.9 . . ?
 C56 C57 H57 118.8 . . ?
 C58 C57 C56 122.5(10) . . ?
 C58 C57 H57 118.8 . . ?
 C048 C183 H183 120.4 . . ?
 C182 C183 C048 119.2(11) . . ?
 C182 C183 H183 120.4 . . ?
 C154 C155 Rh1 69.0(6) . . ?
 C154 C155 C160 126.4(11) . . ?
 C151 C155 Rh1 71.0(6) . . ?
 C151 C155 C154 108.3(9) . . ?
 C151 C155 C160 125.3(11) . . ?
 C160 C155 Rh1 124.5(8) . . ?
 C133 C132 Rh3 72.4(6) . . ?
 C133 C132 C137 129.7(11) . . ?
 C133 C132 C131 108.0(9) . . ?
 C137 C132 Rh3 127.1(7) . . ?
 C131 C132 Rh3 72.1(6) . . ?
 C131 C132 C137 121.9(11) . . ?
 N5 C181 C182 122.0(11) . . ?
 N5 C181 H181 119.0 . . ?
 C182 C181 H181 119.0 . . ?
 C175 C176 H176 119.6 . . ?
 C177 C176 C175 120.8(10) . . ?
 C177 C176 H176 119.6 . . ?
 C188 C193 H19A 109.5 . . ?
 C188 C193 H19B 109.5 . . ?
 C188 C193 H19C 109.5 . . ?
 H19A C193 H19B 109.5 . . ?
 H19A C193 H19C 109.5 . . ?
 H19B C193 H19C 109.5 . . ?
 F26 C212 S7 112.4(10) . . ?
 F27 C212 S7 111.7(9) . . ?
 F27 C212 F26 105.1(9) . . ?
 F25 C212 S7 112.0(8) . . ?
 F25 C212 F26 106.3(10) . . ?
 F25 C212 F27 108.9(12) . . ?
 C153 C152 Rh1 71.5(6) . . ?
 C153 C152 C151 107.2(10) . . ?
 C153 C152 C157 125.3(11) . . ?
 C151 C152 Rh1 71.4(6) . . ?
 C151 C152 C157 126.6(12) . . ?
 C157 C152 Rh1 130.8(9) . . ?
 C104 C103 H103 117.1 . . ?
 C102 C103 C104 125.7(10) . . ?
 C102 C103 H103 117.1 . . ?
 C163 C162 H162 120.8 . . ?
 C161 C162 C163 118.5(11) . . ?
 C161 C162 H162 120.8 . . ?
 C187 C192 H19D 109.5 . . ?
 C187 C192 H19E 109.5 . . ?
 C187 C192 H19F 109.5 . . ?
 H19D C192 H19E 109.5 . . ?
 H19D C192 H19F 109.5 . . ?
 H19E C192 H19F 109.5 . . ?
 C123 C122 Rh4 71.5(6) . . ?
 C123 C122 C121 108.6(9) . . ?
 C123 C122 C127 125.2(11) . . ?
 C121 C122 Rh4 70.5(5) . . ?
 C121 C122 C127 126.1(11) . . ?
 C127 C122 Rh4 127.1(7) . . ?
 C99 C102 H102 118.4 . . ?
 C103 C102 C99 123.2(9) . . ?
 C103 C102 H102 118.4 . . ?
 C99 C98 H98 120.6 . . ?
 C97 C98 C99 118.8(11) . . ?
 C97 C98 H98 120.6 . . ?
 C68 C69 C70 121.8(10) . . ?
 C68 C69 H69 119.1 . . ?
 C70 C69 H69 119.1 . . ?
 C33 C34 C35 121.1(10) . . ?
 C33 C34 H34 119.4 . . ?
 C35 C34 H34 119.4 . . ?
 C134 C139 H13D 109.5 . . ?
 C134 C139 H13E 109.5 . . ?
 C134 C139 H13F 109.5 . . ?
 H13D C139 H13E 109.5 . . ?
 H13D C139 H13F 109.5 . . ?
 H13E C139 H13F 109.5 . . ?
 C178 C177 H177 120.6 . . ?
 C176 C177 C178 118.8(10) . . ?
 C176 C177 H177 120.6 . . ?
 C112 C111 H111 120.4 . . ?
 C110 C111 C112 119.1(10) . . ?
 C110 C111 H111 120.4 . . ?
 H19G C190 H19H 109.5 . . ?
 H19G C190 H19I 109.5 . . ?
 H19H C190 H19I 109.5 . . ?
 C185 C190 H19G 109.5 . . ?
 C185 C190 H19H 109.5 . . ?
 C185 C190 H19I 109.5 . . ?
 C154 C159 H15A 109.5 . . ?
 C154 C159 H15B 109.5 . . ?
 C154 C159 H15C 109.5 . . ?
 H15A C159 H15B 109.5 . . ?
 H15A C159 H15C 109.5 . . ?
 H15B C159 H15C 109.5 . . ?
 C143 C142 Rh2 72.2(8) . . ?
 C143 C142 C141 107.2(13) . . ?
 C143 C142 C147 126.5(17) . . ?
 C141 C142 Rh2 69.2(8) . . ?
 C141 C142 C147 126.2(16) . . ?
 C147 C142 Rh2 125.3(9) . . ?
 F11 C206 S5 111.6(10) . . ?
 F12 C206 S5 112.7(9) . . ?
 F12 C206 F11 105.0(10) . . ?
 F10 C206 S5 111.9(9) . . ?
 F10 C206 F11 106.0(12) . . ?
 F10 C206 F12 109.2(13) . . ?
 C133 C138 H13G 109.5 . . ?
 C133 C138 H13H 109.5 . . ?
 C133 C138 H13I 109.5 . . ?
 H13G C138 H13H 109.5 . . ?
 H13G C138 H13I 109.5 . . ?
 H13H C138 H13I 109.5 . . ?
 C132 C137 H13J 109.5 . . ?
 C132 C137 H13K 109.5 . . ?
 C132 C137 H13L 109.5 . . ?
 H13J C137 H13K 109.5 . . ?
 H13J C137 H13L 109.5 . . ?
 H13K C137 H13L 109.5 . . ?
 C143 C144 Rh2 70.2(6) . . ?
 C145 C144 Rh2 71.0(8) . . ?
 C145 C144 C143 105.8(13) . . ?
 C145 C144 C149 129.5(17) . . ?
 C149 C144 Rh2 127.9(12) . . ?
 C149 C144 C143 124.5(18) . . ?
 C184 C185 Rh5 72.8(7) . . ?
 C184 C185 C186 111.7(11) . . ?
 C184 C185 C190 122.8(11) . . ?
 C186 C185 Rh5 70.3(6) . . ?
 C186 C185 C190 125.4(12) . . ?
 C190 C185 Rh5 125.5(8) . . ?
 C155 C151 Rh1 71.4(6) . . ?
 C155 C151 C152 108.2(10) . . ?
 C155 C151 C156 126.6(10) . . ?
 C152 C151 Rh1 69.6(6) . . ?
 C152 C151 C156 125.1(11) . . ?
 C156 C151 Rh1 125.6(9) . . ?
 C123 C128 H12D 109.5 . . ?
 C123 C128 H12E 109.5 . . ?
 C123 C128 H12F 109.5 . . ?
 H12D C128 H12E 109.5 . . ?
 H12D C128 H12F 109.5 . . ?
 H12E C128 H12F 109.5 . . ?
 N2 C161 C162 125.2(12) . . ?
 N2 C161 H161 117.4 . . ?
 C162 C161 H161 117.4 . . ?
 C194 C195 Rh6 70.7(5) . . ?
 C194 C195 C200 127.2(10) . . ?
 C196 C195 Rh6 70.1(6) . . ?
 C196 C195 C194 110.1(9) . . ?
 C196 C195 C200 122.7(9) . . ?
 C200 C195 Rh6 126.6(8) . . ?
 F14 C205 S6 107.6(6) . . ?
 F15 C205 S6 105.7(7) . . ?
 F15 C205 F14 112.5(8) . . ?
 F13 C205 S6 108.4(7) . . ?
 F13 C205 F14 111.0(8) . . ?
 F13 C205 F15 111.4(8) . . ?
 C135 C131 Rh3 69.0(6) . . ?
 C135 C131 C136 128.8(11) . . ?
 C132 C131 Rh3 68.5(6) . . ?
 C132 C131 C135 106.2(10) . . ?
 C132 C131 C136 125.0(10) . . ?
 C136 C131 Rh3 125.8(7) . . ?
 C142 C143 Rh2 70.4(7) . . ?
 C142 C143 C144 107.2(13) . . ?
 C142 C143 C148 124.7(16) . . ?
 C144 C143 Rh2 70.4(7) . . ?
 C144 C143 C148 128.0(16) . . ?
 C148 C143 Rh2 127.7(9) . . ?
 F17 C204 S4 113.8(11) . . ?
 F16 C204 S4 115.1(11) . . ?
 F16 C204 F17 102.1(12) . . ?
 F18 C204 S4 114.4(11) . . ?
 F18 C204 F17 103.0(12) . . ?
 F18 C204 F16 107.1(13) . . ?
 C186 C191 H19J 109.5 . . ?
 C186 C191 H19K 109.5 . . ?
 C186 C191 H19L 109.5 . . ?
 H19J C191 H19K 109.5 . . ?
 H19J C191 H19L 109.5 . . ?
 H19K C191 H19L 109.5 . . ?
 N23 C97 C98 124.1(11) . . ?
 N23 C97 H97 118.0 . . ?
 C98 C97 H97 118.0 . . ?
 C194 C199 H19M 109.5 . . ?
 C194 C199 H19N 109.5 . . ?
 C194 C199 H19O 109.5 . . ?
 H19M C199 H19N 109.5 . . ?
 H19M C199 H19O 109.5 . . ?
 H19N C199 H19O 109.5 . . ?
 C196 C201 H20D 109.5 . . ?
 C196 C201 H20E 109.5 . . ?
 C196 C201 H20F 109.5 . . ?
 H20D C201 H20E 109.5 . . ?
 H20D C201 H20F 109.5 . . ?
 H20E C201 H20F 109.5 . . ?
 F30 C210 S1 113.0(11) . . ?
 F30 C210 F28 105.0(11) . . ?
 F30 C210 F29 108.1(11) . . ?
 F28 C210 S1 112.3(9) . . ?
 F29 C210 S1 111.1(10) . . ?
 F29 C210 F28 106.8(13) . . ?
 C144 C145 Rh2 72.9(8) . . ?
 C144 C145 C141 113.3(14) . . ?
 C144 C145 C150 116.0(18) . . ?
 C141 C145 Rh2 70.3(7) . . ?
 C141 C145 C150 131(2) . . ?
 C150 C145 Rh2 126.6(12) . . ?
 C198 C203 H20G 109.5 . . ?
 C198 C203 H20H 109.5 . . ?
 C198 C203 H20I 109.5 . . ?
 H20G C203 H20H 109.5 . . ?
 H20G C203 H20I 109.5 . . ?
 H20H C203 H20I 109.5 . . ?
 C195 C200 H20J 109.5 . . ?
 C195 C200 H20K 109.5 . . ?
 C195 C200 H20L 109.5 . . ?
 H20J C200 H20K 109.5 . . ?
 H20J C200 H20L 109.5 . . ?
 H20K C200 H20L 109.5 . . ?
 C122 C127 H12G 109.5 . . ?
 C122 C127 H12H 109.5 . . ?
 C122 C127 H12I 109.5 . . ?
 H12G C127 H12H 109.5 . . ?
 H12G C127 H12I 109.5 . . ?
 H12H C127 H12I 109.5 . . ?
 C121 C126 H12J 109.5 . . ?
 C121 C126 H12K 109.5 . . ?
 C121 C126 H12L 109.5 . . ?
 H12J C126 H12K 109.5 . . ?
 H12J C126 H12L 109.5 . . ?
 H12K C126 H12L 109.5 . . ?
 C155 C160 H16A 109.5 . . ?
 C155 C160 H16B 109.5 . . ?
 C155 C160 H16C 109.5 . . ?
 H16A C160 H16B 109.5 . . ?
 H16A C160 H16C 109.5 . . ?
 H16B C160 H16C 109.5 . . ?
 C142 C141 Rh2 71.2(8) . . ?
 C142 C141 C146 130.1(17) . . ?
 C145 C141 Rh2 72.7(9) . . ?
 C145 C141 C142 106.4(13) . . ?
 C145 C141 C146 122.3(19) . . ?
 C146 C141 Rh2 130.5(9) . . ?
 C131 C136 H13M 109.5 . . ?
 C131 C136 H13N 109.5 . . ?
 C131 C136 H13O 109.5 . . ?
 H13M C136 H13N 109.5 . . ?
 H13M C136 H13O 109.5 . . ?
 H13N C136 H13O 109.5 . . ?
 C153 C158 H15D 109.5 . . ?
 C153 C158 H15E 109.5 . . ?
 C153 C158 H15F 109.5 . . ?
 H15D C158 H15E 109.5 . . ?
 H15D C158 H15F 109.5 . . ?
 H15E C158 H15F 109.5 . . ?
 C152 C157 H15G 109.5 . . ?
 C152 C157 H15H 109.5 . . ?
 C152 C157 H15I 109.5 . . ?
 H15G C157 H15H 109.5 . . ?
 H15G C157 H15I 109.5 . . ?
 H15H C157 H15I 109.5 . . ?
 C151 C156 H15J 109.5 . . ?
 C151 C156 H15K 109.5 . . ?
 C151 C156 H15L 109.5 . . ?
 H15J C156 H15K 109.5 . . ?
 H15J C156 H15L 109.5 . . ?
 H15K C156 H15L 109.5 . . ?
 F3 C209 S3 116.3(15) . . ?
 F3 C209 F2 98.0(17) . . ?
 F3 C209 F1 111.2(19) . . ?
 F2 C209 S3 111.7(16) . . ?
 F1 C209 S3 115.0(15) . . ?
 F1 C209 F2 102.4(17) . . ?
 C143 C148 H14D 109.5 . . ?
 C143 C148 H14E 109.5 . . ?
 C143 C148 H14F 109.5 . . ?
 H14D C148 H14E 109.5 . . ?
 H14D C148 H14F 109.5 . . ?
 H14E C148 H14F 109.5 . . ?
 C142 C147 H14G 109.5 . . ?
 C142 C147 H14H 109.5 . . ?
 C142 C147 H14I 109.5 . . ?
 H14G C147 H14H 109.5 . . ?
 H14G C147 H14I 109.5 . . ?
 H14H C147 H14I 109.5 . . ?
 C141 C146 H14J 109.5 . . ?
 C141 C146 H14K 109.5 . . ?
 C141 C146 H14L 109.5 . . ?
 H14J C146 H14K 109.5 . . ?
 H14J C146 H14L 109.5 . . ?
 H14K C146 H14L 109.5 . . ?
 C144 C149 H14M 109.5 . . ?
 C144 C149 H14N 109.5 . . ?
 C144 C149 H14O 109.5 . . ?
 H14M C149 H14N 109.5 . . ?
 H14M C149 H14O 109.5 . . ?
 H14N C149 H14O 109.5 . . ?
 C145 C150 H15M 109.5 . . ?
 C145 C150 H15N 109.5 . . ?
 C145 C150 H15O 109.5 . . ?
 H15M C150 H15N 109.5 . . ?
 H15M C150 H15O 109.5 . . ?
 H15N C150 H15O 109.5 . . ?

loop_
  _geom_torsion_atom_site_label_1
  _geom_torsion_atom_site_label_2
  _geom_torsion_atom_site_label_3
  _geom_torsion_atom_site_label_4
  _geom_torsion
  _geom_torsion_site_symmetry_1
  _geom_torsion_site_symmetry_2
  _geom_torsion_site_symmetry_3
  _geom_torsion_site_symmetry_4
  _geom_torsion_publ_flag
 Rh3 N10 C25 C26 -174.5(8) . . . . ?
 Rh3 N10 C29 C28 174.9(9) . . . . ?
 Rh3 N11 C19 C18 5.3(9) . . . . ?
 Rh3 N11 C19 C23 -174.6(7) . . . . ?
 Rh3 N11 C20 C21 174.7(7) . . . . ?
 Rh3 N12 C18 C14 178.1(7) . . . . ?
 Rh3 N12 C18 C19 -1.6(11) . . . . ?
 Rh3 N12 C17 C16 178.4(7) . . . . ?
 Rh3 C134 C135 C140 126.1(10) . . . . ?
 Rh3 C134 C135 C131 -62.1(7) . . . . ?
 Rh3 C134 C133 C132 58.6(7) . . . . ?
 Rh3 C134 C133 C138 -121.9(9) . . . . ?
 Rh3 C135 C131 C132 -58.7(7) . . . . ?
 Rh3 C135 C131 C136 119.8(10) . . . . ?
 Rh3 C133 C132 C137 -124.0(11) . . . . ?
 Rh3 C133 C132 C131 63.8(7) . . . . ?
 Rh3 C132 C131 C135 59.0(6) . . . . ?
 Rh3 C132 C131 C136 -119.5(10) . . . . ?
 Rh4 N16 C1 C2 176.9(7) . . . . ?
 Rh4 N16 C5 C6 1.2(10) . . . . ?
 Rh4 N16 C5 C4 -178.4(7) . . . . ?
 Rh4 N15 C6 C10 -179.6(6) . . . . ?
 Rh4 N15 C6 C5 -1.2(10) . . . . ?
 Rh4 N15 C7 C8 179.8(7) . . . . ?
 Rh4 N9 C47 C48 176.2(7) 2_676 . . . ?
 Rh4 N9 C46 C45 -176.7(7) 2_676 . . . ?
 Rh4 C124 C125 C121 -61.1(6) . . . . ?
 Rh4 C124 C125 C130 123.1(10) . . . . ?
 Rh4 C124 C123 C122 60.7(7) . . . . ?
 Rh4 C124 C123 C128 -124.2(9) . . . . ?
 Rh4 C125 C121 C122 -60.5(6) . . . . ?
 Rh4 C125 C121 C126 120.6(10) . . . . ?
 Rh4 C123 C122 C121 61.0(7) . . . . ?
 Rh4 C123 C122 C127 -122.8(10) . . . . ?
 Rh4 C121 C122 C123 -61.7(7) . . . . ?
 Rh4 C121 C122 C127 122.2(10) . . . . ?
 Rh5 N17 C91 C95 -179.0(7) . . . . ?
 Rh5 N17 C91 C90 1.0(10) . . . . ?
 Rh5 N17 C92 C93 177.5(7) . . . . ?
 Rh5 N18 C89 C88 177.5(7) . . . . ?
 Rh5 N18 C90 C91 -1.3(10) . . . . ?
 Rh5 N18 C90 C86 -178.7(7) . . . . ?
 Rh5 N24 C119 C120 -176.5(7) 2_656 . . . ?
 Rh5 N24 C118 C117 170.6(8) 2_656 . . . ?
 Rh5 C188 C187 C186 59.4(7) . . . . ?
 Rh5 C188 C187 C192 -123.4(10) . . . . ?
 Rh5 C188 C184 C189 122.7(10) . . . . ?
 Rh5 C188 C184 C185 -59.9(7) . . . . ?
 Rh5 C187 C186 C185 62.8(6) . . . . ?
 Rh5 C187 C186 C191 -124.6(10) . . . . ?
 Rh5 C184 C185 C186 -59.7(7) . . . . ?
 Rh5 C184 C185 C190 121.6(10) . . . . ?
 Rh5 C186 C185 C184 61.2(8) . . . . ?
 Rh5 C186 C185 C190 -120.1(11) . . . . ?
 Rh6 N21 C79 C80 -177.9(7) . . . . ?
 Rh6 N21 C78 C77 -2.0(10) . . . . ?
 Rh6 N21 C78 C82 175.0(7) . . . . ?
 Rh6 N22 C77 C76 -171.7(8) . . . . ?
 Rh6 N22 C77 C78 9.8(11) . . . . ?
 Rh6 N22 C73 C74 173.6(8) . . . . ?
 Rh6 N23 C101 C100 -173.4(7) . . . . ?
 Rh6 N23 C97 C98 174.8(9) . . . . ?
 Rh6 C194 C198 C197 59.6(7) . . . . ?
 Rh6 C194 C198 C203 -118.7(11) . . . . ?
 Rh6 C194 C195 C196 -59.1(7) . . . . ?
 Rh6 C194 C195 C200 121.8(11) . . . . ?
 Rh6 C197 C196 C195 62.7(7) . . . . ?
 Rh6 C197 C196 C201 -124.9(11) . . . . ?
 Rh6 C197 C198 C194 -60.5(7) . . . . ?
 Rh6 C197 C198 C203 117.8(10) . . . . ?
 Rh6 C196 C195 C194 59.5(7) . . . . ?
 Rh6 C196 C195 C200 -121.4(11) . . . . ?
 Rh1 N6 C179 C175 -178.8(7) . . . . ?
 Rh1 N6 C179 C180 -0.2(10) . . . . ?
 Rh1 N6 C178 C177 -178.4(7) . . . . ?
 Rh1 N8 C71 C72 -171.8(8) 2_676 . . . ?
 Rh1 N8 C70 C69 172.5(9) 2_676 . . . ?
 Rh1 N5 C180 C179 -3.4(10) . . . . ?
 Rh1 N5 C180 C048 174.0(7) . . . . ?
 Rh1 N5 C181 C182 -175.4(8) . . . . ?
 Rh1 C154 C153 C152 59.6(9) . . . . ?
 Rh1 C154 C153 C158 -120.8(12) . . . . ?
 Rh1 C154 C155 C151 -60.3(8) . . . . ?
 Rh1 C154 C155 C160 118.1(11) . . . . ?
 Rh1 C153 C152 C151 62.9(8) . . . . ?
 Rh1 C153 C152 C157 -127.5(12) . . . . ?
 Rh1 C155 C151 C152 -60.2(8) . . . . ?
 Rh1 C155 C151 C156 121.0(13) . . . . ?
 Rh1 C152 C151 C155 61.3(8) . . . . ?
 Rh1 C152 C151 C156 -119.8(12) . . . . ?
 Rh2 N7 C53 C52 -179.5(7) . . . . ?
 Rh2 N7 C49 C50 177.0(7) . . . . ?
 Rh2 N1 C166 C167 -179.1(6) . . . . ?
 Rh2 N1 C166 C165 0.4(9) . . . . ?
 Rh2 N1 C170 C169 178.4(7) . . . . ?
 Rh2 N2 C165 C166 1.7(10) . . . . ?
 Rh2 N2 C165 C164 178.6(6) . . . . ?
 Rh2 N2 C161 C162 179.8(9) . . . . ?
 Rh2 C142 C143 C144 -61.1(9) . . . . ?
 Rh2 C142 C143 C148 122.9(12) . . . . ?
 Rh2 C142 C141 C145 64.7(10) . . . . ?
 Rh2 C142 C141 C146 -127.6(14) . . . . ?
 Rh2 C144 C143 C142 61.1(8) . . . . ?
 Rh2 C144 C143 C148 -123.1(13) . . . . ?
 Rh2 C144 C145 C141 -59.0(11) . . . . ?
 Rh2 C144 C145 C150 123.0(14) . . . . ?
 Rh2 C145 C141 C142 -63.7(9) . . . . ?
 Rh2 C145 C141 C146 127.4(13) . . . . ?
 N16 C1 C2 C3 3.7(15) . . . . ?
 N16 C5 C4 C12 -178.1(8) . . . . ?
 N16 C5 C4 C3 -0.5(13) . . . . ?
 N17 C91 C95 C96 179.5(8) . . . . ?
 N17 C91 C95 C94 0.9(14) . . . . ?
 N17 C91 C90 N18 0.2(12) . . . . ?
 N17 C91 C90 C86 177.7(8) . . . . ?
 N15 C6 C5 N16 0.0(12) . . . . ?
 N15 C6 C5 C4 179.7(8) . . . . ?
 N15 C7 C8 C9 -0.7(15) . . . . ?
 O5 S2 C207 F7 -62.6(9) . . . . ?
 O5 S2 C207 F9 60.4(9) . . . . ?
 O5 S2 C207 F8 177.5(8) . . . . ?
 N10 C25 C26 C27 1.1(15) . . . . ?
 N11 C19 C23 C24 -179.4(8) . . . . ?
 N11 C19 C23 C22 -0.9(14) . . . . ?
 N11 C20 C21 C22 -0.5(16) . . . . ?
 N7 C49 C50 C51 4.1(15) . . . . ?
 N19 C83 C84 N20 -4.6(14) . . . . ?
 N19 C83 C84 C76 176.5(8) . . . . ?
 N19 C83 C82 C78 -179.8(8) . . . . ?
 N19 C83 C82 C81 1.3(13) . . . . ?
 N19 C96 C95 C91 -179.2(8) . . . . ?
 N19 C96 C95 C94 -0.6(13) . . . . ?
 N18 C89 C88 C87 0.6(17) . . . . ?
 N21 C79 C80 C81 1.0(15) . . . . ?
 N14 C13 C14 C18 175.7(8) . . . . ?
 N14 C13 C14 C15 -3.2(14) . . . . ?
 N14 C13 C24 N13 -1.2(14) . . . . ?
 N14 C13 C24 C23 -177.2(8) . . . . ?
 N14 C12 C4 C5 -179.9(8) . . . . ?
 N14 C12 C4 C3 2.7(13) . . . . ?
 N14 C12 C11 N13 0.4(14) . . . . ?
 N14 C12 C11 C10 178.3(8) . . . . ?
 O6 S2 C207 F7 177.3(8) . . . . ?
 O6 S2 C207 F9 -59.7(9) . . . . ?
 O6 S2 C207 F8 57.4(9) . . . . ?
 N22 C77 C76 C84 179.1(9) . . . . ?
 N22 C77 C76 C75 -1.4(15) . . . . ?
 N22 C77 C78 N21 -5.1(13) . . . . ?
 N22 C77 C78 C82 177.7(8) . . . . ?
 O12 S5 C206 F11 61.9(10) . . . . ?
 O12 S5 C206 F12 179.8(10) . . . . ?
 O12 S5 C206 F10 -56.7(13) . . . . ?
 O4 S2 C207 F7 57.2(10) . . . . ?
 O4 S2 C207 F9 -179.8(8) . . . . ?
 O4 S2 C207 F8 -62.7(9) . . . . ?
 N9 C47 C48 C44 1.8(14) . . . . ?
 N1 C166 C167 C171 178.6(7) . . . . ?
 N1 C166 C167 C168 -0.9(12) . . . . ?
 N1 C166 C165 N2 -1.5(11) . . . . ?
 N1 C166 C165 C164 -178.4(7) . . . . ?
 N6 C179 C175 C174 177.4(9) . . . . ?
 N6 C179 C175 C176 -3.8(15) . . . . ?
 N6 C179 C180 N5 2.4(12) . . . . ?
 N6 C179 C180 C048 -175.0(9) . . . . ?
 N6 C178 C177 C176 -1.4(16) . . . . ?
 N24 C119 C120 C116 6.7(15) . . . . ?
 N23 C101 C100 C99 -3.1(15) . . . . ?
 O25 S7 C212 F26 -64.2(10) . . . . ?
 O25 S7 C212 F27 177.9(10) . . . . ?
 O25 S7 C212 F25 55.4(10) . . . . ?
 O11 S5 C206 F11 -175.7(9) . . . . ?
 O11 S5 C206 F12 -57.8(12) . . . . ?
 O11 S5 C206 F10 65.8(12) . . . . ?
 O21 S1 C210 F30 -62.2(11) . . . . ?
 O21 S1 C210 F28 56.4(13) . . . . ?
 O21 S1 C210 F29 176.0(9) . . . . ?
 N12 C18 C14 C13 -176.7(9) . . . . ?
 N12 C18 C14 C15 2.2(14) . . . . ?
 N12 C18 C19 N11 -2.4(12) . . . . ?
 N12 C18 C19 C23 177.5(9) . . . . ?
 N12 C17 C16 C15 4.7(14) . . . . ?
 N13 C24 C23 C19 -176.1(9) . . . . ?
 N13 C24 C23 C22 5.4(14) . . . . ?
 N3 C171 C172 N4 -0.3(13) . . . . ?
 N3 C171 C172 C164 -178.8(8) . . . . ?
 N8 C71 C72 C68 2.2(16) . . . . ?
 N8 C70 C69 C68 -3.1(18) . . . . ?
 N4 C173 C048 C180 -179.5(8) . . . . ?
 N4 C173 C048 C183 -0.5(13) . . . . ?
 N4 C173 C174 N3 -0.5(14) . . . . ?
 N4 C173 C174 C175 -178.3(9) . . . . ?
 N4 C172 C164 C165 177.5(8) . . . . ?
 N4 C172 C164 C163 -0.4(13) . . . . ?
 N20 C85 C96 N19 -0.2(14) . . . . ?
 N20 C85 C96 C95 175.6(8) . . . . ?
 N20 C85 C86 C87 -1.9(14) . . . . ?
 N20 C85 C86 C90 -178.1(9) . . . . ?
 N20 C84 C76 C77 -175.0(9) . . . . ?
 N20 C84 C76 C75 5.5(14) . . . . ?
 C83 N19 C96 C85 -3.5(13) . . . . ?
 C83 N19 C96 C95 -179.1(8) . . . . ?
 C83 C84 C76 C77 3.9(14) . . . . ?
 C83 C84 C76 C75 -175.6(9) . . . . ?
 C83 C82 C78 N21 -174.1(8) . . . . ?
 C83 C82 C78 C77 2.7(13) . . . . ?
 C83 C82 C81 C80 175.8(9) . . . . ?
 O26 S7 C212 F26 173.4(8) . . . . ?
 O26 S7 C212 F27 55.5(12) . . . . ?
 O26 S7 C212 F25 -67.0(10) . . . . ?
 N2 C165 C164 C172 -175.5(8) . . . . ?
 N2 C165 C164 C163 2.5(13) . . . . ?
 C85 N20 C84 C83 0.9(14) . . . . ?
 C85 N20 C84 C76 179.8(8) . . . . ?
 C85 C96 C95 C91 5.1(13) . . . . ?
 C85 C96 C95 C94 -176.3(8) . . . . ?
 C85 C86 C87 C88 -178.6(10) . . . . ?
 C85 C86 C90 N18 177.7(9) . . . . ?
 C85 C86 C90 C91 0.4(14) . . . . ?
 C91 N17 C92 C93 -2.0(13) . . . . ?
 C91 C95 C94 C93 -0.9(14) . . . . ?
 C96 N19 C83 C84 5.7(13) . . . . ?
 C96 N19 C83 C82 -175.8(8) . . . . ?
 C96 C85 C86 C87 -179.6(9) . . . . ?
 C96 C85 C86 C90 4.2(14) . . . . ?
 C96 C95 C94 C93 -179.6(9) . . . . ?
 O19 S1 C210 F30 178.8(10) . . . . ?
 O19 S1 C210 F28 -62.6(13) . . . . ?
 O19 S1 C210 F29 57.0(11) . . . . ?
 O18 S4 C204 F17 -54.5(11) . . . . ?
 O18 S4 C204 F16 62.9(13) . . . . ?
 O18 S4 C204 F18 -172.5(12) . . . . ?
 O10 S5 C206 F11 -57.0(10) . . . . ?
 O10 S5 C206 F12 60.9(12) . . . . ?
 O10 S5 C206 F10 -175.5(11) . . . . ?
 C18 N12 C17 C16 -1.1(14) . . . . ?
 C18 C14 C15 C16 1.3(13) . . . . ?
 C18 C19 C23 C24 0.7(13) . . . . ?
 C18 C19 C23 C22 179.3(9) . . . . ?
 C71 N8 C70 C69 3.5(16) . . . . ?
 C71 C72 C68 C67 178.1(9) . . . . ?
 C71 C72 C68 C69 -1.4(14) . . . . ?
 C1 N16 C5 C6 -178.4(8) . . . . ?
 C1 N16 C5 C4 1.9(13) . . . . ?
 C1 C2 C3 C4 -2.1(15) . . . . ?
 C116 C117 C118 N24 4.9(16) . . . . ?
 C116 C115 C114 C113 178.0(9) . . . . ?
 C13 N14 C12 C4 178.8(8) . . . . ?
 C13 N14 C12 C11 0.0(13) . . . . ?
 C13 C14 C15 C16 -179.8(9) . . . . ?
 C13 C24 C23 C19 0.1(14) . . . . ?
 C13 C24 C23 C22 -178.4(9) . . . . ?
 C14 C18 C19 N11 177.8(8) . . . . ?
 C14 C18 C19 C23 -2.3(13) . . . . ?
 C14 C13 C24 N13 176.7(9) . . . . ?
 C14 C13 C24 C23 0.7(13) . . . . ?
 C14 C15 C16 C17 -4.7(14) . . . . ?
 C173 N4 C172 C171 -1.7(12) . . . . ?
 C173 N4 C172 C164 176.9(8) . . . . ?
 C173 C048 C180 N5 -178.2(8) . . . . ?
 C173 C048 C180 C179 -1.0(13) . . . . ?
 C173 C048 C183 C182 -179.8(9) . . . . ?
 C84 N20 C85 C96 1.4(14) . . . . ?
 C84 N20 C85 C86 -176.2(9) . . . . ?
 C84 C83 C82 C78 -1.3(13) . . . . ?
 C84 C83 C82 C81 179.7(9) . . . . ?
 C84 C76 C75 C74 179.1(9) . . . . ?
 C166 N1 C170 C169 -1.9(14) . . . . ?
 C166 C167 C171 N3 -178.9(8) . . . . ?
 C166 C167 C171 C172 -1.7(12) . . . . ?
 C166 C167 C168 C169 1.5(13) . . . . ?
 C166 C165 C164 C172 1.3(12) . . . . ?
 C166 C165 C164 C163 179.3(8) . . . . ?
 O17 S4 C204 F17 -174.9(10) . . . . ?
 O17 S4 C204 F16 -57.5(13) . . . . ?
 O17 S4 C204 F18 67.1(13) . . . . ?
 C188 C187 C186 Rh5 -59.6(7) . . . . ?
 C188 C187 C186 C185 3.2(11) . . . . ?
 C188 C187 C186 C191 175.7(10) . . . . ?
 C188 C184 C185 Rh5 59.1(7) . . . . ?
 C188 C184 C185 C186 -0.6(12) . . . . ?
 C188 C184 C185 C190 -179.3(9) . . . . ?
 C12 N14 C13 C14 -177.6(8) . . . . ?
 C12 N14 C13 C24 0.3(13) . . . . ?
 C12 C4 C3 C2 178.0(9) . . . . ?
 C119 N24 C118 C117 -7.0(15) . . . . ?
 C56 C55 C54 C51 -177.3(9) . . . . ?
 C56 C61 C62 C63 -179.1(10) . . . . ?
 C56 C61 C60 C65 178.7(9) . . . . ?
 C56 C61 C60 C59 5.0(15) . . . . ?
 C108 C109 C104 C105 -1.6(15) . . . . ?
 C108 C109 C104 C103 176.9(10) . . . . ?
 C108 C109 C110 C111 2.1(17) . . . . ?
 C108 C113 C114 C115 -173.3(9) . . . . ?
 C108 C113 C112 C111 4.3(16) . . . . ?
 C108 C107 C106 C105 0.5(16) . . . . ?
 C66 C65 C64 C63 -178.3(10) . . . . ?
 C66 C65 C60 C61 178.0(9) . . . . ?
 C66 C65 C60 C59 -8.9(16) . . . . ?
 C66 C67 C68 C72 -8.4(17) . . . . ?
 C66 C67 C68 C69 171.1(12) . . . . ?
 C109 C108 C113 C114 178.0(9) . . . . ?
 C109 C108 C113 C112 -4.8(14) . . . . ?
 C109 C108 C107 C106 -0.6(15) . . . . ?
 C109 C104 C105 C106 1.7(17) . . . . ?
 C109 C104 C103 C102 157.4(11) . . . . ?
 C109 C110 C111 C112 -2.7(17) . . . . ?
 C167 C166 C165 N2 178.0(8) . . . . ?
 C167 C166 C165 C164 1.1(12) . . . . ?
 C167 C171 C172 N4 -177.4(8) . . . . ?
 C167 C171 C172 C164 4.0(13) . . . . ?
 C167 C168 C169 C170 -2.3(14) . . . . ?
 C24 N13 C11 C12 -1.2(13) . . . . ?
 C24 N13 C11 C10 -179.1(8) . . . . ?
 C24 C13 C14 C18 -2.3(13) . . . . ?
 C24 C13 C14 C15 178.9(9) . . . . ?
 C24 C23 C22 C21 177.7(9) . . . . ?
 O20 S1 C210 F30 58.0(12) . . . . ?
 O20 S1 C210 F28 176.7(11) . . . . ?
 O20 S1 C210 F29 -63.7(11) . . . . ?
 C171 N3 C174 C173 -1.6(13) . . . . ?
 C171 N3 C174 C175 176.2(9) . . . . ?
 C171 C167 C168 C169 -178.0(8) . . . . ?
 C171 C172 C164 C165 -3.8(12) . . . . ?
 C171 C172 C164 C163 178.3(8) . . . . ?
 C95 C91 C90 N18 -179.8(8) . . . . ?
 C95 C91 C90 C86 -2.3(13) . . . . ?
 C86 C85 C96 N19 177.5(9) . . . . ?
 C86 C85 C96 C95 -6.8(13) . . . . ?
 C86 C87 C88 C89 1.4(16) . . . . ?
 C10 C6 C5 N16 178.3(8) . . . . ?
 C10 C6 C5 C4 -2.1(14) . . . . ?
 C10 C9 C8 C7 0.8(15) . . . . ?
 C19 N11 C20 C21 -1.0(13) . . . . ?
 C19 C18 C14 C13 3.1(13) . . . . ?
 C19 C18 C14 C15 -178.0(8) . . . . ?
 C19 C23 C22 C21 -0.8(15) . . . . ?
 O27 S7 C212 F26 54.9(9) . . . . ?
 O27 S7 C212 F27 -63.0(12) . . . . ?
 O27 S7 C212 F25 174.5(9) . . . . ?
 C65 C66 C67 C68 -177.4(10) . . . . ?
 C65 C60 C59 C58 178.3(11) . . . . ?
 C172 N4 C173 C048 177.3(7) . . . . ?
 C172 N4 C173 C174 2.1(13) . . . . ?
 C172 C164 C163 C162 177.4(9) . . . . ?
 C89 N18 C90 C91 177.9(8) . . . . ?
 C89 N18 C90 C86 0.5(13) . . . . ?
 C6 N15 C7 C8 0.3(14) . . . . ?
 C6 C10 C9 C8 -0.5(15) . . . . ?
 C6 C10 C11 N13 178.7(8) . . . . ?
 C6 C10 C11 C12 0.7(13) . . . . ?
 C6 C5 C4 C12 2.3(13) . . . . ?
 C6 C5 C4 C3 179.9(8) . . . . ?
 C165 N2 C161 C162 1.5(16) . . . . ?
 C165 C166 C167 C171 -0.9(12) . . . . ?
 C165 C166 C167 C168 179.6(8) . . . . ?
 C165 C164 C163 C162 -0.6(13) . . . . ?
 C77 N22 C73 C74 2.7(15) . . . . ?
 C77 C76 C75 C74 -0.4(14) . . . . ?
 C124 C125 C121 Rh4 60.1(6) . . . . ?
 C124 C125 C121 C122 -0.5(10) . . . . ?
 C124 C125 C121 C126 -179.4(9) . . . . ?
 C124 C123 C122 Rh4 -59.1(6) . . . . ?
 C124 C123 C122 C121 2.0(11) . . . . ?
 C124 C123 C122 C127 178.1(9) . . . . ?
 C47 N9 C46 C45 5.0(13) . . . . ?
 C47 C48 C44 C43 -179.6(8) . . . . ?
 C47 C48 C44 C45 2.5(13) . . . . ?
 C179 N6 C178 C177 0.6(14) . . . . ?
 C179 C175 C174 N3 178.2(9) . . . . ?
 C179 C175 C174 C173 -4.0(14) . . . . ?
 C179 C175 C176 C177 2.7(15) . . . . ?
 C125 C124 C123 Rh4 -62.9(6) . . . . ?
 C125 C124 C123 C122 -2.3(11) . . . . ?
 C125 C124 C123 C128 172.8(9) . . . . ?
 C125 C121 C122 Rh4 60.7(6) . . . . ?
 C125 C121 C122 C123 -0.9(11) . . . . ?
 C125 C121 C122 C127 -177.0(9) . . . . ?
 C37 C36 C41 C40 -3.3(13) . . . . ?
 C37 C36 C41 C42 176.7(8) . . . . ?
 C37 C36 C35 C34 1.0(14) . . . . ?
 C37 C32 C31 C30 158.6(10) . . . . ?
 C37 C32 C33 C34 3.4(16) . . . . ?
 C37 C38 C39 C40 -0.2(16) . . . . ?
 C36 C37 C32 C31 175.5(9) . . . . ?
 C36 C37 C32 C33 -2.9(14) . . . . ?
 C36 C37 C38 C39 -3.2(15) . . . . ?
 C36 C41 C40 C39 -0.1(15) . . . . ?
 C36 C41 C42 C43 -163.4(9) . . . . ?
 C36 C35 C34 C33 -0.6(16) . . . . ?
 C9 C10 C6 N15 0.0(13) . . . . ?
 C9 C10 C6 C5 -178.2(9) . . . . ?
 C9 C10 C11 N13 -2.6(14) . . . . ?
 C9 C10 C11 C12 179.4(9) . . . . ?
 C134 C135 C131 Rh3 62.0(7) . . . . ?
 C134 C135 C131 C132 3.2(11) . . . . ?
 C134 C135 C131 C136 -178.3(10) . . . . ?
 C134 C133 C132 Rh3 -58.9(7) . . . . ?
 C134 C133 C132 C137 177.2(10) . . . . ?
 C134 C133 C132 C131 4.9(11) . . . . ?
 C164 C163 C162 C161 -0.8(16) . . . . ?
 C175 C179 C180 N5 -178.9(8) . . . . ?
 C175 C179 C180 C048 3.7(13) . . . . ?
 C175 C176 C177 C178 -0.4(16) . . . . ?
 C5 N16 C1 C2 -3.6(14) . . . . ?
 C5 C4 C3 C2 0.5(13) . . . . ?
 C17 N12 C18 C14 -2.3(14) . . . . ?
 C17 N12 C18 C19 177.9(8) . . . . ?
 C154 C153 C152 Rh1 -59.1(8) . . . . ?
 C154 C153 C152 C151 3.8(13) . . . . ?
 C154 C153 C152 C157 173.5(11) . . . . ?
 C154 C155 C151 Rh1 59.1(8) . . . . ?
 C154 C155 C151 C152 -1.1(13) . . . . ?
 C154 C155 C151 C156 -179.9(11) . . . . ?
 C168 C167 C171 N3 0.5(13) . . . . ?
 C168 C167 C171 C172 177.8(8) . . . . ?
 C168 C169 C170 N1 2.5(14) . . . . ?
 C4 C12 C11 N13 -178.3(8) . . . . ?
 C4 C12 C11 C10 -0.4(13) . . . . ?
 C55 C56 C61 C62 -5.0(16) . . . . ?
 C55 C56 C61 C60 176.0(9) . . . . ?
 C55 C56 C57 C58 -178.2(10) . . . . ?
 F19 C211 S8 O28 -55.0(7) . . . . ?
 F19 C211 S8 O30 65.1(7) . . . . ?
 F19 C211 S8 O29 -176.5(6) . . . . ?
 C82 C83 C84 N20 176.9(9) . . . . ?
 C82 C83 C84 C76 -2.0(13) . . . . ?
 C82 C81 C80 C79 0.5(14) . . . . ?
 C11 N13 C24 C13 1.5(13) . . . . ?
 C11 N13 C24 C23 177.6(8) . . . . ?
 C11 C12 C4 C5 -1.1(13) . . . . ?
 C11 C12 C4 C3 -178.6(9) . . . . ?
 C11 C10 C6 N15 178.8(8) . . . . ?
 C11 C10 C6 C5 0.5(13) . . . . ?
 C11 C10 C9 C8 -179.1(9) . . . . ?
 C94 C93 C92 N17 2.0(16) . . . . ?
 C67 C66 C65 C64 -23.4(16) . . . . ?
 C67 C66 C65 C60 160.1(11) . . . . ?
 C67 C68 C69 C70 -177.6(11) . . . . ?
 C113 C108 C109 C104 -177.7(9) . . . . ?
 C113 C108 C109 C110 1.7(14) . . . . ?
 C113 C108 C107 C106 178.2(10) . . . . ?
 C113 C112 C111 C110 -0.6(17) . . . . ?
 C87 C86 C90 N18 1.3(14) . . . . ?
 C87 C86 C90 C91 -176.0(8) . . . . ?
 C76 C77 C78 N21 176.3(9) . . . . ?
 C76 C77 C78 C82 -0.8(14) . . . . ?
 C30 C27 C28 C29 -177.9(10) . . . . ?
 C30 C27 C26 C25 178.0(9) . . . . ?
 C79 N21 C78 C77 179.5(8) . . . . ?
 C79 N21 C78 C82 -3.5(13) . . . . ?
 C23 C22 C21 C20 1.5(16) . . . . ?
 C187 C188 C184 Rh5 62.5(7) . . . . ?
 C187 C188 C184 C189 -174.8(9) . . . . ?
 C187 C188 C184 C185 2.6(12) . . . . ?
 C187 C186 C185 Rh5 -62.8(6) . . . . ?
 C187 C186 C185 C184 -1.6(11) . . . . ?
 C187 C186 C185 C190 177.1(10) . . . . ?
 C120 C116 C117 C118 3.1(14) . . . . ?
 C120 C116 C115 C114 -179.1(10) . . . . ?
 C78 N21 C79 C80 0.4(13) . . . . ?
 C78 C77 C76 C84 -2.5(14) . . . . ?
 C78 C77 C76 C75 177.0(9) . . . . ?
 C78 C82 C81 C80 -3.2(13) . . . . ?
 C123 C124 C125 Rh4 62.8(6) . . . . ?
 C123 C124 C125 C121 1.6(10) . . . . ?
 C123 C124 C125 C130 -174.1(9) . . . . ?
 C41 C36 C35 C34 179.8(9) . . . . ?
 C41 C40 C39 C38 2.0(16) . . . . ?
 C51 C52 C53 N7 1.1(15) . . . . ?
 C27 C30 C31 C32 -179.1(9) . . . . ?
 C27 C28 C29 N10 -1.3(17) . . . . ?
 C25 N10 C29 C28 1.9(15) . . . . ?
 C61 C56 C55 C54 -163.3(10) . . . . ?
 C61 C56 C57 C58 -2.3(16) . . . . ?
 C61 C60 C59 C58 -8.3(17) . . . . ?
 C7 N15 C6 C10 0.0(13) . . . . ?
 C7 N15 C6 C5 178.4(8) . . . . ?
 C32 C37 C36 C41 -178.0(9) . . . . ?
 C32 C37 C36 C35 0.8(14) . . . . ?
 C32 C37 C38 C39 179.7(10) . . . . ?
 C32 C33 C34 C35 -1.7(17) . . . . ?
 C202 C197 C196 Rh6 123.2(11) . . . . ?
 C202 C197 C196 C195 -174.0(10) . . . . ?
 C202 C197 C196 C201 -1.6(17) . . . . ?
 C202 C197 C198 Rh6 -124.4(12) . . . . ?
 C202 C197 C198 C194 175.1(10) . . . . ?
 C202 C197 C198 C203 -6.5(18) . . . . ?
 C64 C63 C62 C61 -0.4(18) . . . . ?
 C64 C65 C60 C61 1.3(15) . . . . ?
 C64 C65 C60 C59 174.5(11) . . . . ?
 C90 N18 C89 C88 -1.5(14) . . . . ?
 C90 C91 C95 C96 -0.5(13) . . . . ?
 C90 C91 C95 C94 -179.2(8) . . . . ?
 C90 C86 C87 C88 -2.2(15) . . . . ?
 C048 C173 C174 N3 -175.4(8) . . . . ?
 C048 C173 C174 C175 6.7(13) . . . . ?
 C72 C68 C69 C70 1.9(16) . . . . ?
 C104 C109 C110 C111 -178.4(11) . . . . ?
 C104 C103 C102 C99 -177.5(11) . . . . ?
 C44 C43 C42 C41 177.9(8) . . . . ?
 C44 C45 C46 N9 -0.9(14) . . . . ?
 C101 N23 C97 C98 -1.5(17) . . . . ?
 C101 C100 C99 C102 178.6(10) . . . . ?
 C101 C100 C99 C98 1.7(15) . . . . ?
 C117 C116 C120 C119 -8.4(14) . . . . ?
 C117 C116 C115 C114 1.3(16) . . . . ?
 C52 C51 C54 C55 177.6(9) . . . . ?
 C52 C51 C50 C49 -1.2(14) . . . . ?
 C28 C27 C26 C25 -0.3(14) . . . . ?
 C54 C51 C52 C53 175.8(9) . . . . ?
 C54 C51 C50 C49 -178.0(9) . . . . ?
 C135 C134 C133 Rh3 -61.4(6) . . . . ?
 C135 C134 C133 C132 -2.8(11) . . . . ?
 C135 C134 C133 C138 176.7(9) . . . . ?
 C174 N3 C171 C167 179.2(8) . . . . ?
 C174 N3 C171 C172 2.0(13) . . . . ?
 C174 C173 C048 C180 -4.2(13) . . . . ?
 C174 C173 C048 C183 174.8(9) . . . . ?
 C174 C175 C176 C177 -178.5(10) . . . . ?
 C153 C154 C155 Rh1 63.8(8) . . . . ?
 C153 C154 C155 C151 3.4(13) . . . . ?
 C153 C154 C155 C160 -178.1(11) . . . . ?
 C153 C152 C151 Rh1 -63.0(8) . . . . ?
 C153 C152 C151 C155 -1.7(14) . . . . ?
 C153 C152 C151 C156 177.2(11) . . . . ?
 C31 C30 C27 C28 169.8(10) . . . . ?
 C31 C30 C27 C26 -8.4(16) . . . . ?
 C31 C32 C33 C34 -175.1(10) . . . . ?
 C33 C32 C31 C30 -23.0(16) . . . . ?
 C92 N17 C91 C95 0.5(13) . . . . ?
 C92 N17 C91 C90 -179.4(8) . . . . ?
 C92 C93 C94 C95 -0.4(15) . . . . ?
 C133 C134 C135 Rh3 61.7(6) . . . . ?
 C133 C134 C135 C140 -172.2(9) . . . . ?
 C133 C134 C135 C131 -0.4(10) . . . . ?
 C133 C132 C131 Rh3 -64.0(7) . . . . ?
 C133 C132 C131 C135 -4.9(11) . . . . ?
 C133 C132 C131 C136 176.5(9) . . . . ?
 C29 N10 C25 C26 -1.8(14) . . . . ?
 C46 N9 C47 C48 -5.6(13) . . . . ?
 C46 C45 C44 C48 -3.0(13) . . . . ?
 C46 C45 C44 C43 179.0(8) . . . . ?
 C53 N7 C49 C50 -4.3(15) . . . . ?
 C35 C36 C41 C40 177.8(9) . . . . ?
 C35 C36 C41 C42 -2.1(14) . . . . ?
 C170 N1 C166 C167 1.1(12) . . . . ?
 C170 N1 C166 C165 -179.4(8) . . . . ?
 C115 C116 C120 C119 172.0(9) . . . . ?
 C115 C116 C117 C118 -177.3(10) . . . . ?
 C178 N6 C179 C175 2.1(14) . . . . ?
 C178 N6 C179 C180 -179.3(8) . . . . ?
 C184 C188 C187 Rh5 -63.0(7) . . . . ?
 C184 C188 C187 C186 -3.6(11) . . . . ?
 C184 C188 C187 C192 173.6(9) . . . . ?
 C38 C37 C36 C41 4.9(13) . . . . ?
 C38 C37 C36 C35 -176.2(9) . . . . ?
 C38 C37 C32 C31 -7.4(15) . . . . ?
 C38 C37 C32 C33 174.1(10) . . . . ?
 C197 C196 C195 Rh6 -61.1(6) . . . . ?
 C197 C196 C195 C194 -1.6(11) . . . . ?
 C197 C196 C195 C200 177.5(10) . . . . ?
 C100 C99 C102 C103 -10.3(17) . . . . ?
 C100 C99 C98 C97 -0.4(16) . . . . ?
 O16 S4 C204 F17 65.9(12) . . . . ?
 O16 S4 C204 F16 -176.8(12) . . . . ?
 O16 S4 C204 F18 -52.1(14) . . . . ?
 C62 C63 C64 C65 1.4(17) . . . . ?
 C62 C61 C60 C65 -0.4(15) . . . . ?
 C62 C61 C60 C59 -174.0(10) . . . . ?
 C81 C82 C78 N21 4.9(14) . . . . ?
 C81 C82 C78 C77 -178.2(8) . . . . ?
 C20 N11 C19 C18 -178.4(8) . . . . ?
 C20 N11 C19 C23 1.7(12) . . . . ?
 C60 C65 C64 C63 -1.8(16) . . . . ?
 C60 C61 C62 C63 0.0(16) . . . . ?
 C180 N5 C181 C182 1.0(14) . . . . ?
 C180 C179 C175 C174 -1.1(13) . . . . ?
 C180 C179 C175 C176 177.7(8) . . . . ?
 C180 C048 C183 C182 -0.9(15) . . . . ?
 C49 N7 C53 C52 1.7(14) . . . . ?
 C40 C41 C42 C43 16.6(14) . . . . ?
 C26 C27 C28 C29 0.4(15) . . . . ?
 C75 C74 C73 N22 -4.4(16) . . . . ?
 C163 C162 C161 N2 0.4(18) . . . . ?
 C107 C108 C109 C104 1.1(14) . . . . ?
 C107 C108 C109 C110 -179.5(10) . . . . ?
 C107 C108 C113 C114 -0.8(15) . . . . ?
 C107 C108 C113 C112 176.4(9) . . . . ?
 C107 C106 C105 C104 -1.2(17) . . . . ?
 C114 C113 C112 C111 -178.4(10) . . . . ?
 C42 C43 C44 C48 -0.4(15) . . . . ?
 C42 C43 C44 C45 177.4(9) . . . . ?
 C42 C41 C40 C39 179.8(9) . . . . ?
 C189 C184 C185 Rh5 -123.7(10) . . . . ?
 C189 C184 C185 C186 176.6(9) . . . . ?
 C189 C184 C185 C190 -2.1(17) . . . . ?
 C118 N24 C119 C120 1.2(14) . . . . ?
 C196 C197 C198 Rh6 61.5(7) . . . . ?
 C196 C197 C198 C194 1.0(12) . . . . ?
 C196 C197 C198 C203 179.4(10) . . . . ?
 C198 C194 C195 Rh6 61.4(7) . . . . ?
 C198 C194 C195 C196 2.2(12) . . . . ?
 C198 C194 C195 C200 -176.8(11) . . . . ?
 C198 C197 C196 Rh6 -62.4(7) . . . . ?
 C198 C197 C196 C195 0.4(11) . . . . ?
 C198 C197 C196 C201 172.8(11) . . . . ?
 C129 C124 C125 Rh4 -121.9(10) . . . . ?
 C129 C124 C125 C121 176.9(9) . . . . ?
 C129 C124 C125 C130 1.2(16) . . . . ?
 C129 C124 C123 Rh4 121.6(9) . . . . ?
 C129 C124 C123 C122 -177.7(9) . . . . ?
 C129 C124 C123 C128 -2.6(15) . . . . ?
 C99 C98 C97 N23 0.4(18) . . . . ?
 C59 C58 C57 C56 -0.7(18) . . . . ?
 C73 N22 C77 C76 0.2(15) . . . . ?
 C73 N22 C77 C78 -178.3(9) . . . . ?
 C73 C74 C75 C76 3.1(15) . . . . ?
 C105 C104 C103 C102 -24.2(19) . . . . ?
 C130 C125 C121 Rh4 -124.0(9) . . . . ?
 C130 C125 C121 C122 175.5(9) . . . . ?
 C130 C125 C121 C126 -3.4(15) . . . . ?
 C112 C113 C114 C115 9.5(16) . . . . ?
 C50 C51 C52 C53 -1.2(14) . . . . ?
 C50 C51 C54 C55 -5.6(16) . . . . ?
 C140 C135 C131 Rh3 -126.0(10) . . . . ?
 C140 C135 C131 C132 175.3(9) . . . . ?
 C140 C135 C131 C136 -6.3(16) . . . . ?
 C70 N8 C71 C72 -3.2(16) . . . . ?
 C110 C109 C104 C105 178.9(11) . . . . ?
 C110 C109 C104 C103 -2.6(16) . . . . ?
 C57 C56 C55 C54 12.5(15) . . . . ?
 C57 C56 C61 C62 179.0(10) . . . . ?
 C57 C56 C61 C60 0.0(15) . . . . ?
 C57 C58 C59 C60 6.3(18) . . . . ?
 C183 C048 C180 N5 2.7(14) . . . . ?
 C183 C048 C180 C179 -180.0(9) . . . . ?
 C183 C182 C181 N5 0.8(16) . . . . ?
 C155 C154 C153 Rh1 -64.1(7) . . . . ?
 C155 C154 C153 C152 -4.5(13) . . . . ?
 C155 C154 C153 C158 175.0(11) . . . . ?
 C181 N5 C180 C179 179.8(8) . . . . ?
 C181 N5 C180 C048 -2.8(13) . . . . ?
 C181 C182 C183 C048 -0.8(16) . . . . ?
 C176 C175 C174 N3 -0.5(15) . . . . ?
 C176 C175 C174 C173 177.3(9) . . . . ?
 C193 C188 C187 Rh5 118.9(11) . . . . ?
 C193 C188 C187 C186 178.3(10) . . . . ?
 C193 C188 C187 C192 -4.5(17) . . . . ?
 C193 C188 C184 Rh5 -119.6(12) . . . . ?
 C193 C188 C184 C189 3.1(18) . . . . ?
 C193 C188 C184 C185 -179.5(11) . . . . ?
 C103 C104 C105 C106 -176.8(11) . . . . ?
 C192 C187 C186 Rh5 123.1(9) . . . . ?
 C192 C187 C186 C185 -174.0(9) . . . . ?
 C192 C187 C186 C191 -1.5(16) . . . . ?
 C102 C99 C98 C97 -177.6(11) . . . . ?
 C98 C99 C102 C103 166.5(11) . . . . ?
 C139 C134 C135 Rh3 -118.5(9) . . . . ?
 C139 C134 C135 C140 7.6(16) . . . . ?
 C139 C134 C135 C131 179.4(9) . . . . ?
 C139 C134 C133 Rh3 118.8(10) . . . . ?
 C139 C134 C133 C132 177.4(10) . . . . ?
 C139 C134 C133 C138 -3.1(15) . . . . ?
 O9 S3 C209 F3 175.9(17) . . . . ?
 O9 S3 C209 F2 64.6(15) . . . . ?
 O9 S3 C209 F1 -51.6(19) . . . . ?
 C159 C154 C153 Rh1 127.0(11) . . . . ?
 C159 C154 C153 C152 -173.4(11) . . . . ?
 C159 C154 C153 C158 6.2(19) . . . . ?
 C159 C154 C155 Rh1 -127.4(11) . . . . ?
 C159 C154 C155 C151 172.3(11) . . . . ?
 C159 C154 C155 C160 -9.3(18) . . . . ?
 O8 S3 C209 F3 53(2) . . . . ?
 O8 S3 C209 F2 -58.1(15) . . . . ?
 O8 S3 C209 F1 -174.3(16) . . . . ?
 C138 C133 C132 Rh3 121.7(11) . . . . ?
 C138 C133 C132 C137 -2.3(18) . . . . ?
 C138 C133 C132 C131 -174.5(10) . . . . ?
 C137 C132 C131 Rh3 123.0(10) . . . . ?
 C137 C132 C131 C135 -177.9(9) . . . . ?
 C137 C132 C131 C136 3.5(15) . . . . ?
 C144 C145 C141 Rh2 60.4(12) . . . . ?
 C144 C145 C141 C142 -3.3(17) . . . . ?
 C144 C145 C141 C146 -172.2(13) . . . . ?
 C128 C123 C122 Rh4 125.9(10) . . . . ?
 C128 C123 C122 C121 -173.0(9) . . . . ?
 C128 C123 C122 C127 3.1(16) . . . . ?
 C161 N2 C165 C166 -179.7(8) . . . . ?
 C161 N2 C165 C164 -2.9(13) . . . . ?
 O15 S6 C205 F14 -161.8(9) . . . . ?
 O15 S6 C205 F15 77.8(9) . . . . ?
 O15 S6 C205 F13 -41.7(10) . . . . ?
 C195 C194 C198 Rh6 -61.6(7) . . . . ?
 C195 C194 C198 C197 -2.0(12) . . . . ?
 C195 C194 C198 C203 179.8(10) . . . . ?
 C143 C142 C141 Rh2 -62.6(9) . . . . ?
 C143 C142 C141 C145 2.2(14) . . . . ?
 C143 C142 C141 C146 169.8(13) . . . . ?
 C143 C144 C145 Rh2 62.0(9) . . . . ?
 C143 C144 C145 C141 3.0(17) . . . . ?
 C143 C144 C145 C150 -175.1(12) . . . . ?
 C191 C186 C185 Rh5 124.5(10) . . . . ?
 C191 C186 C185 C184 -174.3(10) . . . . ?
 C191 C186 C185 C190 4.4(16) . . . . ?
 C97 N23 C101 C100 2.9(14) . . . . ?
 C199 C194 C198 Rh6 123.9(10) . . . . ?
 C199 C194 C198 C197 -176.5(10) . . . . ?
 C199 C194 C198 C203 5.2(18) . . . . ?
 C199 C194 C195 Rh6 -124.1(11) . . . . ?
 C199 C194 C195 C196 176.7(10) . . . . ?
 C199 C194 C195 C200 -2.3(18) . . . . ?
 C201 C196 C195 Rh6 126.7(12) . . . . ?
 C201 C196 C195 C194 -173.8(11) . . . . ?
 C201 C196 C195 C200 5.3(18) . . . . ?
 C145 C144 C143 Rh2 -62.5(10) . . . . ?
 C145 C144 C143 C142 -1.4(15) . . . . ?
 C145 C144 C143 C148 174.4(13) . . . . ?
 C126 C121 C122 Rh4 -120.4(10) . . . . ?
 C126 C121 C122 C123 178.0(9) . . . . ?
 C126 C121 C122 C127 1.9(16) . . . . ?
 C160 C155 C151 Rh1 -119.4(11) . . . . ?
 C160 C155 C151 C152 -179.6(11) . . . . ?
 C160 C155 C151 C156 1.6(19) . . . . ?
 C141 C142 C143 Rh2 60.6(8) . . . . ?
 C141 C142 C143 C144 -0.5(14) . . . . ?
 C141 C142 C143 C148 -176.4(11) . . . . ?
 F20 C211 S8 O28 179.8(8) . . . . ?
 F20 C211 S8 O30 -60.1(9) . . . . ?
 F20 C211 S8 O29 58.3(8) . . . . ?
 C158 C153 C152 Rh1 121.4(12) . . . . ?
 C158 C153 C152 C151 -175.7(11) . . . . ?
 C158 C153 C152 C157 -6.1(19) . . . . ?
 F21 C211 S8 O28 56.8(9) . . . . ?
 F21 C211 S8 O30 176.8(8) . . . . ?
 F21 C211 S8 O29 -64.8(8) . . . . ?
 C157 C152 C151 Rh1 127.5(14) . . . . ?
 C157 C152 C151 C155 -171.1(12) . . . . ?
 C157 C152 C151 C156 8(2) . . . . ?
 O14 S6 C205 F14 -44.5(10) . . . . ?
 O14 S6 C205 F15 -164.9(9) . . . . ?
 O14 S6 C205 F13 75.6(10) . . . . ?
 C147 C142 C143 Rh2 -121.2(13) . . . . ?
 C147 C142 C143 C144 177.7(13) . . . . ?
 C147 C142 C143 C148 2(2) . . . . ?
 C147 C142 C141 Rh2 119.2(13) . . . . ?
 C147 C142 C141 C145 -176.0(13) . . . . ?
 C147 C142 C141 C146 -8(2) . . . . ?
 C149 C144 C143 Rh2 123.0(15) . . . . ?
 C149 C144 C143 C142 -175.9(14) . . . . ?
 C149 C144 C143 C148 0(2) . . . . ?
 C149 C144 C145 Rh2 -124.0(18) . . . . ?
 C149 C144 C145 C141 177.1(15) . . . . ?
 C149 C144 C145 C150 -1(3) . . . . ?
 C150 C145 C141 Rh2 -121.9(17) . . . . ?
 C150 C145 C141 C142 174.4(15) . . . . ?
 C150 C145 C141 C146 6(2) . . . . ?
 O7 S3 C209 F3 -66.9(19) . . . . ?
 O7 S3 C209 F2 -178.2(12) . . . . ?
 O7 S3 C209 F1 65.7(18) . . . . ?
 O13 S6 C205 F14 77.7(10) . . . . ?
 O13 S6 C205 F15 -42.7(10) . . . . ?
 O13 S6 C205 F13 -162.2(10) . . . . ?

_smtbx_masks_special_details
;
A solvent mask was calculated and 1540 electrons were 
found in a volume of 4655Å³ in 1 void per unit cell. 
This is consistent with the presence of 
20[CF3SO3] per Asymmetric Unit 
which account for 1460 electrons 
per unit cell.
;
loop_
  _smtbx_masks_void_nr
  _smtbx_masks_void_average_x
  _smtbx_masks_void_average_y
  _smtbx_masks_void_average_z
  _smtbx_masks_void_volume
  _smtbx_masks_void_count_electrons
  _smtbx_masks_void_content
 1 -0.534 -0.386 -0.085 4655.1 1540.2 '20 CF3SO3'

_smtbx_masks_void_probe_radius     1.2
_smtbx_masks_void_truncation_radius  1.2
_olex2_submission_special_instructions  'No special instructions were received'

# start Validation Reply Form
_vrf_PLAT973_4
;
PROBLEM: Check Calcd Positive Resid. Density on       Rh3       2.10 eA-3  
RESPONSE: The large residual densities all locate around on heavy
Rh atoms in the range of 0.69-0.964 angstrom and the intensities (1.57-2.10
eA^-3) are all smaller than the 0.1*Z eA^-3 (Z = 45 for Rh). This should
originate from the absorption correction or Fourier truncation error.
;
# end Validation Reply Form
