data_sad_a _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C44 H67 N P2 Si2' _chemical_formula_weight 728.10 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.6755(4) _cell_length_b 15.1358(7) _cell_length_c 16.5849(8) _cell_angle_alpha 103.436(2) _cell_angle_beta 101.043(2) _cell_angle_gamma 107.284(2) _cell_volume 2165.04(17) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9747 _cell_measurement_theta_min 2.2645 _cell_measurement_theta_max 27.2835 _exptl_crystal_description 'block' _exptl_crystal_colour orange _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.117 _exptl_crystal_F_000 792 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.274 _exptl_crystal_size_mid 0.215 _exptl_crystal_size_min 0.112 _exptl_absorpt_coefficient_mu 0.185 _shelx_estimated_absorpt_T_min 0.951 _shelx_estimated_absorpt_T_max 0.980 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.7162 _exptl_absorpt_correction_T_max 0.7455 _exptl_absorpt_process_details 'SADABS-2016/2' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'INCOATEC Microsource' _diffrn_measurement_device_type 'PHOTON 3C7' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 135740 _diffrn_reflns_av_unetI/netI 0.0184 _diffrn_reflns_av_R_equivalents 0.0371 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_theta_min 1.315 _diffrn_reflns_theta_max 27.490 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 9906 _reflns_number_gt 8320 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX3 v2019.11-0' _computing_cell_refinement 'SAINT V8.40B' _computing_data_reduction 'SAINT V8.40B' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'XP Version 5.1' _computing_publication_material 'XP Version 5.1' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0514P)^2^+0.5655P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 9906 _refine_ls_number_parameters 479 _refine_ls_number_restraints 18 _refine_ls_R_factor_all 0.0461 _refine_ls_R_factor_gt 0.0369 _refine_ls_wR_factor_ref 0.1021 _refine_ls_wR_factor_gt 0.0972 _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_restrained_S_all 1.032 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N 0.20080(13) 0.25495(8) 0.60829(8) 0.0365(3) Uani 1 1 d . . . . . C1 C 0.73197(16) 0.48489(10) 0.81368(9) 0.0339(3) Uani 1 1 d . . . . . C6 C 0.87111(17) 0.47411(12) 0.83964(11) 0.0446(3) Uani 1 1 d . . . . . H6 H 0.960401 0.530159 0.864983 0.054 Uiso 1 1 calc R U . . . C7 C 0.25942(15) 0.35306(10) 0.65214(9) 0.0335(3) Uani 1 1 d . . . . . C8 C 0.14620(17) 0.39671(11) 0.61397(11) 0.0461(4) Uani 1 1 d . . . . . C9 C 0.2065(2) 0.44730(16) 0.55176(13) 0.0666(5) Uani 1 1 d . . . . . H9A H 0.231596 0.402288 0.509300 0.100 Uiso 1 1 calc R U . . . H9B H 0.297094 0.504587 0.584098 0.100 Uiso 1 1 calc R U . . . H9C H 0.129404 0.467566 0.521872 0.100 Uiso 1 1 calc R U . . . C10 C 0.1074(2) 0.46755(13) 0.67934(14) 0.0599(5) Uani 1 1 d . . . . . H10A H 0.022397 0.481695 0.649869 0.090 Uiso 1 1 calc R U . . . H10B H 0.195010 0.528017 0.706554 0.090 Uiso 1 1 calc R U . . . H10C H 0.079809 0.438501 0.723663 0.090 Uiso 1 1 calc R U . . . C11 C 0.0014(2) 0.30618(14) 0.56940(16) 0.0743(7) Uani 1 1 d . . . . . H11A H -0.064239 0.299606 0.608370 0.089 Uiso 1 1 calc R U . A 2 H11B H -0.055014 0.312880 0.516063 0.089 Uiso 1 1 calc R U . A 2 C12 C 0.04438(18) 0.21796(12) 0.54772(11) 0.0512(4) Uani 1 1 d . . . . . C15 C 0.28116(16) 0.18989(10) 0.61489(9) 0.0361(3) Uani 1 1 d . . . . . C16 C 0.26042(17) 0.13500(10) 0.67237(10) 0.0406(3) Uani 1 1 d . . . . . C17 C 0.3326(2) 0.06785(11) 0.67307(11) 0.0498(4) Uani 1 1 d . . . . . H17 H 0.316829 0.028529 0.709946 0.060 Uiso 1 1 calc R U . . . C18 C 0.4258(2) 0.05732(13) 0.62168(12) 0.0571(5) Uani 1 1 d . . . . . H18 H 0.473185 0.010754 0.622811 0.069 Uiso 1 1 calc R U . . . P1 P 0.72567(4) 0.60658(2) 0.82921(2) 0.03236(9) Uani 1 1 d . . . . . Si1 Si 0.49002(4) 0.59774(3) 0.76101(2) 0.03205(9) Uani 1 1 d . . . . . C20 C 0.4504(2) 0.11434(13) 0.56852(12) 0.0542(4) Uani 1 1 d . . . . . H20 H 0.517258 0.107651 0.534349 0.065 Uiso 1 1 calc R U . . . C21 C 0.37985(18) 0.18173(11) 0.56343(10) 0.0430(3) Uani 1 1 d . . . . . C22 C 0.4176(2) 0.24491(13) 0.50610(11) 0.0537(4) Uani 1 1 d . . . . . H22 H 0.347882 0.282158 0.504390 0.064 Uiso 1 1 calc R U . . . C23 C 0.5789(3) 0.31864(17) 0.54301(16) 0.0772(6) Uani 1 1 d . . . . . H23A H 0.649924 0.284086 0.545456 0.116 Uiso 1 1 calc R U . . . H23B H 0.591437 0.359086 0.601318 0.116 Uiso 1 1 calc R U . . . H23C H 0.598690 0.360021 0.505914 0.116 Uiso 1 1 calc R U . . . C24 C 0.3945(3) 0.18491(19) 0.41276(13) 0.0817(7) Uani 1 1 d . . . . . H24A H 0.292221 0.136158 0.390106 0.123 Uiso 1 1 calc R U . . . H24B H 0.468018 0.152199 0.411848 0.123 Uiso 1 1 calc R U . . . H24C H 0.408710 0.228128 0.376858 0.123 Uiso 1 1 calc R U . . . C25 C 0.1753(2) 0.15119(12) 0.73938(11) 0.0509(4) Uani 1 1 d . . . . . H25 H 0.128608 0.199947 0.729612 0.061 Uiso 1 1 calc R U . . . C26 C 0.0487(3) 0.05766(15) 0.73371(17) 0.0769(6) Uani 1 1 d . . . . . H26A H -0.022447 0.031125 0.675805 0.115 Uiso 1 1 calc R U . . . H26B H -0.004566 0.072796 0.776690 0.115 Uiso 1 1 calc R U . . . H26C H 0.092492 0.009614 0.745044 0.115 Uiso 1 1 calc R U . . . C27 C 0.2844(3) 0.19263(16) 0.83028(12) 0.0700(6) Uani 1 1 d . . . . . H27A H 0.335056 0.147238 0.840131 0.105 Uiso 1 1 calc R U . . . H27B H 0.228339 0.201935 0.872919 0.105 Uiso 1 1 calc R U . . . H27C H 0.359789 0.255272 0.836032 0.105 Uiso 1 1 calc R U . . . C28 C 0.43425(15) 0.65453(10) 0.86280(9) 0.0328(3) Uani 1 1 d . . . . . C29 C 0.35479(19) 0.59831(11) 0.90686(11) 0.0463(4) Uani 1 1 d . . . . . H29 H 0.328060 0.529698 0.887050 0.056 Uiso 1 1 calc R U . . . C30 C 0.3136(2) 0.63883(13) 0.97824(12) 0.0539(4) Uani 1 1 d . . . . . H30 H 0.259296 0.598212 1.006184 0.065 Uiso 1 1 calc R U . . . C31 C 0.3515(2) 0.73768(13) 1.00828(11) 0.0499(4) Uani 1 1 d . . . . . H31 H 0.327315 0.766171 1.058508 0.060 Uiso 1 1 calc R U . . . C32 C 0.42463(18) 0.79517(11) 0.96533(10) 0.0437(3) Uani 1 1 d . . . . . H32 H 0.448615 0.863491 0.985748 0.052 Uiso 1 1 calc R U . . . C33 C 0.46501(15) 0.75573(10) 0.89194(9) 0.0331(3) Uani 1 1 d . . . . . C34 C 0.6520(2) 0.95434(12) 0.91136(14) 0.0597(5) Uani 1 1 d . . . . . H34 H 0.579783 0.973122 0.941263 0.072 Uiso 1 1 calc R U . . . C35 C 0.7820(2) 0.95087(17) 0.97837(17) 0.0902(8) Uani 1 1 d . . . . . H35A H 0.853131 0.932292 0.949559 0.135 Uiso 1 1 calc R U . . . H35B H 0.741837 0.902966 1.006796 0.135 Uiso 1 1 calc R U . . . H35C H 0.833982 1.015147 1.021598 0.135 Uiso 1 1 calc R U . . . C36 C 0.7071(3) 1.02741(15) 0.8637(2) 0.1028(10) Uani 1 1 d . . . . . H36A H 0.768386 1.005325 0.828697 0.154 Uiso 1 1 calc R U . . . H36B H 0.768041 1.091291 0.905857 0.154 Uiso 1 1 calc R U . . . H36C H 0.620081 1.032325 0.826148 0.154 Uiso 1 1 calc R U . . . C37 C 0.3826(2) 0.84887(12) 0.76811(12) 0.0509(4) Uani 1 1 d . . . . . H37 H 0.420202 0.891873 0.733429 0.061 Uiso 1 1 calc R U . . . C38 C 0.2748(2) 0.75236(16) 0.70374(15) 0.0716(6) Uani 1 1 d . . . . . H38A H 0.194634 0.763302 0.665927 0.107 Uiso 1 1 calc R U . . . H38B H 0.230258 0.708870 0.734884 0.107 Uiso 1 1 calc R U . . . H38C H 0.329845 0.722624 0.668875 0.107 Uiso 1 1 calc R U . . . C39 C 0.2985(2) 0.89766(16) 0.82141(16) 0.0711(6) Uani 1 1 d . . . . . H39A H 0.214557 0.904294 0.782720 0.107 Uiso 1 1 calc R U . . . H39B H 0.367550 0.962193 0.859188 0.107 Uiso 1 1 calc R U . . . H39C H 0.259271 0.857886 0.856639 0.107 Uiso 1 1 calc R U . . . C40 C 0.86646(18) 0.66351(12) 0.77811(11) 0.0465(4) Uani 1 1 d . . . . . H40 H 0.966275 0.662261 0.806968 0.056 Uiso 1 1 calc R U . . . C41 C 0.8210(2) 0.60452(16) 0.68304(13) 0.0634(5) Uani 1 1 d . . . . . H41A H 0.725483 0.607581 0.653302 0.095 Uiso 1 1 calc R U . . . H41B H 0.808722 0.536656 0.678032 0.095 Uiso 1 1 calc R U . . . H41C H 0.899468 0.631414 0.656648 0.095 Uiso 1 1 calc R U . . . C42 C 0.8821(2) 0.76932(14) 0.78786(15) 0.0633(5) Uani 1 1 d . . . . . H42A H 0.954959 0.796876 0.758447 0.095 Uiso 1 1 calc R U . . . H42B H 0.917406 0.806947 0.849290 0.095 Uiso 1 1 calc R U . . . H42C H 0.783968 0.771926 0.762093 0.095 Uiso 1 1 calc R U . . . C43 C 0.79257(17) 0.67066(11) 0.94689(10) 0.0427(3) Uani 1 1 d . . . . . H43 H 0.753848 0.725448 0.956824 0.051 Uiso 1 1 calc R U . . . C44 C 0.9635(2) 0.71508(17) 0.98612(14) 0.0719(6) Uani 1 1 d . . . . . H44A H 1.004787 0.662998 0.983076 0.108 Uiso 1 1 calc R U . . . H44B H 0.987032 0.753687 1.046602 0.108 Uiso 1 1 calc R U . . . H44C H 1.008177 0.757044 0.953857 0.108 Uiso 1 1 calc R U . . . C45 C 0.7202(2) 0.60230(13) 0.99384(11) 0.0580(4) Uani 1 1 d . . . . . H45A H 0.610703 0.574965 0.968042 0.087 Uiso 1 1 calc R U . . . H45B H 0.743164 0.638450 1.054974 0.087 Uiso 1 1 calc R U . . . H45C H 0.760200 0.549499 0.988716 0.087 Uiso 1 1 calc R U . . . P2 P 0.55123(4) 0.83189(3) 0.82983(3) 0.03905(10) Uani 1 1 d . . . . . Si2 Si 0.41630(4) 0.42959(3) 0.74582(3) 0.03502(10) Uani 1 1 d . . . . . C2 C 0.59725(15) 0.40326(10) 0.77498(8) 0.0330(3) Uani 1 1 d . . . . . C3 C 0.61201(18) 0.31215(11) 0.76590(10) 0.0422(3) Uani 1 1 d . . . . . H3 H 0.524030 0.255174 0.740964 0.051 Uiso 1 1 calc R U . . . C4 C 0.7496(2) 0.30224(12) 0.79184(11) 0.0475(4) Uani 1 1 d . . . . . H4 H 0.754486 0.239177 0.784157 0.057 Uiso 1 1 calc R U . . . C5 C 0.87958(19) 0.38302(13) 0.82875(11) 0.0492(4) Uani 1 1 d . . . . . H5 H 0.974052 0.376017 0.846508 0.059 Uiso 1 1 calc R U . . . C13A C 0.0479(4) 0.1867(3) 0.45295(18) 0.0726(9) Uani 0.869(6) 1 d . U P B 1 H13A H -0.055491 0.157332 0.414868 0.109 Uiso 0.869(6) 1 calc R U P B 1 H13B H 0.098185 0.139147 0.445243 0.109 Uiso 0.869(6) 1 calc R U P B 1 H13C H 0.103234 0.243780 0.438524 0.109 Uiso 0.869(6) 1 calc R U P B 1 C14A C -0.0630(3) 0.1300(2) 0.5623(2) 0.0774(10) Uani 0.869(6) 1 d . U P B 1 H14A H -0.163597 0.110302 0.522589 0.116 Uiso 0.869(6) 1 calc R U P B 1 H14B H -0.068652 0.147247 0.622003 0.116 Uiso 0.869(6) 1 calc R U P B 1 H14C H -0.025708 0.076082 0.551675 0.116 Uiso 0.869(6) 1 calc R U P B 1 C13B C 0.015(3) 0.1391(18) 0.4725(17) 0.095(8) Uani 0.131(6) 1 d . U P B 2 H13D H -0.088601 0.120167 0.436845 0.142 Uiso 0.131(6) 1 calc R U P B 2 H13E H 0.028127 0.083714 0.489582 0.142 Uiso 0.131(6) 1 calc R U P B 2 H13F H 0.085506 0.159365 0.439227 0.142 Uiso 0.131(6) 1 calc R U P B 2 C14B C -0.0764(15) 0.1990(14) 0.6067(14) 0.074(6) Uani 0.131(6) 1 d . U P B 2 H14D H -0.177627 0.187929 0.572030 0.111 Uiso 0.131(6) 1 calc R U P B 2 H14E H -0.045084 0.256013 0.657684 0.111 Uiso 0.131(6) 1 calc R U P B 2 H14F H -0.077461 0.141736 0.624975 0.111 Uiso 0.131(6) 1 calc R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.0327(6) 0.0315(6) 0.0385(6) 0.0028(5) 0.0030(5) 0.0124(5) C1 0.0348(7) 0.0374(7) 0.0329(7) 0.0110(6) 0.0106(6) 0.0170(6) C6 0.0347(8) 0.0505(9) 0.0501(9) 0.0163(7) 0.0093(7) 0.0184(7) C7 0.0323(7) 0.0324(6) 0.0359(7) 0.0065(5) 0.0096(5) 0.0146(5) C8 0.0373(8) 0.0405(8) 0.0547(9) 0.0048(7) 0.0012(7) 0.0207(7) C9 0.0797(14) 0.0814(14) 0.0529(11) 0.0275(10) 0.0098(10) 0.0490(12) C10 0.0449(9) 0.0539(10) 0.0845(13) 0.0107(9) 0.0193(9) 0.0304(8) C11 0.0448(10) 0.0559(11) 0.0964(16) -0.0021(11) -0.0142(10) 0.0226(9) C12 0.0382(8) 0.0430(8) 0.0546(10) 0.0015(7) -0.0059(7) 0.0120(7) C15 0.0392(7) 0.0297(6) 0.0343(7) 0.0022(5) 0.0071(6) 0.0134(6) C16 0.0455(8) 0.0310(7) 0.0401(8) 0.0052(6) 0.0108(6) 0.0118(6) C17 0.0643(11) 0.0350(8) 0.0513(9) 0.0132(7) 0.0143(8) 0.0207(7) C18 0.0730(12) 0.0453(9) 0.0619(11) 0.0121(8) 0.0182(9) 0.0374(9) P1 0.02886(17) 0.03237(17) 0.03587(19) 0.01051(14) 0.01004(14) 0.01038(14) Si1 0.03313(19) 0.03024(18) 0.03396(19) 0.00780(15) 0.01027(15) 0.01407(15) C20 0.0650(11) 0.0553(10) 0.0541(10) 0.0116(8) 0.0252(9) 0.0369(9) C21 0.0496(9) 0.0425(8) 0.0379(8) 0.0069(6) 0.0132(7) 0.0215(7) C22 0.0674(11) 0.0597(10) 0.0483(9) 0.0199(8) 0.0289(8) 0.0323(9) C23 0.0796(15) 0.0796(15) 0.0809(15) 0.0335(12) 0.0419(13) 0.0214(12) C24 0.115(2) 0.0951(17) 0.0500(11) 0.0230(11) 0.0385(12) 0.0488(15) C25 0.0603(10) 0.0424(8) 0.0544(10) 0.0156(7) 0.0263(8) 0.0180(8) C26 0.0790(15) 0.0605(12) 0.0994(17) 0.0317(12) 0.0474(13) 0.0168(11) C27 0.0970(16) 0.0679(12) 0.0470(10) 0.0154(9) 0.0285(10) 0.0286(12) C28 0.0319(7) 0.0318(6) 0.0366(7) 0.0098(5) 0.0110(5) 0.0140(5) C29 0.0582(10) 0.0373(8) 0.0560(10) 0.0184(7) 0.0309(8) 0.0223(7) C30 0.0709(12) 0.0537(10) 0.0602(10) 0.0297(8) 0.0407(9) 0.0314(9) C31 0.0644(11) 0.0567(10) 0.0421(8) 0.0152(7) 0.0271(8) 0.0329(8) C32 0.0517(9) 0.0376(7) 0.0423(8) 0.0054(6) 0.0163(7) 0.0200(7) C33 0.0318(7) 0.0318(6) 0.0350(7) 0.0075(5) 0.0086(5) 0.0131(5) C34 0.0493(10) 0.0329(8) 0.0851(13) 0.0005(8) 0.0297(9) 0.0052(7) C35 0.0507(12) 0.0677(13) 0.1024(18) -0.0280(13) 0.0032(12) 0.0047(10) C36 0.108(2) 0.0386(10) 0.148(3) 0.0173(13) 0.0681(19) -0.0042(11) C37 0.0536(10) 0.0480(9) 0.0674(11) 0.0348(8) 0.0237(8) 0.0237(8) C38 0.0612(12) 0.0716(13) 0.0764(14) 0.0277(11) -0.0040(10) 0.0266(10) C39 0.0655(12) 0.0749(13) 0.1033(17) 0.0459(13) 0.0369(12) 0.0451(11) C40 0.0354(8) 0.0548(9) 0.0623(10) 0.0291(8) 0.0239(7) 0.0194(7) C41 0.0693(12) 0.0842(14) 0.0624(12) 0.0357(10) 0.0410(10) 0.0393(11) C42 0.0496(10) 0.0566(10) 0.0993(16) 0.0418(11) 0.0360(10) 0.0176(8) C43 0.0432(8) 0.0374(7) 0.0390(8) 0.0050(6) 0.0032(6) 0.0128(6) C44 0.0503(11) 0.0771(14) 0.0593(12) 0.0071(10) -0.0079(9) 0.0073(10) C45 0.0787(13) 0.0557(10) 0.0392(9) 0.0139(8) 0.0176(9) 0.0235(9) P2 0.0366(2) 0.02947(18) 0.0519(2) 0.01005(16) 0.01959(17) 0.01028(15) Si2 0.03190(19) 0.02864(18) 0.0404(2) 0.00408(15) 0.00528(16) 0.01317(15) C2 0.0363(7) 0.0357(7) 0.0299(6) 0.0098(5) 0.0091(5) 0.0174(6) C3 0.0458(8) 0.0382(7) 0.0425(8) 0.0106(6) 0.0075(7) 0.0194(7) C4 0.0585(10) 0.0481(9) 0.0493(9) 0.0193(7) 0.0156(8) 0.0343(8) C5 0.0441(9) 0.0623(10) 0.0551(10) 0.0249(8) 0.0142(7) 0.0333(8) C13A 0.0761(19) 0.077(2) 0.0471(14) -0.0040(13) -0.0132(12) 0.0402(17) C14A 0.0459(13) 0.0548(16) 0.099(2) 0.0112(14) -0.0089(13) 0.0013(11) C13B 0.077(12) 0.073(13) 0.093(15) 0.000(11) -0.041(11) 0.029(11) C14B 0.029(7) 0.071(12) 0.117(15) 0.046(11) 0.006(7) 0.007(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C7 1.3767(17) . ? N1 C15 1.4348(17) . ? N1 C12 1.5052(19) . ? C1 C6 1.4020(19) . ? C1 C2 1.411(2) . ? C1 P1 1.8207(14) . ? C6 C5 1.377(2) . ? C7 C8 1.5479(19) . ? C7 Si2 1.8097(14) . ? C8 C10 1.524(2) . ? C8 C9 1.524(3) . ? C8 C11 1.542(2) . ? C11 C12 1.500(2) . ? C11 C14B 1.871(17) . ? C12 C13B 1.43(2) . ? C12 C14A 1.528(3) . ? C12 C13A 1.543(3) . ? C12 C14B 1.665(18) . ? C15 C16 1.408(2) . ? C15 C21 1.410(2) . ? C16 C17 1.394(2) . ? C16 C25 1.523(2) . ? C17 C18 1.372(3) . ? C18 C20 1.375(3) . ? P1 C40 1.8441(15) . ? P1 C43 1.8525(15) . ? P1 Si1 2.2926(5) . ? Si1 C28 1.9572(14) . ? Si1 Si2 2.3673(5) . ? C20 C21 1.395(2) . ? C21 C22 1.516(2) . ? C22 C23 1.529(3) . ? C22 C24 1.538(3) . ? C25 C27 1.529(3) . ? C25 C26 1.542(3) . ? C28 C29 1.402(2) . ? C28 C33 1.4136(18) . ? C29 C30 1.387(2) . ? C30 C31 1.371(2) . ? C31 C32 1.371(2) . ? C32 C33 1.4049(19) . ? C33 P2 1.8426(15) . ? C34 C36 1.532(3) . ? C34 C35 1.533(3) . ? C34 P2 1.8629(17) . ? C37 C38 1.518(3) . ? C37 C39 1.523(3) . ? C37 P2 1.8725(17) . ? C40 C41 1.524(3) . ? C40 C42 1.530(2) . ? C43 C45 1.523(2) . ? C43 C44 1.527(2) . ? Si2 C2 1.9073(14) . ? C2 C3 1.4048(19) . ? C3 C4 1.381(2) . ? C4 C5 1.377(3) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C7 N1 C15 124.20(11) . . ? C7 N1 C12 115.65(11) . . ? C15 N1 C12 120.10(11) . . ? C6 C1 C2 121.24(13) . . ? C6 C1 P1 119.26(11) . . ? C2 C1 P1 119.50(10) . . ? C5 C6 C1 120.63(15) . . ? N1 C7 C8 106.34(11) . . ? N1 C7 Si2 134.11(10) . . ? C8 C7 Si2 119.04(10) . . ? C10 C8 C9 108.79(15) . . ? C10 C8 C11 106.91(15) . . ? C9 C8 C11 113.53(17) . . ? C10 C8 C7 115.88(14) . . ? C9 C8 C7 109.32(13) . . ? C11 C8 C7 102.42(13) . . ? C12 C11 C8 108.77(14) . . ? C12 C11 C14B 58.0(7) . . ? C8 C11 C14B 129.0(6) . . ? C13B C12 C11 136.5(9) . . ? C13B C12 N1 115.1(9) . . ? C11 C12 N1 101.10(12) . . ? C11 C12 C14A 112.7(2) . . ? N1 C12 C14A 112.89(16) . . ? C11 C12 C13A 112.4(2) . . ? N1 C12 C13A 110.71(17) . . ? C14A C12 C13A 107.1(2) . . ? C13B C12 C14B 115.5(14) . . ? C11 C12 C14B 72.3(7) . . ? N1 C12 C14B 107.2(6) . . ? C16 C15 C21 120.87(13) . . ? C16 C15 N1 119.71(13) . . ? C21 C15 N1 119.41(13) . . ? C17 C16 C15 118.19(14) . . ? C17 C16 C25 117.98(14) . . ? C15 C16 C25 123.59(13) . . ? C18 C17 C16 121.46(16) . . ? C17 C18 C20 119.83(15) . . ? C1 P1 C40 103.60(7) . . ? C1 P1 C43 107.43(7) . . ? C40 P1 C43 108.76(8) . . ? C1 P1 Si1 110.15(5) . . ? C40 P1 Si1 110.77(6) . . ? C43 P1 Si1 115.41(5) . . ? C28 Si1 P1 98.52(4) . . ? C28 Si1 Si2 105.02(4) . . ? P1 Si1 Si2 85.332(17) . . ? C18 C20 C21 121.76(16) . . ? C20 C21 C15 117.78(15) . . ? C20 C21 C22 118.68(14) . . ? C15 C21 C22 123.49(14) . . ? C21 C22 C23 111.32(16) . . ? C21 C22 C24 112.56(16) . . ? C23 C22 C24 109.76(17) . . ? C16 C25 C27 110.11(15) . . ? C16 C25 C26 113.00(15) . . ? C27 C25 C26 109.03(17) . . ? C29 C28 C33 116.67(12) . . ? C29 C28 Si1 122.87(10) . . ? C33 C28 Si1 120.34(10) . . ? C30 C29 C28 122.64(14) . . ? C31 C30 C29 119.75(15) . . ? C30 C31 C32 119.54(14) . . ? C31 C32 C33 121.76(14) . . ? C32 C33 C28 119.49(13) . . ? C32 C33 P2 121.71(11) . . ? C28 C33 P2 118.77(10) . . ? C36 C34 C35 112.2(2) . . ? C36 C34 P2 108.16(16) . . ? C35 C34 P2 109.62(13) . . ? C38 C37 C39 110.34(17) . . ? C38 C37 P2 109.94(12) . . ? C39 C37 P2 116.49(14) . . ? C41 C40 C42 110.64(16) . . ? C41 C40 P1 109.14(12) . . ? C42 C40 P1 111.36(11) . . ? C45 C43 C44 110.72(15) . . ? C45 C43 P1 109.09(11) . . ? C44 C43 P1 115.90(13) . . ? C33 P2 C34 103.85(8) . . ? C33 P2 C37 101.07(7) . . ? C34 P2 C37 101.58(9) . . ? C7 Si2 C2 122.93(6) . . ? C7 Si2 Si1 114.21(5) . . ? C2 Si2 Si1 106.69(5) . . ? C3 C2 C1 115.83(13) . . ? C3 C2 Si2 127.72(11) . . ? C1 C2 Si2 116.39(10) . . ? C4 C3 C2 122.51(15) . . ? C5 C4 C3 120.54(14) . . ? C4 C5 C6 119.24(14) . . ? C12 C14B C11 49.8(5) . . ? _refine_diff_density_max 0.645 _refine_diff_density_min -0.348 _refine_diff_density_rms 0.036 _shelx_res_file ; TITL sad_a.res in P-1 sad_a.res created by SHELXL-2018/3 at 11:01:14 on 17-May-2022 REM Old TITL sad in P-1 REM SHELXT solution in P-1: R1 0.147, Rweak 0.013, Alpha 0.075 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C41 N4 P4 CELL 0.71073 9.6755 15.1358 16.5849 103.436 101.043 107.284 ZERR 2.0 0.0004 0.0007 0.0008 0.002 0.002 0.002 LATT 1 SFAC C H N SI P UNIT 88 134 2 4 4 TEMP -173 SIZE 0.112 0.215 0.274 L.S. 20 BOND LIST 4 ACTA FMAP 2 PLAN 20 WGHT 0.051400 0.565500 FVAR 0.54306 0.86918 N1 3 0.200796 0.254952 0.608290 11.00000 0.03266 0.03147 = 0.03853 0.00281 0.00303 0.01242 C1 1 0.731967 0.484895 0.813684 11.00000 0.03485 0.03737 = 0.03285 0.01097 0.01058 0.01697 C6 1 0.871105 0.474107 0.839641 11.00000 0.03473 0.05047 = 0.05014 0.01627 0.00926 0.01839 AFIX 43 H6 2 0.960401 0.530159 0.864983 11.00000 -1.20000 AFIX 0 C7 1 0.259420 0.353058 0.652135 11.00000 0.03229 0.03238 = 0.03593 0.00649 0.00961 0.01465 C8 1 0.146205 0.396713 0.613970 11.00000 0.03729 0.04049 = 0.05465 0.00481 0.00119 0.02066 C9 1 0.206452 0.447304 0.551757 11.00000 0.07973 0.08138 = 0.05287 0.02754 0.00977 0.04904 AFIX 137 H9A 2 0.231596 0.402288 0.509300 11.00000 -1.50000 H9B 2 0.297094 0.504587 0.584098 11.00000 -1.50000 H9C 2 0.129404 0.467566 0.521872 11.00000 -1.50000 AFIX 0 C10 1 0.107393 0.467549 0.679345 11.00000 0.04487 0.05394 = 0.08454 0.01072 0.01930 0.03039 AFIX 137 H10A 2 0.022397 0.481695 0.649869 11.00000 -1.50000 H10B 2 0.195010 0.528017 0.706554 11.00000 -1.50000 H10C 2 0.079809 0.438501 0.723663 11.00000 -1.50000 AFIX 0 C11 1 0.001371 0.306182 0.569401 11.00000 0.04475 0.05590 = 0.09636 -0.00210 -0.01416 0.02263 AFIX 23 H11A 2 -0.064239 0.299606 0.608370 11.00000 -1.20000 H11B 2 -0.055014 0.312880 0.516063 11.00000 -1.20000 AFIX 0 C12 1 0.044382 0.217962 0.547716 11.00000 0.03820 0.04302 = 0.05462 0.00154 -0.00588 0.01200 C15 1 0.281156 0.189894 0.614885 11.00000 0.03924 0.02974 = 0.03433 0.00221 0.00707 0.01344 C16 1 0.260423 0.135000 0.672375 11.00000 0.04555 0.03101 = 0.04012 0.00517 0.01085 0.01181 C17 1 0.332569 0.067852 0.673069 11.00000 0.06427 0.03497 = 0.05134 0.01323 0.01433 0.02073 AFIX 43 H17 2 0.316829 0.028529 0.709946 11.00000 -1.20000 AFIX 0 C18 1 0.425776 0.057320 0.621677 11.00000 0.07298 0.04531 = 0.06194 0.01214 0.01823 0.03738 AFIX 43 H18 2 0.473185 0.010754 0.622811 11.00000 -1.20000 AFIX 0 P1 5 0.725668 0.606585 0.829215 11.00000 0.02886 0.03237 = 0.03587 0.01051 0.01004 0.01038 SI1 4 0.490023 0.597738 0.761006 11.00000 0.03313 0.03024 = 0.03396 0.00780 0.01027 0.01407 C20 1 0.450404 0.114338 0.568519 11.00000 0.06500 0.05534 = 0.05412 0.01162 0.02520 0.03688 AFIX 43 H20 2 0.517258 0.107651 0.534349 11.00000 -1.20000 AFIX 0 C21 1 0.379849 0.181730 0.563428 11.00000 0.04965 0.04248 = 0.03787 0.00694 0.01315 0.02150 C22 1 0.417611 0.244908 0.506104 11.00000 0.06736 0.05974 = 0.04830 0.01994 0.02891 0.03228 AFIX 13 H22 2 0.347882 0.282158 0.504390 11.00000 -1.20000 AFIX 0 C23 1 0.578888 0.318641 0.543010 11.00000 0.07963 0.07962 = 0.08086 0.03350 0.04188 0.02140 AFIX 137 H23A 2 0.649924 0.284086 0.545456 11.00000 -1.50000 H23B 2 0.591437 0.359086 0.601318 11.00000 -1.50000 H23C 2 0.598690 0.360021 0.505914 11.00000 -1.50000 AFIX 0 C24 1 0.394549 0.184907 0.412765 11.00000 0.11524 0.09515 = 0.05000 0.02297 0.03853 0.04884 AFIX 137 H24A 2 0.292221 0.136158 0.390106 11.00000 -1.50000 H24B 2 0.468018 0.152199 0.411848 11.00000 -1.50000 H24C 2 0.408710 0.228128 0.376858 11.00000 -1.50000 AFIX 0 C25 1 0.175250 0.151190 0.739385 11.00000 0.06031 0.04244 = 0.05444 0.01556 0.02628 0.01797 AFIX 13 H25 2 0.128608 0.199947 0.729612 11.00000 -1.20000 AFIX 0 C26 1 0.048651 0.057662 0.733715 11.00000 0.07900 0.06050 = 0.09939 0.03170 0.04743 0.01679 AFIX 137 H26A 2 -0.022447 0.031125 0.675805 11.00000 -1.50000 H26B 2 -0.004566 0.072796 0.776690 11.00000 -1.50000 H26C 2 0.092492 0.009614 0.745044 11.00000 -1.50000 AFIX 0 C27 1 0.284409 0.192629 0.830277 11.00000 0.09705 0.06792 = 0.04698 0.01541 0.02847 0.02864 AFIX 137 H27A 2 0.335056 0.147238 0.840131 11.00000 -1.50000 H27B 2 0.228339 0.201935 0.872919 11.00000 -1.50000 H27C 2 0.359789 0.255272 0.836032 11.00000 -1.50000 AFIX 0 C28 1 0.434253 0.654533 0.862804 11.00000 0.03185 0.03179 = 0.03662 0.00979 0.01096 0.01396 C29 1 0.354786 0.598306 0.906858 11.00000 0.05824 0.03725 = 0.05600 0.01843 0.03093 0.02230 AFIX 43 H29 2 0.328060 0.529698 0.887050 11.00000 -1.20000 AFIX 0 C30 1 0.313588 0.638828 0.978236 11.00000 0.07087 0.05369 = 0.06017 0.02973 0.04069 0.03138 AFIX 43 H30 2 0.259296 0.598212 1.006184 11.00000 -1.20000 AFIX 0 C31 1 0.351515 0.737683 1.008279 11.00000 0.06438 0.05672 = 0.04212 0.01521 0.02707 0.03288 AFIX 43 H31 2 0.327315 0.766171 1.058508 11.00000 -1.20000 AFIX 0 C32 1 0.424628 0.795168 0.965330 11.00000 0.05168 0.03762 = 0.04225 0.00535 0.01634 0.01999 AFIX 43 H32 2 0.448615 0.863491 0.985748 11.00000 -1.20000 AFIX 0 C33 1 0.465015 0.755732 0.891936 11.00000 0.03183 0.03182 = 0.03502 0.00753 0.00864 0.01313 C34 1 0.651978 0.954340 0.911355 11.00000 0.04926 0.03291 = 0.08513 0.00049 0.02967 0.00519 AFIX 13 H34 2 0.579783 0.973122 0.941263 11.00000 -1.20000 AFIX 0 C35 1 0.781955 0.950873 0.978372 11.00000 0.05066 0.06773 = 0.10243 -0.02797 0.00321 0.00471 AFIX 137 H35A 2 0.853131 0.932292 0.949559 11.00000 -1.50000 H35B 2 0.741837 0.902966 1.006796 11.00000 -1.50000 H35C 2 0.833982 1.015147 1.021598 11.00000 -1.50000 AFIX 0 C36 1 0.707089 1.027405 0.863721 11.00000 0.10790 0.03863 = 0.14823 0.01727 0.06806 -0.00425 AFIX 137 H36A 2 0.768386 1.005325 0.828697 11.00000 -1.50000 H36B 2 0.768041 1.091291 0.905857 11.00000 -1.50000 H36C 2 0.620081 1.032325 0.826148 11.00000 -1.50000 AFIX 0 C37 1 0.382636 0.848870 0.768107 11.00000 0.05363 0.04799 = 0.06744 0.03477 0.02370 0.02375 AFIX 13 H37 2 0.420202 0.891873 0.733429 11.00000 -1.20000 AFIX 0 C38 1 0.274785 0.752363 0.703744 11.00000 0.06117 0.07159 = 0.07636 0.02766 -0.00398 0.02664 AFIX 137 H38A 2 0.194634 0.763302 0.665927 11.00000 -1.50000 H38B 2 0.230258 0.708870 0.734884 11.00000 -1.50000 H38C 2 0.329845 0.722624 0.668875 11.00000 -1.50000 AFIX 0 C39 1 0.298506 0.897659 0.821414 11.00000 0.06551 0.07490 = 0.10326 0.04588 0.03692 0.04510 AFIX 137 H39A 2 0.214557 0.904294 0.782720 11.00000 -1.50000 H39B 2 0.367550 0.962193 0.859188 11.00000 -1.50000 H39C 2 0.259271 0.857886 0.856639 11.00000 -1.50000 AFIX 0 C40 1 0.866464 0.663507 0.778111 11.00000 0.03536 0.05481 = 0.06226 0.02909 0.02394 0.01941 AFIX 13 H40 2 0.966275 0.662261 0.806968 11.00000 -1.20000 AFIX 0 C41 1 0.820973 0.604524 0.683036 11.00000 0.06926 0.08419 = 0.06238 0.03565 0.04100 0.03926 AFIX 137 H41A 2 0.725483 0.607581 0.653302 11.00000 -1.50000 H41B 2 0.808722 0.536656 0.678032 11.00000 -1.50000 H41C 2 0.899468 0.631414 0.656648 11.00000 -1.50000 AFIX 0 C42 1 0.882104 0.769322 0.787861 11.00000 0.04958 0.05665 = 0.09930 0.04180 0.03604 0.01760 AFIX 137 H42A 2 0.954959 0.796876 0.758447 11.00000 -1.50000 H42B 2 0.917406 0.806947 0.849290 11.00000 -1.50000 H42C 2 0.783968 0.771926 0.762093 11.00000 -1.50000 AFIX 0 C43 1 0.792568 0.670658 0.946888 11.00000 0.04324 0.03737 = 0.03898 0.00496 0.00323 0.01276 AFIX 13 H43 2 0.753848 0.725448 0.956824 11.00000 -1.20000 AFIX 0 C44 1 0.963453 0.715077 0.986121 11.00000 0.05026 0.07709 = 0.05934 0.00713 -0.00795 0.00730 AFIX 137 H44A 2 1.004787 0.662998 0.983076 11.00000 -1.50000 H44B 2 0.987032 0.753687 1.046602 11.00000 -1.50000 H44C 2 1.008177 0.757044 0.953857 11.00000 -1.50000 AFIX 0 C45 1 0.720208 0.602299 0.993841 11.00000 0.07875 0.05572 = 0.03918 0.01388 0.01761 0.02353 AFIX 137 H45A 2 0.610703 0.574965 0.968042 11.00000 -1.50000 H45B 2 0.743164 0.638450 1.054974 11.00000 -1.50000 H45C 2 0.760200 0.549499 0.988716 11.00000 -1.50000 AFIX 0 P2 5 0.551226 0.831891 0.829831 11.00000 0.03658 0.02947 = 0.05186 0.01005 0.01959 0.01028 SI2 4 0.416301 0.429592 0.745815 11.00000 0.03190 0.02864 = 0.04040 0.00408 0.00528 0.01317 C2 1 0.597249 0.403259 0.774979 11.00000 0.03627 0.03573 = 0.02991 0.00975 0.00906 0.01741 C3 1 0.612008 0.312149 0.765899 11.00000 0.04584 0.03825 = 0.04252 0.01057 0.00746 0.01943 AFIX 43 H3 2 0.524030 0.255174 0.740964 11.00000 -1.20000 AFIX 0 C4 1 0.749563 0.302244 0.791845 11.00000 0.05851 0.04813 = 0.04931 0.01934 0.01562 0.03427 AFIX 43 H4 2 0.754486 0.239177 0.784157 11.00000 -1.20000 AFIX 0 C5 1 0.879575 0.383019 0.828752 11.00000 0.04407 0.06233 = 0.05511 0.02490 0.01418 0.03333 AFIX 43 H5 2 0.974052 0.376017 0.846508 11.00000 -1.20000 AFIX 0 SIMU 0.02 0.04 C13A > C14B PART 1 21 C13A 1 0.047898 0.186705 0.452946 21.00000 0.07612 0.07718 = 0.04712 -0.00398 -0.01321 0.04015 AFIX 137 H13A 2 -0.055491 0.157332 0.414868 21.00000 -1.50000 H13B 2 0.098185 0.139147 0.445243 21.00000 -1.50000 H13C 2 0.103234 0.243780 0.438524 21.00000 -1.50000 AFIX 0 C14A 1 -0.063022 0.130014 0.562303 21.00000 0.04591 0.05475 = 0.09943 0.01119 -0.00890 0.00127 AFIX 137 H14A 2 -0.163597 0.110302 0.522589 21.00000 -1.50000 H14B 2 -0.068652 0.147247 0.622003 21.00000 -1.50000 H14C 2 -0.025708 0.076082 0.551675 21.00000 -1.50000 AFIX 0 PART 2 -21 C13B 1 0.015062 0.139141 0.472460 -21.00000 0.07728 0.07304 = 0.09309 0.00044 -0.04132 0.02946 AFIX 137 H13D 2 -0.088601 0.120167 0.436845 -21.00000 -1.50000 H13E 2 0.028127 0.083714 0.489582 -21.00000 -1.50000 H13F 2 0.085506 0.159365 0.439227 -21.00000 -1.50000 AFIX 0 C14B 1 -0.076366 0.198955 0.606664 -21.00000 0.02920 0.07088 = 0.11726 0.04574 0.00623 0.00748 AFIX 137 H14D 2 -0.177627 0.187929 0.572030 -21.00000 -1.50000 H14E 2 -0.045084 0.256013 0.657684 -21.00000 -1.50000 H14F 2 -0.077461 0.141736 0.624975 -21.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM sad_a.res in P-1 REM wR2 = 0.1021, GooF = S = 1.033, Restrained GooF = 1.032 for all data REM R1 = 0.0369 for 8320 Fo > 4sig(Fo) and 0.0461 for all 9906 data REM 479 parameters refined using 18 restraints END WGHT 0.0514 0.5654 REM Highest difference peak 0.645, deepest hole -0.348, 1-sigma level 0.036 Q1 1 0.0431 0.3159 0.5176 11.00000 0.05 0.65 Q2 1 0.3264 0.3819 0.7008 11.00000 0.05 0.31 Q3 1 0.5197 0.4107 0.7608 11.00000 0.05 0.30 Q4 1 0.4932 0.7836 0.8640 11.00000 0.05 0.28 Q5 1 0.7287 0.5377 0.8168 11.00000 0.05 0.27 Q6 1 0.7691 0.6385 0.8908 11.00000 0.05 0.25 Q7 1 0.6219 0.6017 0.7996 11.00000 0.05 0.24 Q8 1 0.1241 0.2342 0.5781 11.00000 0.05 0.24 Q9 1 0.4397 0.7049 0.8745 11.00000 0.05 0.23 Q10 1 0.8038 0.6320 0.8010 11.00000 0.05 0.23 Q11 1 0.4634 0.6301 0.8178 11.00000 0.05 0.22 Q12 1 0.6801 0.3085 0.7981 11.00000 0.05 0.21 Q13 1 0.4393 0.5126 0.7629 11.00000 0.05 0.21 Q14 1 0.2284 0.1457 0.7056 11.00000 0.05 0.21 Q15 1 0.3348 0.1925 0.5914 11.00000 0.05 0.21 Q16 1 0.2084 0.3793 0.6362 11.00000 0.05 0.21 Q17 1 0.1846 0.4235 0.5865 11.00000 0.05 0.20 Q18 1 0.2406 0.2210 0.6114 11.00000 0.05 0.20 Q19 1 0.4585 0.7753 0.9336 11.00000 0.05 0.20 Q20 1 0.7939 0.4830 0.8297 11.00000 0.05 0.20 ; _shelx_res_checksum 49968 _shelx_hkl_file ; -1 0 0 2508.05 65.59 1 0 0 2528.05 65.89 -2 0 0 151.08 3.80 -2 0 0 153.78 3.80 -2 0 0 147.49 5.00 -2 0 0 155.28 5.20 -2 0 0 148.49 5.00 -2 0 0 160.58 4.00 -2 0 0 153.68 3.80 -2 0 0 160.78 4.40 -2 0 0 151.08 4.30 -2 0 0 154.18 3.80 -2 0 0 149.79 4.00 -2 0 0 154.78 4.40 -2 0 0 150.08 5.70 -2 0 0 151.58 4.10 -2 0 0 154.48 4.00 -2 0 0 151.08 4.30 -2 0 0 133.69 12.70 2 0 0 157.28 4.40 2 0 0 155.68 4.10 2 0 0 154.78 3.80 2 0 0 150.88 3.70 2 0 0 157.88 14.40 2 0 0 152.28 4.40 2 0 0 150.38 4.00 2 0 0 154.28 3.70 2 0 0 149.19 3.90 2 0 0 147.19 4.10 2 0 0 152.08 3.80 2 0 0 150.48 3.80 2 0 0 153.38 5.10 2 0 0 155.48 5.20 2 0 0 147.69 5.20 2 0 0 153.78 4.30 2 0 0 150.58 4.10 2 0 0 148.69 4.20 -3 0 0 66.19 3.00 -3 0 0 70.89 2.80 -3 0 0 74.19 2.20 -3 0 0 68.99 2.10 -3 0 0 71.19 2.60 -3 0 0 67.99 2.90 -3 0 0 79.09 3.90 -3 0 0 73.49 3.80 -3 0 0 73.59 2.20 -3 0 0 74.39 2.50 -3 0 0 81.39 14.20 -3 0 0 72.39 2.80 -3 0 0 72.49 2.50 -3 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226.18 7.20 -2 -2 0 225.38 6.30 -2 -2 0 202.98 6.40 -2 -2 0 226.68 5.30 2 2 0 232.38 7.40 2 2 0 222.28 5.80 2 2 0 222.28 6.30 2 2 0 234.48 6.60 2 2 0 231.08 5.50 2 2 0 230.18 5.90 2 2 0 227.78 6.10 2 2 0 225.58 7.40 2 2 0 204.28 18.30 2 2 0 221.68 6.60 2 2 0 231.48 7.30 2 2 0 231.98 6.00 2 2 0 232.98 7.30 2 2 0 237.58 6.80 2 2 0 232.88 5.30 2 2 0 238.28 5.30 -3 -2 0 963.00 25.10 -3 -2 0 1015.70 23.90 -3 -2 0 1031.30 48.50 -3 -2 0 990.00 22.80 -3 -2 0 980.20 23.10 -3 -2 0 992.70 22.60 -3 -2 0 968.50 23.70 -3 -2 0 966.60 22.10 -3 -2 0 1015.70 25.20 -3 -2 0 969.30 23.30 -3 -2 0 989.70 23.30 -3 -2 0 987.60 22.70 -3 -2 0 995.20 25.00 -3 -2 0 983.10 22.70 -3 -2 0 995.20 22.10 -3 -2 0 942.11 23.60 -3 -2 0 1006.60 25.10 -3 -2 0 968.70 22.20 3 2 0 995.10 25.10 3 2 0 995.30 22.00 3 2 0 990.40 22.10 3 2 0 991.40 24.00 3 2 0 947.61 23.10 3 2 0 968.10 22.80 3 2 0 930.31 47.70 3 2 0 974.00 22.70 3 2 0 988.50 22.10 3 2 0 976.80 23.80 3 2 0 976.40 25.20 3 2 0 969.10 25.00 3 2 0 1007.90 25.10 3 2 0 988.90 22.80 3 2 0 981.00 22.30 3 2 0 964.50 23.50 3 2 0 975.10 22.60 3 2 0 983.00 23.90 3 2 0 982.70 23.40 -4 -2 0 10.20 1.10 -4 -2 0 11.00 1.60 -4 -2 0 8.70 1.40 -4 -2 0 10.80 1.50 -4 -2 0 7.40 1.20 -4 -2 0 9.10 1.20 -4 -2 0 18.80 12.10 -4 -2 0 9.40 1.20 -4 -2 0 7.30 0.80 -4 -2 0 7.90 0.90 -4 -2 0 9.60 2.50 -4 -2 0 9.70 1.70 -4 -2 0 8.70 2.40 -4 -2 0 7.70 2.20 -4 -2 0 7.00 2.10 -4 -2 0 12.50 2.80 4 2 0 8.60 1.20 4 2 0 6.80 2.00 4 2 0 8.80 0.80 4 2 0 8.10 1.40 4 2 0 10.10 1.30 4 2 0 8.40 1.50 4 2 0 8.20 1.10 4 2 0 10.50 1.80 4 2 0 2.90 1.50 4 2 0 9.20 0.90 4 2 0 8.20 0.90 4 2 0 8.00 1.60 4 2 0 23.30 15.40 4 2 0 8.60 0.80 4 2 0 5.30 2.00 4 2 0 4.70 1.40 4 2 0 10.60 2.30 -5 -2 0 86.89 4.30 -5 -2 0 89.49 3.10 -5 -2 0 100.79 3.70 -5 -2 0 102.89 4.60 -5 -2 0 94.99 3.20 -5 -2 0 80.39 22.90 -5 -2 0 103.09 3.00 -5 -2 0 94.59 4.10 -5 -2 0 88.19 3.90 -5 -2 0 87.49 5.70 -5 -2 0 94.19 5.80 -5 -2 0 93.69 5.80 -5 -2 0 102.09 6.00 5 2 0 92.59 5.80 5 2 0 99.89 3.10 5 2 0 99.99 3.20 5 2 0 88.69 4.40 5 2 0 93.19 5.70 5 2 0 103.89 4.90 5 2 0 97.09 2.90 5 2 0 98.39 4.70 5 2 0 101.19 6.00 5 2 0 89.69 5.70 5 2 0 102.59 3.80 5 2 0 88.69 3.60 5 2 0 93.89 4.10 5 2 0 95.89 2.90 5 2 0 99.09 3.80 -6 -2 0 14.00 1.50 -6 -2 0 -9.90 15.40 -6 -2 0 10.30 2.00 -6 -2 0 13.00 1.80 -6 -2 0 10.20 1.80 -6 -2 0 11.40 1.60 -6 -2 0 11.50 3.20 -6 -2 0 22.20 21.50 -6 -2 0 11.60 1.70 -6 -2 0 14.70 3.10 -6 -2 0 14.40 1.30 -6 -2 0 14.80 2.20 -6 -2 0 9.60 3.00 6 2 0 11.50 3.00 6 2 0 13.30 1.20 6 2 0 14.20 1.90 6 2 0 19.10 2.80 6 2 0 14.70 2.50 6 2 0 12.10 2.00 6 2 0 11.10 3.30 6 2 0 11.90 1.30 6 2 0 16.70 2.00 6 2 0 9.00 3.20 6 2 0 15.60 3.70 -7 -2 0 55.89 32.60 -7 -2 0 72.19 3.00 -7 -2 0 65.09 4.30 -7 -2 0 69.39 6.30 -7 -2 0 72.59 4.10 -7 -2 0 68.99 3.70 7 2 0 71.89 3.10 7 2 0 72.59 3.70 7 2 0 71.99 5.00 7 2 0 74.89 4.90 7 2 0 70.19 3.80 7 2 0 66.09 3.90 7 2 0 64.69 5.80 -8 -2 0 157.48 6.80 -8 -2 0 166.28 7.50 -8 -2 0 164.88 7.10 -8 -2 0 156.78 6.10 8 2 0 158.88 7.90 8 2 0 170.78 5.40 8 2 0 152.98 6.30 8 2 0 165.28 8.00 -9 -2 0 26.70 3.50 -9 -2 0 31.30 3.50 -9 -2 0 34.40 3.40 -9 -2 0 28.30 4.00 9 2 0 20.70 3.10 9 2 0 33.80 4.90 -10 -2 0 4.70 2.60 -10 -2 0 4.50 2.40 -10 -2 0 1.10 2.20 10 2 0 0.30 2.80 10 2 0 0.80 2.50 12 -3 0 37.70 5.40 -12 3 0 28.90 4.70 11 -3 0 81.39 5.40 11 -3 0 73.69 6.20 -11 3 0 85.19 6.50 -11 3 0 80.89 5.60 10 -3 0 2.80 2.00 10 -3 0 2.60 1.80 10 -3 0 0.30 2.10 10 -3 0 6.60 4.50 10 -3 0 3.70 1.80 10 -3 0 5.30 1.80 10 -3 0 5.40 2.30 -10 3 0 3.20 2.10 -10 3 0 7.10 2.70 -10 3 0 2.80 1.70 -10 3 0 1.70 2.00 9 -3 0 9.80 1.70 9 -3 0 10.80 2.40 9 -3 0 11.40 2.50 9 -3 0 8.00 2.70 9 -3 0 8.10 1.90 9 -3 0 7.10 4.10 -9 3 0 11.70 2.30 -9 3 0 11.30 1.90 -9 3 0 -13.80 32.80 -9 3 0 12.50 2.70 -9 3 0 21.60 4.40 -9 3 0 14.50 2.80 8 -3 0 189.38 5.80 8 -3 0 185.48 7.00 8 -3 0 185.18 7.80 8 -3 0 177.48 5.80 8 -3 0 187.98 6.30 8 -3 0 187.38 9.80 8 -3 0 171.68 7.00 -8 3 0 134.39 34.10 -8 3 0 188.88 7.70 -8 3 0 184.88 6.60 -8 3 0 177.78 6.50 -8 3 0 174.88 5.90 -8 3 0 172.58 7.20 -8 3 0 192.88 9.80 7 -3 0 72.79 3.90 7 -3 0 79.49 3.30 7 -3 0 82.09 3.60 7 -3 0 80.09 3.30 7 -3 0 78.89 3.20 7 -3 0 75.59 4.50 7 -3 0 86.29 3.30 7 -3 0 75.59 4.40 7 -3 0 70.09 5.50 -7 3 0 82.89 5.80 -7 3 0 79.59 3.30 -7 3 0 74.09 5.80 -7 3 0 82.09 3.70 -7 3 0 62.49 21.70 -7 3 0 74.39 3.90 -7 3 0 84.39 4.00 -7 3 0 80.39 3.40 -7 3 0 76.39 4.30 -7 3 0 78.59 4.20 6 -3 0 4.30 0.90 6 -3 0 5.70 1.50 6 -3 0 4.20 0.90 6 -3 0 5.50 1.50 6 -3 0 5.30 1.90 6 -3 0 5.80 1.00 6 -3 0 4.90 1.00 6 -3 0 3.70 1.10 6 -3 0 5.10 1.30 6 -3 0 2.90 1.70 6 -3 0 3.70 1.10 6 -3 0 6.50 1.10 6 -3 0 2.30 1.80 6 -3 0 4.60 2.20 6 -3 0 3.10 1.20 6 -3 0 4.50 1.30 -6 3 0 5.00 0.90 -6 3 0 4.30 14.60 -6 3 0 2.40 1.60 -6 3 0 5.80 1.50 -6 3 0 3.70 1.20 -6 3 0 6.20 2.10 -6 3 0 6.50 1.30 -6 3 0 5.70 1.20 -6 3 0 5.00 1.40 -6 3 0 5.50 1.10 -6 3 0 7.10 1.50 -6 3 0 5.90 1.40 -6 3 0 3.60 14.30 -6 3 0 3.60 1.00 -6 3 0 8.10 2.40 -6 3 0 3.40 2.40 -6 3 0 4.10 1.30 5 -3 0 134.39 4.00 5 -3 0 139.69 6.00 5 -3 0 144.29 4.40 5 -3 0 127.29 5.10 5 -3 0 133.69 6.30 5 -3 0 134.59 4.10 5 -3 0 135.89 4.10 5 -3 0 132.99 6.10 5 -3 0 135.59 4.50 5 -3 0 137.19 6.20 5 -3 0 132.69 4.40 5 -3 0 133.29 4.90 5 -3 0 127.69 4.60 5 -3 0 140.79 4.90 5 -3 0 129.89 4.10 5 -3 0 131.79 4.00 -5 3 0 121.59 23.30 -5 3 0 130.99 4.40 -5 3 0 131.69 4.50 -5 3 0 134.69 4.20 -5 3 0 137.09 4.90 -5 3 0 133.69 5.30 -5 3 0 128.99 3.90 -5 3 0 135.39 4.20 -5 3 0 136.79 4.40 -5 3 0 139.89 5.20 -5 3 0 124.79 6.00 -5 3 0 139.09 4.80 -5 3 0 134.79 6.20 -5 3 0 138.99 6.20 -5 3 0 138.39 6.30 -5 3 0 123.49 21.30 -5 3 0 134.49 4.10 4 -3 0 15.10 2.10 4 -3 0 17.50 1.40 4 -3 0 13.70 1.60 4 -3 0 17.80 1.40 4 -3 0 15.60 1.30 4 -3 0 16.90 1.60 4 -3 0 17.80 2.40 4 -3 0 16.30 1.10 4 -3 0 17.00 1.30 4 -3 0 16.90 1.40 4 -3 0 17.30 1.60 4 -3 0 13.30 2.30 4 -3 0 15.10 1.30 4 -3 0 14.90 1.70 4 -3 0 17.90 1.10 4 -3 0 15.60 2.10 -4 3 0 17.00 1.60 -4 3 0 13.00 2.10 -4 3 0 4.10 8.30 -4 3 0 14.80 1.30 -4 3 0 18.50 1.60 -4 3 0 16.70 1.40 -4 3 0 12.80 2.00 -4 3 0 19.70 2.40 -4 3 0 16.90 1.30 -4 3 0 17.00 1.80 -4 3 0 17.30 1.40 -4 3 0 15.60 1.10 -4 3 0 16.60 1.80 -4 3 0 14.50 1.20 -4 3 0 18.60 1.60 3 -3 0 35.10 2.10 3 -3 0 38.80 1.70 3 -3 0 37.90 1.90 3 -3 0 36.70 1.50 3 -3 0 35.70 1.70 3 -3 0 33.80 1.80 3 -3 0 36.50 2.50 3 -3 0 36.10 1.60 3 -3 0 38.30 1.50 3 -3 0 37.50 2.30 3 -3 0 36.50 2.40 3 -3 0 35.60 2.40 3 -3 0 36.90 1.80 3 -3 0 36.80 1.70 3 -3 0 40.80 1.70 3 -3 0 37.00 1.60 -3 3 0 38.60 1.70 -3 3 0 39.30 2.40 -3 3 0 38.70 1.70 -3 3 0 29.50 7.80 -3 3 0 34.70 2.40 -3 3 0 35.70 1.90 -3 3 0 43.80 2.30 -3 3 0 38.20 1.90 -3 3 0 44.20 1.80 -3 3 0 37.70 1.50 -3 3 0 36.50 2.20 -3 3 0 45.50 9.70 -3 3 0 38.70 1.70 -3 3 0 38.30 1.70 -3 3 0 38.50 2.10 -3 3 0 35.10 2.40 2 -3 0 1137.39 25.70 2 -3 0 1125.19 26.20 2 -3 0 1101.99 26.00 2 -3 0 1135.89 25.00 2 -3 0 1092.49 26.60 2 -3 0 1135.89 25.50 2 -3 0 1139.69 26.30 2 -3 0 1120.39 25.70 2 -3 0 1112.39 25.90 2 -3 0 1136.59 25.50 2 -3 0 1120.49 25.40 2 -3 0 1123.29 25.10 2 -3 0 1098.29 25.50 2 -3 0 1131.49 25.50 2 -3 0 1112.19 25.50 2 -3 0 1113.29 25.90 -2 3 0 1128.79 26.00 -2 3 0 1194.18 25.90 -2 3 0 1130.79 25.60 -2 3 0 1126.19 25.90 -2 3 0 1143.09 25.90 -2 3 0 1091.19 25.90 -2 3 0 1133.99 26.30 -2 3 0 1099.69 25.50 -2 3 0 1117.59 26.00 -2 3 0 1095.29 36.90 -2 3 0 1132.69 26.10 -2 3 0 1101.69 25.40 -2 3 0 1131.29 25.60 1 -3 0 1290.47 34.40 1 -3 0 1318.57 30.00 1 -3 0 1315.77 29.40 1 -3 0 1326.27 29.60 1 -3 0 1274.67 29.70 1 -3 0 1278.27 29.70 1 -3 0 1299.17 29.90 1 -3 0 1327.87 29.90 1 -3 0 1307.37 29.30 1 -3 0 1297.87 29.50 1 -3 0 1307.07 29.70 1 -3 0 1334.77 29.90 1 -3 0 1317.87 30.20 1 -3 0 1339.37 29.50 -1 3 0 1323.17 30.30 -1 3 0 1271.67 30.00 -1 3 0 1324.57 29.80 -1 3 0 1309.07 29.70 -1 3 0 1344.97 29.80 -1 3 0 1279.47 29.50 -1 3 0 1312.07 30.00 -1 3 0 1292.97 29.90 -1 3 0 1295.57 29.30 -1 3 0 1306.47 29.40 -1 3 0 1293.87 29.90 -1 3 0 1309.27 29.30 -1 3 0 1265.97 34.70 0 -3 0 24.10 1.60 0 -3 0 25.00 1.40 0 -3 0 27.10 5.30 0 -3 0 24.40 1.60 0 -3 0 23.60 1.30 0 -3 0 21.40 1.10 0 -3 0 26.60 1.40 0 -3 0 24.30 1.20 0 -3 0 22.70 1.20 0 -3 0 23.90 1.20 0 -3 0 22.20 1.40 0 -3 0 24.30 1.20 0 -3 0 26.40 1.10 0 -3 0 23.50 0.90 0 -3 0 25.40 1.40 0 -3 0 23.20 1.20 0 -3 0 24.10 1.20 0 -3 0 23.30 0.80 0 -3 0 20.10 1.40 0 3 0 25.30 1.10 0 3 0 25.00 1.70 0 3 0 22.20 1.40 0 3 0 25.50 1.30 0 3 0 25.90 1.40 0 3 0 24.80 1.10 0 3 0 25.00 1.40 0 3 0 23.60 1.60 0 3 0 24.60 0.90 0 3 0 24.10 1.50 0 3 0 19.30 4.40 0 3 0 25.50 1.40 0 3 0 22.90 1.20 0 3 0 23.70 1.30 0 3 0 24.50 1.40 0 3 0 24.00 0.90 0 3 0 24.10 1.10 -1 -3 0 458.75 12.10 -1 -3 0 466.05 11.80 -1 -3 0 466.15 11.60 -1 -3 0 452.45 11.10 -1 -3 0 462.25 11.10 -1 -3 0 477.95 10.50 -1 -3 0 461.55 11.60 -1 -3 0 478.75 11.00 -1 -3 0 472.85 10.70 -1 -3 0 458.85 12.00 -1 -3 0 473.95 12.00 -1 -3 0 464.15 12.00 -1 -3 0 442.56 11.20 -1 -3 0 448.46 23.30 -1 -3 0 463.45 11.70 -1 -3 0 465.75 11.90 -1 -3 0 454.65 10.80 1 3 0 475.95 10.50 1 3 0 463.15 11.70 1 3 0 475.95 11.70 1 3 0 459.35 12.10 1 3 0 466.55 10.90 1 3 0 469.45 10.70 1 3 0 466.85 11.10 1 3 0 464.35 11.20 1 3 0 460.25 12.00 1 3 0 473.95 12.10 1 3 0 459.75 11.10 1 3 0 470.75 11.10 1 3 0 472.15 12.00 1 3 0 453.25 11.80 1 3 0 455.95 11.90 -2 -3 0 2.60 1.20 -2 -3 0 1.30 0.40 -2 -3 0 1.20 0.50 -2 -3 0 2.70 1.20 -2 -3 0 2.10 0.80 -2 -3 0 2.60 1.00 -2 -3 0 1.20 0.60 -2 -3 0 1.60 0.60 -2 -3 0 -7.80 6.00 -2 -3 0 1.90 0.70 -2 -3 0 3.20 0.90 -2 -3 0 1.30 0.90 -2 -3 0 0.90 0.80 -2 -3 0 1.10 1.20 -2 -3 0 1.50 0.70 -2 -3 0 1.90 0.30 2 3 0 2.00 1.10 2 3 0 2.50 1.00 2 3 0 1.90 0.80 2 3 0 0.40 1.00 2 3 0 0.10 0.80 2 3 0 0.70 0.70 2 3 0 1.00 1.10 2 3 0 1.40 0.90 2 3 0 3.00 1.30 2 3 0 1.80 0.60 2 3 0 1.60 0.60 2 3 0 1.90 0.80 2 3 0 0.40 6.90 2 3 0 2.10 0.30 2 3 0 1.00 0.70 2 3 0 1.40 0.60 2 3 0 1.30 0.50 -3 -3 0 315.87 10.50 -3 -3 0 323.27 10.70 -3 -3 0 325.37 7.70 -3 -3 0 333.57 8.40 -3 -3 0 322.97 8.00 -3 -3 0 333.67 9.80 -3 -3 0 335.67 8.70 -3 -3 0 320.97 10.50 -3 -3 0 338.87 8.40 -3 -3 0 339.37 28.30 -3 -3 0 329.47 9.20 -3 -3 0 323.67 9.20 -3 -3 0 338.47 10.70 -3 -3 0 324.67 8.80 -3 -3 0 328.27 9.50 -3 -3 0 324.97 8.50 3 3 0 333.47 8.40 3 3 0 347.77 8.70 3 3 0 339.47 8.50 3 3 0 335.97 7.70 3 3 0 331.57 8.10 3 3 0 336.17 9.80 3 3 0 332.47 9.30 3 3 0 333.07 10.70 3 3 0 313.27 8.80 3 3 0 334.37 7.60 3 3 0 336.37 9.80 3 3 0 326.47 10.80 3 3 0 328.67 28.90 3 3 0 333.07 7.80 3 3 0 334.27 8.60 3 3 0 335.77 9.90 3 3 0 349.87 10.90 -4 -3 0 141.09 5.50 -4 -3 0 132.39 6.40 -4 -3 0 135.79 3.80 -4 -3 0 139.39 4.40 -4 -3 0 129.49 6.60 -4 -3 0 138.99 4.20 -4 -3 0 138.99 3.60 -4 -3 0 136.19 4.40 -4 -3 0 139.09 6.50 -4 -3 0 134.69 5.30 -4 -3 0 144.49 27.50 -4 -3 0 136.79 5.00 -4 -3 0 136.69 4.60 -4 -3 0 126.79 4.70 -4 -3 0 137.29 6.60 4 3 0 135.79 3.60 4 3 0 146.69 6.70 4 3 0 135.09 5.50 4 3 0 140.09 6.60 4 3 0 138.79 5.80 4 3 0 136.99 4.50 4 3 0 140.59 3.50 4 3 0 136.79 4.40 4 3 0 136.59 3.90 4 3 0 141.19 5.60 4 3 0 135.09 3.60 4 3 0 131.39 6.50 4 3 0 136.69 4.60 4 3 0 135.89 5.10 4 3 0 131.39 4.30 -5 -3 0 42.10 2.40 -5 -3 0 29.30 4.00 -5 -3 0 46.80 4.50 -5 -3 0 39.80 3.20 -5 -3 0 42.00 2.80 -5 -3 0 37.80 2.60 -5 -3 0 41.60 3.00 -5 -3 0 48.60 5.00 -5 -3 0 35.90 1.90 -5 -3 0 42.90 2.40 -5 -3 0 31.00 19.30 -5 -3 0 43.00 1.70 5 3 0 37.90 4.60 5 3 0 39.80 2.80 5 3 0 34.90 3.20 5 3 0 42.70 1.60 5 3 0 46.90 4.40 5 3 0 44.00 1.60 5 3 0 36.80 3.10 5 3 0 41.70 2.40 5 3 0 45.50 4.20 5 3 0 43.30 1.70 5 3 0 44.30 2.10 5 3 0 46.50 20.80 5 3 0 40.20 4.60 5 3 0 38.90 2.50 5 3 0 39.80 2.70 -6 -3 0 156.18 5.30 -6 -3 0 142.09 5.30 -6 -3 0 138.89 4.40 -6 -3 0 139.09 8.50 -6 -3 0 142.59 4.60 -6 -3 0 158.28 8.60 -6 -3 0 150.98 6.40 -6 -3 0 147.19 5.90 -6 -3 0 149.29 5.80 6 3 0 148.79 6.80 6 3 0 144.49 5.30 6 3 0 135.99 8.30 6 3 0 144.99 4.50 6 3 0 143.89 5.40 6 3 0 145.99 6.70 6 3 0 135.99 8.00 6 3 0 138.29 5.80 -7 -3 0 5.10 1.70 -7 -3 0 6.30 3.50 -7 -3 0 13.50 32.20 -7 -3 0 4.40 1.70 -7 -3 0 2.10 1.20 -7 -3 0 2.60 1.40 7 3 0 2.70 1.70 7 3 0 3.90 2.90 7 3 0 6.90 2.00 7 3 0 1.50 2.20 7 3 0 5.60 1.80 7 3 0 4.90 1.80 7 3 0 3.80 1.40 -8 -3 0 3.60 1.70 -8 -3 0 -1.00 1.50 -8 -3 0 1.20 1.50 -8 -3 0 0.60 1.40 8 3 0 1.60 1.90 8 3 0 0.60 2.10 8 3 0 -0.10 1.90 -9 -3 0 2.50 2.10 -9 -3 0 1.50 1.90 -9 -3 0 -0.40 1.70 -9 -3 0 0.10 1.70 9 3 0 1.90 4.30 9 3 0 3.70 2.30 -10 -3 0 6.70 2.60 -10 -3 0 7.40 2.70 -10 -3 0 8.00 3.10 10 3 0 10.20 3.70 10 3 0 9.20 3.00 12 -4 0 29.50 4.90 -12 4 0 37.20 5.30 11 -4 0 0.30 1.90 11 -4 0 -2.10 2.30 11 -4 0 -1.60 2.30 11 -4 0 -2.60 2.30 -11 4 0 1.90 2.60 -11 4 0 -1.00 2.30 10 -4 0 -2.20 3.70 10 -4 0 4.60 2.70 10 -4 0 -0.20 1.90 10 -4 0 -1.90 1.50 10 -4 0 0.30 1.90 10 -4 0 1.10 1.80 -10 4 0 -0.10 3.50 -10 4 0 2.50 2.00 -10 4 0 4.10 2.20 -10 4 0 2.10 2.00 -10 4 0 -73.59 38.90 -10 4 0 2.40 1.70 9 -4 0 188.78 8.50 9 -4 0 194.28 7.70 9 -4 0 195.18 6.30 9 -4 0 183.28 10.40 9 -4 0 179.88 6.70 -9 4 0 185.18 7.30 -9 4 0 192.98 8.50 -9 4 0 202.48 10.50 -9 4 0 231.58 47.80 -9 4 0 195.38 6.50 -9 4 0 172.88 7.80 8 -4 0 168.58 7.40 8 -4 0 168.98 6.80 8 -4 0 169.08 5.60 8 -4 0 170.88 6.10 8 -4 0 177.78 9.20 8 -4 0 167.98 6.70 8 -4 0 173.68 5.70 -8 4 0 198.18 7.90 -8 4 0 168.38 7.10 -8 4 0 163.78 8.90 -8 4 0 173.08 6.40 -8 4 0 182.58 5.90 -8 4 0 172.18 5.90 -8 4 0 130.19 29.70 -8 4 0 181.28 6.60 7 -4 0 12.90 1.90 7 -4 0 16.10 2.40 7 -4 0 12.00 1.40 7 -4 0 14.90 1.50 7 -4 0 12.80 1.80 7 -4 0 11.60 1.50 7 -4 0 9.30 1.70 7 -4 0 14.00 3.00 7 -4 0 13.70 2.00 -7 4 0 10.40 2.00 -7 4 0 12.90 1.60 -7 4 0 16.80 2.40 -7 4 0 9.90 1.70 -7 4 0 12.80 1.60 -7 4 0 12.10 1.90 -7 4 0 10.90 2.80 -7 4 0 0.90 19.50 -7 4 0 8.00 1.90 -7 4 0 17.80 2.00 6 -4 0 98.19 3.50 6 -4 0 102.09 5.80 6 -4 0 106.79 3.50 6 -4 0 89.79 3.90 6 -4 0 103.99 6.00 6 -4 0 102.79 3.50 6 -4 0 95.09 4.20 6 -4 0 94.49 3.70 6 -4 0 105.29 3.60 6 -4 0 96.89 4.00 6 -4 0 102.49 3.60 6 -4 0 100.39 3.80 6 -4 0 102.09 4.50 6 -4 0 101.89 4.80 6 -4 0 105.19 5.50 6 -4 0 97.89 5.60 -6 4 0 103.49 4.30 -6 4 0 111.89 24.90 -6 4 0 92.79 5.60 -6 4 0 93.89 4.30 -6 4 0 102.49 4.10 -6 4 0 104.79 5.70 -6 4 0 101.09 5.70 -6 4 0 98.49 4.70 -6 4 0 102.29 3.70 -6 4 0 97.79 22.90 -6 4 0 101.19 3.30 -6 4 0 107.19 6.40 -6 4 0 96.89 3.90 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0.80 0.60 -4 4 0 1.70 0.80 -4 4 0 -1.60 1.00 -4 4 0 1.20 0.50 3 -4 0 0.70 0.50 3 -4 0 1.30 0.30 3 -4 0 1.80 0.80 3 -4 0 1.50 0.80 3 -4 0 0.60 1.00 3 -4 0 1.30 0.50 3 -4 0 2.30 0.70 3 -4 0 0.80 0.60 3 -4 0 0.60 0.80 3 -4 0 0.90 0.40 3 -4 0 1.60 0.60 3 -4 0 1.20 0.70 3 -4 0 1.90 0.90 3 -4 0 0.60 0.90 3 -4 0 3.50 1.30 3 -4 0 0.70 0.60 3 -4 0 1.60 0.50 3 -4 0 1.00 0.70 3 -4 0 1.80 0.60 -3 4 0 1.70 0.60 -3 4 0 0.90 0.80 -3 4 0 1.20 0.90 -3 4 0 0.40 0.70 -3 4 0 1.80 0.50 -3 4 0 1.70 0.80 -3 4 0 1.90 0.90 -3 4 0 1.80 0.70 -3 4 0 7.10 5.50 -3 4 0 1.40 0.70 -3 4 0 2.70 0.70 -3 4 0 1.70 0.70 -3 4 0 1.40 0.80 -3 4 0 0.80 0.70 -3 4 0 -0.60 0.60 -3 4 0 5.00 5.70 -3 4 0 1.80 0.80 -3 4 0 0.80 0.80 2 -4 0 373.46 10.40 2 -4 0 362.76 9.60 2 -4 0 383.76 17.20 2 -4 0 395.66 9.90 2 -4 0 384.46 9.20 2 -4 0 378.16 9.70 2 -4 0 385.86 9.10 2 -4 0 386.96 9.50 2 -4 0 384.36 9.40 2 -4 0 374.06 9.50 2 -4 0 382.76 9.70 2 -4 0 365.76 9.20 2 -4 0 385.16 8.90 2 -4 0 395.56 9.60 2 -4 0 382.86 9.50 2 -4 0 404.36 10.30 2 -4 0 378.66 9.30 2 -4 0 381.96 9.50 2 -4 0 383.96 9.40 -2 4 0 385.46 9.90 -2 4 0 388.96 9.40 -2 4 0 377.26 9.80 -2 4 0 393.96 9.90 -2 4 0 386.66 9.40 -2 4 0 386.46 9.40 -2 4 0 382.26 9.50 -2 4 0 375.96 9.20 -2 4 0 377.86 10.50 -2 4 0 392.96 9.60 -2 4 0 383.96 9.60 -2 4 0 385.26 9.40 -2 4 0 380.26 9.30 -2 4 0 387.06 9.40 -2 4 0 363.46 17.60 1 -4 0 62.39 2.20 1 -4 0 65.99 2.10 1 -4 0 65.49 2.10 1 -4 0 67.49 2.60 1 -4 0 63.19 2.30 1 -4 0 67.69 2.00 1 -4 0 65.69 2.50 1 -4 0 61.79 2.00 1 -4 0 63.19 2.60 1 -4 0 65.19 2.70 1 -4 0 61.89 2.20 1 -4 0 65.29 2.50 1 -4 0 58.79 2.80 1 -4 0 59.39 2.60 1 -4 0 63.39 2.20 1 -4 0 62.99 2.40 1 -4 0 56.49 6.10 1 -4 0 64.39 2.70 -1 4 0 67.39 2.60 -1 4 0 66.79 2.50 -1 4 0 65.39 1.80 -1 4 0 63.39 2.80 -1 4 0 62.09 2.10 -1 4 0 66.29 1.80 -1 4 0 65.89 2.20 -1 4 0 61.59 2.60 -1 4 0 63.89 3.00 -1 4 0 67.49 2.10 -1 4 0 68.59 5.60 -1 4 0 67.49 2.00 -1 4 0 67.09 2.40 -1 4 0 67.39 2.10 -1 4 0 57.59 2.60 -1 4 0 65.79 2.20 -1 4 0 71.49 2.60 0 -4 0 923.31 21.00 0 -4 0 966.30 22.00 0 -4 0 949.71 21.60 0 -4 0 924.11 22.20 0 -4 0 909.71 22.10 0 -4 0 925.81 22.30 0 -4 0 943.51 22.50 0 -4 0 984.30 21.20 0 -4 0 907.71 21.20 0 -4 0 916.01 21.30 0 -4 0 941.21 21.50 0 -4 0 931.91 21.50 0 -4 0 917.11 22.30 0 -4 0 942.51 21.40 0 -4 0 967.10 20.90 0 -4 0 926.11 21.90 0 -4 0 937.01 21.50 0 -4 0 933.01 22.10 0 -4 0 919.61 21.60 0 -4 0 945.61 32.70 0 4 0 901.11 22.20 0 4 0 939.51 22.10 0 4 0 923.41 21.70 0 4 0 911.91 22.50 0 4 0 944.11 21.80 0 4 0 916.41 21.40 0 4 0 954.90 31.90 0 4 0 944.01 22.10 0 4 0 945.41 22.60 0 4 0 944.91 20.90 0 4 0 941.51 21.10 0 4 0 889.81 22.80 0 4 0 948.51 21.20 0 4 0 919.11 21.50 0 4 0 948.11 21.60 0 4 0 918.51 21.20 0 4 0 921.31 21.90 0 4 0 921.01 21.70 -1 -4 0 2467.95 55.69 -1 -4 0 2465.55 55.79 -1 -4 0 2472.35 56.09 -1 -4 0 2482.55 55.49 -1 -4 0 2462.25 54.79 -1 -4 0 2448.06 75.19 -1 -4 0 2530.95 55.79 -1 -4 0 2444.26 55.79 -1 -4 0 2452.95 54.79 -1 -4 0 2483.95 56.09 -1 -4 0 2447.16 55.89 1 4 0 2467.25 55.99 1 4 0 2386.56 55.89 1 4 0 2461.55 56.19 1 4 0 2344.47 55.79 1 4 0 2485.75 74.89 1 4 0 2468.65 54.89 1 4 0 2403.66 54.99 1 4 0 2441.56 55.99 1 4 0 2369.66 55.89 1 4 0 2410.36 54.59 1 4 0 2396.36 54.89 1 4 0 2403.16 55.59 1 4 0 2373.86 55.59 1 4 0 2441.46 55.99 -2 -4 0 188.98 5.30 -2 -4 0 182.88 6.00 -2 -4 0 183.78 5.30 -2 -4 0 185.88 4.80 -2 -4 0 190.98 5.00 -2 -4 0 206.78 7.10 -2 -4 0 188.28 6.80 -2 -4 0 190.88 6.00 -2 -4 0 196.28 6.60 -2 -4 0 196.68 6.70 -2 -4 0 203.38 6.30 -2 -4 0 173.48 21.20 -2 -4 0 190.98 6.70 -2 -4 0 177.98 5.50 -2 -4 0 187.58 5.20 -2 -4 0 184.98 4.40 -2 -4 0 197.18 6.90 2 4 0 186.88 4.90 2 4 0 191.88 6.50 2 4 0 193.58 4.50 2 4 0 184.88 6.00 2 4 0 183.08 6.80 2 4 0 183.38 5.30 2 4 0 191.88 7.00 2 4 0 184.88 5.50 2 4 0 196.88 6.90 2 4 0 172.68 6.30 2 4 0 188.58 5.40 2 4 0 194.78 6.70 2 4 0 178.28 5.10 2 4 0 180.68 5.50 -3 -4 0 158.28 6.50 -3 -4 0 170.28 5.70 -3 -4 0 163.28 6.10 -3 -4 0 167.48 5.10 -3 -4 0 147.29 6.50 -3 -4 0 164.28 5.20 -3 -4 0 171.78 7.00 -3 -4 0 161.88 7.00 -3 -4 0 164.38 4.40 -3 -4 0 166.68 5.00 -3 -4 0 148.39 22.40 -3 -4 0 162.58 4.80 -3 -4 0 164.88 4.00 -3 -4 0 171.98 4.80 -3 -4 0 168.98 6.90 3 4 0 161.38 4.80 3 4 0 170.88 6.40 3 4 0 162.98 6.90 3 4 0 149.99 6.00 3 4 0 172.78 7.00 3 4 0 169.38 6.30 3 4 0 158.88 6.90 3 4 0 166.08 5.80 3 4 0 163.58 5.00 3 4 0 164.18 4.50 3 4 0 156.78 6.80 3 4 0 160.08 5.30 3 4 0 165.78 4.10 3 4 0 153.98 23.80 -4 -4 0 161.58 6.10 -4 -4 0 158.38 5.40 -4 -4 0 156.88 4.40 -4 -4 0 153.08 5.00 -4 -4 0 165.28 6.40 -4 -4 0 176.38 5.90 -4 -4 0 157.78 5.30 -4 -4 0 166.98 5.00 -4 -4 0 210.28 30.30 -4 -4 0 159.08 7.20 -4 -4 0 156.88 8.30 -4 -4 0 161.48 7.50 -4 -4 0 165.98 8.00 4 4 0 165.68 5.20 4 4 0 153.98 6.60 4 4 0 171.18 30.40 4 4 0 172.78 6.60 4 4 0 155.78 3.90 4 4 0 160.48 4.10 4 4 0 156.18 5.30 4 4 0 164.88 4.10 4 4 0 159.68 6.00 4 4 0 161.78 5.10 4 4 0 157.68 5.10 4 4 0 164.58 7.60 4 4 0 153.88 6.30 4 4 0 170.28 4.60 4 4 0 160.38 7.60 4 4 0 153.48 8.20 4 4 0 158.68 3.90 4 4 0 147.19 7.30 -5 -4 0 297.87 10.20 -5 -4 0 306.17 8.30 -5 -4 0 308.37 10.00 -5 -4 0 305.07 9.50 -5 -4 0 289.37 11.60 -5 -4 0 314.97 8.50 -5 -4 0 308.67 7.30 -5 -4 0 309.37 9.10 -5 -4 0 286.57 7.70 -5 -4 0 306.27 8.90 -5 -4 0 343.27 43.60 -5 -4 0 316.57 11.80 -5 -4 0 307.37 12.10 5 4 0 308.77 7.40 5 4 0 297.27 11.90 5 4 0 310.57 8.60 5 4 0 312.77 8.00 5 4 0 290.67 9.60 5 4 0 307.77 7.20 5 4 0 313.77 10.70 5 4 0 308.37 8.90 5 4 0 299.17 8.70 5 4 0 282.97 10.20 5 4 0 306.97 11.80 5 4 0 314.47 12.00 -6 -4 0 25.80 4.40 -6 -4 0 31.00 2.50 -6 -4 0 33.40 2.90 -6 -4 0 29.40 2.50 -6 -4 0 5.30 21.60 -6 -4 0 31.10 3.30 -6 -4 0 35.70 3.60 -6 -4 0 26.40 2.20 6 4 0 29.40 2.20 6 4 0 36.90 5.10 6 4 0 32.50 2.90 6 4 0 30.00 3.10 6 4 0 35.70 4.10 6 4 0 33.60 4.00 6 4 0 28.50 2.70 -7 -4 0 46.20 4.00 -7 -4 0 49.50 6.20 -7 -4 0 52.09 3.40 -7 -4 0 53.19 38.70 -7 -4 0 57.29 4.00 -7 -4 0 56.59 3.80 -7 -4 0 55.69 3.00 7 4 0 55.49 6.30 7 4 0 46.60 3.70 7 4 0 51.99 4.60 7 4 0 54.19 3.70 7 4 0 54.79 4.80 -8 -4 0 37.20 3.30 -8 -4 0 28.50 3.40 -8 -4 0 31.20 3.10 -8 -4 0 30.80 3.80 8 4 0 28.10 4.40 8 4 0 33.20 3.70 8 4 0 29.10 4.40 -9 -4 0 0.90 2.00 -9 -4 0 0.50 2.00 -9 -4 0 1.00 1.80 -9 -4 0 -0.70 1.80 9 4 0 2.10 2.80 -10 -4 0 -1.90 2.50 -10 -4 0 0.70 2.40 -10 -4 0 -1.20 2.50 10 4 0 2.20 3.40 12 -5 0 -1.90 2.80 12 -5 0 2.30 3.00 -12 5 0 5.90 2.50 11 -5 0 -0.60 1.90 11 -5 0 -4.00 4.10 11 -5 0 4.10 2.50 11 -5 0 -1.90 2.00 11 -5 0 -0.30 2.00 11 -5 0 0.80 2.00 -11 5 0 0.40 2.00 -11 5 0 -1.90 2.40 -11 5 0 -2.60 2.30 10 -5 0 107.49 5.50 10 -5 0 110.59 4.70 10 -5 0 105.19 4.80 10 -5 0 112.19 6.70 10 -5 0 122.79 9.30 10 -5 0 101.19 5.70 -10 5 0 104.99 6.60 -10 5 0 110.29 5.90 -10 5 0 25.70 32.80 -10 5 0 103.69 5.10 -10 5 0 123.29 8.70 9 -5 0 464.65 12.90 9 -5 0 460.45 19.70 9 -5 0 475.25 12.50 9 -5 0 488.05 15.30 9 -5 0 466.05 12.40 9 -5 0 468.85 14.20 -9 5 0 462.65 12.70 -9 5 0 460.75 13.60 -9 5 0 451.75 15.10 -9 5 0 462.65 14.60 -9 5 0 430.16 56.79 -9 5 0 455.15 17.20 8 -5 0 13.80 3.80 8 -5 0 9.50 2.00 8 -5 0 6.80 1.80 8 -5 0 9.00 1.80 8 -5 0 6.00 1.60 8 -5 0 9.30 2.40 8 -5 0 8.00 1.80 -8 5 0 7.70 1.80 -8 5 0 12.90 1.90 -8 5 0 13.20 2.60 -8 5 0 10.80 1.80 -8 5 0 11.80 2.40 -8 5 0 11.30 2.10 -8 5 0 -15.50 21.80 -8 5 0 9.70 3.10 7 -5 0 3.80 1.30 7 -5 0 3.10 2.20 7 -5 0 5.60 1.60 7 -5 0 4.90 1.60 7 -5 0 4.60 1.00 7 -5 0 4.40 1.10 7 -5 0 3.80 1.20 7 -5 0 6.80 1.60 7 -5 0 3.70 1.30 -7 5 0 5.20 1.70 -7 5 0 4.40 1.40 -7 5 0 -17.30 16.70 -7 5 0 2.40 1.20 -7 5 0 4.30 1.10 -7 5 0 2.70 1.40 -7 5 0 4.10 1.30 -7 5 0 4.90 1.90 -7 5 0 4.10 1.30 -7 5 0 1.00 1.30 6 -5 0 197.08 5.70 6 -5 0 208.78 6.80 6 -5 0 198.48 7.60 6 -5 0 204.58 8.20 6 -5 0 198.08 8.60 6 -5 0 200.28 5.90 6 -5 0 209.48 7.20 6 -5 0 211.48 8.10 6 -5 0 197.38 6.10 6 -5 0 210.08 6.40 6 -5 0 215.08 6.00 6 -5 0 196.48 7.30 6 -5 0 205.88 5.80 6 -5 0 205.28 6.50 6 -5 0 200.68 6.10 6 -5 0 197.98 5.90 -6 5 0 191.88 5.90 -6 5 0 194.78 5.60 -6 5 0 209.48 6.10 -6 5 0 203.98 8.20 -6 5 0 211.68 7.50 -6 5 0 199.78 6.30 -6 5 0 218.48 30.70 -6 5 0 195.58 6.70 -6 5 0 192.48 6.90 -6 5 0 209.78 7.70 -6 5 0 223.68 8.50 -6 5 0 201.48 6.30 -6 5 0 213.08 6.60 -6 5 0 204.98 6.20 -6 5 0 191.08 8.10 -6 5 0 194.68 8.10 5 -5 0 190.38 5.70 5 -5 0 191.58 5.40 5 -5 0 184.88 6.10 5 -5 0 186.98 6.70 5 -5 0 183.28 7.10 5 -5 0 183.38 5.20 5 -5 0 181.78 5.20 5 -5 0 185.08 6.60 5 -5 0 174.78 7.30 5 -5 0 183.88 7.70 5 -5 0 184.78 5.50 5 -5 0 182.58 5.60 -5 5 0 189.88 5.60 -5 5 0 186.38 7.10 -5 5 0 190.78 5.90 -5 5 0 193.28 6.80 -5 5 0 183.58 7.20 -5 5 0 187.68 6.60 -5 5 0 182.08 6.00 -5 5 0 182.08 6.20 -5 5 0 189.08 5.20 -5 5 0 190.98 25.60 -5 5 0 166.88 22.20 -5 5 0 187.58 5.70 -5 5 0 198.98 5.70 -5 5 0 175.88 5.60 4 -5 0 6.30 1.30 4 -5 0 6.90 1.50 4 -5 0 5.50 0.50 4 -5 0 4.50 2.50 4 -5 0 4.60 1.20 4 -5 0 4.70 1.00 4 -5 0 7.50 1.40 4 -5 0 5.60 0.40 4 -5 0 7.20 1.60 4 -5 0 2.60 0.70 4 -5 0 5.00 1.00 4 -5 0 7.20 0.90 4 -5 0 5.90 1.10 4 -5 0 5.90 1.20 4 -5 0 8.70 1.20 4 -5 0 6.20 1.00 -4 5 0 7.60 8.70 -4 5 0 5.40 1.50 -4 5 0 8.60 1.60 -4 5 0 4.50 1.40 -4 5 0 8.00 1.30 -4 5 0 4.40 1.30 -4 5 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198.68 6.00 -4 6 0 207.88 6.10 -4 6 0 185.68 18.20 -4 6 0 198.58 6.50 -4 6 0 200.68 6.40 -4 6 0 196.28 5.90 -4 6 0 195.48 5.80 -4 6 0 176.08 21.10 -4 6 0 199.88 7.00 -4 6 0 207.68 6.60 -4 6 0 211.48 6.90 3 -6 0 64.59 2.80 3 -6 0 68.89 2.20 3 -6 0 67.29 3.00 3 -6 0 58.89 3.20 3 -6 0 62.69 3.10 3 -6 0 63.59 2.70 3 -6 0 65.69 2.90 3 -6 0 64.29 2.80 3 -6 0 65.39 2.50 3 -6 0 67.99 3.50 3 -6 0 69.59 2.90 3 -6 0 63.39 2.60 3 -6 0 67.69 3.00 3 -6 0 61.19 3.10 3 -6 0 66.99 2.50 3 -6 0 69.29 2.70 3 -6 0 61.29 2.50 -3 6 0 50.29 10.50 -3 6 0 59.29 3.30 -3 6 0 62.59 2.60 -3 6 0 65.79 2.90 -3 6 0 60.79 2.70 -3 6 0 65.29 2.60 -3 6 0 62.69 2.90 -3 6 0 62.09 3.40 -3 6 0 62.09 2.80 -3 6 0 63.49 2.70 -3 6 0 66.99 3.10 -3 6 0 68.19 2.80 -3 6 0 58.49 3.00 -3 6 0 65.79 2.80 -3 6 0 64.09 2.70 -3 6 0 63.09 3.70 2 -6 0 0.90 0.80 2 -6 0 1.10 0.90 2 -6 0 0.50 1.00 2 -6 0 0.40 0.80 2 -6 0 -0.50 0.80 2 -6 0 0.90 0.90 2 -6 0 -0.10 0.60 2 -6 0 -0.30 0.70 2 -6 0 -1.00 0.90 2 -6 0 0.10 0.60 2 -6 0 -0.20 0.80 2 -6 0 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128.99 3.10 -1 -6 0 118.79 4.40 -1 -6 0 126.59 3.40 -1 -6 0 141.49 5.00 -1 -6 0 135.99 4.30 -1 -6 0 131.59 3.10 -1 -6 0 134.69 19.00 -1 -6 0 122.89 5.00 -1 -6 0 128.39 5.30 1 6 0 129.29 5.50 1 6 0 145.39 18.50 1 6 0 122.89 4.20 1 6 0 124.99 3.50 1 6 0 128.89 4.00 1 6 0 124.19 4.30 1 6 0 132.99 5.50 1 6 0 139.89 4.50 1 6 0 129.69 5.10 1 6 0 130.29 5.20 1 6 0 126.19 5.30 1 6 0 134.09 3.90 1 6 0 137.19 5.20 1 6 0 131.99 4.90 1 6 0 124.79 5.20 1 6 0 132.29 5.20 -2 -6 0 -0.10 1.00 -2 -6 0 0.80 1.20 -2 -6 0 0.70 1.20 -2 -6 0 -0.30 0.60 -2 -6 0 -0.10 1.20 -2 -6 0 0.50 1.00 -2 -6 0 0.30 0.30 -2 -6 0 -0.30 0.70 -2 -6 0 0.40 1.00 -2 -6 0 -19.80 9.90 -2 -6 0 0.70 0.90 -2 -6 0 0.30 0.60 -2 -6 0 -0.40 0.60 2 6 0 -0.40 0.70 2 6 0 0.30 0.90 2 6 0 0.20 0.80 2 6 0 -0.30 0.90 2 6 0 0.30 0.40 2 6 0 -1.40 1.00 2 6 0 -0.40 0.70 2 6 0 0.70 1.40 2 6 0 1.20 1.30 2 6 0 1.50 0.80 2 6 0 0.30 11.10 2 6 0 0.40 1.20 -3 -6 0 87.89 21.70 -3 -6 0 100.49 5.70 -3 -6 0 103.89 4.80 -3 -6 0 95.09 3.00 -3 -6 0 87.99 5.10 -3 -6 0 95.49 5.20 -3 -6 0 95.29 2.50 -3 -6 0 97.99 4.20 -3 -6 0 94.79 3.80 -3 -6 0 99.69 5.00 -3 -6 0 101.79 4.50 -3 -6 0 77.69 5.10 -3 -6 0 97.69 3.70 -3 -6 0 94.39 3.60 -3 -6 0 94.49 3.30 3 6 0 91.59 5.00 3 6 0 90.29 5.40 3 6 0 91.59 4.60 3 6 0 91.59 5.40 3 6 0 94.49 3.20 3 6 0 100.69 5.50 3 6 0 100.89 3.80 3 6 0 91.19 5.00 3 6 0 89.59 3.60 3 6 0 95.89 5.00 3 6 0 95.29 2.60 3 6 0 102.09 4.10 3 6 0 88.29 3.80 -4 -6 0 177.48 5.60 -4 -6 0 195.38 7.00 -4 -6 0 182.58 6.00 -4 -6 0 188.28 5.10 -4 -6 0 186.38 8.50 -4 -6 0 185.98 5.80 -4 -6 0 174.78 7.00 4 6 0 177.48 5.90 4 6 0 185.68 5.30 4 6 0 190.08 7.80 4 6 0 178.48 7.00 4 6 0 184.78 8.00 4 6 0 191.18 8.60 4 6 0 196.88 6.50 4 6 0 187.78 6.10 -5 -6 0 5.30 1.30 -5 -6 0 5.20 1.30 -5 -6 0 5.80 2.80 -5 -6 0 2.10 1.50 -5 -6 0 3.30 1.60 -5 -6 0 3.70 1.30 5 6 0 4.10 1.70 5 6 0 2.70 1.70 5 6 0 2.50 1.80 5 6 0 4.50 1.20 5 6 0 3.00 1.70 5 6 0 3.20 2.50 -6 -6 0 9.50 1.80 -6 -6 0 12.90 2.60 -6 -6 0 8.80 3.60 -6 -6 0 15.80 2.70 -6 -6 0 8.20 31.00 -6 -6 0 7.60 1.70 -6 -6 0 9.80 1.70 6 6 0 10.70 2.20 6 6 0 5.90 3.20 6 6 0 10.60 3.00 6 6 0 11.20 2.80 6 6 0 8.70 2.30 -7 -6 0 31.70 3.70 -7 -6 0 33.70 5.50 -7 -6 0 23.20 3.50 -7 -6 0 24.30 3.80 -7 -6 0 24.80 3.10 -7 -6 0 20.20 2.50 -7 -6 0 14.20 31.40 7 6 0 33.60 5.50 7 6 0 29.30 3.60 7 6 0 25.40 4.30 7 6 0 27.10 4.50 7 6 0 32.40 3.70 -8 -6 0 23.70 3.90 -8 -6 0 17.90 3.30 -8 -6 0 21.10 2.80 8 6 0 15.90 3.90 8 6 0 18.70 4.20 8 6 0 21.20 3.40 -9 -6 0 1.90 2.50 -9 -6 0 3.10 2.60 9 6 0 1.60 2.90 9 6 0 5.60 3.30 12 -7 0 1.50 5.20 12 -7 0 0.60 2.50 12 -7 0 -0.60 2.60 12 -7 0 3.50 2.50 12 -7 0 -1.60 2.30 12 -7 0 0.00 3.00 -12 7 0 3.10 2.90 -12 7 0 1.00 2.40 11 -7 0 11.00 3.10 11 -7 0 6.30 2.40 11 -7 0 8.40 4.40 11 -7 0 8.60 2.20 11 -7 0 11.80 2.40 11 -7 0 8.90 2.90 -11 7 0 12.20 4.80 -11 7 0 13.00 3.30 -11 7 0 10.70 4.20 -11 7 0 12.60 2.70 10 -7 0 16.30 3.40 10 -7 0 21.70 2.60 10 -7 0 15.70 2.60 10 -7 0 22.50 5.10 10 -7 0 25.20 3.50 10 -7 0 20.40 2.60 -10 7 0 24.60 3.30 -10 7 0 24.60 2.90 -10 7 0 18.30 2.60 -10 7 0 13.50 3.40 -10 7 0 20.70 4.50 9 -7 0 1.00 1.60 9 -7 0 -0.50 1.70 9 -7 0 0.00 2.70 9 -7 0 0.20 1.70 9 -7 0 1.60 2.10 9 -7 0 0.80 1.70 -9 7 0 0.60 1.50 -9 7 0 -1.40 1.60 -9 7 0 -0.30 1.40 -9 7 0 -58.79 25.20 -9 7 0 1.10 2.00 -9 7 0 0.10 1.90 -9 7 0 -1.30 2.60 8 -7 0 158.78 6.50 8 -7 0 156.18 5.80 8 -7 0 160.08 5.70 8 -7 0 169.98 7.50 8 -7 0 162.78 5.60 8 -7 0 153.48 8.20 8 -7 0 155.88 6.80 -8 7 0 185.48 37.80 -8 7 0 157.58 5.90 -8 7 0 168.38 7.00 -8 7 0 167.48 7.50 -8 7 0 167.38 5.90 -8 7 0 164.88 7.50 -8 7 0 150.88 8.20 -8 7 0 163.38 6.40 7 -7 0 42.50 3.70 7 -7 0 45.20 3.30 7 -7 0 52.09 2.90 7 -7 0 46.80 4.30 7 -7 0 48.80 3.20 7 -7 0 49.10 3.30 7 -7 0 49.70 3.00 -7 7 0 47.90 3.40 -7 7 0 102.79 27.00 -7 7 0 49.00 4.10 -7 7 0 51.39 4.30 -7 7 0 46.60 3.40 -7 7 0 45.10 3.20 -7 7 0 55.39 4.00 -7 7 0 46.80 3.00 6 -7 0 -0.20 1.70 6 -7 0 0.50 1.00 6 -7 0 0.80 1.30 6 -7 0 -0.20 1.00 6 -7 0 0.20 0.70 6 -7 0 0.20 0.90 6 -7 0 0.20 1.00 6 -7 0 1.00 0.70 6 -7 0 0.20 1.20 6 -7 0 0.20 1.10 -6 7 0 0.40 1.10 -6 7 0 1.90 1.50 -6 7 0 3.20 1.40 -6 7 0 -0.80 1.20 -6 7 0 5.40 14.20 -6 7 0 0.10 1.10 -6 7 0 -1.30 1.30 -6 7 0 1.10 1.40 -6 7 0 1.20 1.20 -6 7 0 1.20 1.00 -6 7 0 7.80 14.30 -6 7 0 0.10 1.00 -6 7 0 -1.50 0.90 5 -7 0 180.38 5.60 5 -7 0 185.48 6.30 5 -7 0 181.28 5.80 5 -7 0 167.98 5.40 5 -7 0 181.18 5.60 5 -7 0 189.48 5.50 5 -7 0 184.28 4.40 5 -7 0 173.68 5.40 5 -7 0 184.98 5.70 5 -7 0 188.08 5.50 5 -7 0 179.38 4.60 5 -7 0 178.38 6.60 5 -7 0 179.58 7.10 5 -7 0 175.18 5.70 5 -7 0 175.08 5.20 5 -7 0 167.58 5.80 5 -7 0 187.08 7.00 -5 7 0 177.38 5.80 -5 7 0 183.28 23.80 -5 7 0 183.38 6.80 -5 7 0 174.98 5.90 -5 7 0 186.08 5.60 -5 7 0 166.18 6.70 -5 7 0 179.98 6.80 -5 7 0 181.58 5.70 -5 7 0 172.88 5.30 -5 7 0 176.08 6.90 -5 7 0 170.58 6.20 -5 7 0 181.38 5.70 -5 7 0 173.48 6.30 -5 7 0 210.58 24.20 -5 7 0 177.68 6.70 4 -7 0 4.90 1.00 4 -7 0 4.10 1.30 4 -7 0 2.20 1.40 4 -7 0 3.60 0.90 4 -7 0 4.50 1.00 4 -7 0 5.80 1.10 4 -7 0 7.50 1.20 4 -7 0 3.60 0.90 4 -7 0 4.30 0.70 4 -7 0 2.90 1.00 4 -7 0 2.60 1.30 4 -7 0 3.40 1.20 4 -7 0 3.90 1.50 4 -7 0 5.10 1.10 4 -7 0 7.30 1.40 -4 7 0 4.00 1.30 -4 7 0 4.80 1.00 -4 7 0 2.80 1.20 -4 7 0 4.10 1.20 -4 7 0 4.40 1.10 -4 7 0 6.00 1.20 -4 7 0 5.70 9.80 -4 7 0 6.10 1.50 -4 7 0 -3.40 7.10 -4 7 0 3.80 1.30 -4 7 0 4.60 1.20 -4 7 0 4.30 1.30 -4 7 0 6.40 1.10 -4 7 0 5.50 1.70 -4 7 0 3.80 1.20 -4 7 0 4.30 1.00 -4 7 0 3.80 1.20 3 -7 0 170.38 6.00 3 -7 0 158.08 6.10 3 -7 0 158.18 5.00 3 -7 0 158.68 4.80 3 -7 0 154.38 5.70 3 -7 0 157.38 5.30 3 -7 0 153.58 5.10 3 -7 0 157.58 5.30 3 -7 0 155.48 5.20 3 -7 0 168.08 5.70 3 -7 0 155.58 5.10 3 -7 0 156.68 4.70 3 -7 0 162.38 4.40 3 -7 0 155.98 4.60 3 -7 0 157.08 4.90 3 -7 0 157.58 5.00 3 -7 0 164.88 5.60 3 -7 0 161.08 5.30 3 -7 0 163.38 4.80 3 -7 0 161.28 5.80 -3 7 0 160.58 4.50 -3 7 0 152.48 5.90 -3 7 0 158.18 5.60 -3 7 0 160.68 5.00 -3 7 0 153.88 5.30 -3 7 0 159.38 4.90 -3 7 0 166.08 4.90 -3 7 0 166.78 4.80 -3 7 0 161.88 5.70 -3 7 0 161.08 5.00 -3 7 0 160.58 5.60 -3 7 0 161.08 14.90 -3 7 0 166.68 6.60 -3 7 0 166.88 5.10 -3 7 0 155.18 4.80 2 -7 0 2.50 0.90 2 -7 0 1.60 0.80 2 -7 0 2.20 0.80 2 -7 0 2.90 1.10 2 -7 0 1.80 0.80 2 -7 0 1.70 0.70 2 -7 0 3.30 1.30 2 -7 0 4.20 1.10 2 -7 0 1.80 0.70 2 -7 0 2.30 0.80 2 -7 0 2.70 0.80 2 -7 0 2.00 1.30 2 -7 0 2.60 1.10 2 -7 0 0.90 0.90 2 -7 0 1.30 1.00 2 -7 0 1.00 0.80 2 -7 0 1.80 0.80 2 -7 0 2.00 0.90 2 -7 0 2.30 4.10 2 -7 0 2.90 1.00 -2 7 0 3.20 1.10 -2 7 0 2.50 1.00 -2 7 0 3.60 1.00 -2 7 0 0.20 0.90 -2 7 0 2.20 0.70 -2 7 0 2.90 0.90 -2 7 0 2.60 0.90 -2 7 0 2.10 1.20 -2 7 0 2.70 0.70 -2 7 0 1.10 1.10 -2 7 0 0.50 3.90 -2 7 0 1.70 0.80 -2 7 0 1.00 0.70 -2 7 0 2.90 1.00 1 -7 0 69.89 2.60 1 -7 0 72.59 3.10 1 -7 0 69.29 3.40 1 -7 0 72.09 2.80 1 -7 0 71.49 3.00 1 -7 0 72.29 3.30 1 -7 0 74.39 3.60 1 -7 0 70.39 2.70 1 -7 0 76.39 3.10 1 -7 0 68.79 3.10 1 -7 0 71.89 2.30 1 -7 0 72.49 2.70 1 -7 0 74.49 3.20 1 -7 0 67.29 2.50 1 -7 0 58.99 10.30 1 -7 0 76.99 3.80 1 -7 0 79.09 3.80 1 -7 0 70.29 3.80 1 -7 0 72.09 2.70 1 -7 0 73.99 3.00 -1 7 0 64.29 3.30 -1 7 0 68.39 9.00 -1 7 0 72.39 2.40 -1 7 0 79.99 3.30 -1 7 0 71.69 4.00 -1 7 0 72.29 2.60 -1 7 0 68.59 2.80 -1 7 0 64.59 2.80 -1 7 0 71.59 3.50 -1 7 0 71.49 3.10 -1 7 0 69.19 2.60 -1 7 0 75.49 2.80 -1 7 0 68.39 3.80 -1 7 0 69.29 2.70 -1 7 0 74.69 3.70 -1 7 0 67.99 2.90 0 -7 0 12.80 1.40 0 -7 0 16.30 1.70 0 -7 0 13.90 1.00 0 -7 0 12.30 1.60 0 -7 0 15.40 2.10 0 -7 0 16.50 9.60 0 -7 0 16.10 1.30 0 -7 0 13.10 0.90 0 -7 0 12.20 1.50 0 -7 0 11.00 1.20 0 -7 0 16.50 1.30 0 -7 0 13.50 0.90 0 -7 0 15.50 2.20 0 -7 0 13.80 1.70 0 -7 0 13.00 1.80 0 -7 0 11.10 1.50 0 -7 0 14.70 1.30 0 -7 0 14.40 1.10 0 -7 0 15.10 1.50 0 7 0 13.70 1.30 0 7 0 18.00 2.00 0 7 0 15.10 1.70 0 7 0 16.00 9.10 0 7 0 13.70 1.00 0 7 0 12.20 1.80 0 7 0 14.30 1.30 0 7 0 16.60 1.20 0 7 0 14.20 2.10 0 7 0 14.60 2.20 0 7 0 13.90 2.40 0 7 0 13.40 1.70 0 7 0 12.90 1.90 0 7 0 12.90 1.40 0 7 0 9.50 1.50 0 7 0 13.10 2.80 -1 -7 0 180.48 5.50 -1 -7 0 193.78 7.00 -1 -7 0 175.48 6.60 -1 -7 0 191.08 5.60 -1 -7 0 183.48 4.70 -1 -7 0 185.78 6.50 -1 -7 0 182.88 4.50 -1 -7 0 185.28 4.30 -1 -7 0 158.08 22.10 -1 -7 0 194.18 6.40 -1 -7 0 185.18 7.10 -1 -7 0 184.58 6.40 -1 -7 0 178.28 5.90 -1 -7 0 177.58 6.70 -1 -7 0 180.28 5.10 -1 -7 0 191.98 6.80 -1 -7 0 182.68 5.60 -1 -7 0 184.48 5.10 1 7 0 184.38 6.70 1 7 0 185.28 6.80 1 7 0 189.48 6.90 1 7 0 191.18 7.20 1 7 0 187.18 4.80 1 7 0 179.28 6.20 1 7 0 192.28 7.30 1 7 0 174.68 5.60 1 7 0 183.48 6.70 1 7 0 184.08 5.30 1 7 0 180.78 6.60 1 7 0 179.88 6.90 1 7 0 190.58 5.20 1 7 0 190.08 5.90 1 7 0 187.68 6.00 1 7 0 190.48 22.20 -2 -7 0 191.78 6.50 -2 -7 0 202.18 7.20 -2 -7 0 204.08 4.90 -2 -7 0 209.88 7.40 -2 -7 0 205.38 6.10 -2 -7 0 210.18 5.60 -2 -7 0 197.78 7.70 -2 -7 0 202.98 7.80 -2 -7 0 203.48 7.90 -2 -7 0 199.28 27.30 -2 -7 0 196.58 5.40 -2 -7 0 192.48 7.40 -2 -7 0 204.18 6.20 -2 -7 0 190.48 6.90 2 7 0 205.48 8.00 2 7 0 202.48 5.00 2 7 0 193.78 7.60 2 7 0 187.28 7.60 2 7 0 194.48 6.20 2 7 0 210.38 27.50 2 7 0 202.78 5.90 2 7 0 187.68 6.30 2 7 0 206.88 6.50 2 7 0 193.88 7.70 2 7 0 208.18 5.60 2 7 0 205.78 8.00 2 7 0 199.58 7.80 2 7 0 203.68 6.40 2 7 0 191.58 7.10 -3 -7 0 320.17 8.90 -3 -7 0 326.07 10.30 -3 -7 0 312.67 8.40 -3 -7 0 327.37 8.00 -3 -7 0 300.17 42.20 -3 -7 0 328.17 10.10 -3 -7 0 321.87 11.60 -3 -7 0 319.87 8.90 3 7 0 313.07 9.30 3 7 0 334.47 11.30 3 7 0 307.97 8.70 3 7 0 316.07 11.10 3 7 0 305.07 9.10 3 7 0 315.07 11.40 3 7 0 319.87 10.40 3 7 0 315.17 8.20 -4 -7 0 16.50 1.90 -4 -7 0 18.50 1.70 -4 -7 0 16.00 2.50 -4 -7 0 14.40 1.80 -4 -7 0 17.90 3.40 -4 -7 0 26.00 2.90 4 7 0 18.10 1.60 4 7 0 14.90 2.20 4 7 0 19.50 2.60 4 7 0 16.10 3.30 4 7 0 16.30 3.00 4 7 0 19.30 2.10 4 7 0 21.40 3.20 -5 -7 0 25.60 2.40 -5 -7 0 21.10 2.90 -5 -7 0 29.80 2.50 -5 -7 0 25.50 4.40 -5 -7 0 25.30 2.20 -5 -7 0 24.60 3.10 5 7 0 22.40 4.10 5 7 0 21.10 3.00 5 7 0 30.70 4.30 5 7 0 25.40 3.70 -6 -7 0 4.20 2.70 -6 -7 0 5.70 2.60 -6 -7 0 3.40 1.80 -6 -7 0 3.20 1.60 -6 -7 0 3.70 1.50 -6 -7 0 26.80 36.40 -6 -7 0 0.40 1.70 6 7 0 6.60 2.70 6 7 0 4.60 1.80 6 7 0 6.70 2.90 6 7 0 4.40 3.50 6 7 0 2.40 2.30 -7 -7 0 31.00 2.90 -7 -7 0 29.80 5.80 -7 -7 0 32.80 4.00 -7 -7 0 25.20 3.20 -7 -7 0 30.90 3.90 7 7 0 23.40 5.40 7 7 0 35.60 4.10 7 7 0 41.00 5.40 7 7 0 40.50 5.00 7 7 0 32.70 4.00 -8 -7 0 38.30 4.60 -8 -7 0 46.50 5.10 8 7 0 31.00 4.40 8 7 0 39.90 5.60 8 7 0 44.60 5.80 -9 -7 0 4.80 2.90 9 7 0 4.20 3.70 12 -8 0 0.90 3.20 12 -8 0 5.30 3.30 12 -8 0 12.40 6.00 12 -8 0 7.10 2.70 12 -8 0 2.50 2.50 12 -8 0 7.00 2.90 -12 8 0 5.50 3.10 -12 8 0 7.10 2.80 -12 8 0 7.30 4.40 11 -8 0 -4.80 4.10 11 -8 0 2.30 2.90 11 -8 0 1.70 1.90 11 -8 0 1.60 2.30 11 -8 0 -0.90 1.90 -11 8 0 0.60 2.50 -11 8 0 1.70 2.00 -11 8 0 1.60 2.70 -11 8 0 -1.90 3.10 10 -8 0 3.10 1.70 10 -8 0 1.60 1.90 10 -8 0 3.10 2.10 10 -8 0 2.80 3.40 10 -8 0 1.80 3.10 10 -8 0 4.80 2.50 -10 8 0 4.10 3.80 -10 8 0 4.90 3.20 -10 8 0 3.10 2.40 -10 8 0 2.30 1.90 -10 8 0 4.00 2.50 -10 8 0 -1.40 1.60 9 -8 0 101.09 6.30 9 -8 0 93.69 7.00 9 -8 0 93.09 4.30 9 -8 0 95.09 5.60 9 -8 0 93.09 4.30 9 -8 0 88.69 4.70 -9 8 0 84.79 5.90 -9 8 0 91.59 6.00 -9 8 0 95.49 7.20 -9 8 0 89.89 4.60 -9 8 0 92.69 4.40 -9 8 0 77.99 35.60 -9 8 0 87.79 5.20 8 -8 0 232.98 8.30 8 -8 0 241.38 9.00 8 -8 0 242.78 9.40 8 -8 0 235.48 8.50 8 -8 0 240.08 7.50 -8 8 0 246.18 9.70 -8 8 0 237.78 8.30 -8 8 0 235.58 11.70 -8 8 0 203.08 33.60 -8 8 0 249.68 7.80 -8 8 0 239.78 9.60 7 -8 0 16.20 1.90 7 -8 0 17.40 1.90 7 -8 0 21.40 3.10 7 -8 0 20.80 2.20 7 -8 0 19.80 2.40 7 -8 0 20.00 3.20 7 -8 0 20.40 2.70 -7 8 0 19.10 3.00 -7 8 0 21.20 2.50 -7 8 0 24.60 2.80 -7 8 0 11.70 16.40 -7 8 0 20.80 2.30 -7 8 0 18.40 2.90 -7 8 0 17.00 2.00 -7 8 0 19.90 3.10 6 -8 0 14.20 1.60 6 -8 0 11.20 1.60 6 -8 0 10.70 2.20 6 -8 0 10.90 2.10 6 -8 0 12.80 1.80 6 -8 0 12.60 1.80 6 -8 0 11.40 1.60 6 -8 0 15.30 2.80 -6 8 0 15.00 2.50 -6 8 0 0.40 12.70 -6 8 0 12.40 2.10 -6 8 0 14.90 1.70 -6 8 0 13.90 2.50 -6 8 0 -1.00 17.10 -6 8 0 12.80 1.80 -6 8 0 13.90 1.80 -6 8 0 12.80 2.40 -6 8 0 14.90 2.40 -6 8 0 13.50 2.20 -6 8 0 14.10 1.90 5 -8 0 145.99 4.80 5 -8 0 138.99 6.10 5 -8 0 131.99 5.40 5 -8 0 143.99 4.40 5 -8 0 148.29 3.90 5 -8 0 143.69 5.10 5 -8 0 139.39 5.10 5 -8 0 140.09 4.70 5 -8 0 148.59 5.10 5 -8 0 153.88 5.70 5 -8 0 148.29 4.80 5 -8 0 143.29 6.10 5 -8 0 136.49 5.60 5 -8 0 147.59 4.90 5 -8 0 139.79 5.30 -5 8 0 147.79 5.70 -5 8 0 147.49 5.20 -5 8 0 140.69 5.20 -5 8 0 142.49 5.40 -5 8 0 144.89 5.00 -5 8 0 119.79 17.70 -5 8 0 143.19 5.80 -5 8 0 146.79 5.30 -5 8 0 145.49 5.80 -5 8 0 149.99 6.10 -5 8 0 133.29 5.70 -5 8 0 139.59 4.80 -5 8 0 157.18 21.60 -5 8 0 160.78 5.90 -5 8 0 147.89 5.20 -5 8 0 147.49 4.90 4 -8 0 -0.70 1.10 4 -8 0 1.20 1.30 4 -8 0 0.30 0.50 4 -8 0 1.70 1.10 4 -8 0 0.60 0.80 4 -8 0 -0.20 0.80 4 -8 0 1.00 0.90 4 -8 0 0.00 0.80 4 -8 0 0.30 0.70 4 -8 0 -0.20 0.80 4 -8 0 0.10 0.70 4 -8 0 1.10 0.80 4 -8 0 -0.30 1.00 4 -8 0 1.20 1.20 4 -8 0 -0.90 1.00 4 -8 0 0.20 0.80 -4 8 0 0.10 1.10 -4 8 0 3.30 6.80 -4 8 0 1.00 1.00 -4 8 0 0.20 0.80 -4 8 0 0.40 0.90 -4 8 0 0.90 1.20 -4 8 0 0.00 0.90 -4 8 0 0.80 0.90 -4 8 0 -0.10 1.10 -4 8 0 0.30 0.80 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688.73 17.40 2 -8 0 690.83 16.30 2 -8 0 685.93 17.00 2 -8 0 686.93 16.50 2 -8 0 711.03 17.00 2 -8 0 694.23 17.40 -2 8 0 687.73 16.50 -2 8 0 680.63 16.30 -2 8 0 689.53 18.40 -2 8 0 692.93 18.00 -2 8 0 686.33 18.80 -2 8 0 703.83 16.70 -2 8 0 678.23 17.70 -2 8 0 681.53 16.60 -2 8 0 701.93 16.30 -2 8 0 677.73 16.50 -2 8 0 731.43 20.50 -2 8 0 706.63 22.90 1 -8 0 315.87 8.10 1 -8 0 313.87 8.70 1 -8 0 308.77 8.80 1 -8 0 322.57 9.20 1 -8 0 328.17 8.50 1 -8 0 303.07 8.20 1 -8 0 305.47 9.10 1 -8 0 309.07 10.10 1 -8 0 280.97 20.20 1 -8 0 320.27 10.00 1 -8 0 312.27 8.70 1 -8 0 317.17 9.50 1 -8 0 301.97 8.10 1 -8 0 311.07 9.90 1 -8 0 309.57 8.80 1 -8 0 320.07 8.80 1 -8 0 299.97 8.00 1 -8 0 315.87 7.70 -1 8 0 310.87 9.50 -1 8 0 297.37 8.60 -1 8 0 315.77 10.20 -1 8 0 314.37 8.50 -1 8 0 317.27 7.80 -1 8 0 345.47 8.40 -1 8 0 319.07 18.20 -1 8 0 315.77 9.00 -1 8 0 305.57 8.50 -1 8 0 311.47 8.00 -1 8 0 319.27 9.50 -1 8 0 312.47 9.90 -1 8 0 301.87 10.30 -1 8 0 318.47 9.40 -1 8 0 301.67 8.10 0 -8 0 11.80 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447.26 11.40 -5 10 0 431.76 12.40 -5 10 0 421.46 11.10 -5 10 0 440.96 12.70 -5 10 0 451.95 11.70 -5 10 0 429.76 13.60 -5 10 0 425.66 11.90 -5 10 0 410.66 12.10 -5 10 0 392.46 26.00 -5 10 0 426.86 11.90 -5 10 0 406.16 30.20 -5 10 0 442.26 11.50 -5 10 0 447.16 12.00 -5 10 0 441.46 13.30 -5 10 0 411.96 12.80 4 -10 0 92.99 3.80 4 -10 0 94.59 5.00 4 -10 0 88.39 4.00 4 -10 0 89.09 3.60 4 -10 0 91.09 4.80 4 -10 0 95.19 5.20 4 -10 0 92.09 4.10 4 -10 0 89.39 3.80 4 -10 0 89.89 3.60 4 -10 0 91.59 3.20 4 -10 0 96.79 4.60 4 -10 0 90.39 3.40 4 -10 0 98.79 4.60 4 -10 0 94.19 4.00 4 -10 0 94.39 3.60 -4 10 0 90.79 4.30 -4 10 0 100.49 4.00 -4 10 0 89.09 3.80 -4 10 0 93.29 4.00 -4 10 0 96.49 3.70 -4 10 0 91.19 5.50 -4 10 0 89.19 4.50 -4 10 0 95.29 4.10 -4 10 0 105.69 10.90 -4 10 0 96.19 4.80 -4 10 0 89.19 12.10 -4 10 0 88.09 4.90 -4 10 0 91.99 3.90 3 -10 0 16.80 2.70 3 -10 0 19.70 2.20 3 -10 0 21.50 1.90 3 -10 0 20.90 2.40 3 -10 0 20.30 1.70 3 -10 0 20.30 2.80 3 -10 0 20.80 1.40 3 -10 0 16.30 1.80 3 -10 0 17.80 2.30 3 -10 0 23.20 1.70 3 -10 0 20.20 2.50 3 -10 0 20.10 1.70 3 -10 0 25.90 2.90 3 -10 0 23.60 2.30 3 -10 0 23.20 2.40 -3 10 0 20.50 1.80 -3 10 0 22.00 3.20 -3 10 0 18.40 2.20 -3 10 0 20.90 1.80 -3 10 0 27.80 3.10 -3 10 0 22.40 1.80 -3 10 0 17.80 2.30 -3 10 0 24.60 2.10 -3 10 0 21.60 2.00 -3 10 0 23.90 2.30 2 -10 0 50.89 2.30 2 -10 0 50.49 2.60 2 -10 0 57.59 2.40 2 -10 0 52.29 2.60 2 -10 0 47.60 3.00 2 -10 0 57.89 3.80 2 -10 0 51.09 2.60 2 -10 0 50.89 3.60 2 -10 0 50.99 2.60 2 -10 0 51.59 3.00 2 -10 0 53.69 3.00 2 -10 0 53.39 2.60 2 -10 0 55.89 3.20 2 -10 0 50.99 3.70 2 -10 0 38.40 7.60 2 -10 0 46.90 3.00 -2 10 0 51.99 2.60 -2 10 0 42.00 3.60 -2 10 0 50.19 2.80 -2 10 0 56.89 2.60 -2 10 0 52.39 3.20 -2 10 0 55.89 2.80 -2 10 0 59.19 3.30 -2 10 0 46.20 6.90 -2 10 0 61.09 3.70 -2 10 0 55.29 3.50 -2 10 0 52.19 4.20 -2 10 0 56.19 2.40 1 -10 0 21.00 2.90 1 -10 0 21.10 2.40 1 -10 0 25.60 2.10 1 -10 0 23.70 2.50 1 -10 0 25.10 3.20 1 -10 0 22.10 1.90 1 -10 0 21.10 1.80 1 -10 0 24.50 2.00 1 -10 0 23.10 1.90 1 -10 0 8.20 11.50 1 -10 0 23.80 2.70 1 -10 0 25.20 2.30 1 -10 0 26.20 2.50 1 -10 0 25.80 1.40 1 -10 0 23.20 2.20 1 -10 0 24.60 1.50 -1 10 0 27.90 3.30 -1 10 0 25.50 1.60 -1 10 0 21.00 1.70 -1 10 0 25.80 2.10 -1 10 0 21.60 2.30 -1 10 0 22.50 2.60 -1 10 0 25.40 2.10 -1 10 0 23.50 2.40 -1 10 0 20.80 2.60 -1 10 0 27.60 3.50 -1 10 0 22.80 2.20 -1 10 0 16.70 9.30 -1 10 0 30.40 2.30 -1 10 0 27.30 3.30 0 -10 0 13.30 1.60 0 -10 0 23.70 14.60 0 -10 0 15.00 2.30 0 -10 0 16.60 1.90 0 -10 0 15.20 2.10 0 -10 0 13.90 1.10 0 -10 0 12.50 2.70 0 -10 0 15.30 2.10 0 -10 0 12.10 2.20 0 -10 0 11.10 1.60 0 -10 0 15.00 1.40 0 -10 0 9.90 1.50 0 -10 0 19.30 2.40 0 -10 0 17.40 2.80 0 10 0 14.80 2.30 0 10 0 16.80 2.40 0 10 0 12.30 2.50 0 10 0 12.60 1.60 0 10 0 12.00 2.20 0 10 0 11.40 2.10 0 10 0 22.40 13.60 0 10 0 17.30 2.20 0 10 0 15.10 2.30 0 10 0 14.90 1.40 0 10 0 14.20 2.80 0 10 0 13.50 1.60 0 10 0 15.30 2.80 -1 -10 0 5.70 1.90 -1 -10 0 3.40 1.20 -1 -10 0 1.20 1.20 -1 -10 0 1.30 1.20 -1 -10 0 2.70 1.00 -1 -10 0 3.00 1.40 -1 -10 0 1.60 0.90 -1 -10 0 0.90 1.70 1 10 0 2.50 1.20 1 10 0 0.10 1.40 1 10 0 3.10 1.40 1 10 0 2.50 1.70 1 10 0 1.80 1.50 1 10 0 2.00 1.90 1 10 0 5.00 2.10 -2 -10 0 26.40 3.30 -2 -10 0 29.50 4.10 -2 -10 0 28.80 2.40 -2 -10 0 23.00 2.90 -2 -10 0 26.30 1.90 2 10 0 27.90 2.20 2 10 0 32.20 4.40 2 10 0 23.00 3.40 2 10 0 32.60 3.60 2 10 0 32.90 4.30 2 10 0 30.60 3.20 -3 -10 0 5.30 1.60 -3 -10 0 6.90 2.10 -3 -10 0 8.40 2.90 -3 -10 0 9.00 2.30 3 10 0 8.60 2.90 3 10 0 3.10 2.40 3 10 0 3.20 2.30 3 10 0 4.90 2.00 3 10 0 10.50 3.20 -4 -10 0 61.49 3.80 -4 -10 0 63.49 4.40 -4 -10 0 66.99 4.70 -4 -10 0 74.59 6.40 4 10 0 64.99 4.50 4 10 0 67.39 5.80 4 10 0 63.79 4.70 4 10 0 61.99 6.70 4 10 0 61.49 6.20 -5 -10 0 0.70 3.20 -5 -10 0 3.70 2.10 -5 -10 0 4.20 1.90 -5 -10 0 4.80 2.20 5 10 0 8.00 3.20 5 10 0 5.10 2.40 5 10 0 4.70 2.80 5 10 0 11.70 3.60 5 10 0 5.70 2.70 -6 -10 0 2.40 1.80 -6 -10 0 -3.70 3.50 -6 -10 0 2.50 2.00 6 10 0 0.70 2.00 6 10 0 1.90 3.50 6 10 0 -1.10 3.30 6 10 0 0.80 2.90 6 10 0 4.40 3.50 -7 -10 0 26.60 6.70 -7 -10 0 16.60 2.80 -7 -10 0 16.40 4.40 -7 -10 0 24.80 4.20 7 10 0 23.10 4.30 7 10 0 26.00 5.60 7 10 0 21.30 4.80 7 10 0 20.00 3.80 11 -11 0 19.70 3.10 11 -11 0 24.80 4.60 11 -11 0 16.00 3.30 11 -11 0 20.50 3.10 11 -11 0 15.70 4.60 11 -11 0 16.30 2.90 11 -11 0 19.60 4.10 -11 11 0 20.40 4.30 -11 11 0 21.60 3.70 -11 11 0 18.20 3.20 -11 11 0 10.80 3.70 -11 11 0 13.20 4.30 -11 11 0 15.30 3.20 10 -11 0 111.39 8.00 10 -11 0 112.89 5.50 10 -11 0 114.79 7.00 10 -11 0 112.99 5.60 10 -11 0 110.39 5.20 -10 11 0 110.99 6.60 -10 11 0 97.79 7.90 -10 11 0 111.89 7.30 -10 11 0 106.39 5.60 -10 11 0 107.19 5.60 9 -11 0 157.28 6.00 9 -11 0 154.08 8.20 9 -11 0 151.18 6.20 9 -11 0 167.68 8.40 9 -11 0 140.29 7.30 9 -11 0 153.78 6.00 -9 11 0 145.79 8.00 -9 11 0 147.29 6.30 -9 11 0 150.88 6.30 -9 11 0 145.29 8.10 -9 11 0 142.39 6.90 -9 11 0 155.88 8.50 8 -11 0 27.40 3.80 8 -11 0 32.30 2.90 8 -11 0 30.90 2.90 8 -11 0 30.80 3.10 8 -11 0 27.50 3.50 8 -11 0 32.40 4.10 -8 11 0 31.60 4.20 -8 11 0 33.90 3.20 -8 11 0 30.80 3.40 -8 11 0 29.20 4.00 -8 11 0 25.30 2.80 -8 11 0 31.10 4.20 7 -11 0 8.80 2.10 7 -11 0 11.50 2.60 7 -11 0 9.90 2.10 7 -11 0 11.50 1.90 -7 11 0 14.20 2.40 -7 11 0 9.20 1.90 -7 11 0 10.90 17.40 -7 11 0 8.40 2.40 -7 11 0 9.90 2.60 -7 11 0 8.00 2.70 -7 11 0 12.10 2.20 6 -11 0 9.10 1.50 6 -11 0 9.30 1.80 6 -11 0 7.60 1.60 6 -11 0 4.70 2.20 6 -11 0 7.90 1.90 6 -11 0 5.10 1.70 6 -11 0 7.60 2.50 -6 11 0 13.00 1.90 -6 11 0 6.00 1.90 -6 11 0 4.60 1.70 -6 11 0 7.60 2.30 -6 11 0 7.80 1.80 -6 11 0 8.30 2.40 -6 11 0 8.60 13.60 -6 11 0 11.50 2.10 5 -11 0 4.80 1.70 5 -11 0 2.70 1.50 5 -11 0 4.80 1.60 5 -11 0 5.60 1.30 5 -11 0 3.40 0.90 5 -11 0 5.10 1.40 5 -11 0 4.20 1.50 5 -11 0 3.40 1.50 5 -11 0 5.00 1.20 5 -11 0 5.40 1.40 -5 11 0 -3.60 8.00 -5 11 0 3.60 1.30 -5 11 0 4.60 2.00 -5 11 0 6.10 1.90 -5 11 0 19.70 13.10 -5 11 0 8.50 1.60 -5 11 0 4.00 1.40 -5 11 0 3.60 1.50 -5 11 0 5.00 1.80 -5 11 0 2.80 1.30 -5 11 0 7.20 1.90 -5 11 0 4.20 1.40 4 -11 0 145.09 4.50 4 -11 0 132.19 5.00 4 -11 0 129.29 7.20 4 -11 0 139.69 6.40 4 -11 0 141.39 4.50 4 -11 0 146.09 6.90 4 -11 0 135.09 5.70 4 -11 0 136.49 4.20 4 -11 0 142.49 5.60 4 -11 0 140.09 4.90 4 -11 0 144.19 5.40 4 -11 0 140.69 4.80 4 -11 0 133.39 5.40 -4 11 0 144.19 6.20 -4 11 0 116.49 6.10 -4 11 0 140.89 5.40 -4 11 0 141.89 5.10 -4 11 0 142.49 5.00 -4 11 0 119.39 6.90 -4 11 0 139.09 4.80 -4 11 0 131.89 5.10 -4 11 0 146.39 5.30 3 -11 0 92.19 4.10 3 -11 0 91.69 3.50 3 -11 0 83.69 4.80 3 -11 0 83.69 4.80 3 -11 0 87.59 2.80 3 -11 0 87.09 4.10 3 -11 0 87.99 4.30 3 -11 0 84.09 4.20 3 -11 0 88.89 4.10 3 -11 0 82.99 3.30 3 -11 0 80.09 4.40 3 -11 0 87.69 3.50 3 -11 0 88.59 2.80 -3 11 0 90.49 3.70 -3 11 0 81.69 3.80 -3 11 0 85.19 3.50 -3 11 0 86.09 4.30 -3 11 0 87.59 4.90 -3 11 0 94.99 3.80 -3 11 0 91.49 3.80 -3 11 0 81.39 4.40 -3 11 0 88.79 5.70 -3 11 0 89.79 4.30 2 -11 0 5.10 1.40 2 -11 0 2.90 1.80 2 -11 0 2.80 0.90 2 -11 0 5.50 1.00 2 -11 0 3.60 1.60 2 -11 0 4.90 1.40 2 -11 0 2.50 6.10 2 -11 0 2.70 1.20 2 -11 0 3.90 1.20 2 -11 0 4.60 1.60 2 -11 0 3.80 1.10 2 -11 0 2.00 1.30 2 -11 0 3.90 1.10 2 -11 0 2.60 1.80 2 -11 0 5.60 1.20 -2 11 0 3.50 1.40 -2 11 0 4.80 1.40 -2 11 0 6.10 1.30 -2 11 0 4.10 1.10 -2 11 0 5.10 1.90 -2 11 0 5.50 1.60 -2 11 0 3.70 1.70 -2 11 0 3.90 1.50 -2 11 0 4.90 2.00 -2 11 0 4.90 1.70 1 -11 0 17.00 2.20 1 -11 0 20.00 1.80 1 -11 0 19.20 2.60 1 -11 0 16.00 1.80 1 -11 0 17.60 1.30 1 -11 0 19.30 2.40 1 -11 0 24.70 12.90 1 -11 0 20.00 3.20 1 -11 0 17.10 1.90 1 -11 0 23.40 3.20 1 -11 0 22.40 2.30 1 -11 0 22.60 2.10 -1 11 0 21.80 2.80 -1 11 0 20.20 3.30 -1 11 0 20.30 1.60 -1 11 0 16.70 2.70 -1 11 0 15.90 10.20 -1 11 0 20.30 2.30 -1 11 0 18.60 2.50 -1 11 0 15.70 1.60 -1 11 0 17.50 2.30 -1 11 0 19.50 3.20 -1 11 0 15.60 1.80 0 -11 0 177.38 7.30 0 -11 0 186.68 5.60 0 -11 0 181.88 6.90 0 -11 0 193.38 8.30 0 -11 0 188.38 6.20 0 -11 0 179.78 7.10 0 -11 0 180.08 7.10 0 -11 0 167.88 5.60 0 -11 0 186.38 7.40 0 -11 0 194.28 6.20 0 11 0 191.48 7.10 0 11 0 176.18 6.70 0 11 0 183.48 5.90 0 11 0 196.18 7.80 0 11 0 182.18 5.40 0 11 0 161.78 8.20 0 11 0 181.78 7.10 -1 -11 0 78.69 5.20 -1 -11 0 90.79 5.00 -1 -11 0 76.99 5.30 -1 -11 0 77.09 3.80 -1 -11 0 83.49 4.80 -1 -11 0 77.49 4.50 1 11 0 80.29 5.00 1 11 0 76.29 5.60 1 11 0 64.69 5.20 1 11 0 69.19 4.30 1 11 0 84.09 5.10 1 11 0 85.29 4.70 1 11 0 78.89 3.50 -2 -11 0 29.10 3.40 -2 -11 0 23.80 2.50 -2 -11 0 26.70 4.20 -2 -11 0 22.60 3.60 2 11 0 21.20 3.30 2 11 0 14.50 3.10 2 11 0 24.20 3.70 2 11 0 26.20 4.20 -3 -11 0 98.09 5.40 -3 -11 0 104.09 4.70 -3 -11 0 98.49 5.90 -3 -11 0 86.19 6.80 3 11 0 92.79 6.80 3 11 0 95.29 6.80 3 11 0 98.59 5.30 3 11 0 86.99 5.70 3 11 0 76.59 6.20 -4 -11 0 115.09 6.50 -4 -11 0 102.29 7.70 -4 -11 0 107.29 6.20 -4 -11 0 110.89 5.00 4 11 0 122.59 8.10 4 11 0 118.49 6.90 4 11 0 124.89 7.90 4 11 0 125.39 6.40 4 11 0 117.49 8.20 -5 -11 0 2.40 1.70 -5 -11 0 4.20 3.60 -5 -11 0 1.10 1.80 -5 -11 0 0.20 1.70 5 11 0 3.60 2.60 5 11 0 5.70 3.10 5 11 0 4.90 3.80 5 11 0 3.10 2.90 -6 -11 0 3.20 2.40 -6 -11 0 0.50 2.00 -6 -11 0 -1.80 1.90 -6 -11 0 -0.50 4.50 6 11 0 4.00 2.80 6 11 0 1.60 3.10 6 11 0 2.20 3.60 6 11 0 1.20 2.30 11 -12 0 4.70 2.70 11 -12 0 6.80 2.70 11 -12 0 6.20 2.40 11 -12 0 1.30 2.80 11 -12 0 9.40 3.40 11 -12 0 11.20 4.00 11 -12 0 3.00 2.90 -11 12 0 12.10 3.70 -11 12 0 7.50 4.20 -11 12 0 10.20 3.40 -11 12 0 7.50 3.30 -11 12 0 6.80 2.80 -11 12 0 10.20 2.90 10 -12 0 -0.50 1.80 10 -12 0 -1.30 2.20 10 -12 0 0.50 2.20 10 -12 0 -0.90 2.30 -10 12 0 -3.00 2.00 -10 12 0 -1.50 2.30 -10 12 0 3.60 2.80 -10 12 0 -0.20 1.80 9 -12 0 6.20 2.60 9 -12 0 9.80 3.00 9 -12 0 9.30 2.50 9 -12 0 4.50 1.90 9 -12 0 5.70 2.00 9 -12 0 7.20 2.20 -9 12 0 11.10 3.20 -9 12 0 3.80 2.40 -9 12 0 3.30 2.00 -9 12 0 4.50 2.60 -9 12 0 6.20 2.70 -9 12 0 4.70 2.00 8 -12 0 22.70 2.60 8 -12 0 26.80 4.20 8 -12 0 23.90 3.40 8 -12 0 19.50 2.70 8 -12 0 20.60 2.50 -8 12 0 20.80 3.60 -8 12 0 20.20 2.70 -8 12 0 17.70 3.40 -8 12 0 23.70 3.30 -8 12 0 21.40 3.60 -8 12 0 18.40 2.50 7 -12 0 22.20 3.10 7 -12 0 23.40 2.80 7 -12 0 22.80 3.70 7 -12 0 28.00 2.90 7 -12 0 23.20 2.60 -7 12 0 21.30 3.40 -7 12 0 25.50 2.80 -7 12 0 23.20 3.80 -7 12 0 12.30 17.80 -7 12 0 26.70 2.90 -7 12 0 21.40 3.10 -7 12 0 22.10 2.90 6 -12 0 34.00 3.20 6 -12 0 35.20 3.10 6 -12 0 39.90 4.00 6 -12 0 35.10 4.20 6 -12 0 37.90 2.90 6 -12 0 37.40 3.20 -6 12 0 40.00 4.80 -6 12 0 42.20 4.60 -6 12 0 35.40 3.00 -6 12 0 43.40 4.10 -6 12 0 8.80 15.70 -6 12 0 34.10 3.20 -6 12 0 37.00 4.00 -6 12 0 31.20 2.80 5 -12 0 85.09 4.40 5 -12 0 89.59 3.90 5 -12 0 86.69 6.10 5 -12 0 90.79 4.40 5 -12 0 90.49 5.70 5 -12 0 89.99 5.10 5 -12 0 80.29 3.30 5 -12 0 88.49 3.40 5 -12 0 84.79 5.40 5 -12 0 80.99 3.80 -5 12 0 88.49 4.50 -5 12 0 87.19 5.10 -5 12 0 88.39 4.10 -5 12 0 82.79 4.20 -5 12 0 89.09 6.00 -5 12 0 77.69 4.30 -5 12 0 69.99 7.70 -5 12 0 79.49 5.20 -5 12 0 88.69 4.00 -5 12 0 73.19 7.70 4 -12 0 107.59 4.20 4 -12 0 106.69 4.50 4 -12 0 96.99 4.50 4 -12 0 104.39 3.90 4 -12 0 100.79 4.80 4 -12 0 114.89 4.90 4 -12 0 104.49 6.00 4 -12 0 108.19 5.80 4 -12 0 99.79 5.10 4 -12 0 107.79 4.80 -4 12 0 102.39 4.40 -4 12 0 100.69 5.70 -4 12 0 108.19 5.40 -4 12 0 107.99 4.70 -4 12 0 107.29 4.70 -4 12 0 101.39 4.40 -4 12 0 110.99 4.90 -4 12 0 98.09 6.40 -4 12 0 110.79 4.40 3 -12 0 2.50 1.60 3 -12 0 2.20 1.20 3 -12 0 2.20 1.10 3 -12 0 1.80 1.00 3 -12 0 0.60 1.50 3 -12 0 2.50 1.70 3 -12 0 4.20 1.70 3 -12 0 1.10 1.10 3 -12 0 2.00 1.20 3 -12 0 -0.60 1.30 -3 12 0 2.00 1.50 -3 12 0 0.70 2.10 -3 12 0 4.70 2.20 -3 12 0 2.90 1.30 -3 12 0 3.40 1.40 -3 12 0 3.10 1.90 -3 12 0 2.90 1.20 -3 12 0 0.00 1.40 -3 12 0 2.50 1.20 2 -12 0 0.60 1.50 2 -12 0 -0.10 1.30 2 -12 0 0.50 1.20 2 -12 0 0.20 1.10 2 -12 0 -0.60 0.80 2 -12 0 -2.50 5.30 2 -12 0 0.40 1.10 2 -12 0 1.20 1.70 2 -12 0 -0.10 7.10 2 -12 0 -0.80 0.80 2 -12 0 -1.00 1.10 2 -12 0 0.30 1.10 2 -12 0 -0.70 1.20 2 -12 0 0.50 1.60 -2 12 0 -0.70 1.10 -2 12 0 1.20 1.10 -2 12 0 -0.10 1.40 -2 12 0 1.00 1.70 -2 12 0 -2.60 1.50 -2 12 0 -0.50 1.60 -2 12 0 -0.90 1.30 -2 12 0 -0.10 1.00 -2 12 0 0.20 1.10 -2 12 0 0.90 1.80 1 -12 0 256.27 8.90 1 -12 0 259.47 39.80 1 -12 0 232.48 9.20 1 -12 0 243.58 7.80 1 -12 0 229.68 8.20 1 -12 0 226.88 8.70 1 -12 0 259.07 10.00 1 -12 0 233.48 7.40 -1 12 0 223.88 9.00 -1 12 0 242.98 7.00 -1 12 0 250.97 7.50 -1 12 0 241.68 9.70 -1 12 0 255.87 10.50 -1 12 0 252.37 8.40 -1 12 0 225.28 8.10 -1 12 0 229.38 9.90 0 -12 0 57.49 4.10 0 -12 0 63.09 4.40 0 -12 0 63.59 7.20 0 -12 0 64.19 3.80 0 -12 0 53.89 3.80 0 12 0 66.79 4.20 0 12 0 67.59 3.40 0 12 0 67.89 4.20 0 12 0 58.99 4.40 0 12 0 67.69 5.60 -1 -12 0 103.49 4.60 -1 -12 0 115.99 6.60 -1 -12 0 99.19 6.40 -1 -12 0 117.69 5.80 -1 -12 0 111.49 5.70 -1 -12 0 111.39 6.00 1 12 0 108.39 7.10 1 12 0 108.39 6.20 1 12 0 122.69 7.30 1 12 0 103.79 5.00 1 12 0 114.59 5.80 1 12 0 104.29 5.90 -2 -12 0 131.29 7.60 -2 -12 0 132.79 6.60 -2 -12 0 127.19 6.70 -2 -12 0 127.89 6.40 -2 -12 0 128.99 5.40 2 12 0 129.09 8.10 2 12 0 122.49 7.80 2 12 0 139.99 7.60 2 12 0 114.69 6.70 2 12 0 131.59 6.40 -3 -12 0 209.88 8.70 -3 -12 0 201.58 8.60 -3 -12 0 216.58 9.20 -3 -12 0 200.58 7.30 -3 -12 0 195.58 10.10 3 12 0 183.58 9.80 3 12 0 215.28 9.40 3 12 0 225.58 8.60 3 12 0 189.28 10.00 3 12 0 210.08 10.50 -4 -12 0 24.50 4.30 -4 -12 0 36.90 4.80 -4 -12 0 32.90 3.40 -4 -12 0 31.60 5.50 -4 -12 0 26.60 3.70 4 12 0 33.40 5.40 4 12 0 28.00 4.70 4 12 0 30.60 5.30 4 12 0 31.30 5.30 4 12 0 23.00 3.80 -5 -12 0 4.50 2.50 -5 -12 0 5.70 2.50 -5 -12 0 4.70 2.30 -5 -12 0 -1.30 2.90 -5 -12 0 5.10 2.70 5 12 0 6.20 3.60 5 12 0 4.80 3.10 5 12 0 2.50 3.90 5 12 0 1.70 4.70 5 12 0 1.10 2.70 -6 -12 0 1.30 2.20 -6 -12 0 2.60 2.50 -6 -12 0 5.80 4.90 -6 -12 0 6.50 2.90 6 12 0 -3.40 3.70 6 12 0 8.10 4.70 6 12 0 5.50 3.20 11 -13 0 5.70 2.90 11 -13 0 3.40 2.50 11 -13 0 5.70 3.20 11 -13 0 4.40 3.00 -11 13 0 8.30 3.70 -11 13 0 7.70 2.90 -11 13 0 3.10 3.50 -11 13 0 6.20 3.60 10 -13 0 -2.40 2.00 10 -13 0 -3.40 1.80 10 -13 0 2.20 2.70 10 -13 0 1.00 2.60 10 -13 0 2.00 1.90 10 -13 0 -2.50 2.40 -10 13 0 -1.80 2.60 -10 13 0 0.30 2.50 -10 13 0 -0.20 2.60 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2.70 5 -13 0 32.30 4.10 5 -13 0 23.90 4.40 5 -13 0 24.40 2.10 5 -13 0 25.60 3.40 -5 13 0 29.90 4.20 -5 13 0 25.00 4.00 -5 13 0 24.70 2.90 -5 13 0 26.20 3.20 -5 13 0 27.00 2.60 -5 13 0 27.80 2.60 4 -13 0 -0.30 1.60 4 -13 0 1.00 1.10 4 -13 0 1.50 1.20 4 -13 0 3.00 1.90 4 -13 0 3.40 1.60 4 -13 0 -0.70 1.40 4 -13 0 1.30 1.40 4 -13 0 4.90 1.50 4 -13 0 0.20 1.30 4 -13 0 0.90 1.80 -4 13 0 1.20 1.60 -4 13 0 1.20 2.30 -4 13 0 1.40 1.40 -4 13 0 0.60 1.30 -4 13 0 -0.70 1.70 -4 13 0 0.60 1.60 -4 13 0 1.70 1.50 -4 13 0 2.40 1.20 -4 13 0 1.80 1.60 3 -13 0 25.40 2.00 3 -13 0 26.70 2.30 3 -13 0 30.00 3.10 3 -13 0 29.70 3.30 3 -13 0 21.50 3.40 3 -13 0 25.80 3.10 3 -13 0 29.40 3.20 3 -13 0 23.40 2.70 -3 13 0 24.30 2.50 -3 13 0 22.50 2.10 -3 13 0 19.60 3.20 -3 13 0 26.60 2.50 -3 13 0 31.50 3.50 -3 13 0 29.50 4.30 -3 13 0 30.00 2.80 -3 13 0 31.70 3.30 -3 13 0 25.20 2.40 2 -13 0 9.80 1.40 2 -13 0 11.80 3.20 2 -13 0 11.80 2.30 2 -13 0 12.30 2.40 2 -13 0 10.90 1.90 2 -13 0 8.40 1.60 2 -13 0 9.30 2.30 -2 13 0 11.40 2.50 -2 13 0 10.50 2.60 -2 13 0 10.70 2.00 -2 13 0 10.60 2.90 -2 13 0 9.90 2.60 -2 13 0 12.70 1.80 -2 13 0 7.70 1.80 1 -13 0 18.70 3.40 1 -13 0 25.00 3.00 1 -13 0 18.30 2.50 1 -13 0 16.50 13.50 1 -13 0 27.50 3.40 1 -13 0 20.20 2.80 1 -13 0 25.50 3.20 -1 13 0 28.80 3.80 -1 13 0 25.40 2.60 -1 13 0 21.00 3.20 -1 13 0 24.70 3.80 -1 13 0 20.80 4.10 -1 13 0 22.10 2.60 0 -13 0 3.40 1.70 0 -13 0 6.60 2.60 0 -13 0 2.60 1.40 0 -13 0 5.70 2.00 0 -13 0 3.40 2.00 0 -13 0 -4.30 17.40 0 -13 0 3.40 2.00 0 13 0 4.90 2.00 0 13 0 4.40 2.40 0 13 0 3.10 2.00 0 13 0 4.20 2.30 0 13 0 2.90 1.60 0 13 0 5.20 2.80 -1 -13 0 19.80 3.20 -1 -13 0 20.30 2.40 -1 -13 0 24.80 4.10 -1 -13 0 23.10 3.20 -1 -13 0 20.30 3.60 -1 -13 0 17.70 2.90 1 13 0 22.50 3.70 1 13 0 20.60 3.20 1 13 0 20.90 3.90 1 13 0 16.50 3.20 1 13 0 23.60 4.50 -2 -13 0 8.90 2.10 -2 -13 0 10.20 2.50 -2 -13 0 7.80 2.90 -2 -13 0 9.40 2.60 -2 -13 0 6.40 2.30 -2 -13 0 14.10 3.70 2 13 0 11.90 3.30 2 13 0 10.30 3.10 2 13 0 7.80 2.50 2 13 0 13.40 4.10 2 13 0 7.70 2.90 -3 -13 0 5.30 3.40 -3 -13 0 2.90 2.10 -3 -13 0 0.70 1.60 -3 -13 0 -0.90 2.90 3 13 0 0.90 2.60 3 13 0 1.00 2.70 3 13 0 0.30 2.60 3 13 0 -0.20 2.20 -4 -13 0 10.20 4.20 -4 -13 0 8.70 2.50 -4 -13 0 13.80 3.30 -4 -13 0 11.70 2.80 -4 -13 0 11.40 2.90 4 13 0 5.80 3.70 4 13 0 8.80 3.30 4 13 0 6.00 3.90 4 13 0 14.70 4.60 -5 -13 0 9.30 4.70 -5 -13 0 9.10 2.80 -5 -13 0 7.20 3.40 -5 -13 0 6.30 2.70 -5 -13 0 7.20 2.40 5 13 0 9.80 4.00 5 13 0 7.90 4.30 5 13 0 8.20 4.20 5 13 0 11.30 4.30 5 13 0 12.40 3.80 11 -14 0 25.90 4.50 11 -14 0 27.90 3.50 11 -14 0 35.60 5.50 -11 14 0 36.90 4.40 -11 14 0 46.20 6.20 -11 14 0 37.40 5.80 -11 14 0 38.90 5.30 10 -14 0 1.40 2.00 10 -14 0 -0.50 2.10 10 -14 0 -1.30 2.10 10 -14 0 1.20 2.60 10 -14 0 3.10 3.00 10 -14 0 2.50 2.60 10 -14 0 -2.90 2.60 -10 14 0 2.00 2.40 -10 14 0 2.40 2.80 -10 14 0 1.40 2.80 -10 14 0 0.30 2.10 -10 14 0 2.10 2.90 -10 14 0 4.60 3.00 9 -14 0 2.10 2.70 9 -14 0 6.30 3.10 9 -14 0 1.40 2.00 9 -14 0 3.50 2.50 9 -14 0 5.90 3.00 9 -14 0 2.60 2.30 -9 14 0 4.60 2.30 -9 14 0 3.50 2.60 -9 14 0 8.00 3.40 -9 14 0 3.10 2.80 -9 14 0 2.50 2.90 8 -14 0 63.19 4.30 8 -14 0 68.79 5.60 8 -14 0 58.29 4.20 8 -14 0 62.89 4.20 8 -14 0 67.19 4.00 -8 14 0 52.99 4.80 -8 14 0 65.59 5.50 -8 14 0 65.19 4.50 -8 14 0 53.89 4.80 -8 14 0 56.69 6.00 -8 14 0 61.79 4.30 7 -14 0 21.00 3.80 7 -14 0 20.70 3.10 7 -14 0 20.70 2.50 7 -14 0 24.10 2.70 7 -14 0 23.60 3.90 -7 14 0 16.10 2.50 -7 14 0 15.70 2.40 -7 14 0 20.30 3.10 -7 14 0 16.60 3.40 6 -14 0 48.80 2.60 6 -14 0 59.19 5.30 6 -14 0 48.90 3.60 6 -14 0 53.09 5.60 6 -14 0 57.59 4.20 6 -14 0 46.30 3.30 6 -14 0 44.60 2.30 -6 14 0 47.50 3.50 -6 14 0 45.80 4.10 -6 14 0 52.99 3.80 -6 14 0 43.90 3.70 -6 14 0 52.99 4.90 -6 14 0 55.89 3.70 -6 14 0 50.29 5.10 5 -14 0 109.59 5.30 5 -14 0 115.69 5.00 5 -14 0 114.09 4.60 5 -14 0 113.59 7.00 5 -14 0 118.19 5.60 -5 14 0 114.49 6.40 -5 14 0 119.39 5.20 -5 14 0 133.99 8.10 -5 14 0 117.19 5.60 -5 14 0 114.69 5.00 -5 14 0 105.39 5.00 -5 14 0 114.49 6.60 4 -14 0 127.09 5.70 4 -14 0 137.99 7.50 4 -14 0 126.19 6.00 4 -14 0 124.89 4.80 4 -14 0 123.09 5.70 4 -14 0 133.69 4.70 4 -14 0 122.79 6.90 4 -14 0 125.49 5.80 -4 14 0 136.49 8.30 -4 14 0 128.29 5.30 -4 14 0 142.99 7.20 -4 14 0 123.79 5.30 -4 14 0 140.19 6.40 -4 14 0 141.39 5.30 3 -14 0 150.38 6.90 3 -14 0 147.69 7.80 3 -14 0 147.99 6.70 3 -14 0 148.49 5.50 3 -14 0 153.08 6.50 3 -14 0 152.18 5.50 -3 14 0 150.08 6.10 -3 14 0 135.79 8.10 -3 14 0 151.28 5.60 -3 14 0 149.49 6.80 -3 14 0 154.38 7.40 -3 14 0 147.59 5.80 2 -14 0 0.70 1.40 2 -14 0 2.50 1.50 2 -14 0 0.70 0.90 2 -14 0 1.90 1.30 2 -14 0 -1.60 1.50 2 -14 0 -0.30 2.20 2 -14 0 0.70 1.50 2 -14 0 1.40 2.10 -2 14 0 -0.50 1.70 -2 14 0 2.00 2.10 -2 14 0 -0.90 2.30 -2 14 0 2.30 2.40 -2 14 0 2.90 2.10 -2 14 0 1.80 1.40 -2 14 0 2.80 1.50 1 -14 0 1.20 1.60 1 -14 0 0.40 1.50 1 -14 0 5.90 2.30 1 -14 0 12.80 14.10 1 -14 0 0.50 1.70 1 -14 0 2.10 1.70 1 -14 0 1.40 1.60 -1 14 0 -1.00 1.40 -1 14 0 1.40 2.80 -1 14 0 -2.40 1.90 -1 14 0 3.50 2.10 -1 14 0 0.60 2.20 -1 14 0 0.90 1.60 -1 14 0 1.20 1.50 0 -14 0 126.19 6.50 0 -14 0 123.09 6.60 0 -14 0 107.19 7.10 0 -14 0 115.19 6.00 0 -14 0 109.89 5.10 0 14 0 102.29 6.30 0 14 0 109.69 7.30 0 14 0 121.29 6.10 0 14 0 106.39 6.20 0 14 0 111.29 7.50 -1 -14 0 44.70 4.00 -1 -14 0 44.60 4.10 -1 -14 0 30.90 4.10 -1 -14 0 41.50 3.40 -1 -14 0 40.70 4.80 -1 -14 0 35.10 4.80 1 14 0 43.80 4.30 1 14 0 38.90 5.00 1 14 0 44.10 4.80 1 14 0 44.20 5.90 1 14 0 49.10 5.10 -2 -14 0 12.90 3.70 -2 -14 0 12.50 2.50 -2 -14 0 17.20 3.90 -2 -14 0 11.80 2.90 -2 -14 0 14.70 3.10 2 14 0 8.80 3.40 2 14 0 12.80 4.20 2 14 0 10.60 3.40 2 14 0 15.20 3.50 2 14 0 14.60 3.70 -3 -14 0 7.10 3.50 -3 -14 0 5.50 2.40 -3 -14 0 6.10 3.70 -3 -14 0 4.70 2.50 -3 -14 0 4.80 2.10 -3 -14 0 1.00 2.70 3 14 0 8.00 3.00 3 14 0 3.10 5.60 3 14 0 6.30 3.30 3 14 0 5.80 3.50 3 14 0 3.70 3.70 -4 -14 0 1.00 3.30 -4 -14 0 -2.90 3.60 -4 -14 0 -1.60 1.70 -4 -14 0 0.90 2.40 -4 -14 0 -1.10 2.20 -4 -14 0 0.90 2.20 4 14 0 -5.70 3.50 4 14 0 -1.80 3.30 4 14 0 2.30 3.80 4 14 0 0.60 3.70 4 14 0 0.40 2.60 10 -15 0 8.10 3.00 10 -15 0 13.80 3.90 10 -15 0 9.00 2.60 10 -15 0 5.70 3.20 10 -15 0 12.90 3.70 10 -15 0 7.20 3.30 -10 15 0 12.10 3.80 -10 15 0 8.80 3.20 -10 15 0 15.00 4.40 -10 15 0 8.90 2.90 9 -15 0 26.30 3.30 9 -15 0 22.80 3.20 9 -15 0 19.10 3.10 9 -15 0 20.60 3.20 9 -15 0 21.00 4.40 9 -15 0 34.00 4.70 -9 15 0 22.40 3.90 -9 15 0 28.40 3.70 -9 15 0 24.90 4.80 -9 15 0 26.90 3.60 -9 15 0 21.80 6.50 8 -15 0 34.20 3.50 8 -15 0 35.10 3.30 8 -15 0 26.70 3.10 8 -15 0 34.80 3.40 8 -15 0 33.10 3.80 -8 15 0 32.90 3.70 -8 15 0 32.20 4.10 -8 15 0 34.10 3.60 -8 15 0 33.00 4.60 -8 15 0 35.50 5.20 7 -15 0 25.60 2.10 7 -15 0 28.60 4.50 7 -15 0 24.60 2.80 7 -15 0 29.30 2.90 7 -15 0 28.70 3.50 -7 15 0 33.30 4.80 -7 15 0 31.80 3.40 -7 15 0 29.10 3.20 -7 15 0 31.10 3.30 -7 15 0 26.00 4.30 6 -15 0 44.70 3.60 6 -15 0 44.70 3.60 6 -15 0 46.30 5.40 6 -15 0 44.20 4.00 6 -15 0 43.70 3.30 6 -15 0 47.70 5.00 -6 15 0 41.20 3.80 -6 15 0 39.80 4.90 -6 15 0 37.60 3.30 -6 15 0 36.50 3.40 -6 15 0 42.90 3.40 5 -15 0 105.29 6.50 5 -15 0 106.09 7.10 5 -15 0 97.89 4.30 5 -15 0 100.19 4.80 5 -15 0 100.19 5.50 5 -15 0 105.79 5.50 -5 15 0 103.99 5.00 -5 15 0 109.49 8.00 -5 15 0 101.39 4.80 -5 15 0 90.79 5.20 -5 15 0 99.29 4.80 -5 15 0 104.69 6.70 4 -15 0 21.90 3.80 4 -15 0 17.70 3.70 4 -15 0 12.90 2.30 4 -15 0 17.80 2.70 4 -15 0 14.20 2.90 4 -15 0 18.40 2.90 -4 15 0 15.10 3.10 -4 15 0 22.70 3.90 -4 15 0 20.50 3.90 -4 15 0 17.70 2.40 -4 15 0 19.30 2.40 -4 15 0 20.60 3.90 -4 15 0 22.90 3.00 3 -15 0 2.60 2.30 3 -15 0 1.50 1.50 3 -15 0 -1.80 2.00 3 -15 0 -0.80 1.40 3 -15 0 2.40 1.80 3 -15 0 0.10 1.50 -3 15 0 -2.70 1.90 -3 15 0 -0.30 2.20 -3 15 0 1.10 1.90 -3 15 0 0.20 1.50 -3 15 0 1.30 1.40 -3 15 0 3.80 2.80 2 -15 0 2.80 1.60 2 -15 0 3.90 2.10 2 -15 0 1.50 1.50 2 -15 0 0.70 1.60 2 -15 0 -1.20 1.90 2 -15 0 1.50 2.20 2 -15 0 2.40 1.30 -2 15 0 2.00 3.00 -2 15 0 1.30 2.20 -2 15 0 0.70 1.50 -2 15 0 -0.30 1.90 -2 15 0 0.30 2.30 1 -15 0 11.40 3.10 1 -15 0 7.50 2.20 1 -15 0 10.80 2.50 1 -15 0 4.70 2.30 1 -15 0 7.20 2.00 1 -15 0 7.80 2.30 -1 15 0 8.20 2.50 -1 15 0 10.30 3.90 -1 15 0 9.20 3.30 -1 15 0 6.70 2.60 -1 15 0 6.90 2.30 0 -15 0 16.00 3.70 0 -15 0 18.50 3.50 0 -15 0 19.60 2.70 0 -15 0 21.10 3.20 0 -15 0 22.20 3.70 0 -15 0 18.00 3.40 0 15 0 19.50 3.60 0 15 0 17.70 3.20 0 15 0 18.30 4.80 0 15 0 16.30 3.70 0 15 0 17.40 3.90 -1 -15 0 51.29 4.00 -1 -15 0 55.19 6.20 -1 -15 0 44.90 5.20 -1 -15 0 54.09 6.10 -1 -15 0 49.30 4.90 -1 -15 0 66.69 5.20 1 15 0 46.30 4.70 1 15 0 50.99 5.90 1 15 0 43.20 5.30 1 15 0 64.69 7.00 1 15 0 47.20 6.80 -2 -15 0 35.10 5.50 -2 -15 0 49.60 5.50 -2 -15 0 39.20 5.40 -2 -15 0 40.70 4.80 -2 -15 0 39.80 4.70 -2 -15 0 32.50 3.50 2 15 0 50.79 7.30 2 15 0 35.40 5.50 2 15 0 33.50 5.00 2 15 0 44.80 5.70 -3 -15 0 7.60 3.00 -3 -15 0 4.70 4.20 -3 -15 0 8.30 5.80 -3 -15 0 7.50 2.90 -3 -15 0 7.10 2.80 -3 -15 0 4.90 2.90 3 15 0 5.30 4.00 3 15 0 4.10 3.40 3 15 0 9.20 4.60 3 15 0 7.80 3.50 3 15 0 3.20 3.80 9 -16 0 10.40 2.90 9 -16 0 5.80 2.60 9 -16 0 4.40 2.40 9 -16 0 2.90 2.60 9 -16 0 12.50 3.60 9 -16 0 11.20 2.60 9 -16 0 13.60 3.90 -9 16 0 5.90 3.10 -9 16 0 6.30 2.90 -9 16 0 11.20 3.00 -9 16 0 13.90 4.30 -9 16 0 4.50 3.00 8 -16 0 1.30 2.30 8 -16 0 -1.00 2.10 8 -16 0 0.10 1.30 8 -16 0 -0.90 2.60 8 -16 0 -1.90 2.40 8 -16 0 -2.40 3.00 -8 16 0 -1.00 2.40 -8 16 0 0.50 3.70 -8 16 0 0.50 2.30 -8 16 0 2.60 1.90 7 -16 0 -0.90 1.90 7 -16 0 0.00 2.50 7 -16 0 1.40 1.80 -7 16 0 1.40 1.90 -7 16 0 2.90 3.60 -7 16 0 0.80 2.60 -7 16 0 5.60 3.50 6 -16 0 47.50 3.40 6 -16 0 42.10 4.80 6 -16 0 56.69 4.30 6 -16 0 47.40 3.60 6 -16 0 53.19 4.60 6 -16 0 59.79 6.30 -6 16 0 47.10 3.70 -6 16 0 52.99 5.90 -6 16 0 50.99 4.00 -6 16 0 46.40 4.00 -6 16 0 39.00 4.10 5 -16 0 25.20 3.40 5 -16 0 20.00 3.80 5 -16 0 36.00 4.90 5 -16 0 26.30 3.90 5 -16 0 23.10 2.90 5 -16 0 29.20 3.70 -5 16 0 23.20 3.40 -5 16 0 21.20 2.80 -5 16 0 27.10 5.30 -5 16 0 28.80 4.20 -5 16 0 20.20 2.80 4 -16 0 30.00 3.70 4 -16 0 31.20 3.00 4 -16 0 38.70 4.00 4 -16 0 31.80 4.60 4 -16 0 31.20 4.90 4 -16 0 29.20 2.80 -4 16 0 33.90 4.40 -4 16 0 30.40 4.00 -4 16 0 31.30 3.20 -4 16 0 41.00 6.00 -4 16 0 29.20 3.00 -4 16 0 31.50 3.50 3 -16 0 82.89 5.50 3 -16 0 81.19 5.30 3 -16 0 95.19 5.70 3 -16 0 83.89 4.40 3 -16 0 88.19 6.40 3 -16 0 80.39 4.30 -3 16 0 82.09 4.80 -3 16 0 76.49 5.90 -3 16 0 81.29 5.80 -3 16 0 83.29 5.00 -3 16 0 87.39 7.30 2 -16 0 17.20 3.40 2 -16 0 21.40 3.10 2 -16 0 24.50 4.10 2 -16 0 19.00 3.40 2 -16 0 15.90 2.40 -2 16 0 25.10 4.70 -2 16 0 23.30 3.90 -2 16 0 23.20 3.10 -2 16 0 23.70 3.90 1 -16 0 11.40 2.20 1 -16 0 13.60 3.30 1 -16 0 14.00 3.20 1 -16 0 14.40 4.20 1 -16 0 13.80 2.70 -1 16 0 11.20 3.90 -1 16 0 12.90 2.90 -1 16 0 18.60 4.40 -1 16 0 9.90 3.50 -1 16 0 9.60 3.30 0 -16 0 5.00 2.90 0 -16 0 2.90 2.40 0 -16 0 2.20 2.30 0 -16 0 5.00 4.00 0 16 0 5.50 2.70 0 16 0 2.70 2.50 0 16 0 5.40 4.20 0 16 0 5.40 3.90 0 16 0 0.80 2.90 -1 -16 0 2.60 2.10 -1 -16 0 3.40 2.40 -1 -16 0 3.30 2.90 -1 -16 0 -0.80 2.70 -1 -16 0 4.30 2.20 -1 -16 0 -2.50 2.10 1 16 0 3.20 2.70 1 16 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0 -11 4 -0.80 1.10 0 -11 4 1.10 1.30 0 -11 4 0.10 0.80 0 -11 4 18.70 9.70 0 -11 4 2.50 11.00 0 -11 4 1.50 1.30 0 -11 4 0.50 1.10 0 -11 4 1.20 0.80 -1 11 -4 34.00 2.80 -1 11 -4 39.10 2.80 -1 11 -4 43.10 3.60 -1 11 -4 35.80 2.30 -1 11 -4 35.90 2.70 -1 11 -4 35.20 2.20 -1 11 -4 36.80 3.00 -1 11 -4 31.50 3.60 -1 11 -4 36.00 3.70 -1 11 -4 32.10 2.20 -1 11 -4 33.70 2.00 1 -11 4 33.50 2.10 1 -11 4 38.10 2.60 1 -11 4 28.80 3.20 1 -11 4 33.60 2.70 1 -11 4 36.10 1.80 1 -11 4 34.80 1.90 1 -11 4 41.30 3.60 1 -11 4 37.00 3.10 1 -11 4 32.10 1.60 1 -11 4 36.40 1.90 1 -11 4 31.40 2.80 1 -11 4 36.10 1.90 1 -11 4 30.70 2.00 1 -11 4 36.70 2.50 -2 11 -4 74.19 4.60 -2 11 -4 73.19 3.90 -2 11 -4 74.69 4.10 -2 11 -4 75.59 3.60 -2 11 -4 73.79 2.50 -2 11 -4 67.19 4.40 -2 11 -4 69.69 2.40 -2 11 -4 72.79 4.50 -2 11 -4 73.29 4.70 -2 11 -4 74.29 3.70 -2 11 -4 88.19 5.30 -2 11 -4 74.79 3.10 2 -11 4 73.49 3.30 2 -11 4 73.89 4.40 2 -11 4 69.99 4.70 2 -11 4 64.39 3.60 2 -11 4 66.19 3.10 2 -11 4 73.89 3.40 2 -11 4 70.39 4.20 2 -11 4 72.69 3.80 2 -11 4 75.09 2.90 2 -11 4 76.79 3.50 2 -11 4 73.09 4.40 2 -11 4 71.59 2.90 2 -11 4 65.19 3.70 2 -11 4 81.99 4.50 2 -11 4 71.09 5.00 2 -11 4 79.09 4.40 2 -11 4 68.09 2.90 2 -11 4 66.99 3.00 -3 11 -4 22.20 2.80 -3 11 -4 19.30 1.30 -3 11 -4 20.90 2.80 -3 11 -4 21.10 2.90 -3 11 -4 23.40 2.70 -3 11 -4 23.00 2.30 -3 11 -4 22.40 1.30 -3 11 -4 16.10 2.60 -3 11 -4 24.20 3.30 -3 11 -4 18.70 2.70 -3 11 -4 20.50 2.50 -3 11 -4 18.70 1.80 3 -11 4 30.30 3.80 3 -11 4 18.20 1.70 3 -11 4 20.40 2.20 3 -11 4 19.40 2.50 3 -11 4 21.40 2.50 3 -11 4 19.60 2.70 3 -11 4 18.10 2.00 3 -11 4 19.80 1.80 3 -11 4 19.10 2.10 3 -11 4 21.40 2.20 3 -11 4 19.20 1.90 3 -11 4 19.60 2.60 3 -11 4 19.50 2.50 3 -11 4 16.90 2.70 3 -11 4 20.50 2.00 3 -11 4 20.50 1.80 3 -11 4 18.10 2.10 -4 11 -4 25.10 2.70 -4 11 -4 28.10 2.40 -4 11 -4 26.10 2.20 -4 11 -4 21.30 3.00 -4 11 -4 30.00 2.30 -4 11 -4 24.00 2.20 -4 11 -4 27.90 3.40 -4 11 -4 32.00 3.90 -4 11 -4 26.90 3.30 -4 11 -4 27.10 2.00 4 -11 4 30.30 3.10 4 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3 -4 46.80 1.40 3 3 -4 44.70 2.40 3 3 -4 46.30 2.40 3 3 -4 49.40 2.90 3 3 -4 48.60 2.40 3 3 -4 47.90 3.50 3 3 -4 48.90 1.80 3 3 -4 49.10 3.70 3 3 -4 41.80 3.70 3 3 -4 45.50 2.00 -3 -3 4 49.99 3.50 -3 -3 4 45.90 1.90 -3 -3 4 43.80 3.50 -3 -3 4 47.40 2.80 -3 -3 4 52.39 3.00 -3 -3 4 49.99 2.70 -3 -3 4 46.20 2.60 -3 -3 4 45.30 2.90 -3 -3 4 83.69 18.80 -3 -3 4 47.40 2.20 -3 -3 4 47.60 1.50 -3 -3 4 46.10 3.60 -3 -3 4 47.50 2.40 -3 -3 4 52.19 3.70 -3 -3 4 44.60 1.70 -3 -3 4 48.40 2.40 2 3 -4 773.12 21.60 2 3 -4 759.72 17.50 2 3 -4 762.42 18.90 2 3 -4 766.02 19.10 2 3 -4 775.92 18.30 2 3 -4 724.13 19.30 2 3 -4 779.72 18.10 2 3 -4 767.52 17.30 2 3 -4 740.03 17.10 2 3 -4 777.92 20.30 2 3 -4 796.92 39.60 2 3 -4 792.72 20.00 2 3 -4 762.32 18.20 2 3 -4 760.02 17.60 2 3 -4 740.53 19.10 2 3 -4 770.42 19.80 -2 -3 4 764.02 18.00 -2 -3 4 770.82 18.90 -2 -3 4 722.33 19.00 -2 -3 4 794.62 19.30 -2 -3 4 790.02 20.20 -2 -3 4 774.12 19.50 -2 -3 4 764.82 17.20 -2 -3 4 769.42 19.50 -2 -3 4 774.32 20.10 -2 -3 4 772.32 17.50 -2 -3 4 757.82 19.40 -2 -3 4 790.12 19.90 -2 -3 4 788.42 17.30 -2 -3 4 765.02 18.70 -2 -3 4 670.53 38.40 -2 -3 4 771.12 17.50 -2 -3 4 771.32 18.10 -2 -3 4 779.12 18.20 -2 -3 4 774.82 19.00 1 3 -4 75.89 3.80 1 3 -4 77.39 3.50 1 3 -4 70.49 2.70 1 3 -4 75.39 2.10 1 3 -4 78.09 3.50 1 3 -4 69.69 12.90 1 3 -4 75.29 3.10 1 3 -4 71.99 2.90 1 3 -4 76.19 2.10 1 3 -4 74.09 3.60 1 3 -4 73.99 2.30 1 3 -4 75.09 2.40 1 3 -4 74.09 1.80 1 3 -4 74.69 2.10 1 3 -4 76.29 3.70 1 3 -4 76.49 2.80 1 3 -4 72.89 3.20 -1 -3 4 80.49 2.80 -1 -3 4 66.79 13.60 -1 -3 4 79.49 3.20 -1 -3 4 74.39 2.10 -1 -3 4 79.59 3.90 -1 -3 4 71.79 3.10 -1 -3 4 75.09 3.30 -1 -3 4 79.89 3.70 -1 -3 4 72.39 3.70 -1 -3 4 77.49 2.00 -1 -3 4 68.09 3.40 -1 -3 4 71.99 3.00 -1 -3 4 74.59 2.20 -1 -3 4 74.99 1.90 -1 -3 4 75.09 3.40 -1 -3 4 72.39 2.70 -1 -3 4 78.29 3.50 -1 -3 4 76.89 2.20 -1 -3 4 75.69 2.30 0 3 -4 13.10 1.60 0 3 -4 10.10 1.40 0 3 -4 9.70 1.40 0 3 -4 11.50 1.60 0 3 -4 11.70 0.80 0 3 -4 13.10 1.70 0 3 -4 11.40 1.10 0 3 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2.10 -4 4 -7 35.40 2.50 -4 4 -7 39.70 2.30 -4 4 -7 44.10 4.10 -4 4 -7 40.30 3.20 -4 4 -7 42.70 4.40 -4 4 -7 40.30 3.50 -4 4 -7 40.80 1.20 -4 4 -7 44.70 4.00 4 -4 7 35.80 3.00 4 -4 7 44.50 2.80 4 -4 7 44.20 3.90 4 -4 7 34.50 14.30 4 -4 7 40.50 2.40 4 -4 7 32.40 3.60 4 -4 7 39.90 2.60 4 -4 7 40.80 2.20 4 -4 7 40.50 3.20 4 -4 7 39.70 2.20 4 -4 7 35.50 2.20 4 -4 7 38.90 2.10 4 -4 7 37.00 4.40 4 -4 7 41.40 2.00 4 -4 7 35.20 4.00 -5 4 -7 16.90 2.70 -5 4 -7 10.10 20.20 -5 4 -7 11.00 1.40 -5 4 -7 11.70 1.60 -5 4 -7 12.40 2.40 -5 4 -7 11.80 3.20 -5 4 -7 8.90 2.30 -5 4 -7 10.20 1.80 5 -4 7 8.50 1.50 5 -4 7 5.60 19.80 5 -4 7 12.80 1.60 5 -4 7 15.00 3.30 5 -4 7 11.60 2.00 5 -4 7 11.00 1.30 5 -4 7 11.60 1.60 5 -4 7 9.90 1.90 5 -4 7 11.90 1.70 -6 4 -7 76.89 4.70 -6 4 -7 79.29 5.50 -6 4 -7 72.69 4.80 -6 4 -7 77.99 4.40 -6 4 -7 82.19 30.20 -6 4 -7 84.99 6.60 -6 4 -7 85.09 3.60 6 -4 7 77.69 3.60 6 -4 7 79.19 3.50 6 -4 7 115.39 32.00 6 -4 7 70.49 6.30 6 -4 7 82.29 3.70 6 -4 7 68.59 4.30 6 -4 7 81.59 4.70 6 -4 7 73.49 3.70 -7 4 -7 253.27 10.90 -7 4 -7 269.07 10.50 -7 4 -7 272.17 9.20 -7 4 -7 255.17 10.00 -7 4 -7 250.57 12.10 -7 4 -7 315.37 49.80 7 -4 7 242.88 7.80 7 -4 7 273.37 7.90 7 -4 7 262.67 8.00 7 -4 7 260.37 9.70 7 -4 7 285.57 13.30 7 -4 7 260.77 9.80 7 -4 7 139.79 39.80 7 -4 7 267.07 8.20 -8 4 -7 142.49 6.70 -8 4 -7 149.59 7.90 -8 4 -7 143.39 8.40 -8 4 -7 -2.10 31.50 -8 4 -7 152.48 11.40 -8 4 -7 140.99 7.50 8 -4 7 160.38 6.10 8 -4 7 147.59 5.60 8 -4 7 152.88 7.50 8 -4 7 110.89 44.70 8 -4 7 146.69 7.10 8 -4 7 164.98 6.10 8 -4 7 150.28 5.80 8 -4 7 156.98 10.50 -9 4 -7 3.20 2.40 -9 4 -7 -0.10 2.20 -9 4 -7 1.30 2.70 -9 4 -7 -0.80 2.50 9 -4 7 -3.50 4.50 9 -4 7 1.80 2.20 9 -4 7 3.00 2.00 9 -4 7 1.50 2.10 9 -4 7 0.40 2.10 9 -4 7 6.60 2.50 -10 4 -7 6.10 3.40 -10 4 -7 5.00 3.10 -10 4 -7 5.90 3.30 -10 4 -7 8.80 3.30 10 -4 7 2.00 2.40 10 -4 7 10.10 3.80 10 -4 7 4.60 2.60 10 -4 7 7.80 3.10 10 -4 7 3.30 2.90 11 3 -7 5.40 3.40 11 3 -7 6.50 3.80 11 3 -7 5.40 3.50 -11 -3 7 4.30 2.50 10 3 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3.70 -6 -3 7 13.80 1.40 5 3 -7 12.00 1.90 5 3 -7 14.40 3.20 5 3 -7 11.60 1.70 5 3 -7 14.90 0.90 5 3 -7 29.20 17.90 5 3 -7 10.10 3.00 5 3 -7 16.70 1.60 5 3 -7 12.30 1.40 5 3 -7 13.90 2.20 5 3 -7 14.50 2.00 5 3 -7 14.30 1.10 5 3 -7 12.40 2.90 5 3 -7 15.00 2.50 -5 -3 7 16.20 2.80 -5 -3 7 14.80 3.20 -5 -3 7 13.30 3.10 -5 -3 7 14.10 2.20 -5 -3 7 15.70 2.00 -5 -3 7 12.60 1.30 -5 -3 7 15.20 2.10 -5 -3 7 15.80 1.70 -5 -3 7 12.80 1.40 -5 -3 7 12.50 2.70 -5 -3 7 18.40 3.70 -5 -3 7 14.70 1.40 -5 -3 7 14.90 1.20 -5 -3 7 35.10 22.50 4 3 -7 136.39 5.50 4 3 -7 144.39 6.00 4 3 -7 134.99 4.20 4 3 -7 139.89 8.10 4 3 -7 143.19 7.20 4 3 -7 146.49 5.00 4 3 -7 135.59 3.50 4 3 -7 137.09 4.80 4 3 -7 143.29 7.20 4 3 -7 145.89 6.10 4 3 -7 138.19 3.50 4 3 -7 143.79 5.70 4 3 -7 135.29 3.90 4 3 -7 129.79 24.00 4 3 -7 141.39 4.20 4 3 -7 148.89 7.70 -4 -3 7 131.59 4.80 -4 -3 7 142.49 4.00 -4 -3 7 138.69 5.40 -4 -3 7 133.79 7.10 -4 -3 7 136.59 6.70 -4 -3 7 137.59 4.20 -4 -3 7 133.39 7.30 -4 -3 7 178.78 32.60 -4 -3 7 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106.99 2.80 2 3 -7 111.89 5.80 2 3 -7 107.39 5.70 2 3 -7 101.69 3.10 2 3 -7 106.19 2.80 -2 -3 7 108.49 5.60 -2 -3 7 107.99 4.30 -2 -3 7 94.99 4.30 -2 -3 7 102.29 4.40 -2 -3 7 84.49 20.40 -2 -3 7 111.59 5.90 -2 -3 7 107.39 3.90 -2 -3 7 104.59 2.90 -2 -3 7 102.79 2.90 -2 -3 7 106.39 3.60 -2 -3 7 119.19 6.30 -2 -3 7 104.89 4.80 -2 -3 7 104.39 3.80 -2 -3 7 98.39 3.20 -2 -3 7 109.99 3.50 -2 -3 7 106.59 3.30 -2 -3 7 101.79 5.20 -2 -3 7 114.29 5.00 1 3 -7 27.00 1.50 1 3 -7 25.80 2.30 1 3 -7 28.30 0.90 1 3 -7 30.70 3.30 1 3 -7 9.80 12.30 1 3 -7 26.20 3.50 1 3 -7 22.40 3.10 1 3 -7 27.70 1.30 1 3 -7 30.80 2.10 1 3 -7 34.10 2.80 1 3 -7 28.80 3.20 1 3 -7 29.10 2.00 1 3 -7 30.70 0.80 1 3 -7 30.80 2.20 1 3 -7 28.30 2.00 1 3 -7 27.30 1.40 -1 -3 7 28.60 1.70 -1 -3 7 26.40 2.40 -1 -3 7 28.20 3.00 -1 -3 7 25.40 3.10 -1 -3 7 28.30 2.00 -1 -3 7 27.10 3.10 -1 -3 7 34.40 3.90 -1 -3 7 28.40 1.40 -1 -3 7 29.70 2.10 -1 -3 7 28.70 2.00 -1 -3 7 29.70 2.10 -1 -3 7 10.20 14.00 -1 -3 7 29.10 1.90 -1 -3 7 29.10 2.60 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21.20 1.10 1 -3 7 22.10 1.60 1 -3 7 24.70 2.80 1 -3 7 22.60 1.90 1 -3 7 21.20 3.00 1 -3 7 23.20 2.00 1 -3 7 23.10 2.40 1 -3 7 26.60 14.60 1 -3 7 20.20 1.70 1 -3 7 18.40 1.70 1 -3 7 24.70 1.50 1 -3 7 20.20 1.30 1 -3 7 23.50 1.70 1 -3 7 16.80 2.50 1 -3 7 23.60 3.30 1 -3 7 20.70 1.30 -2 3 -7 352.76 8.70 -2 3 -7 348.77 10.70 -2 3 -7 359.36 9.20 -2 3 -7 370.16 8.70 -2 3 -7 355.16 8.70 -2 3 -7 375.56 12.50 -2 3 -7 367.66 9.80 -2 3 -7 353.46 11.80 -2 3 -7 329.27 31.40 -2 3 -7 358.06 11.00 -2 3 -7 369.16 9.60 -2 3 -7 363.66 9.90 -2 3 -7 352.16 9.10 -2 3 -7 352.96 9.10 -2 3 -7 362.16 11.80 -2 3 -7 360.16 12.00 2 -3 7 369.66 10.30 2 -3 7 388.26 12.20 2 -3 7 338.47 9.00 2 -3 7 371.26 11.60 2 -3 7 357.86 10.80 2 -3 7 382.46 9.40 2 -3 7 378.26 12.00 2 -3 7 367.06 8.70 2 -3 7 368.46 9.20 2 -3 7 388.36 33.40 2 -3 7 394.86 9.40 2 -3 7 374.06 9.70 2 -3 7 364.36 8.90 2 -3 7 360.06 9.60 2 -3 7 373.96 12.60 2 -3 7 358.96 9.30 -3 3 -7 389.76 9.40 -3 3 -7 386.36 11.20 -3 3 -7 379.26 11.50 -3 3 -7 370.86 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31.40 2.00 4 -3 7 31.50 4.40 -5 3 -7 46.20 5.30 -5 3 -7 51.29 4.30 -5 3 -7 52.19 3.70 -5 3 -7 51.39 3.90 -5 3 -7 46.50 24.90 -5 3 -7 42.70 2.60 -5 3 -7 48.40 4.60 -5 3 -7 41.60 3.10 5 -3 7 50.49 2.80 5 -3 7 51.69 2.80 5 -3 7 48.30 3.20 5 -3 7 48.90 2.60 5 -3 7 47.90 3.40 5 -3 7 53.69 2.80 5 -3 7 11.20 22.30 5 -3 7 49.70 2.40 5 -3 7 52.49 6.00 5 -3 7 49.80 2.70 -6 3 -7 160.68 39.40 -6 3 -7 175.58 6.60 -6 3 -7 180.48 8.30 -6 3 -7 173.68 7.50 -6 3 -7 174.18 5.60 -6 3 -7 177.18 9.60 6 -3 7 169.58 7.00 6 -3 7 170.28 6.00 6 -3 7 180.98 5.80 6 -3 7 155.88 9.50 6 -3 7 179.38 6.00 6 -3 7 164.68 37.40 6 -3 7 180.58 5.70 -7 3 -7 225.28 10.00 -7 3 -7 212.28 9.20 -7 3 -7 218.58 11.40 -7 3 -7 278.77 52.29 -7 3 -7 210.78 9.00 7 -3 7 230.88 7.60 7 -3 7 125.09 39.50 7 -3 7 225.58 7.40 7 -3 7 230.38 7.30 7 -3 7 249.38 9.20 7 -3 7 234.18 9.30 7 -3 7 242.48 7.10 7 -3 7 225.28 12.20 -8 3 -7 22.80 3.30 -8 3 -7 26.50 3.90 -8 3 -7 20.40 3.70 -8 3 -7 17.70 3.10 8 -3 7 21.20 3.70 8 -3 7 19.10 5.70 8 -3 7 15.30 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22.40 -3 -3 8 758.12 17.90 -3 -3 8 774.92 18.70 -3 -3 8 755.02 20.10 -3 -3 8 772.22 19.90 -3 -3 8 792.52 21.80 -3 -3 8 768.62 18.60 2 3 -8 1.10 1.30 2 3 -8 0.80 1.00 2 3 -8 -0.60 1.70 2 3 -8 0.20 1.00 2 3 -8 0.20 0.50 2 3 -8 -0.40 0.50 2 3 -8 -0.90 1.60 2 3 -8 0.00 0.90 2 3 -8 0.80 1.80 2 3 -8 0.50 0.70 2 3 -8 0.40 0.70 2 3 -8 -0.90 1.10 2 3 -8 0.50 0.90 2 3 -8 1.10 0.70 2 3 -8 -0.20 0.40 2 3 -8 8.00 14.50 -2 -3 8 1.70 1.30 -2 -3 8 0.20 0.80 -2 -3 8 0.70 1.00 -2 -3 8 0.40 0.60 -2 -3 8 18.70 13.00 -2 -3 8 1.60 1.10 -2 -3 8 3.60 1.80 -2 -3 8 0.50 0.90 -2 -3 8 0.50 0.70 -2 -3 8 -0.40 0.70 -2 -3 8 1.60 1.00 -2 -3 8 -2.80 1.30 -2 -3 8 1.90 1.90 -2 -3 8 1.90 1.70 -2 -3 8 0.00 0.90 -2 -3 8 0.40 0.50 1 3 -8 32.10 1.10 1 3 -8 35.40 3.00 1 3 -8 30.40 2.20 1 3 -8 34.80 2.40 1 3 -8 34.60 1.00 1 3 -8 39.80 4.10 1 3 -8 32.30 3.80 1 3 -8 30.40 1.00 1 3 -8 32.40 12.80 1 3 -8 37.80 2.40 1 3 -8 30.00 2.20 1 3 -8 32.40 1.90 1 3 -8 40.40 4.00 1 3 -8 32.80 0.90 1 3 -8 29.60 2.60 1 3 -8 32.60 1.50 1 3 -8 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7.40 2 -3 8 130.19 27.50 2 -3 8 121.39 5.40 2 -3 8 138.79 4.60 2 -3 8 137.19 4.20 2 -3 8 131.59 4.20 2 -3 8 132.99 4.60 2 -3 8 132.29 6.60 2 -3 8 129.89 6.30 -3 3 -8 772.52 18.80 -3 3 -8 783.52 57.89 -3 3 -8 782.32 21.20 -3 3 -8 777.42 18.80 -3 3 -8 799.82 21.00 -3 3 -8 806.02 18.70 -3 3 -8 809.32 19.40 -3 3 -8 787.42 23.40 -3 3 -8 807.22 21.90 -3 3 -8 785.22 22.90 -3 3 -8 793.62 22.40 -3 3 -8 779.72 18.50 -3 3 -8 810.72 23.30 -3 3 -8 808.02 18.00 -3 3 -8 802.02 19.80 -3 3 -8 795.22 17.90 3 -3 8 785.02 18.70 3 -3 8 783.02 20.50 3 -3 8 785.32 19.10 3 -3 8 799.92 19.00 3 -3 8 824.42 19.10 3 -3 8 764.12 18.60 3 -3 8 804.02 22.70 3 -3 8 777.22 23.40 3 -3 8 820.72 19.20 3 -3 8 781.92 19.90 3 -3 8 773.02 22.00 3 -3 8 742.53 20.70 3 -3 8 781.02 18.90 3 -3 8 886.51 54.09 3 -3 8 798.82 19.90 3 -3 8 822.12 23.00 -4 3 -8 12.70 2.80 -4 3 -8 10.40 3.30 -4 3 -8 8.00 1.30 -4 3 -8 8.50 2.20 -4 3 -8 7.50 1.40 -4 3 -8 7.90 1.30 -4 3 -8 12.00 2.40 -4 3 -8 8.60 1.80 -4 3 -8 10.20 1.20 -4 3 -8 7.10 1.50 -4 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91.09 32.70 -6 -3 9 66.39 4.90 -6 -3 9 72.19 3.10 -6 -3 9 74.89 3.80 -6 -3 9 76.39 4.00 -6 -3 9 62.69 2.70 -6 -3 9 74.79 7.50 5 3 -9 71.69 3.50 5 3 -9 63.39 5.90 5 3 -9 65.59 6.00 5 3 -9 68.79 4.10 5 3 -9 76.39 5.90 5 3 -9 77.19 31.60 5 3 -9 71.79 2.30 5 3 -9 70.99 4.20 5 3 -9 66.69 3.60 5 3 -9 74.09 4.70 5 3 -9 70.09 3.10 5 3 -9 77.89 3.20 -5 -3 9 68.79 4.60 -5 -3 9 70.29 2.80 -5 -3 9 74.69 6.10 -5 -3 9 70.89 4.00 -5 -3 9 77.79 5.90 -5 -3 9 66.99 3.50 -5 -3 9 70.39 3.00 -5 -3 9 72.89 4.20 -5 -3 9 71.09 2.40 -5 -3 9 72.29 3.40 -5 -3 9 63.09 3.80 -5 -3 9 67.69 3.00 -5 -3 9 66.29 6.20 -5 -3 9 81.49 37.10 4 3 -9 50.79 5.30 4 3 -9 53.89 2.20 4 3 -9 56.19 2.60 4 3 -9 45.60 3.40 4 3 -9 52.69 1.90 4 3 -9 47.30 3.60 4 3 -9 59.79 24.40 4 3 -9 53.99 3.50 4 3 -9 49.80 3.20 4 3 -9 58.79 5.40 4 3 -9 51.89 3.10 -4 -3 9 50.29 2.30 -4 -3 9 58.09 6.50 -4 -3 9 52.99 3.50 -4 -3 9 51.49 4.10 -4 -3 9 49.70 2.20 -4 -3 9 50.19 3.50 -4 -3 9 55.49 2.70 -4 -3 9 52.39 2.90 -4 -3 9 51.29 2.00 -4 -3 9 53.69 2.50 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43.50 2.40 0 3 -9 41.10 3.10 0 3 -9 38.60 2.40 0 3 -9 40.80 1.30 0 3 -9 43.30 2.30 0 -3 9 42.00 2.00 0 -3 9 41.10 3.00 0 -3 9 39.30 2.30 0 -3 9 48.10 4.20 0 -3 9 33.70 4.30 0 -3 9 43.30 4.50 0 -3 9 39.20 2.90 0 -3 9 41.60 3.90 0 -3 9 57.49 19.80 0 -3 9 38.50 2.50 0 -3 9 44.90 2.20 0 -3 9 42.40 2.70 0 -3 9 39.90 2.20 0 -3 9 40.90 1.80 0 -3 9 41.20 2.60 -1 3 -9 81.59 4.50 -1 3 -9 78.29 2.90 -1 3 -9 80.89 3.10 -1 3 -9 87.69 3.70 -1 3 -9 86.99 3.20 -1 3 -9 80.49 2.90 -1 3 -9 84.79 3.40 -1 3 -9 89.99 5.40 -1 3 -9 88.29 4.40 -1 3 -9 80.59 4.80 -1 3 -9 76.99 3.50 -1 3 -9 84.19 2.40 -1 3 -9 85.99 5.50 -1 3 -9 86.99 5.70 -1 3 -9 53.19 21.30 -1 3 -9 90.19 6.00 1 -3 9 79.99 5.10 1 -3 9 82.39 3.10 1 -3 9 82.39 3.20 1 -3 9 82.39 3.90 1 -3 9 77.29 3.10 1 -3 9 84.69 3.60 1 -3 9 81.79 3.60 1 -3 9 86.89 24.60 1 -3 9 85.89 6.00 1 -3 9 86.19 5.40 1 -3 9 78.39 3.30 1 -3 9 84.89 2.60 1 -3 9 82.09 4.40 1 -3 9 83.69 5.30 1 -3 9 86.09 3.30 1 -3 9 83.59 3.20 1 -3 9 87.29 3.70 1 -3 9 78.19 4.10 -2 3 -9 90.89 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1.60 3 4 -14 35.30 37.10 3 4 -14 61.59 4.10 3 4 -14 74.29 7.80 3 4 -14 61.79 4.30 3 4 -14 65.59 4.70 3 4 -14 64.89 5.10 -3 -4 14 58.59 7.40 -3 -4 14 66.09 4.70 -3 -4 14 65.49 3.60 -3 -4 14 62.59 4.00 -3 -4 14 65.59 5.10 -3 -4 14 62.49 3.00 -3 -4 14 82.99 38.00 -3 -4 14 58.79 3.90 2 4 -14 59.19 4.90 2 4 -14 46.30 3.60 2 4 -14 41.40 3.70 2 4 -14 46.70 4.40 2 4 -14 56.79 34.60 2 4 -14 48.40 3.80 2 4 -14 50.99 6.50 -2 -4 14 47.70 3.00 -2 -4 14 47.10 3.60 -2 -4 14 41.30 6.20 -2 -4 14 46.30 3.50 -2 -4 14 46.40 3.10 -2 -4 14 52.79 4.10 -2 -4 14 47.50 2.70 -2 -4 14 11.60 35.30 1 4 -14 -2.70 34.80 1 4 -14 5.60 2.50 1 4 -14 6.50 2.00 1 4 -14 8.70 3.40 1 4 -14 6.30 2.10 1 4 -14 7.60 2.70 1 4 -14 8.20 1.90 -1 -4 14 7.00 3.50 -1 -4 14 11.00 1.80 -1 -4 14 7.40 2.10 -1 -4 14 5.30 1.90 -1 -4 14 14.20 36.70 -1 -4 14 8.30 1.80 -1 -4 14 8.10 1.60 0 4 -14 2.80 2.20 0 4 -14 1.70 1.90 0 4 -14 -2.70 2.60 0 4 -14 43.40 36.50 0 4 -14 2.80 2.00 0 4 -14 1.30 1.50 0 -4 14 3.60 1.40 0 -4 14 2.50 1.80 0 -4 14 4.60 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-1 21 1.70 2.80 -4 -1 21 6.30 3.30 3 1 -21 5.80 3.10 -3 -1 21 8.50 3.10 -3 -1 21 12.60 3.80 2 1 -21 20.40 4.20 -2 -1 21 20.30 3.60 -2 -1 21 22.10 4.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 55966